CN104449405B - A kind of Multifunction liquid shoe polish and preparation method thereof - Google Patents
A kind of Multifunction liquid shoe polish and preparation method thereof Download PDFInfo
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- CN104449405B CN104449405B CN201510004581.0A CN201510004581A CN104449405B CN 104449405 B CN104449405 B CN 104449405B CN 201510004581 A CN201510004581 A CN 201510004581A CN 104449405 B CN104449405 B CN 104449405B
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- shoe polish
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/04—Aqueous dispersions
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- Dispersion Chemistry (AREA)
- Organic Chemistry (AREA)
- Treatment And Processing Of Natural Fur Or Leather (AREA)
Abstract
The invention discloses a kind of Multifunction liquid shoe polish and preparation method thereof, containing following material in described Multifunction liquid shoe polish: Brazil wax, synthesis paraffin, Cera Flava, alkylphenol polyoxyethylene OP-10, silicone oil, lanoline, octadecanol, hexadecanol, ethanol, Oleum Terebinthinae, fatty alcohol-polyoxyethylene ether AESA, oil black nigrosine, glycerol, 5% ethyl hydroxybenzoate alcoholic solution, essence, distilled water. The Multifunction liquid shoe polish that the present invention makes, it is possible to profound moisten, maintenance, cleaning leather, make leather shoes keep long-time gloss, and there is deep layer moisten leather and water-proof function so that leather pliable, high resilience, delay the aging of leather.
Description
Technical field
This product relates to belonging to household chemicals field, more particularly to a kind of Multifunction liquid shoe polish and preparation method thereof.
Background technology
Along with economic development, improving constantly of people's living standard, leather shoes have become as a requisite part in the shoe chest of every household, but hold rag crouching and wipe the behavior of leather shoes by shoe chest, it is clear that do not correspond with nowadays allegro life. traditional solid and paste shoe polish expend people's too many time, and tradition shoe polish generally requires after smearing and first dries, then repeatedly certain luminosity can be obtained with shoe brush polishing again, and coloring is poor, non-watertight, antidusting effect is bad, life-time service is also easily generated folding line, can not effectively soften and maintain cortex, and the liquid shoe polish of commercial type often can only play glazing, the one-side surface actions such as cleaning, and leather shoes can not be given with the maintenance of comprehensive profound level, time one, long leather shoes high-grade more also there will be deformation, fade, scratch, the problem such as come unglued, therefore people need a convenient to use, effect is substantially lasting, and the shoe polish that profound can moisten leather shoes occurs.
Summary of the invention
Shortcoming for above-mentioned prior art, the present invention provides a kind of Multifunction liquid shoe polish and preparation method thereof, overcome after tradition shoe polish is smeared need first to dry, coloring is poor, non-watertight, antidusting effect is bad, and the difficult problem that gloss is bad, the maintenance of leather shoes profound level can also be given simultaneously, slow down aging speed.
To achieve these goals, the present invention provides a kind of Multifunction liquid shoe polish, and described Multifunction liquid shoe polish contains following material and content thereof:
Can according to the needs that essence fragrance is different, described essence can be one or more in Fructus Citri Limoniae essence, peach flavor, Bulbus Lilii essence, osmanthus flower fragrance, rose essence, Fructus Cucumidis sativi essence, flavoring pineapple essence.
Described Multifunction liquid shoe polish preparation method, comprises the steps:
Step one: take 1-5ml distilled water, adds 2-15ml ethanol, 0.5-3g fatty alcohol-polyoxyethylene ether AESA, stirring and dissolving, forms solution A;
Step 2: 3-10g synthesizes paraffin, 0.5-6g Brazil wax, 3-10g Cera Flava join to put in beaker in 60～95 DEG C of water-baths and heat, add 1-7g octadecanol, 1-5g hexadecanol, 2-7g silicone oil, 5-15ml Oleum Terebinthinae, 3-12g lanoline, 5-15g emulsifier op-10 until completely dissolved, continue to heat in water-bath, after the mixture in beaker melts completely, add 0.1-3g oil black nigrosine, be stirred for oil phase;
Step 3: remaining distilled water is placed in 60～95 DEG C of water-baths and heats, for aqueous phase;
Step 4: when oil phase, aqueous phase reach identical temperature, aqueous phase is poured in oil phase, and limit edged stirs towards same direction, obtains emulsion bases;
Step 5: emulsion bases is cooled to 45～50 DEG C, adds 0.05-0.7ml essence, 0.1-0.6g5% ethyl hydroxybenzoate alcoholic solution, 1-5ml glycerol, and stirring is cooled to room temperature and namely obtains liquid shoe polish.
Preferably, in described step 4, aqueous phase is that thread shape is poured in oil phase.
Preferably, the speed stirred towards same direction on limit edged described in step 4 is 75-85r/min.
Preferably, described step 2 and step 3 are all placed in 75 DEG C of water-baths to heat.
Various compositions in the present invention are as follows:
Oleum Terebinthinae is the liquid that a kind of clear, colorless has fragranced, and it is as a kind of excellent organic solvent, and its tack is stronger, it is possible to well other formula components be attached on black leather shoes. Spread upon and leather shoes can effectively prevent soaking of water, make leather shoes totally not spend, coordinate Cera Flava can be effectively improved water proofing property.
Oil black nigrosine strong coloring force, photo absorption performance is strong, because caking property is strong in coating, so the firm performance of color is good. Wiping casting skin footwear color even, will not produce aberration, and oil black nigrosine can also produce extinction effect, makes casting skin footwear seem that outward appearance is soft.
Brazil wax is a kind of nontoxic pure natural wax, has high gloss, very easily emulsifying, has good Oil keeping, and its maximum advantage is to have the unexistent high glossiness of other wax.
Cera Flava can make shoe polish be not easy to dry up, and it is convenient to preserve, and does not worry that shoe polish can become withered and harden, thus causing using. Cera Flava can be absorbed by leather part and form layer protecting film at leather surface, can strengthen the flexibility of leather and can slow down the aging speed of leather, the former coating of leather surface being had certain tint retention, does not affect adhesion strength when leather surface reuses. Environmentally friendly, there is biological degradability.
Excellent synthetic wax and lanoline combine and are dispersed into minimum micro-and nano-particles, along with penetrating agent glycerol penetrates into leather deep layer thus playing the effect of interior lubrication and nourishing, softness that leather through so processing will show and sense of fullness, other wax phase immiscible penetrate into leather coating simultaneously, after surface waxiness is worn, the waxiness of deep layer will slowly migrate out so that this shoe polish brightness persistently, heavily wipe property good.
Silicone oil is the general name of the polydimethylsiloxane of a series of different molecular quality. It is colourless transparent oil liquid, odorless, tasteless, stable chemical nature, and hydrophobicity is strong, can mix with lanoline etc., and is prone to coating, has fabulous lubricant effect, to no skin irritation.
Beneficial effect: the present invention is compared with prior art, the Multifunction liquid shoe polish made, can be profound moisten, maintenance, cleaning leather, not only having general liquid shoe polish and carry easy and convenient feature, and have Multifunctional shoe care composition, it can clean leather shoe surface, leather shoes are made to keep long-time gloss, and there is deep moist leather and water-proof function so that leather pliable, high resilience, thus delay the aging of leather. In a word, the invention enables shoe polish that the nursing of leather shoes is settled at one go, once completed, time saving and energy saving, thus the nursing for various medium-to-high grade leather shoes provides stable guarantee.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.
Embodiment 1
The Multifunction liquid shoe polish of the present embodiment is prepared as follows:
Step one: take 3ml distilled water, adds 8ml ethanol, 2g fatty alcohol-polyoxyethylene ether AESA, stirring and dissolving, forms solution A;
Step 2: 5g synthesizes paraffin, 3g Brazil wax, 6g Cera Flava join to put in beaker in 85 DEG C of water-baths and heat, add 4g octadecanol, 4g hexadecanol, 5g silicone oil, 8ml Oleum Terebinthinae, 8g lanoline, 10g emulsifier op-10 until completely dissolved, continue to heat in water-bath, after the mixture in beaker melts completely, add 2g oil black nigrosine, be stirred for oil phase;
Step 3: 80ml distilled water is placed in 85 DEG C of water-baths and heats, for aqueous phase;
Step 4: when oil phase, aqueous phase reach identical temperature, aqueous phase becomes thread shape to pour in oil phase, and limit edged stirs towards same direction, and speed is 75r/min, obtains emulsion bases;
Step 5: emulsion bases is cooled to 50 DEG C, adds 0.09ml essence, 0.3g5% ethyl hydroxybenzoate alcoholic solution, 3ml glycerol, and stirring is cooled to room temperature and namely obtains liquid shoe polish. Described essence can be one or more in Fructus Citri Limoniae essence, peach flavor, Bulbus Lilii essence, osmanthus flower fragrance, rose essence, Fructus Cucumidis sativi essence, flavoring pineapple essence.
Embodiment 2
The Multifunction liquid shoe polish of the present embodiment is prepared as follows:
Step one: take 5ml distilled water, adds 8ml ethanol, 3g fatty alcohol-polyoxyethylene ether AESA, stirring and dissolving, forms solution A;
Step 2: 6g synthesizes paraffin, 3g Brazil wax, 7g Cera Flava join to put in beaker in 75 DEG C of water-baths and heat, add 2g octadecanol, 2g hexadecanol, 4g silicone oil, 10ml Oleum Terebinthinae, 8g lanoline, 10g emulsifier op-10 until completely dissolved, continue to heat in water-bath, after the mixture in beaker melts completely, add 1g oil black nigrosine, be stirred for oil phase;
Step 3: 90ml distilled water is placed in 75 DEG C of water-baths and heats, for aqueous phase;
Step 4: when oil phase, aqueous phase reach identical temperature, aqueous phase becomes thread shape to pour in oil phase, and limit edged stirs towards same direction, and speed is 85r/min, obtains emulsion bases;
Step 5: emulsion bases is cooled to 50 DEG C, adds 0.2ml essence, 0.5g5% ethyl hydroxybenzoate alcoholic solution, 4ml glycerol, and stirring is cooled to room temperature and namely obtains liquid shoe polish. Described essence can be one or more in Fructus Citri Limoniae essence, peach flavor, Bulbus Lilii essence, osmanthus flower fragrance, rose essence, Fructus Cucumidis sativi essence, flavoring pineapple essence.
Physical and chemical index and the result of embodiment 1,2 are as follows:
Character: this product is that viscosity is suitable for, and glossiness is suitable for, the pure and fresh simple and elegant black emulsion of abnormal smells from the patient.
The Multifunction liquid shoe polish that Example 1,2 prepares, recording pH value is 6.5-7.5.
The Multifunction liquid shoe polish that embodiment 1,2 prepares is packaged in transparent plastic bottle, within one month, observes without denaturalization phenomenon in the refrigerator cold-storages of 4 DEG C. 24h in the calorstat of 55 DEG C, shoe polish is without layering, the phenomenon such as rotten.
Being placed in plastic bottle by shoe polish made for embodiment, room temperature stands to be investigated 6 months, and without lamination, unchanged by rear glossiness, abnormal smells from the patient is unchanged, without denaturalization phenomenon.
Shoe polish obtained by embodiment is packaged in 3000r/min in tool plug test tube, and centrifugal 20min, without lamination.
Shoe polish obtained by embodiment is coated leather shoe surface, uniformly and without obvious granule.
Described Multifunction liquid shoe polish resultant effect is investigated
Wipe, following with leather shoes examination, the effect reached and carry out liquid shoe polish effect that Evaluation operation example 1,2 produces. Adopt public-opinion poll point system, choose the leather shoes of 80 pairs of different brands as object on probation, be arbitrarily divided into two groups, polish shoes with the liquid shoe polish of embodiment 1,2 preparation respectively. Use every day twice, use two months time. Every result of use total score is 5 points: 5 be divided into best result, represents very well, very satisfied; 4 are divided into better; 3 are divided into and can accept; Less than 3 points is bad, it is impossible to accept. It it is below every average. Result is shown in table 1 below:
Table 1
| Result of use | The every average of embodiment 1 | The every average of embodiment 2 |
| Spatter property | 4.9 | 4.9 |
| Alimentary | 4.7 | 4.8 |
| Glossiness | 4.9 | 4.9 |
| Water proofing property | 4.7 | 4.8 |
In sum, the liquid shoe polish that the present invention is made has the effects such as good guard, dust-proof, waterproof, blast, nourishing.
The invention is not limited in above-described embodiment; without departing under present invention spirit and real situation thereof; those of ordinary skill in the art can make various corresponding change and deformation according to the present invention; these phases tackle amendment or the equivalent replacement that the present invention carries out, and it all should be encompassed in the middle of the scope of claim protection of the present invention.
Claims (4)
1. a Multifunction liquid shoe polish preparation method, comprises the steps:
Step one: take 1-5ml distilled water, adds 2-15ml ethanol, 0.5-3g fatty alcohol-polyoxyethylene ether, stirring and dissolving, forms solution A;
Step 2: 3-10g synthesizes paraffin, 0.5-6g Brazil wax, 3-10g Cera Flava join to put in beaker in 60～95 DEG C of water-baths and heat, add 1-7g octadecanol, 1-5g hexadecanol, 2-7g silicone oil, 5-15ml Oleum Terebinthinae, 3-12g lanoline, 5-15g emulsifier op-10 until completely dissolved, continue to heat in water-bath, after the mixture in beaker melts completely, add 0.1-3g oil black nigrosine, be stirred for oil phase;
Step 3: distilled water remaining in total amount 50-100ml is placed in 60～95 DEG C of water-baths and heats, for aqueous phase;
Step 4: when oil phase, aqueous phase reach identical temperature, aqueous phase is poured in oil phase, and limit edged stirs towards same direction, obtains emulsion bases;
Step 5: emulsion bases is cooled to 45～50 DEG C, adds 0.05-0.7ml essence, 0.1-0.6g5% ethyl hydroxybenzoate alcoholic solution, 1-5ml glycerol, and stirring is cooled to room temperature and namely obtains liquid shoe polish.
2. Multifunction liquid shoe polish preparation method according to claim 1, it is characterised in that: in described step 4, aqueous phase is that thread shape is poured in oil phase.
3. Multifunction liquid shoe polish preparation method according to claim 1, it is characterised in that: the speed that limit edged described in step 4 is stirred towards same direction is 75-85r/min.
4. Multifunction liquid shoe polish preparation method according to any one of claim 1-3, it is characterised in that: described step 2 and step 3 are all placed in 75 DEG C of water-baths to heat.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510004581.0A CN104449405B (en) | 2015-01-06 | 2015-01-06 | A kind of Multifunction liquid shoe polish and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510004581.0A CN104449405B (en) | 2015-01-06 | 2015-01-06 | A kind of Multifunction liquid shoe polish and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104449405A CN104449405A (en) | 2015-03-25 |
| CN104449405B true CN104449405B (en) | 2016-06-15 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105419649A (en) * | 2015-12-01 | 2016-03-23 | 赵雅珺 | Liquid shoe polish |
| CN106479734A (en) * | 2016-10-14 | 2017-03-08 | 柳州立洁科技有限公司 | A kind of leatherware cleaning-nursing agent |
| CN108330024B (en) * | 2018-05-03 | 2020-08-18 | 上海奥威日化有限公司 | Cleaning agent composition |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1265409A (en) * | 1999-08-10 | 2000-09-06 | 戴紫风 | Formulation and production process of multipurpose shoe cream |
| CN102634285B (en) * | 2012-03-27 | 2013-08-28 | 河北永泰柯瑞特化工有限公司 | Fur brightener composition and preparation method and application thereof |
| CN102876237B (en) * | 2012-10-12 | 2014-04-16 | 苏州谷力生物科技有限公司 | Leather care oil |
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Inventor after: Sun Shuping Inventor after: Hou Dongxiao Inventor after: An Shuxiang Inventor after: He Xiaoyuan Inventor after: Liu Jing Inventor after: Sun Mei Inventor before: Sun Shuping Inventor before: Hou Dongxiao Inventor before: An Shuxiang |
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