CN109293453B - Biological organic fertilizer special for citrus fruit trees and preparation method thereof - Google Patents

Biological organic fertilizer special for citrus fruit trees and preparation method thereof Download PDF

Info

Publication number
CN109293453B
CN109293453B CN201811503491.6A CN201811503491A CN109293453B CN 109293453 B CN109293453 B CN 109293453B CN 201811503491 A CN201811503491 A CN 201811503491A CN 109293453 B CN109293453 B CN 109293453B
Authority
CN
China
Prior art keywords
microbial agent
organic fertilizer
fermentation microbial
leaves
secondary fermentation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201811503491.6A
Other languages
Chinese (zh)
Other versions
CN109293453A (en
Inventor
隋岩
陈丽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jinggangshan University
Original Assignee
Jinggangshan University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jinggangshan University filed Critical Jinggangshan University
Priority to CN201811503491.6A priority Critical patent/CN109293453B/en
Publication of CN109293453A publication Critical patent/CN109293453A/en
Application granted granted Critical
Publication of CN109293453B publication Critical patent/CN109293453B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/02Superphosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C9/00Fertilisers containing urea or urea compounds
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/50Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Fertilizers (AREA)

Abstract

The invention provides a special bio-organic fertilizer for citrus fruit trees. The raw materials comprise 40-70% of chicken and duck manure, 20-30% of crude crushed camphol residual branches and leaves, 10-20% of humic acid super absorbent resin and 2-9% of inorganic nutrient. Adjusting the water content to 40-60%, inoculating 0.5-3% of primary fermentation microbial agent, fermenting, turning over regularly, and fermenting at 50-70deg.C for 5-10 days. Transferring the primary fermented and decomposed product to a secondary fermentation workshop, adding a secondary fermentation microbial agent, and continuously decomposing for 7-15 days at the temperature of 35-40 ℃ to complete the decomposition. Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging. The product meets the requirements of biological organic fertilizer industry standard NY884-2012, is beneficial to realizing the water-saving irrigation, yield and income increase and disease resistance enhancement of citrus fruit trees, and realizes changing waste into valuables.

Description

Biological organic fertilizer special for citrus fruit trees and preparation method thereof
Technical Field
The invention relates to the technical field of agricultural fertilizers, in particular to a special bio-organic fertilizer with water saving, water retaining and slow release functions of a micro-fertilizer for citrus fruit trees and a preparation method thereof.
Background
The growth and development of crops can not separate moisture and fertilizer. The traditional inorganic or inorganic compound fertilizer has the effect of increasing the yield and income of agriculture, but the damage to soil and environment caused by long-term application threatens the sustainable development problem of agriculture, protects the ecological environment, develops organic ecological agriculture, and also puts more demands on bio-organic fertilizer. Meanwhile, drought and water shortage frequently occur in China in recent years, which threatens agricultural production, realizes high-efficiency utilization of water resources and meets the national strategic requirements of grain safety.
From the application point of saving water and adding micro-fertilizer, we invented a humic acid super absorbent resin (ZL 201410120234. X) with the functions of saving water and slowly releasing micro-fertilizer, but not containing the functions of bio-organic fertilizer, if the two can be combined into one, the foundation is provided for the subsequent water-saving irrigation while the fertilizer is applied.
Meanwhile, the special bio-organic fertilizer is developed by utilizing different waste resources, which is beneficial to changing waste into valuables and meets the market development requirement. The borneol camphora branches and leaves are the best resources for extracting natural borneol, are developed into a mature technology, but are limited by the content of the natural borneol and the extraction technology, the general crude product yield is about 1%, about 99% of borneol camphora residual branches and leaves are by-products after being extracted by steam distillation, jiangxi is taken as a main production area of the natural borneol, the annual borneol camphora residual branches and leaves can reach 5-8 ten thousand tons, and certain enterprises crush the borneol camphora residual branches and leaves to be made into low-added-value products such as borneol incense and sell the borneol camphora products, and the other enterprises directly use the borneol camphora residual branches and leaves as fuel, so that the problem of how to improve the utilization value of the borneol camphora residual branches and leaves is always an urgent need of the natural borneol enterprises. The residual branches and leaves of borneol camphor also contain a small part of natural borneol, limonene, alpha-pinene, beta-pinene and other substances which are beneficial components for enhancing the disease resistance of citrus fruit trees. If the microbial organic fertilizer can be used as an auxiliary material to be mixed with livestock manure to prepare the microbial organic fertilizer, the microbial organic fertilizer can be helpful for enhancing the efficacy of the microbial organic fertilizer for citrus fruit trees, and no related research and application report exists at present.
The invention selects borneol branches and leaves remained after borneol is extracted from a natural borneol factory as auxiliary materials, and adds humic acid super absorbent resin and livestock manure which are self-developed and the like to prepare the special bio-organic fertilizer for citrus fruit trees with the functions of water saving, water retention and slow release of trace fertilizer through a microbial fermentation technology.
Disclosure of Invention
The invention aims to provide a special bio-organic fertilizer for citrus fruit trees with water saving, water retaining and micro-fertilizer slow release functions and a preparation method thereof.
The aim of the invention is achieved by the following technical scheme:
(1) The raw materials are mixed according to the following weight ratio: 40-70% of chicken and duck feces, 20-30% of crude crushed borneol camphor residual branches and leaves, 10-20% of humic acid super absorbent resin and 2-9% of inorganic nutrients. After the water content is regulated to 40-60%, inoculating 0.5-3% of primary fermentation microbial agent for fermentation, turning over and throwing once every other day, controlling the temperature between 50-70 ℃ and fermenting for 5-10 days.
(2) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, adding 0.5-3% of secondary fermentation microbial agent, and continuously decomposing for 7-15 days at 35-40 ℃ to complete the decomposition.
(3) Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging.
The crude crushed borneol camphor residual branches and leaves are obtained by crushing the borneol camphor branches and leaves after extracting natural borneol by steam distillation.
The humic acid super absorbent resin is prepared according to the method of patent ZL201410120234.X, which is a humic acid super absorbent resin with the functions of water saving, water retention and slow release of trace fertilizer.
The inorganic nutrient is one or more of calcium superphosphate, potassium sulfate, diammonium phosphate and urea.
The primary fermentation microbial agent is one or more of commercial lactobacillus, bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria, and when the primary fermentation microbial agent is more than two, the proportion of each component is equal weight or is prepared according to actual use conditions.
The secondary fermentation microbial agent is one or more of azotobacter, phosphate-dissolving bacteria, potassium-dissolving bacteria, bacillus and saccharomycetes sold in the market, and when the secondary fermentation microbial agent is more than two, the proportion of each component is equal weight or the components are blended according to actual use conditions.
The invention has the following advantages:
1. the humic acid super absorbent resin with the functions of saving water and keeping water and slowly releasing the micro-fertilizer is introduced into the bio-organic fertilizer, so that conditions can be created for water-saving irrigation while the organic fertilizer is applied.
2. The method provides an effective strategy for full coverage utilization of borneol camphor branch and leaf resources, and utilizes borneol plants to extract natural borneol and then residual borneol camphor branch and leaf as auxiliary materials to produce the special bio-organic fertilizer for citrus fruit trees, thereby fully playing the promotion role of beneficial substances in the bio-organic fertilizer on the growth and development of the citrus fruit trees.
3. The secondary fermentation technology is adopted, the high-temperature fermentation technology is adopted in the primary fermentation process, germs and eggs can be effectively killed, and the low-temperature fermentation technology is adopted in the secondary fermentation process, so that a large amount of beneficial microbial agents can survive in the product;
4. the prepared special bio-organic fertilizer for citrus trees has high fertilizer efficiency and strong disease resistance, can meet the growth and development requirements of the citrus trees, can particularly greatly reduce the incidence rate of yellow dragon disease of the citrus trees, and can save and utilize water resources.
Detailed Description
Example 1:
(1) The raw materials are mixed according to the following weight ratio: 60% of chicken and duck manure, 25% of crude crushed borneol camphor residual branches and leaves, 10% of humic acid super absorbent resin and 5% of inorganic nutrients. Adjusting the water content to 40-60%, inoculating 0.5% primary fermentation microbial agent, fermenting, turning over and throwing once every other day, and fermenting at 60-65deg.C for 10 days. The inorganic nutrient is potassium sulfate and urea which are mixed according to the mass ratio of 1:1, and the primary fermentation microbial agent is mixed according to the equal weight ratio of lactobacillus, bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria.
(2) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, adding 2% of secondary fermentation microbial agent (mixed by mass ratio of bacillus, saccharomycetes and the like), and continuously decomposing for 15 days at the temperature of 35-40 ℃ to finish the decomposition.
(3) Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging.
Example 2:
(1) The raw materials are mixed according to the following weight ratio: 65% of chicken and duck feces, 20% of crude crushed borneol camphor residual branches and leaves, 10% of humic acid super absorbent resin and 5% of inorganic nutrients. Adjusting the water content to 40-60%, inoculating 1% primary fermentation microbial agent, fermenting, turning over and throwing once every other day, and fermenting at 60-65deg.C for 8 days. The inorganic nutrient is mixed by the equal weight ratio of calcium superphosphate and urea, and the primary fermentation microbial agent is mixed by the equal weight ratio of bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria.
(2) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, adding 2% of secondary fermentation microbial agent (mixing nitrogen-fixing bacteria, phosphate-dissolving bacteria and bacillus in mass ratio), and continuously decomposing for 15 days at 35-40 ℃ to complete decomposition.
(3) Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging.
Example 3:
(1) The raw materials are mixed according to the following weight ratio: 55% of chicken and duck feces, 25% of crude crushed borneol camphor residual branches and leaves, 12% of humic acid super absorbent resin and 8% of inorganic nutrients. Adjusting the water content to 40-60%, inoculating 1% primary fermentation microbial agent, fermenting, turning over and throwing once every other day, and fermenting at 50-60deg.C for 7 days. Inorganic nutrients are mixed by weight proportion of calcium superphosphate, potassium sulfate, diammonium phosphate, urea and the like, and the primary fermentation microbial agent is mixed by weight proportion of bacillus subtilis, thermophilic side spore mold and thermophilic heterotrophic ammonia oxidizing bacteria.
(2) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, adding 2% of secondary fermentation microbial agent (nitrogen-fixing bacteria, phosphate-dissolving bacteria, potassium-dissolving bacteria, bacillus, saccharomycetes and the like in mass ratio, and mixing), and continuously decomposing for 12 days at 35-40 ℃ to complete the decomposition.
(3) Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging.
The bio-organic fertilizer prepared by the method is detected by referring to the industry standard NY884-2012, and the result is shown in Table 1.
TABLE 1 biological organic fertilizer technical index
Project Industry standard Example 1 Example 2 Example 3
Number of viable bacteria (cfu) ≥0.20 0.26 0.27 0.29
Organic matter (dry basis)% ≥40.0 50 49 55
Moisture, percent ≤30.0 25 25 27
pH 5.5-8.5 7.1 7.0 6.7
Fecal coliform count, number of coliform bacteria/g ≤100 65 70 58
Mortality of ascariasis eggs% ≥95 98 96 99
Expiration date, month ≥6 9 8 9
The bio-organic fertilizer produced by the method is applied to the adult navel orange fruit trees in adjacent plots with equivalent conditions for experiments, the control group is not applied with the bio-organic fertilizer, and the experimental results are shown in Table 2 under the same conditions of other management modes.
TABLE 2 Effect of bioorganic fertilizer on navel orange planting
Project Control group Example 1 Example 2 Example 3
Yield (kg/mu) 1046 1215 1208 1230
Incidence of yellow Dragon disease (%) 5 1 1 0

Claims (1)

1. A special bio-organic fertilizer for citrus fruit trees is characterized in that: the preparation method comprises the following steps: (1) mixing the following raw materials in parts by weight: 40-70% of chicken and duck feces, 20-30% of crude crushed borneol camphor residual branches and leaves, 10-20% of humic acid super absorbent resin and 2-9% of inorganic nutrients; after the water content is regulated to 40-60%, inoculating 0.5-3% of primary fermentation microbial agent for fermentation, turning over and throwing once every other day, controlling the temperature between 50-70 ℃ and fermenting for 5-10 days; (2) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, adding 0.5-3% of secondary fermentation microbial agent, and continuously decomposing for 7-15 days at 35-40 ℃ to complete decomposition; (3) Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging; the crude crushed borneol camphor residual branches and leaves are obtained by crushing the borneol camphor branches and leaves after extracting natural borneol by steam distillation; the inorganic nutrient is one or more of calcium superphosphate, potassium sulfate, diammonium phosphate and urea; the primary fermentation microbial agent is one or more of commercial lactobacillus, bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria, and when the primary fermentation microbial agent is more than two, the ligands of the components are equal in weight or can be prepared; the secondary fermentation microbial agent is one or more of azotobacter, phosphate-dissolving bacteria, potassium-dissolving bacteria, bacillus and saccharomycetes sold in the market, and when the secondary fermentation microbial agent is more than two, the ligands of the components are equal in weight or can be prepared.
CN201811503491.6A 2018-12-10 2018-12-10 Biological organic fertilizer special for citrus fruit trees and preparation method thereof Active CN109293453B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811503491.6A CN109293453B (en) 2018-12-10 2018-12-10 Biological organic fertilizer special for citrus fruit trees and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811503491.6A CN109293453B (en) 2018-12-10 2018-12-10 Biological organic fertilizer special for citrus fruit trees and preparation method thereof

Publications (2)

Publication Number Publication Date
CN109293453A CN109293453A (en) 2019-02-01
CN109293453B true CN109293453B (en) 2024-01-09

Family

ID=65141960

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811503491.6A Active CN109293453B (en) 2018-12-10 2018-12-10 Biological organic fertilizer special for citrus fruit trees and preparation method thereof

Country Status (1)

Country Link
CN (1) CN109293453B (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103229706A (en) * 2013-05-20 2013-08-07 湖南省烟草公司永州市公司 Organic matrix for culturing tobacco seedlings
CN103865002A (en) * 2014-03-28 2014-06-18 井冈山大学 High-water absorption humic acid resin with water conserving, water retention and trace fertilizer sustained-release functions
CN104261911A (en) * 2014-09-22 2015-01-07 烟台中正新技术有限公司 Method for preparing organic fertilizer by using plant residues as raw material
CN104909899A (en) * 2015-06-04 2015-09-16 贵州汇民力生物科技有限公司 Production technology of special organic fertilizer for peanut
CN105837285A (en) * 2016-03-25 2016-08-10 镇远县醉美果业有限公司 Preparation method of compound fertilizer for red peaches

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103229706A (en) * 2013-05-20 2013-08-07 湖南省烟草公司永州市公司 Organic matrix for culturing tobacco seedlings
CN103865002A (en) * 2014-03-28 2014-06-18 井冈山大学 High-water absorption humic acid resin with water conserving, water retention and trace fertilizer sustained-release functions
CN104261911A (en) * 2014-09-22 2015-01-07 烟台中正新技术有限公司 Method for preparing organic fertilizer by using plant residues as raw material
CN104909899A (en) * 2015-06-04 2015-09-16 贵州汇民力生物科技有限公司 Production technology of special organic fertilizer for peanut
CN105837285A (en) * 2016-03-25 2016-08-10 镇远县醉美果业有限公司 Preparation method of compound fertilizer for red peaches

Also Published As

Publication number Publication date
CN109293453A (en) 2019-02-01

Similar Documents

Publication Publication Date Title
CN103086769B (en) Dragon fruit-purposed high-potassium organic fertilizer prepared from domestic sludge and fowl manure and production method thereof
CN103304280B (en) Ecological organic fertilizer for preparing golden camellia tea residues and production method thereof
CN102358710B (en) Ecological fertilizer, preparation method, and application of ecological fertilizer in agricultural or forestry production
CN103058748B (en) Preparation method of compound biological pesticide fertilizer special for peach trees and compound biological pesticide fertilizer special for peach trees therefrom
CN104961611A (en) Microbial organic fertilizer having saline-alkali soil improvement function
CN103664353A (en) Microbial organic compound fertilizer based on traditional Chinese medicine waste and preparation method thereof
CN103664352A (en) Microbial organic compound fertilizer based on plant and animal waste and preparation method thereof
CN103274772A (en) Microbial fertilizer produced by utilizing agricultural wastes
CN103664286A (en) Organic leaf surface fertilizer rich in organic selenium and vitamins and preparation method for organic leaf surface fertilizer
CN103664354A (en) Organic-selenium-enriched microorganism organic composite fertilizer and preparation method thereof
CN108821873A (en) Rice hull carbon base manure material and preparation method thereof and its application in Rice Cropping
CN105237249A (en) Compound fertilizer for promoting increasing of production and income of maize
CN105237058A (en) Bio-organic fertilizer and preparation method thereof
CN103833460A (en) Microbial organic compound fertilizer rich in essential amino acids and preparation method thereof
CN103524228A (en) Special biofertilizer for cucumbers and preparation method thereof
CN105753526A (en) Method for composting by utilizing straw
CN107188633A (en) A kind of compound method of vegetable cultivation ecological fertilizer
CN109020688A (en) Anaerobism adds the method for aerobic fermentation production ecological organic fertilier
CN101560122A (en) Special compound fertilizer for bamboo and preparing method thereof
CN111499455A (en) Bio-organic fertilizer and preparation method and application thereof
CN109279993B (en) Biological organic fertilizer and preparation method thereof
CN101255073B (en) Method for preparing stone slope greening base material by steam explosion of plant straw and solid-state fermentation
CN116553971B (en) Special fertilizer for planting waxberries and preparation method thereof
CN110015936B (en) Functional organic fertilizer for improving saline-alkali soil and preparation method thereof
CN103787729A (en) Organic fertilizer and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant