CN109276477A - A kind of bubble sense mousse composition and its application in cosmetics - Google Patents
A kind of bubble sense mousse composition and its application in cosmetics Download PDFInfo
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- CN109276477A CN109276477A CN201811145705.7A CN201811145705A CN109276477A CN 109276477 A CN109276477 A CN 109276477A CN 201811145705 A CN201811145705 A CN 201811145705A CN 109276477 A CN109276477 A CN 109276477A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/14—Liposomes; Vesicles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
Abstract
The invention belongs to cosmetic field, it is related to a kind of bubble sense mousse composition and preparation method.By weight percentage with the bubble sense mousse composition, be 10%-40% comprising acrylic acid (ester) class cross-linked polymer sodium -2, stabilizer is 5-35% and dispersing agent polyalcohol is 50-70%.Bubble sense mousse composition of the invention can provide slim and graceful tender texture in cosmetics, flexible bubble sense of touch, stable mousse sand ice-like dumb light appearance can be formed, it is provided for cosmetics and fine and smooth moistens salubrious skin sense, slim and graceful ventilated membrane, no stranding mud phenomenon and closed greasy residual sense are formed in skin surface.Simple process is easy to operate simultaneously, has the characteristics that cold can to match, good dispersion, nothing " flake ", not fugitive dust.
Description
Technical field
The invention belongs to a kind of compositions of cosmetic composition technical field more particularly to a kind of bubble sense mousse to combine
Object and its application in cosmetics.
Background technique
As Cosmetic Market consumption accounting share was increasing in recent years, consumer constantly proposes the cognition degree of cosmetics
Height has the cosmetics of innovative appearance and good experience sense quality by the approval of more and more consumers and likes, such as
Genius water swaggers foundation emulsion, pigment frost, concealer, sunscreen stick and ampoule bottle essence etc..
However passes through market survey and find that it is actually rare on the market to have bubble sense mousse quality product.
Xiang Qiongbiao etc. has been reported a kind of water lock moisture-keeping composition with mousse quality, and discovery connects containing Sodium Polyacrylate
The composition of branch starch, quaternary ammonium salt -51 and ceramide can persistently be skin replenishing water and preserving moisture, with the quality as mousse, use
When there is unique skin sense, but because its production technology each component containing ceramide can only add one by one in the composition, and formula at
This is relatively high, and compared with acrylic acid (ester) the class cross-linked polymer sodium -2 of phase homogenous quantities, viscosity wants small.
Li Jiaxin etc. to a kind of mousse type cloth veneer film formulation the study found that Sodium Polyacrylate can be used as skin sense conditioner,
Form the sliding fine and smooth texture of children in mobility, perfection fitting skin concavo-convex portion is easily quickly absorbed by the skin, but with phase homogenous quantities
Acrylic acid (ester) class cross-linked polymer sodium -2 compare, viscosity wants small, and in cosmetics be in bright looking quality.
Acrylic acid (ester) class cross-linked polymer sodium -2 is a kind of white powder, is expanded after water suction, intolerant to ion, in cosmetics
Field is used for thickener, and in pH6.5 or more, few additive can be such that product viscosity is promoted, and the salubrious appearance of transparence is presented.When it contains
When amount improves, mousse shape sand ice appearance can be formed, but cause the pH value in product to increase at this time, while the appearance is in cold environment
Medium viscosity can sharply decline, unstable, high viscosity required for being unable to maintain that and Sha Bing quality.And improve the acrylic acid of additive amount
(ester) class cross-linked polymer sodium -2 is easy conglomeration in water and is not easy to disperse, and cost increases, while having dust raising phenomenon.
In product development process, discovery will appear appearance using the cosmetics of acrylic acid (ester) class cross-linked polymer sodium -2
Quality and the unstable problem of viscosity, it is desirable to provide a kind of composition technology, by by acrylic acid (ester) class cross-linked polymer sodium-
2 improve its preparation while playing the superior functionality of acrylic acid (ester) class cross-linked polymer sodium -2 with the combination of additive
The stability of product increases its market utility value.However it temporarily there are no the relevant report of such technology.
The prior art (CN107951805A, publication date 2018.4.24) though reporting a kind of solarization containing dendrobium candidum after repair
Multiple gel and preparation method thereof, application of the major embodiment Dendrobium officinale polysaccharide as core active ingredient in after-sun recovery field,
It is that the husky ice appearance of graininess illusion is reached as thickener using Sodium Polyacrylate.There is the crosslinking of open acrylic acid (ester) class poly- simultaneously
Application of the object sodium -2 in the formula is closed, however from the technology production technology it can be found that thickener is both needed to impregnate swelling completely
After dispersion, progress heat is with processing, and time-consuming for production technology, is not easy to disperse, easy fugitive dust and generation " flake " phenomenon；From embodiment
It is visible in 1-3 detection performance to be resisted cold stability test by 48h, but whether can be not have by shelf life stability requirement in 3 years
It refers to.
Therefore, develop it is a kind of form stable mousse sand ice-like dumb light appearance, simple process is easy to operate, have cold can match,
Good dispersion, nothing " flake ", not fugitive dust the features such as mousse quality combination have great market application prospect.
Summary of the invention
It is an object of that present invention to provide a kind of bubble sense mousse compositions.
Bubble sense mousse composition of the invention can provide slim and graceful tender texture, flexible bubble sense of touch, and be formed
Stable mousse sand ice-like dumb light appearance, for cosmetics provide it is fine and smooth moisten salubrious skin sense, formed in skin surface slim and graceful ventilative
Film, no stranding mud phenomenon and closed greasy residual sense.Simultaneously simple process it is easy to operate, have cold can match, good dispersion, nothing
" flake ", not fugitive dust the features such as.
Further aim of the present invention is to provide a kind of application of bubble sense mousse composition in cosmetics.
Further aim of the present invention is to provide a kind of cosmetics of bubbles sense mousse composition.
In order to solve the above technical problems, the concrete scheme that the present invention uses is as follows:
On the one hand, the present invention provides a kind of bubble sense mousse compositions comprising the component of following weight percent meter:
Acrylic acid (ester) class cross-linked polymer sodium -2 is 10-40%, stabilizer 5-35%, polyalcohol 50-70%.
When the additional amount of stabilizer is 10-40%, the stability for promoting husky ice mousse quality can be helped；When dispersing agent plus
When to enter amount be 5-35%, composition rapid dispersion and hydration in water can help to, help maintains dumb light shape sand ice mousse low temperature
Stability.
As a preferred embodiment, including following components in percentage by weight: acrylic acid (ester) class cross-linked polymeric
Object sodium -2 is 20-35%, stabilizer 10-25%, polyalcohol 50-65%.
As an implementation, the acrylic acid in the present composition (ester) class cross-linked polymer sodium -2, stabilizer, more
The weight fraction ratio of first alcohol is 1:(0.25~3.5): (1~8)；It can provide slim and graceful tender texture, flexible bubble sense of touch,
And stable husky ice-like mousse dumb light appearance is formed, it is provided for cosmetics and fine and smooth moistens salubrious skin sense.It is formed gently in skin surface
It is full of ventilated membrane, no stranding mud phenomenon and closed greasy residual sense.Simultaneously simple process it is easy to operate, have cold can match, fine dispersion
Property, nothing " flake ", not fugitive dust the features such as.
As a preferred embodiment, acrylic acid (ester) class cross-linked polymer sodium -2 in the present composition, steady
Determine agent, the weight fraction ratio of polyalcohol is 1:(0.3~2.5): (1~6).
A kind of acrylic acid (ester) class cross-linked polymer sodium-as more preferably embodiment, in the present composition
2, stabilizer, polyalcohol weight fraction ratio be 1:(0.3~2): (1~5).
In the present invention, the stabilizer includes poloxamer188, hydroxypropyl starch phosphate, xanthan gum, hydroxypropyl first
One of base cellulose and carragheen are a variety of.
As a preferred embodiment, the optional poloxamer188 of the stabilizer, hydroxypropyl starch phosphate,
Xanthan gum, hydroxypropyl methyl cellulose.
As a kind of more preferably embodiment, the stabilizer is poloxamer188, hydroxypropul starch phosphoric acid
Ester, xanthan gum.
As a kind of highly preferred embodiment, the stabilizer is poloxamer188 and hydroxypropul starch phosphoric acid
Ester.
The polyalcohol added in bubble sense mousse composition of the invention is selected from 1,2- propylene glycol, 1,3- propylene glycol, fourth two
One of alcohol, dipropylene glycol, methyl propanediol are a variety of.
As a preferred embodiment, the polyalcohol includes one of 1,3-PD, methyl propanediol
Or it is a variety of.
As a kind of more preferably embodiment, the polyalcohol is methyl propanediol.
In one embodiment of the invention, when acrylic acid (ester) class cross-linked polymer sodium -2, poloxamer188 and hydroxypropyl
Base starch phosphate and methyl propanediol are added according to 1:0.5:1.83 ratio reaches best effects.
On the other hand, the present invention provides a kind of preparation methods of composition, comprising the following steps:
(1) successively polyalcohol, acrylic acid (ester) class cross-linked polymer sodium -2 and stabilizer are added in clean reaction kettle；
(2) mixing is stirred at low speed at normal temperature；
(3) closed storage under room temperature, it is spare.
Composition of the invention is mainly used in cosmetics, but specific cosmetics are not particularly limited.Cosmetics
It can be gel, emulsion, cream or makeup removing type cosmetics；Preferably, the emulsion-type cosmetics are moisturizing lotion, skin care essence
China, eye essence or body lotion；Or it is preferred, the makeup removing type cosmetics include makeup removing breast or makeup removing frost.
Preferably, the cosmetics are gel product.
It is further preferred that the gel type cosmetics are moisturizing gel or sleep mask.
Wherein, the weight percent that the cosmetics contain the bubble sense mousse composition is 1-8%；Preferably 2-
5%；The bubble sense of touch of elasticity can be provided to cosmetics, bring stable Sorbet mousse dumb light quality, skin sense is clearly moistened not
It is sticky, slim and graceful ventilated membrane is formed in skin surface, and skin is free of a burden, noresidue sense.
It is that the present invention obtains the utility model has the advantages that
1, bubble sense mousse composition of the invention can provide slim and graceful tender texture, flexible bubble sense of touch, and shape
At stable mousse sand ice-like dumb light appearance, for cosmetics provide it is fine and smooth moisten salubrious skin sense, skin surface formed it is slim and graceful thoroughly
Air film, no stranding mud phenomenon and closed greasy residual sense.Simultaneously simple process it is easy to operate, have cold can match, good dispersion, nothing
" flake ", not fugitive dust the features such as.Its is highly-safe, can prevent the loss of keratoderma moisture, thus realize skin care,
It is provided for cosmetics and fine and smooth moistens salubrious skin sense.
Specific embodiment
Technical solution of the present invention is further illustrated below by way of specific embodiment, and specific embodiment does not represent to this hair
The limitation of bright protection scope.Other people according to the present invention theory made it is some it is nonessential modification and adjustment still fall within this hair
Bright protection scope.
The formula and preparation method of 1 mousse composition I of embodiment
Preparation method:
(1) polyalcohol, acrylic acid (ester) class cross-linked polymer sodium -2 and stabilizer are successively weighed according to above table, are added
Into clean reaction kettle；
(2) low speed 500rpm/min stirring 5min is uniformly mixed at normal temperature；
(3) closed storage under room temperature, it is spare.
The formula and preparation method of 2 mousse composition II of embodiment
The preparation method is the same as that of Example 1, obtains mousse composition II.
The formula and preparation method of 3 mousse composition III of embodiment
The preparation method is the same as that of Example 1, obtains mousse composition III.
The formula and preparation method of 4 mousse composition IV of embodiment
After mixing evenly by above-mentioned each component, mousse composition additive IV is obtained.
The formula and preparation method of 5 mousse composition V of embodiment
The preparation method is the same as that of Example 1, obtains mousse composition V.
The formula and preparation method of 6 mousse composition VI of embodiment
The preparation method is the same as that of Example 1, obtains mousse composition VI.
The formula and preparation method of 7 mousse composition VII of embodiment
The preparation method is the same as that of Example 1, obtains mousse composition VII.
The formula and preparation method of 8 mousse composition VIII of embodiment
The preparation method is the same as that of Example 1, obtains mousse composition VIII.
The formula and preparation method of 9 mousse composition IX of embodiment
The preparation method is the same as that of Example 1, obtains mousse composition IX.
Comparative example 1
Compared with embodiment 2, in addition to not adding stabilizer, other ingredients and its content are the same as embodiment 2.
Comparative example 2
Compared with embodiment 2, in addition to the content of polyalcohol is insufficient, other ingredients and its content are the same as embodiment 2.
Comparative example 3
Compared with embodiment 2, form sediment in addition to acrylic acid (ester) class cross-linked polymer sodium -2 is substituted for Sodium Polyacrylate grafting
Powder, other ingredients and its content are the same as embodiment 2.
Comparative example 4
Compared with embodiment 2, in addition to the type of polyalcohol is substituted for glycerol, other ingredients and its same embodiment of content
2。
Comparative example 5
Compared with embodiment 7, in addition to changing stabilizer type into ammonium acryloyl taurate/VP copolymer, other
Ingredient and its content with embodiment 7.
Comparative example 6
Compared with embodiment 2, in addition to acrylic acid (ester) class cross-linked polymer sodium -2 measures deficiency, other compositions and its content are same
Embodiment 2.
Comparative example 7
Compared with embodiment 8, stabilizer type changes Sodium Polyacrylate, other compositions and its content into embodiment 8.
Comparative example 8
Compared with embodiment 2, stabiliser content is insufficient, and other compositions and its content are the same as embodiment 2.
Embodiment 10<physical and chemical stability test>
Mousse composition additive II prepared by mousse composition additive I prepared by embodiment 1, embodiment 2, implement
The mousse of mousse composition additive V, the preparation of comparative example 1 prepared by the mousse composition additive III of the preparation of example 3, embodiment 5
The mousse composition additive of mousse composition additive XI, the preparation of comparative example 3 prepared by composition additive X, comparative example 2
The mousse composition additive XV and comparative example of mousse composition additive XIII, the preparation of comparative example 6 prepared by XII, comparative example 4
8 preparation mousse composition additive XVII be dissolved in the deionized water containing 1% Phenoxyethanol respectively, respectively obtain 2% it is saturating
Bright gel, and study on the stability is carried out by the following terms test request respectively.
In 25 DEG C, 60%RH is stood room temperature sample, compares test.
Cold-resistant test: freezer compartment of refrigerator is placed 10 days.
40 DEG C of Acceleration studies: experiment condition is 40 DEG C ± 2 DEG C, and 75%RH ± 5%RH is placed 3 months.
Cold cycling: -18 DEG C, 25%RH；25 DEG C, 60%RH；40 DEG C, 75%RH, for 24 hours, totally 5 recycle each temperature.
Light stablizes (instrument): intensity of illumination 0.35W/M2, test 26.4 hours, 45 DEG C of blackboard temperature, humidity 50%.
Light stablizes (outdoor): natural light irradiation 10 days.
Appearance: the visual observations under room temperature and non-direct sunlight of materialsing
PH (dilution method) is carried out with reference to [GB/T13531.1].
Viscosity: standing 24 hours for the sample prepared at 25 DEG C, with Brookfield DVII RV viscosimeter, turns
Axis TD is measured at 5rpm, or is measured using its equivalent way.
As can be seen from Table 1, under 2% same concentrations, to the embodiment of the present invention 1, embodiment 2, embodiment 3 and embodiment
5 mousse composition additive I, II, III and V's is prepared transparent gel, and every physical and chemical testing index variation is without exception,
Has stable bubble sense mousse quality, good dumb light appearance, preparation process is simple, no fugitive dust, nothing " flake " and conglomeration
Phenomenon, favorable dispersibility are easy to cold and match, and physical and chemical testing index is substantially better than comparative example 1-4, comparative example 6 and comparative example 8.
And under same concentrations, the mousse composition additive X of comparative example 1 and the mousse composition additive of comparative example 8
The transparent gel that XVII is prepared, compared with the embodiment of the present invention 2, due to lacking stabilizer element or stabilizer additive amount not
Foot makes the viscosity degradation during its cold-resistant and cold cycling stability test, while bubble sense mousse quality also occurs
Change.
During the mousse composition additive XI of comparative example 2 prepares transparent gel, because of polyol amount deficiency, propylene
Sour (ester) class cross-linked polymer sodium -2 and stabilizer can not be soaked all, while fugitive dust, " flake " and clustering phenomena occur, with reality
It applies example 2 to compare, needing more times just can be uniformly dispersed and sufficiently hydration is just able to maintain transparent appearance, while pH is obviously wanted
Height also occurs rubbing mud phenomenon with the hands, therefore does not meet preparation process requirement.
The transparent gel prepared by the mousse composition additive XII of comparative example 3, is in bubble sense mousse quality but polarisation is bright
Appearance also easily absorbs although skin sense is merrily and lightheartedly breathed freely, occurs rubbing mud phenomenon with the hands.It is compared with embodiment 2, from test data it is found that admiring
This composition additive XII also can keep stable viscosity and product appearance, but poly- the third of same amount at different temperatures
It is poly- that the viscosity that olefin(e) acid sodium graft starch provides in the product is less than acrylic acid (ester) class crosslinking in mousse compositions of additives II
The viscosity namely acrylic acid (ester) class cross-linked polymer sodium -2 that conjunction object sodium -2 provides are in product development more for excellent in cost
Gesture.
From the detection of the properties of comparative example 4 as it can be seen that transparent gel prepared by mousse composition additive XIII has gas
Bubble sense mousse appearance, has a good dispersibility, but skin sense quality sticks greasy partially, or even has and rubs mud phenomenon with the hands and occur.Although in difference
At a temperature of product can keep good appearance, but viscosity stability test data decreases, unstable, with 2 phase of embodiment
Than because polyalcohol type is different, notable difference occurs in product performance indexes.
Compared with Example 1, it is seen that the transparent gel prepared by the mousse composition additive XV of comparative example 6, because of propylene
Sour -2 additive amount of (ester) class cross-linked polymer sodium is insufficient, and the gel of formation has mobility, while can not form bubble sense mousse
Quality and dumb light appearance, skin sense quality is thick and heavy, is not easy to absorb.
The detection of 1 mousse composition properties of table
Thus, it could be seen that acrylic acid (ester) class cross-linked polymer sodium -2, stabilizer and polyalcohol three it is mutually coordinated under, can make
Standby slim and graceful tender texture, flexible bubble sense of touch, and stable mousse sand ice-like dumb light appearance is formed, it is provided for cosmetics
Fine and smooth to moisten salubrious skin sense, quality is luxurious easily to be absorbed, and forms slim and graceful ventilated membrane, no stranding mud phenomenon in skin surface.Technique simultaneously
It is simple to operation, have the characteristics that cold can to match, good dispersion, nothing " flake ", not fugitive dust.
In addition, the mousse composition additive IV-IX of the embodiment of the present invention 4 and embodiment 6-9 can also prepare every test
The cosmetics of all standard compliant stable mousse sand ice-like dumb light appearance.
Meanwhile 1-9 of the embodiment of the present invention is in the course of the research, find embodiment 2 mousse composition II in product
Appearance and skin sense experience are upper most popular, thus, under the same conditions, it is best that embodiment 2, which plays properties of product effect,.
11 product skin of embodiment sensing is commented
(1) preparation of sleep mask
Application Example 2,7 and 8
It is accounted for and is slept according to the additive amount of mousse composition additive II, VII and VIII of Application Example 2,7 and 8 in the following table 2
The weight percent of dormancy facial mask total amount is 2%, while 3 sections of sleep masks being prepared as steps described below.
The preparation step of sleep mask is as follows:
Step 1: each component in A phase is added in sequence in clean oily phase pot, is stirred at an elevated temperature to 70-75 DEG C
Heat preservation 10min is mixed, dissolution is abundant.
Step 2: B phase raw material being sequentially added in clean reaction kettle and is sufficiently dissolved, and is warming up to 80-85 DEG C of stirring heat preservation
15min.It vacuumizes, A phase is pumped into reaction kettle, after 1200rpm homogeneous 5min, 800rpm insulated and stirred 10min, cooling water drop
Temperature is to 60 DEG C.Under low speed homogeneous be added in advance scattered C phase, 10-15min is sufficiently stirred, continues to be cooled to 45 DEG C, successively plus
Enter D phase and the good E phase of predissolve, stirs.
Step 3: being cooled to 37 DEG C of inspection qualifications, and sleep mask is prepared in 100 mesh filter-cloth filterings.
(2) Comparison study example 3,5 and 7
According to final content of each component of Comparison study example 3, comparative example 5, comparative example 7 in the following table 2 in sleep mask,
And the additive amount of mousse composition additive XII, XIV, XVI are 2%, are prepared 3 according to the preparation step of Application Example
Money sleep mask.
The sleep mask of 2 Application Example 2,7,8 of table and Comparison study example 3,5,7 composition
Subject totally 72 are randomly selected, is divided into 6 groups, every group 12；Wherein, a sleep mask is used for every group.
Experience one week uses 3 times altogether, record subject feedback's overall merit marking situation, and number is as shown in table 3.Score value is set to 0-5
Point: 0 point of meaning with thumb down, 1 point indicates cannot be distinguished, and 2 points indicate acceptable reluctantly, and 3 points are satisfied with, and 4 points of expressions are felt quite pleased,
5 points indicate especially satisfied, and score value is higher to indicate subject to usage experience satisfaction, preference degree and the desire to purchase of the sample more
It is high.
3 sleep mask applicating evaluating grade form of table
As can be seen from Table 3, real according to the present invention in the case where the weight percent of mousse composition is all is 2%
Apply the sleep mask that is prepared of mousse composition additive II, VII and VIII of example 2,7 and 8, the satisfaction of subject, happiness
The number of good degree and desire to purchase evaluated is substantially higher in the number of Comparison study example 3, comparative example 5 and comparative example 7, explanation
Liking for subject is obviously more obtained using the sleep mask that is prepared of mousse composition additive II, VII and VIII.
Husky ice mousse quality, bubble sense of touch, slim and graceful soft and smooth, non-greasy, noresidue sense, without rub with the hands mud, without at informal voucher, moisten
The in-service evaluation clearly and easily absorbed is fine, obtains the approval and approval of subject.Simultaneously to the physics and chemistry of this three sections of products
Performance indicator observation analysis is all tested by items.
Comparative example 3, comparative example 5 and comparative example 7 compare in the experience ratings consumers of husky ice mousse quality and bubble sense of touch
It is satisfied, but exist compared with embodiment 3,7 and 8 in other usage experiences obvious insufficient.
It according to the sleep mask that the mousse composition additive XII of comparative example 3 is prepared, is connect by Sodium Polyacrylate
Branch starch prepares mousse sand ice quality and bubble sense of touch, and product appearance requires detection under the conditions of carrying out to it respectively, can be stable
Keep mousse sand ice quality and bubble sense of touch appearance.Compared with Example 2, but product appearance polarisation is bright, while can cause to smear
In the process at informal voucher phenomenon, and trap wants slow, also causes to rub mud phenomenon with the hands after absorption, thus causes subject to the production
Product satisfaction, preference degree and desire to purchase are relatively low.
According to the sleep mask that the mousse composition additive XIV of comparative example 5 is prepared, compared with Example 7, outside
It sees and slim and graceful soft and smooth, non-greasy, noresidue sense and moist salubrious these usage experiences evaluation is equally matched；Because using acryloyl two
N-methyltaurine ammonium/VP copolymer is as stabilizer, so that the infiltration rate during smearing is very slow, hence it is evident that at informal voucher phenomenon,
Cause subject more less better than sleep mask prepared by embodiment 7 to the satisfaction of the product, preference degree and desire to purchase.Together
When the product that is prepared according to comparative example 5 in the test of cold-resistant and cold cycling, viscosity decline is obvious, and Material is thinning, and causes to admire
This husky ice quality, bubble sense of touch and dumb light appearance have significant change.
Compared with Example 8, according to third that the mousse composition additive XV of comparative example 7 is using 1,3-PD dispersion
The sleep mask that olefin(e) acid (ester) class cross-linked polymer sodium -2 and Sodium Polyacrylate are prepared, under each temperature test conditions of the product
Be able to maintain stable husky ice quality, bubble sense of touch, dumb light appearance, be provided simultaneously with it is slim and graceful it is soft and smooth, moisten salubrious and easily absorb
Usage experience, but the product that prepared lower than embodiment 8 in the favorable comment degree of greasy, residual sense and stranding mud phenomenon experience, while by
Or not that examination person is to the product customer satisfaction, fancy grade and desire to purchase keep the attitude that maintains an equal level.
In addition, the embodiment of the present invention 1,3,4-6,9 mousse composition additive I, III, IV-VI and IX be added to sleep
In facial mask, every product for testing all standard compliant stable mousse sand ice-like dumb light appearance can also be prepared, and provide fine and smooth
Salubrious skin sense is moistened, forms slim and graceful ventilated membrane, no stranding mud phenomenon and closed greasy residual sense in skin surface.
Claims (10)
1. composition as described in claim 1, which is characterized in that the component including following weight percent: acrylic acid (ester) class
- 2 10-40% of cross-linked polymer sodium, stabilizer 5-35%, polyalcohol 50-70%.
2. composition as described in claim 1, which is characterized in that including following components in percentage by weight: acrylic acid (ester)
Class cross-linked polymer sodium -2 is 20-35%, stabilizer 10-25%, polyalcohol 50-65%.
3. composition as described in claim 1, which is characterized in that acrylic acid (ester) the class cross-linked polymer sodium -2 is stablized
Agent, polyalcohol weight percent compare be 1:0.25~3.5:1~8；It is preferred that 1:0.3~2.5:1~6；More preferable 1:0.3~2:
1~5.
4. composition as described in claim 1, which is characterized in that the stabilizer includes poloxamer188, hydroxypropul starch
One of phosphate, xanthan gum, hydroxypropyl methyl cellulose and carragheen are a variety of；Preferably, the stabilizer includes
Poloxamer188, hydroxypropyl starch phosphate, xanthan gum and hydroxypropyl methyl cellulose；More preferably, the stabilizer
For poloxamer188, hydroxypropyl starch phosphate, xanthan gum；Highly preferred, the stabilizer is poloxamer188 and hydroxyl
Propyl starch phosphate.
5. composition as described in claim 1, which is characterized in that the polyalcohol include 1,2-PD, 1,3-PD,
One of butanediol, dipropylene glycol, methyl propanediol are a variety of；Preferably, the polyalcohol includes 1,3-PD and first
One of base propylene glycol is a variety of；More preferably, the polyalcohol is methyl propanediol.
6. a kind of method for preparing composition described in claim 1-5, which comprises the following steps:
(1) successively polyalcohol, acrylic acid (ester) class cross-linked polymer sodium -2 and stabilizer are added in clean reaction kettle；
(2) mixing is stirred at low speed at normal temperature；
(3) closed storage under room temperature, it is spare.
7. any composition of claim 1-5 prepares the application in cosmetics.
8. a kind of cosmetics of any composition of 1-5 containing claim, which is characterized in that contain the combination in cosmetics
The weight percent of object is 1-8%；Preferably 2-5%.
9. according to claim 7-8 application or cosmetics, which is characterized in that the cosmetics include gel, emulsion,
Cream or makeup removing type cosmetics；Preferably, the emulsion-type cosmetics are moisturizing lotion, facial treatment essence, eye essence or body
Cream；Or it is preferred, the makeup removing type cosmetics include makeup removing breast or makeup removing frost.
10. application according to claim 9 or cosmetics, which is characterized in that the cosmetics are gel product；It is preferred that
, the gel type cosmetics are moisturizing gel or sleep mask.
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Effective date of registration: 20220812 Address after: No.23 Xianke Er Road, Huadong Town, Huadu District, Guangzhou City, Guangdong Province 510800 Patentee after: GUANGZHOU KENENG COSMETIC RESEARCH Co.,Ltd. Patentee after: GUANGDONG DANZ GROUP Co.,Ltd. Address before: No.23 Xianke Er Road, Huadong Town, Huadu District, Guangzhou City, Guangdong Province 510800 Patentee before: GUANGZHOU KENENG COSMETIC RESEARCH Co.,Ltd. Patentee before: GUANGZHOU BAIYUN LIANJIA FINE CHEMICAL PLANT Patentee before: GUANGDONG DANZ GROUP Co.,Ltd. |