CN107349135A - A kind of transparent cleansing composition and preparation method thereof - Google Patents
A kind of transparent cleansing composition and preparation method thereof Download PDFInfo
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- CN107349135A CN107349135A CN201710561221.XA CN201710561221A CN107349135A CN 107349135 A CN107349135 A CN 107349135A CN 201710561221 A CN201710561221 A CN 201710561221A CN 107349135 A CN107349135 A CN 107349135A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/044—Suspensions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
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Abstract
The invention discloses a kind of transparent cleansing composition and preparation method thereof, by weight percentage, its raw material includes this composition:Nonionic surfactant 0.5~30%;Anion surfactant 0.5~20%;Synthetic polymer 0.1~10%;Polyalcohol 1~30%;Surplus is deionized water;Nertralizer regulation pH value is 4.5 8.5.Compared with the prior art, the invention has the advantages that:(1) inventive formulation solves the problems, such as that makeup remover is easily dripped in use, avoids that makeup remover is sticky in use, residual oil is, it is necessary to the problem of secondary cleaning.(2) product of the present invention is in addition to excellent makeup removing ability, above all also with excellent transparent appearance while with suspending power, can be suspended particle used for cosmetic, various moulding hydrogel sheets, make product that clear, aesthetic appearance be presented, the usage experience sense of pleasure is brought to consumer, increases added value of product.
Description
Technical field
The present invention relates to a kind of cleansing cosmetic, and in particular to a kind of transparent cleansing composition, and this composition
Preparation method;Belong to cosmetic technical field.
Background technology
Makeup removing is to remove the dirt of skin surface, particularly for the purpose of removing makeup cosmetic.Makeup removing passes through removing
Makeup cosmetic keeps the effect of skin cleaning so as to reach.With going from strength to strength for color make-up market, cleansing cosmetic is increasingly
By the extensive concern of consumer.Consumer does not require nothing more than the makeup removing effect of brilliance, while it is attractive in appearance to pursue product appearance, user
Just, makeup removing brings pleasure mood simultaneously.
At present, common makeup removal products are mainly makeup remover and makeup remover.Following lack be present in this makeup remover or makeup remover
Fall into:(1) there is the problem of easily drippage in makeup remover in use, in-convenience in use.And makeup remover is deposited in use
, it is necessary to secondary cleaning sticky, the residual oil the problem of, increase makeup removing program.(2) with market demand more and more higher, makeup removing
Product will not only meet the purposes of makeup removing, more visually there is fine perception;And what makeup removal products played makeup removing is usually
Nonionic surfactant;In order to easy to use, polymer need to be added and play thickening effect;But it with the addition of and have thickening concurrently and hang
The polymer of i, then product will be opaque;If not adding polymer, be unable to Effective Suspension particle used for cosmetic or
The hydrogel sheet of various moulding;Therefore, research and development are a kind of integrates makeup removing, suspension and transparent makeup removal products, is association area
Technical problem urgently to be resolved hurrily.
The content of the invention
The purpose of the present invention is overcome the deficiencies in the prior art, there is provided a kind of makeup removing ability is strong, and outward appearance is clear, and with excellent
The transparent cleansing composition of different suspending power.
It is a further object of the present invention to provide the preparation method of the transparent cleansing composition.
The present invention adopts the following technical scheme that to achieve these goals:
A kind of transparent cleansing composition, by weight percentage, its raw material includes:
Surplus is deionized water;Nertralizer regulation pH value is 4.5-8.5.
Preferably, a kind of transparent cleansing composition, by weight percentage, its raw material includes:
Surplus is deionized water;Nertralizer regulation pH value is 6.0-8.0.
In above-mentioned transparent cleansing composition,
Described nonionic surfactant is PEG-7 glyceryl cocoates, polysorbate -20, PEG-40 hydrogenation castors
Sesame oil, PEG-60 rilanit specials, PEG-6 caprylic/caprics glyceride, PEG-7 caprylic/caprics glyceride, the PEG-8 octanoic acids/last of the ten Heavenly stems
Acid glyceride, olive oil PEG-7 esters, olive oil PEG-8 esters, ethylene oxide/propylene oxide copolymer (such as PPG-26- fourths
Alcohol polyethers -26, poloxamer 184), ethylene oxide/butylene oxide copolymer, and polyglyceryl fatty acid ester class, poly alkyl alcohol
One kind or any combination mixture in the nonionic surfactants such as oxygen ethene ethers.
Preferable nonionic surfactant is PEG-7 glyceryl cocoates, polysorbate -20, PEG-40 hydrogenation castors
One or more combination in sesame oil, PPG-26- butylol polyethers -26, PEG-6 caprylic/caprics glyceride and poloxamer 184.
Described anion surfactant is sodium alkyl sulfate, alkanol polyethers sodium sulphate, alkanol sodium phosphate, alkanol polyethers
Sodium phosphate, alkanol polyethers sulfuric ester TEA salt, lauroyl amido MEA- sulfosuccinates disodium, lauroyl amido polyether sulphur base
Succinate disodium, lauroyl amido sodium diacelate/potassium, sodium lauroyl sarcosine/potassium, myristoyl-N-methylaminoacetic acid sodium/potassium, palm
Acylsarcosine sodium/potassium, cocoyl sarcosine sodium/potassium, cocoyl sarcosine TEA salt, sodium lauroyl glutamate/potassium, cocounut oil acyl
Sodium glutamate/potassium, cocoyl glutamic acid TEA salt, sodium cocoyl glycinate/potassium, two (lauramide glutamine) lysines
Sodium, cocounut oil acyl Sodium L-alaninate/potassium, laurate Sodium L-alaninate, cocoyl alanine TEA salt, sodium methyl cocoyl taurate/
Potassium, methyl oleoyl taurate/potassium, methyl lauroyl sodium taurocholate/potassium, cocounut oil acyl methyl taurine sodium taurocholate/potassium,
One or more combination in the anion surfactants such as laurate sodium taurocholate/potassium, lauroyl silk amino acid sodium.
Preferable anion surfactant is laureth sodium sulfovinate, sodium lauroyl sarcosine, lauroyl flesh ammonia
One or more combination in sour potassium and cocounut oil acyl Sodium L-alaninate.
Described synthetic polymer is acrylic acid (ester) analog copolymer, acrylic acid (ester) class cross-linked polymer, third
Olefin(e) acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, acrylic acid (ester) class/methacrylic acid of stereth -20
Ester copolymer, acrylic acid (ester) class/Methacrylate Crosspolymer of stereth -20, acrylic acid (ester) class/palm oil
In the polymer such as the acrylate copolymer of alcohol polyethers -25, acrylic acid (ester) class/vinyl neodecanoate cross-linked polymer, carbomer
One or more combination.
Preferable synthetic polymer is acrylic acid (ester) analog copolymer, acrylic acid (ester) class/stereth -20
One or both of Methacrylate Crosspolymer combines.
Described polyalcohol is that glycerine, butanediol, propane diols, DPG, sorbierite, pentanediol, hexylene glycol etc. are polynary
One or more combination in alcohol.
Also include nertralizer and preservative in described composition;Described nertralizer is sodium hydroxide, potassium hydroxide, essence
One of propylhomoserin, triethanolamine, aminomethyl propanol, tetrahydroxypropyl ethylenediamine etc. or any combination mixture;Described anti-corrosion
Agent is the one of which such as Phenoxyethanol, methyl hydroxybenzoate, methylisothiazolinone, Chlorphenesin, parahydroxyacet-ophenone or several groups
Close.
The preparation method of above-mentioned transparent cleansing composition, its step are as follows:
(1) each raw material is weighed by said ratio;
(2) first deionized water, polyalcohol, anion surfactant, nonionic surfactant are stirred;
(3) under agitation, pre-dispersed good synthetic polymer is added, is heated to 80-85 DEG C, stir insulation
30min;
(4) under agitation, nertralizer is slowly added to, adjusts PH;
(5) 40-45 DEG C of addition preservative is cooled to, is stirred.
The present invention by add specific anion surfactant solve the problems, such as it is transparent while selected by adding
Water-soluble polymer can reach it is not only transparent but also with certain suspending power effect.
Compared with the prior art, the invention has the advantages that:
(1) inventive formulation solves the problems, such as that makeup remover is easily dripped in use, and avoiding makeup remover makes
Sticky during, residual oil is, it is necessary to the problem of secondary cleaning.
(2) product of the present invention is in addition to excellent makeup removing ability, it is most important that also has while with suspending power
There is excellent transparent appearance, the particle used for cosmetic of can suspending, various moulding hydrogel sheets, product is presented clear, beautiful outer
See, the usage experience sense of pleasure is brought to consumer, increase added value of product.
Embodiment
With reference to specific embodiment, the present invention is furture elucidated, it should be understood that these embodiments are merely to illustrate the present invention
Rather than limitation the scope of the present invention, after the present invention has been read, various equivalences of the those skilled in the art to the present invention
The modification of form falls within the application appended claims limited range.
Embodiment 1:
The transparent makeup removing gel preparation method is as follows:First acrylic acid (ester) analog copolymer is carried out with part water it is pre-dispersed,
It is standby.Then water, PEG-7 glyceryl cocoates, laureth sodium sulfovinate and propane diols are weighed, is stirring evenly and then adding into pre-
Scattered acrylic acid (ester) analog copolymer, is heated to 80-85 DEG C, and stir insulation 30min.Then under agitation, slowly
NaOH is added, regulation pH value is in 4.5-8.5.Finally, it is cooled to 40-45 DEG C and adds appropriate preservative, stirs.
Product appearance is transparent, and makeup removing effect is good, can suspended gel particle, and 48 DEG C, place 48h, it is unchanged.
Comparative example 1:
The transparent makeup removing gel preparation method is as follows:First acrylic acid (ester) analog copolymer is carried out with part water it is pre-dispersed,
It is standby.Then water, PEG-7 glyceryl cocoates, propane diols are weighed, is stirring evenly and then adding into pre-dispersed good acrylic acid (ester) class
Copolymer, 80-85 DEG C is heated to, stir insulation 30min.Then under agitation, NaOH is slowly added to, regulation pH value exists
4.5-8.5.Finally, it is cooled to 40-45 DEG C and adds appropriate preservative, stirs.
As different from Example 1, laureth sodium sulfovinate is not added in comparative example, the gel finally given is in half
Saturating outward appearance.
Embodiment 2:
The transparent makeup removing gel preparation method is as follows:First acrylic acid (ester) analog copolymer is carried out with part water it is pre-dispersed,
It is standby.Then water, PEG-6 caprylic/caprics glyceride, sodium lauroyl sarcosine, hexylene glycol and DPG are weighed, is stirred
Pre-dispersed good acrylic acid (ester) analog copolymer is added afterwards, is heated to 80-85 DEG C, and stir insulation 30min.Then stirring
Under, triethanolamine is slowly added to, regulation pH value is in 4.5-8.5.Finally, it is cooled to 40-45 DEG C and adds appropriate preservative, stirring is equal
It is even.
Product appearance is transparent, and makeup removing effect is good, can suspended gel petal, and 48 DEG C, place 48h, it is unchanged.
Comparative example 2:
The transparent makeup removing gel preparation method is as follows:First acrylic acid (ester) analog copolymer is carried out with part water it is pre-dispersed,
It is standby.Then water, PEG-6 caprylic/caprics glyceride, sodium lauroyl sarcosine, hexylene glycol and DPG are weighed, is stirred
Pre-dispersed good acrylic acid (ester) class/methacrylate copolymer of docosyl alcohol polyethers -25 is added afterwards, is heated to 80-85 DEG C, is stirred
Mix uniformly insulation 30min.Then under agitation, triethanolamine is slowly added to, regulation pH value is in 4.5-8.5.Finally, it is cooled to
40-45 DEG C adds appropriate preservative, stirs.
Change acrylic acid (ester) analog copolymer into acrylic acid (ester) class/first of docosyl alcohol polyethers -25 as different from Example 2
Base acrylate copolymer finally can also obtain a transparent gel shape makeup removal products, but unlike comparative example to used for cosmetic
Particle and various moulding hydrogel sheets are without suspending power, and room temperature 1-2h occurs floating or sunk after addition.Outside to product
Sight has a strong impact on that consumer experience sense is poor.
Embodiment 3:
The transparent makeup removing gel preparation method is as follows:First by acrylic acid (ester) class/methacrylate of stereth -20
Cross-linked polymer carried out with part water it is pre-dispersed, it is standby.Then weigh water, polysorbate -20, lauroyl flesh glycine potassium,
Butanediol and glycerine, it is stirring evenly and then adding into pre-dispersed good acrylic acid (ester) class/methacrylate of stereth -20 and hands over
Linked polymer, 80-85 DEG C is heated to, stir insulation 30min.Then under agitation, KOH is slowly added to, regulation pH value exists
4.5-8.5.Finally, it is cooled to 40-45 DEG C and adds appropriate preservative, stirs.
Product appearance is transparent, and makeup removing effect is good, and can suspend polyethylene friction particles used for cosmetic, and 48 DEG C, 48h is placed,
It is unchanged.
Embodiment 4:
The transparent makeup removing gel preparation method is as follows:First by acrylic acid (ester) class/methacrylate of stereth -20
Cross-linked polymer carried out with part water it is pre-dispersed, it is standby.Then water, poloxamer 184, cocounut oil acyl Sodium L-alaninate, fourth two are weighed
Alcohol and hexylene glycol, it is stirring evenly and then adding into pre-dispersed good acrylic acid (ester) class/methacrylate of stereth -20 crosslinking
Polymer, 80-85 DEG C is heated to, stir insulation 30min.Then under agitation, arginine is slowly added to, regulation pH value exists
4.5-8.5.Finally, it is cooled to 40-45 DEG C and adds appropriate preservative, stirs.
Product appearance is transparent, and makeup removing effect is good, can suspended gel petal, and 48 DEG C, place 48h, it is unchanged.
Embodiment 5:
The transparent makeup removing gel preparation method is as follows:First acrylic acid (ester) analog copolymer is carried out with part water it is pre-dispersed,
It is standby.Then water, Cremophor RH40, PPG-26- butylol polyethers -26, PEG-7 glyceryl cocoates, cocounut oil acyl are weighed
Sodium L-alaninate, butanediol and hexylene glycol, pre-dispersed good acrylic acid (ester) analog copolymer is stirring evenly and then adding into, is heated to 80-
85 DEG C, stir insulation 30min.Then under agitation, arginine is slowly added to, regulation pH value is in 4.5-8.5.Finally, drop
Temperature stirs to the 40-45 DEG C of appropriate preservative of addition.
Product appearance is transparent, and makeup removing effect is good, can suspended gel petal, and 48 DEG C, place 48h, it is unchanged.
Other contents (not enumerated in embodiment) that the present invention is included are also transparent with product appearance, makeup removing effect
It is good, can suspended gel petal or the characteristics of other moulding hydrogels or polyethylene particles, and 48 DEG C, place 48h, it is unchanged.
The above is only the basic explanation under present inventive concept, and is made according to technical scheme any etc.
Effect conversion, all should belong to protection scope of the present invention.
Claims (12)
- A kind of 1. transparent cleansing composition, it is characterised in that:It includes following raw material by weight percentage:Surplus is deionized water;Nertralizer regulation pH value is 4.5-8.5.
- A kind of 2. transparent cleansing composition according to claim 1, it is characterised in that:It include it is following by weight percentage The raw material of meter:Surplus is deionized water;Nertralizer regulation pH value is 6.0-8.0.
- A kind of 3. transparent cleansing composition according to claim 1 or 2, it is characterised in that:Described non-ionic surface is lived Property agent be PEG-7 glyceryl cocoates, polysorbate -20, Cremophor RH40, PEG-60 rilanit specials, PEG-6 Caprylic/capric glyceride, PEG-7 caprylic/caprics glyceride, PEG-8 caprylic/caprics glyceride, olive oil PEG-7 esters, olive Olive oil PEG-8 esters, ethylene oxide/propylene oxide copolymer, ethylene oxide/butylene oxide copolymer, polyglyceryl fatty acid ester One or more combination in class, fatty alcohol polyethenoxy ether class nonionic surfactant.
- A kind of 4. transparent cleansing composition according to claim 3, it is characterised in that:Described nonionic surfactant It is pungent for PEG-7 glyceryl cocoates, polysorbate -20, Cremophor RH40, PPG-26- butylol polyethers -26, PEG-6 One or more combination in acid/glycerol decanoate and poloxamer 184.
- A kind of 5. transparent cleansing composition according to claim 1 or 2, it is characterised in that:Described anionic surface is lived Property agent be sodium alkyl sulfate, alkanol polyethers sodium sulphate, alkanol sodium phosphate, alkanol polyethers sodium phosphate, alkanol polyethers sulfuric ester TEA Salt, lauroyl amido MEA- sulfosuccinates disodium, lauroyl amido polyether sulphur base succinate disodium, lauroyl amido two Sodium acetate/potassium, sodium lauroyl sarcosine/potassium, myristoyl-N-methylaminoacetic acid sodium/potassium, palmitoyl sarcosine sodium/potassium, cocounut oil acyl flesh ammonia Sour sodium/potassium, cocoyl sarcosine TEA salt, sodium lauroyl glutamate/potassium, sodium cocoyl glutamate/potassium, cocoyl paddy ammonia Sour TEA salt, sodium cocoyl glycinate/potassium, two (lauramide glutamine) Sodium lysinates, cocounut oil acyl Sodium L-alaninate/potassium, bay Sour Sodium L-alaninate, cocoyl alanine TEA salt, sodium methyl cocoyl taurate/potassium, methyl oleoyl taurate/potassium, Methyl lauroyl sodium taurocholate/potassium, cocounut oil acyl methyl taurine sodium taurocholate/potassium, laurate sodium taurocholate/potassium, lauroyl One or more combination in the anion surfactants such as silk amino acid sodium.
- A kind of 6. transparent cleansing composition according to claim 5, it is characterised in that:Anion surfactant is bay One or more of groups in alcohol polyethers sodium sulfovinate, sodium lauroyl sarcosine, potassium lauroyl sarcosine and cocounut oil acyl Sodium L-alaninate Close.
- A kind of 7. transparent cleansing composition according to claim 1 or 2, it is characterised in that:Described synthesizing water-solubility gathers Compound is acrylic acid (ester) analog copolymer, acrylic acid (ester) class cross-linked polymer, acrylic acid (ester) class/C10-30 alkylol acrylamides acid Ester cross-linked polymer, acrylic acid (ester) class/methacrylate copolymer of stereth -20, acrylic acid (ester) class/stearyl alcohol The Methacrylate Crosspolymer of polyethers -20, acrylic acid (ester) class/acrylate copolymer of Palmitoleyl alcohol polyethers -25, propylene One or more combination in sour (ester) class/vinyl neodecanoate cross-linked polymer, carbomer polymer.
- A kind of 8. transparent cleansing composition according to claim 7, it is characterised in that:Synthetic polymer is propylene One or both of sour (ester) analog copolymer, acrylic acid (ester) class/Methacrylate Crosspolymer of stereth -20 Combination.
- A kind of 9. transparent cleansing composition according to claim 1 or 2, it is characterised in that:Described polyalcohol be glycerine, One or more combination in butanediol, propane diols, DPG, sorbierite, pentanediol, hexylene glycol.
- A kind of 10. transparent cleansing composition according to claim 1 or 2, it is characterised in that:Described nertralizer is hydrogen-oxygen Change the one or more combination in sodium, potassium hydroxide, arginine, triethanolamine, aminomethyl propanol, tetrahydroxypropyl ethylenediamine.
- A kind of 11. transparent cleansing composition according to claim 1 or 2, it is characterised in that:Also wrapped in described composition Include preservative;Described preservative is Phenoxyethanol, methyl hydroxybenzoate, methylisothiazolinone, Chlorphenesin, parahydroxyacet-ophenone Middle one or more combination.
- 12. the preparation method of the transparent cleansing composition described in claim 1 or 2, it is characterised in that:Its step is as follows:(1) each raw material is weighed by proportioning;(2) first deionized water, polyalcohol, anion surfactant, nonionic surfactant are stirred;(3) under agitation, pre-dispersed good synthetic polymer is added, is heated to 80-85 DEG C, stir insulation 30min;(4) under agitation, nertralizer is slowly added to, adjusts PH;Obtain product.
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Cited By (16)
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