CN109453099A - Paris polyphylla composition and preparation method thereof - Google Patents
Paris polyphylla composition and preparation method thereof Download PDFInfo
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- CN109453099A CN109453099A CN201811609239.3A CN201811609239A CN109453099A CN 109453099 A CN109453099 A CN 109453099A CN 201811609239 A CN201811609239 A CN 201811609239A CN 109453099 A CN109453099 A CN 109453099A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses paris polyphylla compositions, mainly it is made of the following raw material by weight, 10-12 parts of Rhizoma Paridis extract, 3-4 parts of bletilla striata extract, 2-2.5 parts of Herba Abri extract, 2-2.5 parts of curculigo orchioides extract and 5-6 parts of grape seed oil, the paris polyphylla composition is as aging ingredient in cosmetics；And the preparation method of paris polyphylla composition.The present invention has the advantages that in stable condition, pro-skin easily absorbs, and anti-aging effects are good.
Description
Technical field
The present invention relates to technical field of cosmetic preparation.It is more particularly related to a kind of paris polyphylla combination
Object and preparation method thereof.
Background technique
With advancing age, skin can gradually aging, be mainly shown as that wrinkle increases, it is cutis laxa, obscure, rough
And pigmentation, seriously affect beauty.For delay skin aging, people carry out daily skin shield frequently with anti-aging cosmetics
Reason, the market demand of anti-aging cosmetics is very big, wherein Chinese herbal medicine skin care because its green natural, it is pure it is mild, toxic side effect is small
The advantages that, it is pursued by more and more people.Shennongjia is located at Northwest of Hubei Province border area, domestic medicinal plant and its abundant, seven leaves one
Branch flower resources advantage is obvious, is applied in cosmetics also not after paris polyphylla is extracted as main activity of fighting against senium ingredient
It appears in the newspapers.
Summary of the invention
It is an object of the present invention to provide a kind of paris polyphylla compositions, by Rhizoma Paridis extract, the bletilla striata
Extract, Herba Abri extract, curculigo orchioides extract and grape seed oil are prepared according to a certain percentage, make the advantage knot between each component
It closes, generates synergistic effect, improve the anti-aging effects of composition.
It is an object of the present invention to provide a kind of preparation method of paris polyphylla composition, by by paris polyphylla
Extract, bletilla striata extract, Herba Abri extract, curculigo orchioides extract according to certain sequence mix after, by gained mixed liquor one into
After row ultra high pressure treatment, then with grape seed oil mixing and emulsifying, can make the structural state of composition it is uniform, stablize, reduce composition
Sensitization and improve the anti-aging performance of composition, keep face cream obtained in stable condition, property is mild, and skin sense is good, anti-aging
Effect is good.
In order to realize purposes and other advantages according to the present invention, provide a kind of paris polyphylla composition, mainly by
The following raw material composition by weight, 10-12 parts of Rhizoma Paridis extract, 3-4 parts of bletilla striata extract, Herba Abri extract
2-2.5 parts, 2-2.5 parts of curculigo orchioides extract and 5-6 parts of grape seed oil, the paris polyphylla composition are used as aging ingredient
In cosmetics.The cosmetics include lotion, face cream and facial mask.
Preferably, the paris polyphylla composition, is mainly made of the following raw material by weight, seven leaves one
11 parts of flower extract of branch, 3.5 parts of bletilla striata extract, 2.2 parts of Herba Abri extract, 2.2 parts of curculigo orchioides extract and grape seed oil 5.5
Part, the paris polyphylla composition is as aging ingredient in face cream.
The preparation method of paris polyphylla composition, includes the following steps:
Step 1: weighing the Rhizoma Paridis extract of 10-12 parts by weight, it is added into the water of 50-60 parts by weight, surpasses
After sound dispersion, the sodium hydroxide solution for being 10% with mass fraction adjusts pH value to 7.3 ± 0.05, sequentially adds 3-4 weight
Part bletilla striata extract, the Herba Abri extract of 2-2.5 parts by weight and the curculigo orchioides extract of 2-2.5 parts by weight, after ultrasonic disperse,
Obtain mixed liquor one；
Step 2: the mixed liquor one packing after sealing, is placed in ultrahigh pressure vessel, into Polythene Bag in 400-
Pressure maintaining 20-25min under 500Mpa obtains mixed liquor two；
Step 3: the grape seed oil of 5-6 parts by weight and the glyceryl stearate of 1-1.2 parts by weight are added into the mixed liquor two
Acid esters, in 45-50 DEG C, the emulsified 3-6min of 2400-2600r/min to get the paris polyphylla composition.
Preferably, the preparation method of the paris polyphylla composition, the Rhizoma Paridis extract are 11 weights
Part is measured, the bletilla striata extract is 3.5 parts by weight, and the Herba Abri extract is 2.2 parts by weight, and the curculigo orchioides extract is
2.2 parts by weight, the grape seed oil are 5.5 parts by weight, and the stearine is 1.1 parts by weight.
Preferably, the preparation method of the paris polyphylla composition further includes being added into face cream base-material and accounting for face
The paris polyphylla composition of the 5-8% of white base-material quality, mixes 2-4min under 50-55 DEG C, 300-400r/min, system
Obtain face cream.The face cream base-material is by emollient, moisturizer, emulsifier and water composition.
Preferably, the preparation method of the paris polyphylla composition, the preparation of the Rhizoma Paridis extract
Method are as follows: A, by after paris polyphylla coarse powder crosses 20 meshes, extracting screen underflow adds water, and adjusting its moisture content is 45-50%, obtains
Paris polyphylla wet-milling；B, the paris polyphylla wet-milling is subjected to hot pressing steam and sprays quick-fried processing, steam explosion pressure is 2.2-
2.5MPa, saturated-steam temperature are 180-200 DEG C, dwell time 2-3min, and then instantaneous pressure release obtains paris polyphylla detonation
Powder；C, it by after paris polyphylla priming powder freeze-drying, through supercritical carbon dioxide extracting, obtains the paris polyphylla and mentions
Take object, the supercritical carbon dioxide extracting condition are as follows: 45-50 DEG C of extraction temperature, extracting pressure 18-20MPa, extraction time 3-
4h, extraction flow 40L/h.
The present invention is include at least the following beneficial effects:
The first, Rhizoma Paridis extract can be anti-oxidant in the present invention, removes free radical, enhances skin elasticity；The bletilla striata mentions
Object energy Cress is taken, germiparity is accelerated；Herba Abri extract can expand blood vessel, accelerate blood circulation；Curculigo orchioides extract energy
Skin-nourishing is supplemented, the immunity of skin is improved；Grape seed oil can it is anti-oxidant, remove free radical, moisturizing, by said components according to
Certain ratio is prepared, so that the advantage between each component combines, is generated synergistic effect, is improved the anti-aging effects of composition；
The second, the present invention is by by Rhizoma Paridis extract, bletilla striata extract, Herba Abri extract, curculigo orchioides extract
According to certain sequence mixing after, carry out ultra high pressure treatment, then with grape seed oil mixing and emulsifying, the structural state of composition can be made equal
One, stablize, reduce the sensitization of composition and improve the anti-aging performance of composition, keep face cream obtained in stable condition, pro-skin,
It easily absorbs, anti-aging effects are good.
Third, the present invention provides a kind of preparation methods of Rhizoma Paridis extract, by supercritical carbon dioxide
Increase hot pressing steam before extraction and spray quick-fried processing, the dissolution of active constituent in paris polyphylla can be effectively facilitated, improve seven Ye Yizhi
The anti-aging ability of flower extract.
Further advantage, target and feature of the invention will be partially reflected by the following instructions, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Detailed description of the invention
Fig. 1 is the Flexible change figure of the sample use front and back skin of the embodiment of the present invention 2,4,6.
Specific embodiment
Below with reference to embodiment and attached drawing, the present invention is described in further detail, to enable those skilled in the art's reference
Specification word can be implemented accordingly.
It should be noted that experimental method described in following embodiments is unless otherwise specified conventional method, institute
Reagent and material are stated, unless otherwise specified, is commercially obtained.
Embodiment 1:
A kind of paris polyphylla composition, is mainly made of the following raw material by weight, Rhizoma Paridis extract
10 parts, 3 parts of bletilla striata extract, 2 parts of Herba Abri extract, 2 parts of curculigo orchioides extract and 5 parts of grape seed oil.
A kind of preparation method of paris polyphylla composition, includes the following steps:
Step 1: weighing the Rhizoma Paridis extract of 10 parts by weight, it is added into the water of 50 parts by weight, ultrasonic disperse
Afterwards, the sodium hydroxide solution for being 10% with mass fraction adjusts pH value to 7.3 ± 0.05, sequentially adds the bletilla striata of 3 parts by weight
The curculigo orchioides extract of extract, the Herba Abri extract of 2 parts by weight and 2 parts by weight after ultrasonic disperse, obtains mixed liquor one；
Step 2: the mixed liquor one packing after sealing, is placed in ultrahigh pressure vessel into Polythene Bag, in
Pressure maintaining 25min under 400Mpa obtains mixed liquor two；
Step 3: the grape seed oil of 5 parts by weight and the stearine of 1 parts by weight are added into the mixed liquor two,
In 45 DEG C, the emulsified 6min of 2400r/min to get the paris polyphylla composition.
It further include the 5% paris polyphylla composition for accounting for face cream base-material quality being added into face cream base-material, in 50
DEG C, mix 4min under 300r/min, face cream is made.The face cream base-material contains 6% saualane by weight percentage, 3%
Shea butter, 2% jojoba oil, 8% glycerol, 2% propylene glycol, 1% cetearyl alcohol acid alcohol, 1% stearine is remaining
Amount is water, and the preparation method of the face cream base-material is (1) by saualane, shea butter, jojoba oil, cetearyl alcohol acid alcohol and sweet
The mixing of oleostearin acid esters, heating stirring obtain oily phase to being completely dissolved；(2) glycerol, propylene glycol and water are uniformly mixed, heating is stirred
It mixes to being completely dissolved, obtains water phase；(3) by oily mutually and after water phase mixes, stirring and emulsifying to get.
The specification of Rhizoma Paridis extract in the present embodiment is 20:1, and the specification of bletilla striata extract is 10:1, chicken bone
The specification of careless extract is 10:1, is purchased from Xi'an Bioisystech Co., Ltd, Tianrui；The specification of curculigo orchioides extract is 8:1, purchase
In Hunan Lang Lin living resources limited liability company；Other components in the present embodiment are conventional commercial.
Embodiment 2:
A kind of paris polyphylla composition, is mainly made of the following raw material by weight, Rhizoma Paridis extract
11 parts, 3.5 parts of bletilla striata extract, 2.2 parts of Herba Abri extract, 2.2 parts of curculigo orchioides extract and 5.5 parts of grape seed oil.
A kind of preparation method of paris polyphylla composition, includes the following steps:
Step 1: weighing the Rhizoma Paridis extract of 11 parts by weight, it is added into the water of 55 parts by weight, ultrasonic disperse
Afterwards, the sodium hydroxide solution for being 10% with mass fraction adjusts pH value to 7.3 ± 0.05, sequentially adds the white of 3.5 parts by weight
The curculigo orchioides extract of splendid achnatherum extract, the Herba Abri extract of 2.2 parts by weight and 2.2 parts by weight after ultrasonic disperse, obtains mixed liquor
One；
Step 2: the mixed liquor one packing after sealing, is placed in ultrahigh pressure vessel into Polythene Bag, in
Pressure maintaining 22min under 450Mpa obtains mixed liquor two；
Step 3: the grape seed oil of 5.5 parts by weight and the glycerol stearate of 1.1 parts by weight are added into the mixed liquor two
Ester, in 45 DEG C, the emulsified 5min of 2500r/min to get the paris polyphylla composition.
It further include that the 6.5% paris polyphylla composition for accounting for face cream base-material quality is added into face cream base-material, in
52 DEG C, mix 3min under 350r/min, face cream is made.The face cream base-material contain 6% saualane by weight percentage,
3% shea butter, 2% jojoba oil, 8% glycerol, 2% propylene glycol, 1% cetearyl alcohol acid alcohol, 1% glycerol stearate
Ester, surplus are water, and the preparation method of the face cream base-material is that (1) is sour by saualane, shea butter, jojoba oil, cetearyl alcohol
Pure and mild stearine mixing, heating stirring obtain oily phase to being completely dissolved；(2) glycerol, propylene glycol and water are uniformly mixed,
Heating stirring obtains water phase to being completely dissolved；(3) by oily mutually and after water phase mixes, stirring and emulsifying to get.
The specification of Rhizoma Paridis extract in the present embodiment is 20:1, and the specification of bletilla striata extract is 10:1, chicken bone
The specification of careless extract is 10:1, is purchased from Xi'an Bioisystech Co., Ltd, Tianrui；The specification of curculigo orchioides extract is 8:1, purchase
In Hunan Lang Lin living resources limited liability company；Other components in the present embodiment are conventional commercial.
Embodiment 3:
A kind of paris polyphylla composition, is mainly made of the following raw material by weight, Rhizoma Paridis extract
12 parts, 4 parts of bletilla striata extract, 2.5 parts of Herba Abri extract, 2.5 parts of curculigo orchioides extract and 6 parts of grape seed oil.
A kind of preparation method of paris polyphylla composition, includes the following steps:
Step 1: weighing the Rhizoma Paridis extract of 12 parts by weight, it is added into the water of 60 parts by weight, ultrasonic disperse
Afterwards, the sodium hydroxide solution for being 10% with mass fraction adjusts pH value to 7.3 ± 0.05, sequentially adds the bletilla striata of 4 parts by weight
The curculigo orchioides extract of extract, the Herba Abri extract of 2.5 parts by weight and 2.5 parts by weight after ultrasonic disperse, obtains mixed liquor one；
Step 2: the mixed liquor one packing after sealing, is placed in ultrahigh pressure vessel into Polythene Bag, in
Pressure maintaining 20min under 500Mpa obtains mixed liquor two；
Step 3: the grape seed oil of 6 parts by weight and the glycerol stearate of 1.2 parts by weight are added into the mixed liquor two
Ester, in 50 DEG C, the emulsified 3min of 2600r/min to get the paris polyphylla composition.
It further include the 8% paris polyphylla composition for accounting for face cream base-material quality being added into face cream base-material, in 55
DEG C, mix 2min under 400r/min, face cream is made.The face cream base-material contains 6% saualane by weight percentage, 3%
Shea butter, 2% jojoba oil, 8% glycerol, 2% propylene glycol, 1% cetearyl alcohol acid alcohol, 1% stearine is remaining
Amount is water, and the preparation method of the face cream base-material is (1) by saualane, shea butter, jojoba oil, cetearyl alcohol acid alcohol and sweet
The mixing of oleostearin acid esters, heating stirring obtain oily phase to being completely dissolved；(2) glycerol, propylene glycol and water are uniformly mixed, heating is stirred
It mixes to being completely dissolved, obtains water phase；(3) by oily mutually and after water phase mixes, stirring and emulsifying to get.
The specification of Rhizoma Paridis extract in the present embodiment is 20:1, and the specification of bletilla striata extract is 10:1, chicken bone
The specification of careless extract is 10:1, is purchased from Xi'an Bioisystech Co., Ltd, Tianrui；The specification of curculigo orchioides extract is 8:1, purchase
In Hunan Lang Lin living resources limited liability company；Other components in the present embodiment are conventional commercial.
Embodiment 4:
On the basis of embodiment 2, the Rhizoma Paridis extract is self-control, it is specific the preparation method comprises the following steps: A, by seven leaves
After a flower coarse powder, 20 meshes are crossed, extracting screen underflow adds water, and adjusting its moisture content is 48%, obtains paris polyphylla wet-milling；B,
The paris polyphylla wet-milling is subjected to hot pressing steam and sprays quick-fried processing, steam explosion pressure is 2.3MPa, saturated-steam temperature 190
DEG C, dwell time 2.5min, then instantaneous pressure release obtains paris polyphylla priming powder；C, by the paris polyphylla priming powder
After freeze-drying, through supercritical carbon dioxide extracting, the Rhizoma Paridis extract, the supercritical carbon dioxide extracting are obtained
Condition are as follows: 48 DEG C of extraction temperature, extracting pressure 19MPa, extraction time 3.5h, extraction flow 40L/h.The same embodiment of remaining condition
2。
Embodiment 5:
On the basis of embodiment 2, the mixed liquor one is directly added into grape seed oil and 1.1 weight of 5.5 parts by weight
The stearine of part, in 45 DEG C, the emulsified 5min of 2500r/min to get the paris polyphylla composition.Remaining condition
With embodiment 2.
Embodiment 6:
A kind of paris polyphylla composition, is mainly made of the following raw material by weight, Rhizoma Paridis extract
11 parts and 5.5 parts of grape seed oil.
A kind of preparation method of paris polyphylla composition, includes the following steps:
Step 1: weighing the Rhizoma Paridis extract of 11 parts by weight, it is added into the water of 35 parts by weight, ultrasonic disperse
Afterwards, the sodium hydroxide solution for being 10% with mass fraction adjusts pH value to 7.3 ± 0.05, obtains mixed liquor one；
Step 2: the mixed liquor one packing after sealing, is placed in ultrahigh pressure vessel into Polythene Bag, in
Pressure maintaining 22min under 450Mpa obtains mixed liquor two；
Step 3: the grape seed oil of 5.5 parts by weight and the glycerol stearate of 1.1 parts by weight are added into the mixed liquor two
Ester, in 45 DEG C, the emulsified 5min of 2500r/min to get the paris polyphylla composition.
It further include that the 6.5% paris polyphylla composition for accounting for face cream base-material quality is added into face cream base-material, in
52 DEG C, mix 3min under 350r/min, face cream is made.The face cream base-material contain 6% saualane by weight percentage,
3% shea butter, 2% jojoba oil, 8% glycerol, 2% propylene glycol, 1% cetearyl alcohol acid alcohol, 1% glycerol stearate
Ester, surplus are water, and the preparation method of the face cream base-material is that (1) is sour by saualane, shea butter, jojoba oil, cetearyl alcohol
Pure and mild stearine mixing, heating stirring obtain oily phase to being completely dissolved；(2) glycerol, propylene glycol and water are uniformly mixed,
Heating stirring obtains water phase to being completely dissolved；(3) by oily mutually and after water phase mixes, stirring and emulsifying to get.
The specification of Rhizoma Paridis extract in the present embodiment is 20:1, and the specification of bletilla striata extract is 10:1, chicken bone
The specification of careless extract is 10:1, is purchased from Xi'an Bioisystech Co., Ltd, Tianrui；The specification of curculigo orchioides extract is 8:1, purchase
In Hunan Lang Lin living resources limited liability company；Other components in the present embodiment are conventional commercial.
Experimental example 1: stability experiment
Using high and low temperature test and the face of thermal cycling test measurement embodiment 2, embodiment 4, embodiment 5 and embodiment 6
The stability of frost, the results are shown in Table 1.
1 stability experiment result of table
As shown in Table 1, in above-mentioned sample, the stability of the sample of embodiment 4 and embodiment 6 is best, followed by embodiment 2
Sample, the stability of the sample of embodiment 5 is worst.
Experimental example 2: patch experiment
Randomly select 50 volunteers, the age 25-40 years old, no allergies, weigh respectively 0.02g embodiment 2, embodiment 4,
The sample of embodiment 5 and embodiment 6 is added into the coyote hole of spot examination adhesive tape, then applys spot examination adhesive tape on volunteer
The selected location at back, while light pressing room is affixed on sample uniformly on skin to drive away air one by one, continues 48 hours, it is real
It during testing, advises volunteer to avoid aggravating activities, does not have a bath, avoid scratching, reduce and perspire, and avoid solar radiation, apply 48 hours
Afterwards, removal spot tries adhesive tape, removes remaining sample with wet soft paper or cotton swab, first observed is made in 30 minutes in interval, and in 72,96
Hour makees the 2nd time and the 3rd observation respectively.Patch experiment skin adverse reaction rating scale be shown in Table 2 and experimental result be shown in Table
3。
2 skin adverse reaction rating scale of table
3 patch experimental result of table
As shown in Table 3, the sample of embodiment 4 and embodiment 6,50 subjects are negative (0), illustrate 4 He of embodiment
The sample of embodiment 6 has no adverse reaction to human body, the sample of embodiment 2, has 1 people faint erythema occur in 50 subjects
(1), other subjects are negative (0), illustrate that the sample of embodiment 2 has no adverse reaction substantially to human body, the sample of embodiment 5
Product have 19 people faint erythema (1) occur in 50 subjects, have 3 people erythema occur, other subjects are negative (0), say
The sample of bright embodiment 2 has adverse reaction to human body.
Experimental example 3: human experimentation
90 volunteers are chosen, the age 30-35 years old, no allergies were randomly divided into 3 groups, every group of 30 people, in subject face
The left and right sides symmetric position select 5 × 5cm2The region of size is as Experimental Area, wherein in the face of every group of subject
The sample of suitable embodiment 2, embodiment 4 or embodiment 6 is smeared in left side respectively, and the embodiment 2 of equivalent is smeared on the right side of face
The face cream base-material of middle preparation is smeared twice daily, cleans face with mild facial cleanser before smearing, is used continuously 12 weeks, and point
Not behind 4,8,10 and 12 weeks of smearing, with the skin elasticity R2 in the test experiments region skinanalysis apparatus (German CK, MPA580)
Value (R2: skin springback capacity and the ratio between maximum tension amount when having a negative pressure when no negative pressure, closer to 1, get over ratio by the elasticity of skin
It is good), each Experimental Area measures 5 times, is averaged.Experimental result is as shown in Figure 1.As shown in Figure 1, using embodiment 2, implementation
Skin elasticity after 6 sample of example 4 and embodiment is improved compared with using face cream base-material, wherein uses 4 sample of embodiment
Skin elasticity afterwards is best, followed by embodiment 2 and embodiment 6.
Although the embodiments of the present invention have been disclosed as above, but its is not only in the description and the implementation listed
With it can be fully applied to various fields suitable for the present invention, for those skilled in the art, can be easily
Realize other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, the present invention is simultaneously unlimited
In specific details and legend shown and described herein.
Claims (6)
1. paris polyphylla composition, which is characterized in that be mainly made of the following raw material by weight, paris polyphylla mentions
Take 10-12 parts of object, 3-4 parts of bletilla striata extract, 2-2.5 parts of Herba Abri extract, 2-2.5 parts of curculigo orchioides extract and grape seed oil 5-
6 parts, the paris polyphylla composition is as aging ingredient in cosmetics.
2. paris polyphylla composition as described in claim 1, which is characterized in that mainly by the following raw material by weight
Composition, 11 parts of Rhizoma Paridis extract, 3.5 parts of bletilla striata extract, 2.2 parts of Herba Abri extract, 2.2 parts of curculigo orchioides extract and
5.5 parts of grape seed oil, the paris polyphylla composition is as aging ingredient in face cream.
3. the preparation method of paris polyphylla composition, which comprises the steps of:
Step 1: weighing the Rhizoma Paridis extract of 10-12 parts by weight, it is added into the water of 50-60 parts by weight, ultrasound point
After dissipating, the sodium hydroxide solution for being 10% with mass fraction adjusts pH value to 7.3 ± 0.05, sequentially adds 3-4 parts by weight
The curculigo orchioides extract of bletilla striata extract, the Herba Abri extract of 2-2.5 parts by weight and 2-2.5 parts by weight after ultrasonic disperse, obtains mixed
Close liquid one；
Step 2: the mixed liquor one packing after sealing, is placed in ultrahigh pressure vessel, into Polythene Bag in 400-
Pressure maintaining 20-25min under 500Mpa obtains mixed liquor two；
Step 3: the grape seed oil of 5-6 parts by weight and the glycerol stearate of 1-1.2 parts by weight are added into the mixed liquor two
Ester, in 45-50 DEG C, the emulsified 3-6min of 2400-2600r/min to get the paris polyphylla composition.
4. the preparation method of paris polyphylla composition as claimed in claim 3, which is characterized in that the paris polyphylla mentions
Taking object is 11 parts by weight, and the bletilla striata extract is 3.5 parts by weight, and the Herba Abri extract is 2.2 parts by weight, the thizoma curculiginis
Extract is 2.2 parts by weight, and the grape seed oil is 5.5 parts by weight, and the stearine is 1.1 parts by weight.
5. the preparation method of paris polyphylla composition as claimed in claim 3, which is characterized in that further include, to face cream base
The paris polyphylla composition for accounting for the 5-8% of face cream base-material quality is added in material, under 50-55 DEG C, 300-400r/min
2-4min is mixed, face cream is made.
6. the preparation method of paris polyphylla composition as claimed in claim 3, which is characterized in that the paris polyphylla mentions
Take object the preparation method comprises the following steps: A, by after paris polyphylla coarse powder, cross 20 meshes, extracting screen underflow adds water, and adjusting its moisture content is
45-50% obtains paris polyphylla wet-milling；B, the paris polyphylla wet-milling is subjected to hot pressing steam and sprays quick-fried processing, steam explosion pressure
For 2.2-2.5MPa, saturated-steam temperature is 180-200 DEG C, dwell time 2-3min, and then instantaneous pressure release obtains seven Ye Yizhi
Flower priming powder；C, by after paris polyphylla priming powder freeze-drying, through supercritical carbon dioxide extracting, seven leaf one is obtained
Branch flower extract, the supercritical carbon dioxide extracting condition are as follows: 45-50 DEG C of extraction temperature, extracting pressure 18-20MPa, extraction
Time 3-4h, extraction flow 40L/h.
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