CN109512702A - Mirror surface persistence lip glaze and preparation method thereof - Google Patents

Mirror surface persistence lip glaze and preparation method thereof Download PDF

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Publication number
CN109512702A
CN109512702A CN201811638278.6A CN201811638278A CN109512702A CN 109512702 A CN109512702 A CN 109512702A CN 201811638278 A CN201811638278 A CN 201811638278A CN 109512702 A CN109512702 A CN 109512702A
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parts
mixture
permethyl
mirror surface
lip glaze
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CN109512702B (en
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李静
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GONGJU BIOCHEMISTRY SCIENCE & TECHNOLOGY (KUNSHAN) Co Ltd
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GONGJU BIOCHEMISTRY SCIENCE & TECHNOLOGY (KUNSHAN) Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26—Aluminium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585—Organosilicon compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42—Colour properties
    • A61K2800/43—Pigments; Dyes
    • A61K2800/436—Interference pigments, e.g. Iridescent, Pearlescent
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48—Thickener, Thickening system

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Abstract

The present invention relates to a kind of mirror surface persistence lip glaze and preparation method thereof, and lip glaze includes the component of following parts by weight: 15-35 parts of Permethyl 99A；C30‑45Alkyl dimethicone and C30‑451-3 parts of the mixture of alkene；40-55 parts of mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis；3-5 parts of thickener；12-18 parts of dimethyl silicone polymer；1.5-4 parts of tridecanol trimellitate；0.3-0.5 parts of preservative；4.5-11 parts of functional additive.Primary raw material uses trimethyl silicane acid resin and isomery dodecane in this formula, the former has excellent film forming, the waterproofness of height, superpower transfer resistance, therefore product can generate thin film in lip；The latter has volatility, has lubricity when use, can volatilize after use, therefore while guaranteeing to be easy makeup, extra grease can vapor away again, generate dry and comfortable effect.

Description

Mirror surface persistence lip glaze and preparation method thereof
Technical field
The present invention relates to lip glaze, and in particular to a kind of mirror surface persistence lip glaze and preparation method thereof.
Background technique
Common lip gloss is from having lip brush on the market, and health easy to use, gloss is beautiful, but has smearing to compare under normal conditions Viscous thick and heavy feeling and easy de- adornment；And lipstick makeup after stain power is good, salubrious non-greasy, persistence is good, but lipstick color is not It reaches vivid and uses in consumer as accidentally dropped easy modification fracture.Lip glaze is that a kind of lip Cosmetics of novel vogue are used Product, it is the combination of lipstick and lip gloss, and compared with common lipstick, lip gloss, lip honey, the color saturation of lip glaze is high, appearance It is glittering and translucent, tender texture water profit.It is inadequate that current lip glaze haves the shortcomings that be not easy makeup and makeup removing, mirror surface persistence.
Summary of the invention
In order to overcome drawbacks described above, the present invention provides a kind of mirror surface persistence lip glaze, which has merged lip gloss brilliance The lasting adornment effect of glossy and common lip glaze, comfortable, soft, not sticky give consumer is convenient, unique makeup by.
The present invention is to solve technical solution used by its technical problem:
A kind of mirror surface persistence lip glaze, the component including following parts by weight: 15-35 parts of Permethyl 99A；C30-45Alkyl is poly- Dimethyl siloxane and C30-451-3 parts of the mixture of alkene；The mixture 40- of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis 55 parts；3-5 parts of thickener；12-18 parts of dimethyl silicone polymer；1.5-4 parts of tridecanol trimellitate；Preservative 0.3- 0.5 part and functional additive 4.5-11 parts.
Preferably, the functional additive includes mica, pearl powder, toner and tocopherol acetate.
Preferably, in the functional additive each component parts by weight are as follows: 1-4 parts of mica；Pearl powder 2-4 powder；Color 2-4 parts and tocopherol acetate 0.5-1 parts of powder.
Preferably, the C30-45Alkyl dimethicone and C30-45Weight ratio both in the mixture of alkene are as follows: C30-45Alkyl dimethicone: C30-45Alkene is 3-4:1.
Preferably, the thickener is fumed silica, and the preservative is Phenoxyethanol.
Preferably, viscosity of the dimethyl silicone polymer at 25 DEG C is 5000cP.
Preferably, in the mixture of the Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis two components parts by weight Are as follows: 6-9 parts and 1-3 parts of trimethyl silicane alkoxy esters of silicon acis of Permethyl 99A.
Preferably, the component including following parts by weight: 20-30 parts of Permethyl 99A；C30-45Alkyl dimethicone And C30-451.0-2 parts of the mixture of alkene；40-50 parts of mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis；Poly- two 12-18 parts of methylsiloxane；1.5-4 parts of tridecanol trimellitate；0.5 part of Phenoxyethanol；3-5 parts of fumed silica； 1-3 parts of mica；2-3 parts of pearl powder；2-3 parts and tocopherol acetate 0.5-1 parts of toner.
The present invention also provides a kind of preparation methods of mirror surface persistence lip glaze, and steps are as follows:
Step 1: weighing the toner and tridecanol trimellitate of formula ratio, is uniformly mixed, must mix by three rollers Object A；
Step 2: it weighs the Permethyl 99A of formula ratio, the mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis, gather Dimethyl siloxane is in after mixing, rising to 80-85 DEG C for the temperature of agitated kettle, then weigh the gas phase of formula ratio in agitated kettle Silica and mica are added in agitated kettle, and high-speed stirred must mix until fumed silica and the dispersion of mica substantially uniformity Object B；
Step 3: the C of formula ratio is weighed30-45Alkyl dimethicone and C30-45The mixture of alkene is placed in step Agitated kettle in two continues stirring until the mixture, which is dissolved completely in mixture B, obtains mixture C；
Step 4: the pearl powder of mixture A and formula ratio being added and mixed colours into mixture C, after the completion of toning again The preservative and tocopherol acetate of formula ratio is added, is finally uniformly mixed.
Preferably, suitable tridecyl trimellitate is added in step 1 to pre-process toner.
The beneficial effects of the present invention are:
1) primary raw material uses trimethyl silicane acid resin and isomery dodecane in this formula, and trimethyl silicane acid resin has excellent The waterproofness of different film forming, height, superpower transfer resistance, therefore product can generate thin film in lip, be not easy to take off Adornment；And isomery dodecane mainly utilizes its volatility, has lubricity when in use, can gradually volatilize after use, therefore While guaranteeing to be easy makeup, it can be vapored away again using rear extra grease, generate dry and comfortable effect；
2) lip glaze different from the past adds the system of a large amount of powder thickenings, and this system is equipped with silicon wax (i.e. C30-45Alkyl poly- two Methylsiloxane and C30-45The mixture of alkene), silica gel (i.e. dimethyl silicone polymer) and a small amount of silica (i.e. gas phase titanium dioxide Silicon), while providing thickening to interior material and suspending, the gloss for avoiding the increase of a large amount of powders and eliminating grease itself, simultaneously These raw materials with thickening function also have extraordinary compatibility with body material, therefore this system improves product film forming Brightness and stability afterwards is good；
3) because lip product major function is improvement complexion, so addition colorant and pearl powder etc. are necessarily needed in formula, three The silicone oils such as methane-siliconic acid resin raw material is poor for the dispersibility of toner, therefore the conjunction outstanding using dispersibility in toning Toner is pre-processed at lipid (such as tridecyl trimellitate), is added in system to increase the interior compatibility expected；
4) this lip glaze state is liquid, therefore is easy makeup, can be removed ornaments and formal dress easily when makeup removing using oiliness makeup remover, but Matt different from common lip glaze, the present invention is bright with the soft quality as cashmere, outstanding covering power, color saturation, gloss The lasting adornment effect of the beautiful glossy and common lip glaze for gently covering lips such as second layer skin, having merged lip gloss brilliance, comfortable, soft, Not sticky give consumer is convenient, unique makeup by.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
A kind of mirror surface persistence lip glaze, the component including following parts by weight: 15-35 parts of Permethyl 99A；C30-45Alkyl is poly- Dimethyl siloxane and C30-451-3 parts of the mixture of alkene；The mixture 40- of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis 55 parts；3-5 parts of thickener；12-18 parts of dimethyl silicone polymer；1.5-4 parts of tridecanol trimellitate；Preservative 0.3- 0.5 part and functional additive 4.5-11 parts；The thickener is fumed silica, and the preservative is Phenoxyethanol, institute Stating viscosity of the dimethyl silicone polymer at 25 DEG C is 5000cP.
The functional additive includes mica, pearl powder, toner and tocopherol acetate, in the functional additive The parts by weight of each component are as follows: 1-4 parts of mica；Pearl powder 2-4 powder；2-4 parts and tocopherol acetate 0.5-1 parts of toner.Pearly-lustre Powder and toner can improve the complexion of lip, and lips are moistened while VE makes user feel dry and comfortable.
The C30-45Alkyl dimethicone and C30-45Weight ratio both in the mixture of alkene are as follows: C30-45Alkane Base dimethyl silicone polymer: C30-45Alkene is 3-4:1, which is commercial product, is purchased from Momentive company, and mix Also contain a small amount of cyclomethicone in object, wherein C30-45Alkyl dimethicone is active constituent.It is described different The parts by weight of two components in the mixture of dodecane and trimethyl silicane alkoxy esters of silicon acis are as follows: 6-9 parts of Permethyl 99A part；Front three The mixture of 1-3 parts of base silane oxygroup esters of silicon acis, Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis is commercial product, is purchased from Momentive company.
Preferably, this mirror surface persistence lip glaze includes the component of following parts by weight: 20-30 parts of Permethyl 99A；C30-45Alkane Base dimethyl silicone polymer and C30-451.0-2 parts of the mixture of alkene；Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis it is mixed Close object 40-50 parts；12-18 parts of dimethyl silicone polymer；1.5-4 parts of tridecanol trimellitate；0.5 part of Phenoxyethanol；Gas 3-5 parts of aerosil；1-3 parts of mica；2-3 parts of pearl powder；2-3 parts and tocopherol acetate 0.5-1 parts of toner.
A kind of preparation method of mirror surface persistence lip glaze, steps are as follows:
Step 1: after the toner of formula ratio is first pre-processed with suitable tridecyl trimellitate, then ten with formula ratio Three alkanol trimellitates pass through three rollers together and are uniformly mixed, and obtain mixture A；It is right because in this formula being silicone oil constituents It is poor in the dispersibility of toner, therefore toner is pre-processed using synthesis lipid such as tridecyl trimellitate, it adds The compatibility that product can be increased in system, improves the stability of product；
Step 2: it weighs the Permethyl 99A of formula ratio, the mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis, gather Dimethyl siloxane is in after mixing, rising to 80-85 DEG C for the temperature of agitated kettle, then weigh the gas phase of formula ratio in agitated kettle Silica and mica are added in agitated kettle, and high-speed stirred must mix until fumed silica and the dispersion of mica substantially uniformity Object B；
Step 3: the C of formula ratio is weighed30-45Alkyl dimethicone and C30-45The mixture of alkene is placed in step Agitated kettle in two continues stirring until the mixture, which is dissolved completely in mixture B, obtains mixture C；
Step 4: the pearl powder of mixture A and formula ratio and addition are mixed colours into mixture C, after the completion of toning The preservative and tocopherol acetate of formula ratio are added, is finally uniformly mixed.
Embodiment 1
Component including following parts by weight:
15 parts of Permethyl 99A；C30-45Alkyl dimethicone and C30-451.0 parts of the mixture of alkene；Permethyl 99A With 40 parts of mixture of trimethyl silicane alkoxy esters of silicon acis；12 parts of dimethyl silicone polymer (5000cP)；The inclined benzene three of tridecanol 1.5 parts of acid esters；0.3 part of Phenoxyethanol；3 parts of fumed silica；1 part of mica；2 parts of pearl powder；2 parts of toner；Tocopheryl acetate 0.5 part of ester；
The preparation method is as follows:
Step 1: weighing the toner and tridecanol trimellitate of formula ratio, is uniformly mixed, must mix by three rollers Object A；
Step 2: it weighs the Permethyl 99A of formula ratio, the mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis, gather Dimethyl siloxane is in after mixing, rising to 80-85 DEG C for the temperature of agitated kettle, then weigh the gas phase of formula ratio in agitated kettle Silica and mica are added in agitated kettle, and high-speed stirred must mix until fumed silica and the dispersion of mica substantially uniformity Object B；
Step 3: the C of formula ratio is weighed30-45Alkyl dimethicone and C30-45The mixture of alkene is placed in step Agitated kettle in two continues stirring until the mixture, which is dissolved completely in mixture B, obtains mixture C；
Step 4: the pearl powder and mixture A for weighing formula ratio are added and mix colours into mixture C, after the completion of toning The preservative and tocopherol acetate of formula ratio are added, is finally uniformly mixed.
Embodiment 2
Component including following parts by weight:
20 parts of Permethyl 99A；C30-45Alkyl dimethicone and C30-451.5 parts of the mixture of alkene；Permethyl 99A With 40 parts of mixture of trimethyl silicane alkoxy esters of silicon acis；14 parts of dimethyl silicone polymer (5000cP)；The inclined benzene three of tridecanol 2 parts of acid esters；0.4 part of Phenoxyethanol；4 parts of fumed silica；2 parts of mica；3 parts of pearl powder；3 parts of toner；Tocopherol acetate 0.5 part；
The preparation method is the same as that of Example 1.
Embodiment 3
Component including following parts by weight:
25 parts of Permethyl 99A；C30-45Alkyl dimethicone and C30-452.0 parts of the mixture of alkene；Permethyl 99A With 45 parts of mixture of trimethyl silicane alkoxy esters of silicon acis；16 parts of dimethyl silicone polymer (5000cP)；The inclined benzene three of tridecanol 3 parts of acid esters；0.5 part of Phenoxyethanol；5 parts of fumed silica；3 parts of mica；2 parts of pearl powder；4 parts of toner；Tocopherol acetate 0.8 part；
The preparation method is the same as that of Example 1.
Embodiment 4
Component including following parts by weight:
30 parts of Permethyl 99A；C30-45Alkyl dimethicone and C30-452.5 parts of the mixture of alkene；Permethyl 99A With 50 parts of mixture of trimethyl silicane alkoxy esters of silicon acis；18 parts of dimethyl silicone polymer (5000cP)；The inclined benzene three of tridecanol 3.5 parts of acid esters；0.5 part of Phenoxyethanol；4 parts of fumed silica；4 parts of mica；3 parts of pearl powder；3 parts of toner；Tocopheryl acetate 1 part of ester；
The preparation method is the same as that of Example 1.
Embodiment 5
Component including following parts by weight:
35 parts of Permethyl 99A；C30-45Alkyl dimethicone and C30-453.0 parts of the mixture of alkene；Permethyl 99A With 55 parts of mixture of trimethyl silicane alkoxy esters of silicon acis；18 parts of dimethyl silicone polymer (5000cP)；The inclined benzene three of tridecanol 4 parts of acid esters；0.5 part of Phenoxyethanol；5 parts of fumed silica；3 parts of mica；4 parts of pearl powder；3 parts of toner；Tocopherol acetate 1 Part；
The preparation method is the same as that of Example 1.
Comparative example 1:
Component including following parts by weight:
45 parts of Permethyl 99A；Complex thickener (Permethyl 99A, distearyl dimethylammonium hectorite and propylene glycol carbonate Mixture) 10 parts；8.0 parts of beeswax；30 parts of mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis；Polydimethylsiloxanes 7 parts of alkane (100cP)；4 parts of vaseline；8 parts of tridecanol trimellitate；0.3 part of Phenoxyethanol；Skin improver (poly- diformazan Radical siloxane/vinyl dimethicone cross polymer and fumed silica) 6 parts；4 parts of mica；Pearl powder 1.5 Part；1.5 parts of toner；0.5 part of tocopherol acetate；
Preparation method:
Step 1: weighing the toner and tridecanol trimellitate of formula ratio, is uniformly mixed, must mix by three rollers Object A；
Step 2: it weighs the Permethyl 99A of formula ratio, the mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis, gather Dimethyl siloxane is in after mixing, rising to 80-85 DEG C for the temperature of agitated kettle, then weigh the skin of formula ratio in agitated kettle Improver and mica are added in agitated kettle, and high-speed stirred obtains mixture until fumed silica and the dispersion of mica substantially uniformity B；
Step 3: complex thickener, beeswax and the vaseline for weighing formula ratio are placed in agitated kettle in step 2, continue to stir It mixes until the mixture, which is dissolved completely in mixture B, obtains mixture C；
Step 4: the pearl powder and mixture A for weighing formula ratio are added and mix colours into mixture C, after the completion of toning The preservative and tocopherol acetate of formula ratio are added, is finally uniformly mixed.
Disadvantage: Material is too hard, and viscosity is excessively high, and glossiness is too low；Illustrate that the thickener performance in this system is bad.
Comparative example 2:
Component including following parts by weight:
45 parts of Permethyl 99A；4.0 parts of beeswax；30 parts of mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis；It is poly- 15 parts of dimethyl siloxane (5000cP)；4 parts of vaseline；10 parts of tridecanol trimellitate；0.3 part of Phenoxyethanol；Gas phase 3 parts of silica；4 parts of mica；1.5 parts of pearl powder；1.5 parts of toner；0.5 part of tocopherol acetate；
The preparation method is as follows:
Step 1: weighing the toner and tridecanol trimellitate of formula ratio, is uniformly mixed, must mix by three rollers Object A；
Step 2: it weighs the Permethyl 99A of formula ratio, the mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis, gather Dimethyl siloxane is in after mixing, rising to 80-85 DEG C for the temperature of agitated kettle, then weigh the gas phase of formula ratio in agitated kettle Silica and mica are added in agitated kettle, and high-speed stirred must mix until fumed silica and the dispersion of mica substantially uniformity Object B；
Step 3: the beeswax and vaseline that weigh formula ratio are placed in the agitated kettle in step 2, continue stirring until this is mixed Conjunction object, which is dissolved completely in mixture B, obtains mixture C；
Step 4: the pearl powder and mixture A for weighing formula ratio are added and mix colours into mixture C, after the completion of toning The preservative and tocopherol acetate of formula ratio are added, is finally uniformly mixed.
Advantage: by increasing highly viscous dimethyl silicone polymer, the viscosity of system had not only been increased, but also has improved product The brightness of smearing；
Disadvantage: stability test as a result, it has been found that, the system place after a week, there is segregation phenomenon, illustrate each component Between compatibility it is poor, that is, beeswax etc. and body material poor compatibility.
Comparative example 3:
Component including following parts by weight:
45 parts of Permethyl 99A；C30-45Alkyl dimethicone and C30-453.0 parts of the mixture of alkene；Permethyl 99A With 35 parts of mixture of trimethyl silicane alkoxy esters of silicon acis；15 parts of dimethyl silicone polymer；4 parts of tridecanol trimellitate； 0.5 part of Phenoxyethanol；2 parts of fumed silica；4 parts of mica；2 parts of pearl powder；2 parts of toner；1 part of tocopherol acetate；
The preparation method is as follows:
Step 1: weighing the toner and tridecanol trimellitate of formula ratio, is uniformly mixed, must mix by three rollers Object A；
Step 2: it weighs the Permethyl 99A of formula ratio, the mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis, gather Dimethyl siloxane is in after mixing, rising to 80-85 DEG C for the temperature of agitated kettle, then weigh the gas phase of formula ratio in agitated kettle Silica and mica are added in agitated kettle, and high-speed stirred must mix until fumed silica and the dispersion of mica substantially uniformity Object B；
Step 3: the C of formula ratio is weighed30-45Alkyl dimethicone and C30-45The mixture of alkene is placed in step Agitated kettle in two continues stirring until the mixture, which is dissolved completely in mixture B, obtains mixture C；
Step 4: the pearl powder and mixture A for weighing formula ratio are added and mix colours into mixture C, after the completion of toning The preservative and tocopherol acetate of formula ratio are added, is finally uniformly mixed.
Advantage: by the way that beeswax is changed to silicon wax (C30-45Alkyl dimethicone and C30-45The mixture of alkene) simultaneously Vaseline is eliminated, by stability test, the stability of the system is preferable, and improves product using effect to a certain extent Persistence；
Disadvantage: persistence does not still reach expected requirement, illustrates that the film former content in the system is relatively low.
Carry out following evaluation to embodiment and comparative example: color, smear, moistens degree, persistence and stability at glossiness Evaluated, evaluation method is scored 5 points of systems using 12 people, wherein 5 points is excellent, 4 points be it is good, 3 points be it is general, 2 points be it is poor, 1 point is average value that is excessively poor, as a result taking 12 people to score, and evaluation result is as shown in table 1:
Table 1: test result list
Assessment item Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Comparative example 1 Comparative example 2 Comparative example 3
Color 4.8 4.6 5.0 4.5 5.0 3.2 4.2 4.1
Glossiness 4.6 4.1 4.8 4.6 4.9 1.8 2.8 4.2
Smear 4.2 4.2 4.6 4.0 4.8 1.6 2.9 4.5
Moisten degree 4.3 4.2 4.9 4.2 4.5 1.5 3.2 4.1
Persistence 4.2 4.8 4.4 5.0 4.4 1.8 2.8 3.8
Stability 4.4 4.7 4.6 4.8 4.8 2.3 2.6 4.5
Can verify from the test result analysis above to comparative example and embodiment: primary raw material uses front three in this formula Base silicic acid resin and isomery dodecane, therefore product can generate thin film in lip, be not easy de- adornment；And guarantee to be easy makeup While, it can be vapored away again using rear extra grease, generate dry and comfortable effect；This system is equipped with silicon wax, silica gel and a small amount of Silica can retain the gloss of grease itself, while these raw materials with thickening function are also with body material with very good Compatibility, therefore this system improve product film forming after brightness and stability it is good.
Lip glaze product in above-described embodiment meets the requirement of following technical indicator: product viscosity 10000-21000cps (TC#10RPM/25℃)；Residual quantity of heavy metal control: lead≤10ppm；Arsenic≤2ppm；Mercury≤1ppm；Bacterium, mould and yeast Bacterium < 100cfu/unit；Excrement colibacillus group, Pseudomonas aeruginosa, Gold production staphylococcus, which must not be, to be detected；To ensure that the present invention Actual use function and its security performance.
It should be pointed out that for those of ordinary skill in the art, without departing from the inventive concept of the premise, may be used also To make several modifications and improvements, these are all within the scope of protection of the present invention.Therefore, the scope of protection of the patent of the present invention should be with Subject to appended claims.

Claims (10)

1. a kind of mirror surface persistence lip glaze, it is characterised in that: the component including following parts by weight: 15-35 parts of Permethyl 99A； C30-45Alkyl dimethicone and C30-451-3 parts of the mixture of alkene；Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis 40-55 parts of mixture；3-5 parts of thickener；12-18 parts of dimethyl silicone polymer；1.5-4 parts of tridecanol trimellitate； 0.3-0.5 parts and functional additive 4.5-11 parts of preservative.
2. mirror surface persistence lip glaze according to claim 1, it is characterised in that: the functional additive include mica, Pearl powder, toner and tocopherol acetate.
3. mirror surface persistence lip glaze according to claim 2, it is characterised in that: each component in the functional additive Parts by weight are as follows: 1-4 parts of mica；Pearl powder 2-4 powder；2-4 parts and tocopherol acetate 0.5-1 parts of toner.
4. mirror surface persistence lip glaze according to claim 1, it is characterised in that: the C30-45Alkyl dimethicone And C30-45Weight ratio both in the mixture of alkene are as follows: C30-45Alkyl dimethicone: C30-45Alkene is 3-4:1.
5. mirror surface persistence lip glaze according to claim 1, it is characterised in that: the thickener is fumed silica, The preservative is Phenoxyethanol.
6. mirror surface persistence lip glaze according to claim 1, it is characterised in that: the dimethyl silicone polymer is at 25 DEG C Viscosity be 5000cP.
7. mirror surface persistence lip glaze according to claim 1, it is characterised in that: the Permethyl 99A and trimethyl silicane alcoxyl The parts by weight of two components in the mixture of base esters of silicon acis are as follows: 6-9 parts of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis 1-3 Part.
8. mirror surface persistence lip glaze described in any one of -7 according to claim 1, it is characterised in that: including following parts by weight Component: 20-30 parts of Permethyl 99A；C30-45Alkyl dimethicone and C30-451.0-2 parts of the mixture of alkene；Different ten 40-50 parts of mixture of dioxane and trimethyl silicane alkoxy esters of silicon acis；12-18 parts of dimethyl silicone polymer；The inclined benzene of tridecanol Three 1.5-4 parts of acid esters；0.5 part of Phenoxyethanol；3-5 parts of fumed silica；1-3 parts of mica；2-3 parts of pearl powder；2-3 parts of toner With 0.5-1 parts of tocopherol acetate.
9. a kind of preparation method of mirror surface persistence lip glaze according to claim 1-8, it is characterised in that: step It is as follows:
Step 1: weighing the toner and tridecanol trimellitate of formula ratio, is uniformly mixed by three rollers, obtains mixture A；
Step 2: the Permethyl 99A of formula ratio, the mixture of Permethyl 99A and trimethyl silicane alkoxy esters of silicon acis, poly- diformazan are weighed Radical siloxane is in after mixing, rising to 80-85 DEG C for the temperature of agitated kettle in agitated kettle, then weighs the gas phase dioxy of formula ratio SiClx and mica are added in agitated kettle, and high-speed stirred obtains mixture B until fumed silica and the dispersion of mica substantially uniformity；
Step 3: the C of formula ratio is weighed30-45Alkyl dimethicone and C30-45The mixture of alkene is placed in step 2 Agitated kettle continues stirring until the mixture, which is dissolved completely in mixture B, obtains mixture C；
Step 4: the pearl powder of mixture A and formula ratio being added and mixed colours into mixture C, added after the completion of toning The preservative and tocopherol acetate of formula ratio are finally uniformly mixed.
10. preparation method according to claim 9, it is characterised in that: suitable three benzenetricarboxylic acid ten is added in step 1 Three esters pre-process toner.
CN201811638278.6A 2018-12-29 2018-12-29 Mirror surface lasting lip glaze and preparation method thereof Active CN109512702B (en)

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CN112999113B (en) * 2021-01-29 2022-11-01 广州卡迪莲化妆品科技有限公司 Anti-fading toner and preparation method thereof
CN114224747A (en) * 2021-11-24 2022-03-25 上海蔻沣生物科技有限公司 Modified powder, preparation method thereof and cosmetic containing modified powder

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