CN109279993B - Biological organic fertilizer and preparation method thereof - Google Patents

Biological organic fertilizer and preparation method thereof Download PDF

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CN109279993B
CN109279993B CN201811503480.8A CN201811503480A CN109279993B CN 109279993 B CN109279993 B CN 109279993B CN 201811503480 A CN201811503480 A CN 201811503480A CN 109279993 B CN109279993 B CN 109279993B
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microbial agent
organic fertilizer
primary
fermentation microbial
fermentation
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CN109279993A (en
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隋岩
陈丽
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Jinggangshan University
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Jinggangshan University
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/02Superphosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/50Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/133Renewable energy sources, e.g. sunlight
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Soil Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a biological organic fertilizer and a preparation method thereof. The technological process includes chicken and duck feces 40-60%, borneol camphor residual branch and leaf small segment 20-30%, humic acid 10-20% and inorganic nutrient 2-9%. Adjusting the water content to 40-60%, inoculating 0.5-3% of primary fermentation microbial agent, fermenting, turning over and throwing once every other day, and fermenting at 50-70deg.C for 5-10 days. Transferring the primary fermented and decomposed product to a secondary fermentation workshop, inoculating 0.5-2% of secondary fermentation microbial agent, and continuously decomposing for 7-15 days at 35-40 ℃ to complete the decomposition. Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging. The produced bio-organic fertilizer meets the requirements of the bio-organic fertilizer industry standard NY884-2012, is beneficial to realizing the yield and income increase and the disease resistance enhancement of citrus fruit trees, and realizes changing waste into valuables.

Description

Biological organic fertilizer and preparation method thereof
Technical Field
The invention relates to the technical field of agricultural fertilizers, in particular to a special bio-organic fertilizer for citrus fruit trees, which is produced by using borneol camphor residual branches and leaves as auxiliary materials, and a preparation method thereof.
Background
China is a large agricultural country, and agricultural production is not separated from fertilizer use. The traditional inorganic or inorganic compound fertilizer is really used for increasing the yield and income of agriculture, but the damage to soil and environment caused by long-term application threatens the sustainable development problem of agriculture, protects the ecological environment, develops organic ecological agriculture, and increases the demand for bio-organic fertilizer year by year. The special bio-organic fertilizer is developed by utilizing different waste resources, which is beneficial to realizing changing waste into valuables and meets the market development requirement.
The borneol camphora branches and leaves are the best resources for extracting natural borneol, are developed into a mature technology, but are limited by the content of the natural borneol and the extraction technology, the general crude product yield is about 1%, about 99% of borneol camphora residual branches and leaves are by-products after being extracted by steam distillation, jiangxi is taken as a main production area of the natural borneol, the annual borneol camphora residual branches and leaves can reach 5-8 ten thousand tons, and certain enterprises crush the borneol camphora residual branches and leaves to be made into low-added-value products such as borneol incense and sell the borneol camphora products, and the other enterprises directly use the borneol camphora residual branches and leaves as fuel, so that the problem of how to improve the utilization value of the borneol camphora residual branches and leaves is always an urgent need of the natural borneol enterprises. The residual branches and leaves of borneol camphor also contain a small part of natural borneol, limonene, alpha-pinene, beta-pinene and other substances which are beneficial components for enhancing the disease resistance of citrus fruit trees. If the microbial organic fertilizer can be used as an auxiliary material to be mixed with livestock manure to prepare the microbial organic fertilizer, the microbial organic fertilizer can be helpful for enhancing the efficacy of the microbial organic fertilizer for citrus fruit trees, and no related research and application report exists at present.
Disclosure of Invention
The invention aims to provide a special bio-organic fertilizer for citrus fruit trees, which is high in fertilizer efficiency and strong in disease resistance, by using the residual branches and leaves of borneol camphor trees as auxiliary materials.
The aim of the invention is achieved by the following technical scheme:
(1) Sun-drying residual branches and leaves of Cinnamomum camphora, and coarsely pulverizing into small segments of 0.5-10 cm for use;
(2) The raw materials are mixed according to the following weight ratio: 40-60% of chicken and duck manure, 20-30% of borneol camphor residual branch and leaf small segments, 10-20% of humic acid and 2-9% of inorganic nutrients. Adjusting the water content to 40-60%, inoculating 0.5-3% of primary fermentation microbial agent, fermenting, turning over and throwing once every other day, and fermenting at 50-70deg.C for 5-10 days.
(3) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, inoculating 0.5-2% of secondary fermentation microbial agent, and continuously decomposing for 7-15 days at 35-40 ℃ to complete the decomposition.
(4) Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging.
The inorganic nutrient in the step (2) is one or more of calcium superphosphate, potassium sulfate, diammonium phosphate, urea, copper sulfate, ferrous sulfate, cerium nitrate and lanthanum nitrate;
the primary fermentation microbial agent in the step (2) is one or more of lactobacillus, bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria, and when the primary fermentation microbial agent is more than two, the ligands of the components are prepared in equal weight or proportion;
the secondary fermentation microbial agent in the step (3) is one or more of azotobacter, phosphate-dissolving bacteria, potassium-dissolving bacteria, bacillus and saccharomycetes sold in the market, and when the secondary fermentation microbial agent is more than two, the ligands of the components are prepared in equal weight or proportion.
The biological organic fertilizer is used for planting citrus fruit trees.
The invention has the following advantages:
1. the method provides an effective strategy for full coverage utilization of borneol camphor branch and leaf resources, and utilizes borneol plants to extract natural borneol and then residual borneol camphor branch and leaf as auxiliary materials to produce the special bio-organic fertilizer for citrus fruit trees, thereby fully playing the promotion role of beneficial substances in the bio-organic fertilizer on the growth and development of the citrus fruit trees.
2. The secondary fermentation technology is adopted, the high-temperature fermentation technology is adopted in the primary fermentation process, germs and eggs can be effectively killed, and the low-temperature fermentation technology is adopted in the secondary fermentation process, so that a large amount of beneficial microbial agents can survive in the product;
3. the prepared special bio-organic fertilizer for citrus trees has high fertilizer efficiency and strong disease resistance, can meet the growth and development requirements of the citrus trees, and particularly can greatly reduce the incidence rate of yellow dragon disease of the citrus trees;
Detailed Description
Example 1
1) Sun-drying residual branches and leaves of Cinnamomum camphora, and coarsely pulverizing into 1 cm small sections for later use;
2) The raw materials are mixed according to the following weight ratio: 53% of chicken and duck manure, 25% of borneol camphor residual branch and leaf small sections, 15% of humic acid and 7% of inorganic nutrients. The water content of the microbial inoculum is regulated to be about 45 percent, and 1 percent of primary fermentation microbial inoculum is inoculated for fermentation, and the microbial inoculum is turned and thrown once every other day, and the fermentation is carried out for 7 days at the temperature of 60-65 ℃. The inorganic nutrient is calcium superphosphate, potassium sulfate, urea and lanthanum nitrate which are mixed according to the proportion of 5:3:5:1, and the primary fermentation microbial agent is mixed according to the equal weight ratio of lactobacillus, bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria.
3) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, inoculating 0.5% of secondary fermentation microbial agent (mixed by mass ratio of bacillus, saccharomycetes and the like), and continuously decomposing for 15 days at the temperature of 35-40 ℃ to finish the decomposition.
4) Drying the fermented material in the sun or at low temperature, controlling the water content below 30%, pulverizing, sieving, and packaging.
Example 2
1) Sun-drying residual branches and leaves of Cinnamomum camphora, and coarsely pulverizing into 2 cm pieces for use;
2) The raw materials are mixed according to the following weight ratio: 50% of chicken and duck manure, 30% of borneol camphor residual branch and leaf small sections, 12% of humic acid and 8% of inorganic nutrients. The water content of the microbial inoculum is regulated to be about 45 percent, and 1 percent of primary fermentation microbial inoculum is inoculated for fermentation, and the microbial inoculum is turned and thrown once every other day, and the fermentation is carried out for 7 days at the temperature of 60-65 ℃. The inorganic nutrient is calcium superphosphate, urea and lanthanum nitrate which are mixed according to the proportion of 8:5:1, and the primary fermentation microbial agent is mixed according to the equal weight ratio of bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria.
3) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, inoculating 0.8% of secondary fermentation microbial agent (mixing nitrogen-fixing bacteria and bacillus in the mass ratio), and continuously decomposing for 15 days at 35-40 ℃ to complete the decomposition.
4) Drying the fermented material in the sun or at low temperature, controlling the water content below 30%, pulverizing, sieving, and packaging.
Example 3
1) Sun-drying residual branches and leaves of Cinnamomum camphora, and coarsely pulverizing into small sections of 0.5 cm for use;
2) The raw materials are mixed according to the following weight ratio: 41% of chicken and duck manure, 30% of borneol camphor residual branch and leaf small sections, 20% of humic acid and 9% of inorganic nutrients. The water content of the microbial inoculum is regulated to be about 45 percent, and 1 percent of primary fermentation microbial inoculum is inoculated for fermentation, and the microbial inoculum is turned and thrown once every other day, and the fermentation is carried out for 7 days at the temperature of 60-65 ℃. Inorganic nutrients are calcium superphosphate, potassium sulfate, diammonium phosphate, urea, copper sulfate, ferrous sulfate and cerium nitrate which are mixed according to the proportion of 6:4:3:4:0.5:0.5:0.3, and the primary fermentation microbial agent is prepared by mixing bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria according to the equal weight ratio.
3) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, inoculating 1% of secondary fermentation microbial agent (mixing azotobacter, phosphate-dissolving bacteria, potassium-dissolving bacteria, bacillus, saccharomycetes and the like in mass ratio), and continuously decomposing for 15 days at the temperature of 35-40 ℃ to finish the decomposition.
4) Drying the fermented material in the sun or at low temperature, controlling the water content below 30%, pulverizing, sieving, and packaging.
Example 4
The humic acid is used for replacing the residual branches and leaves of borneol camphor as comparison, and the specific steps are as follows:
1) The raw materials are mixed according to the following weight ratio: 53% of chicken and duck manure, 40% of humic acid and 7% of inorganic nutrients. The water content of the microbial inoculum is regulated to be about 45 percent, and 1 percent of primary fermentation microbial inoculum is inoculated for fermentation, and the microbial inoculum is turned and thrown once every other day, and the fermentation is carried out for 7 days at the temperature of 60-65 ℃. The inorganic nutrient is calcium superphosphate, potassium sulfate, urea and lanthanum nitrate which are mixed according to the proportion of 5:3:5:1, and the primary fermentation microbial agent is mixed according to the equal weight ratio of lactobacillus, bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria.
2) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, inoculating 0.5% of secondary fermentation microbial agent (mixed by mass ratio of bacillus, saccharomycetes and the like), and continuously decomposing for 15 days at the temperature of 35-40 ℃ to finish the decomposition.
3) Drying the fermented material in the sun or at low temperature, controlling the water content below 30%, pulverizing, sieving, and packaging.
The bio-organic fertilizers of examples 1-4 prepared by the method were tested with reference to industry standard NY884-2012, and the bio-organic fertilizers of examples 1-4 were used for comparison study of adult navel orange trees in adjacent plots, and experimental results are shown in table 1 under the same field management mode. TABLE 1 biological organic fertilizer technical index and application experiment result
From table 1, it can be seen that the organic fertilizer prepared by the invention can effectively reduce the incidence of yellow dragon disease.

Claims (1)

1. A preparation method of a bio-organic fertilizer for enhancing disease resistance of citrus fruit trees is characterized by comprising the following steps: (1) Sun-drying residual branches and leaves of Cinnamomum camphora, and coarsely pulverizing into small segments of 0.5-10 cm for use; (2) mixing the following raw materials in parts by weight: 40-60% of chicken and duck manure, 20-30% of borneol camphor residual branch and leaf small segments, 10-20% of humic acid and 2-9% of inorganic nutrient, adjusting the water content to 40-60% and then inoculating 0.5-3% of primary fermentation microbial agent for fermentation, turning over and throwing once every day, and controlling the temperature between 50-70 ℃ for fermentation for 5-10 days to obtain a primary fermentation thoroughly decomposed product, wherein the turning over and throwing times need to be increased if the temperature is too high; (3) Transferring the primary fermented and decomposed product to a secondary fermentation workshop, inoculating 0.5-2% of secondary fermentation microbial agent, and continuously decomposing for 7-15 days at 35-40 ℃ to complete decomposition; (4) Drying the fermented material in the sun or at low temperature, controlling the water content to 20-40%, pulverizing, sieving, and packaging; the inorganic nutrient in the step (2) is one or more of calcium superphosphate, potassium sulfate, diammonium phosphate, urea, copper sulfate, ferrous sulfate, cerium nitrate and lanthanum nitrate; the primary fermentation microbial agent in the step (2) is one or more of lactobacillus, bacillus subtilis, thermophilic side spore mould and thermophilic heterotrophic ammonia oxidizing bacteria, and when the primary fermentation microbial agent is two or more than two, the ligands of the components are equal in weight or can be prepared; the secondary fermentation microbial agent in the step (3) is one or more of azotobacter, phosphate-dissolving bacteria, potassium-dissolving bacteria, bacillus and saccharomycetes sold in the market, and when the secondary fermentation microbial agent is two or more than two, the ligands of the components are prepared in an equal weight or proportion.
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Publication number Priority date Publication date Assignee Title
CN109937845A (en) * 2019-02-22 2019-06-28 霍山岳衡茧丝绸有限公司 A kind of production method improving Dendrobidium huoshanness alkaloid matrix
CN111574297A (en) * 2020-04-28 2020-08-25 四川施利旺农业科技开发有限公司 Special biochar-based fertilizer for cinnamomum camphora trees and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103229706A (en) * 2013-05-20 2013-08-07 湖南省烟草公司永州市公司 Organic matrix for culturing tobacco seedlings
CN104261911A (en) * 2014-09-22 2015-01-07 烟台中正新技术有限公司 Method for preparing organic fertilizer by using plant residues as raw material
CN105837285A (en) * 2016-03-25 2016-08-10 镇远县醉美果业有限公司 Preparation method of compound fertilizer for red peaches
CN106045735A (en) * 2016-08-25 2016-10-26 谭仁燕 Microbial organic fertilizer for preventing and treating peach leaf curl and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103229706A (en) * 2013-05-20 2013-08-07 湖南省烟草公司永州市公司 Organic matrix for culturing tobacco seedlings
CN104261911A (en) * 2014-09-22 2015-01-07 烟台中正新技术有限公司 Method for preparing organic fertilizer by using plant residues as raw material
CN105837285A (en) * 2016-03-25 2016-08-10 镇远县醉美果业有限公司 Preparation method of compound fertilizer for red peaches
CN106045735A (en) * 2016-08-25 2016-10-26 谭仁燕 Microbial organic fertilizer for preventing and treating peach leaf curl and preparation method thereof

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