CN113171331A - Ice crystal amino acid shower gel and preparation method thereof - Google Patents
Ice crystal amino acid shower gel and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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Abstract
The invention relates to the technical field of daily cosmetics, in particular to ice crystal amino acid shower gel and a preparation method thereof. The ice crystal amino acid shower gel comprises glycerol, a composite surfactant, taurine, a natural plant extract, an acrylic acid (ester) copolymer, coconut oil amide DEA, essence, a preservative, deionized water and the like. By using the composite surfactant, the suspension stabilizer and the natural plant extract with specific compositions, the shower gel product has the appearance characteristics of unique ice crystal patterns, is strong in moisturizing capability, is moist but not greasy, and simultaneously has excellent effects of mildly cleaning, moisturizing, caring skin and the like.
Description
Technical Field
The invention relates to the technical field of daily cosmetics, in particular to ice crystal amino acid shower gel and a preparation method thereof.
Background
The shower gel is a common skin cleaning product, and has good touch and efficacy compared with the traditional soap. The original function of the shower gel is mainly to clean the skin of the whole body, and along with the improvement of the living standard of people, the pure skin cleaning can not meet the requirements of consumers. In addition to cleansing skin, consumers expect body washes to have some skin care benefits, such as: whitening, bacteriostasis, skin tightening and the like, and the future development trend comprises the aspects of moisture retention, nourishing, safety, mildness, beautiful appearance and the like. The main components of the shower gel comprise a surfactant, a skin feel regulator, a humectant, a pH regulator, a viscosity regulator, a pearling agent, essence, a preservative, a chelating agent, a functional additive and the like, wherein the most important is to screen the appropriate surfactant, skin feel regulator and functional additive. The shower gel sold in the market at present has various varieties and large quality difference, and has a large improvement space in aspects of appearance style, skin care effect and the like.
Disclosure of Invention
The invention aims to provide ice crystal amino acid shower gel and a preparation method thereof, and the ice crystal amino acid shower gel has the appearance characteristics of unique ice crystal patterns by using a composite surfactant, a suspension stabilizer and a natural plant extract which are specially composed, has strong moisturizing capability and is moist but not greasy, and also has excellent effects of mildness, cleanness, moisturizing, skin care and the like.
In order to achieve the purpose, the invention adopts the technical scheme that:
the ice crystal amino acid shower gel comprises the following components in percentage by weight:
phase A: 5-15% of glycerol, 17-45% of composite surfactant and the balance of deionized water;
phase B: 5-25% of taurine and 3-7% of natural plant extract;
and C phase: 3-20% of acrylic acid (ester) copolymer, 6-15% of deionized water and 0-1% of sodium hydroxide;
phase D: 1-5% of cocamide DEA, a proper amount of essence and 1-3% of preservative;
phase E: 0.1 to 1 percent of taurine.
Preferably, the shower gel consists of the following components in percentage by weight:
phase A: 8-12% of glycerol, 25-35% of composite surfactant and the balance of deionized water;
phase B: 12-18% of taurine and 4-6% of natural plant extract;
and C phase: 8-12% of acrylic acid (ester) copolymer, 8-12% of deionized water and 0.2-0.8% of sodium hydroxide;
phase D: 2-4% of cocamide DEA, a proper amount of essence and 1.5-2.5% of preservative;
phase E: 0.2 to 0.8 percent of taurine.
Preferably, the shower gel consists of the following components in percentage by weight:
phase A: 10% of glycerol, 30% of composite surfactant and the balance of deionized water;
phase B: 15% of taurine and 5% of natural plant extract;
and C phase: 10% of acrylic acid (ester) copolymer, 10% of deionized water and 0.5% of sodium hydroxide;
phase D: 3% of cocamide DEA, a proper amount of essence and 2% of preservative;
phase E: 0.5 percent of taurine.
Preferably, the composite surfactant in the phase A consists of the following components: 15-25% of sodium laureth sulfate, 1-10% of sodium lauroyl sarcosinate and 1-10% of disodium laureth sulfosuccinate.
Preferably, the natural plant extract in phase B consists of: 1-3% of seaweed extract and 2-4% of ginger root extract.
Preferably, the essence in phase D is selected from mint essence, lemon essence or rose essence.
Preferably, the preservative in phase D is phenoxyethanol.
Further, the invention also provides a preparation method of the ice crystal amino acid shower gel, which comprises the following steps:
(1) adding the phase A component into a stirring kettle, heating to 80-90 ℃, and stirring until the phase A component is completely dissolved;
(2) adding the phase B component, and stirring until the phase B component is completely dissolved;
(3) cooling to 60-65 deg.C, adding C phase component, and stirring to transparent;
(4) cooling to 45-50 deg.C, adding phase D component, and stirring;
(5) adding the phase E component, stirring for 4-6 minutes, stopping stirring, and standing to obtain the ice crystal amino acid shower gel.
Taurine (Taurine) is a sulfur-containing amino acid with a simple structure in an animal body, has a chemical name of 2-aminoethanesulfonic acid, is odorless, is neutral in dilute solution and stable to heat, and is combined with cholic acid in human and animal bile to exist in a combined form. Research finds that the taurine has the capability of activating skin cells and can continuously provide quick and durable energy supplement and multiple protection for young skin. The taurine also has the effects of improving the immunity of the skin and resisting the invasion of the external environment to the skin.
The seaweed extract is mainly used as a humectant and a skin conditioner in cosmetics and skin care products, mainly contains seaweed gel, vitamins, amino acids and the like, is a natural moisturizing and softening agent, can promote cell regeneration, has the function of strengthening skin metabolism, has a unique function of removing cutin, can refresh the skin and prevent wrinkles.
The ginger root extract is mainly used as an antioxidant, an anti-inflammatory agent, a skin conditioner and a physical sun-screening agent in cosmetics and skin care products, has a certain inhibiting effect on dermatophytes, streptomyces albus and oral germs, but has poor inhibiting effect on common mold and the like; can enhance skin activity, activate skin, and has antioxidant and antiaging effects; can also promote hair growth, and can be used as hair promoter; it also has effects in keeping moisture and inhibiting odor.
Compared with the prior art, the invention has the beneficial effects that: (1) taurine has the functions of moisturizing and relieving skin, and is amino acid required by human body. The solubility of taurine in water, surfactant and polyalcohol is different, and when the addition amount reaches a certain concentration, taurine can be precipitated from the material body to form crystals. During bathing, the precipitated taurine can be dissolved again due to the addition of water, so that the moisturizing effect is enhanced. (2) Sodium laureth sulfate, sodium lauroyl sarcosinate and disodium laureth sulfosuccinate in the composite surfactant have the functions of cleaning and foaming, and glycerin has the function of assisting in moisturizing, so that the solubility of taurine in water is reduced, and crystals are more easily separated out. The acrylic acid (ester) copolymer has the suspension stabilizing effect, can ensure that precipitated taurine crystals are uniformly distributed, has a spatial network structure which can form steric hindrance, and can also promote the directional crystallization of the taurine crystals to form various different shapes. (3) According to the ice crystal amino acid shower gel, the composite surfactant, the suspension stabilizer and the natural plant extract which are specially composed are used, so that the shower gel product has the appearance characteristics of a unique ice crystal pattern, is strong in moisturizing capability and moist but not greasy, and simultaneously has excellent effects of mildly cleaning, moisturizing, caring skin and the like.
Drawings
FIG. 1 is one of photographs of the appearance of ice crystal amino acid shower gel;
figure 2 is a second photograph of the appearance of ice crystal amino acid shower gel.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention. The materials, reagents and the like used are all commercially available reagents and materials unless otherwise specified. The present invention will be described in further detail with reference to the following data in conjunction with specific examples.
Example 1
The ice crystal amino acid shower gel comprises the following components in percentage by weight:
phase A: 5% of glycerin, 25% of sodium laureth sulfate, 8% of sodium lauroyl sarcosinate, 2% of disodium laureth sulfosuccinate and the balance of deionized water;
phase B: 10% of taurine, 1% of seaweed extract of folium megalophyllae and 4% of ginger root extract;
and C phase: 8% of acrylic acid (ester) copolymer, 12% of deionized water and 0.2% of sodium hydroxide;
phase D: 1% of cocamide DEA, 3% of mint essence and 3% of phenoxyethanol;
phase E: 0.2 percent of taurine.
The preparation method of the ice crystal amino acid shower gel comprises the following steps:
(1) adding the phase A component into a stirring kettle, heating to 80 ℃, and stirring until the phase A component is completely dissolved;
(2) adding the phase B component, and stirring until the phase B component is completely dissolved;
(3) cooling to 65 ℃, adding the C phase component, and uniformly stirring until the mixture is transparent;
(4) cooling to 45 ℃, adding the phase D component, and stirring uniformly;
(5) adding the phase E component, stirring for 4 minutes, stopping stirring, and standing to obtain the ice crystal amino acid shower gel.
Example 2
The ice crystal amino acid shower gel comprises the following components in percentage by weight:
phase A: 15% of glycerol, 15% of sodium laureth sulfate, 2% of sodium lauroyl sarcosinate, 8% of disodium laureth sulfosuccinate and the balance of deionized water;
phase B: 20% of taurine, 3% of a kelp extract and 2% of a ginger root extract;
and C phase: 12% of acrylic acid (ester) copolymer, 8% of deionized water and 0.8% of sodium hydroxide;
phase D: 5% of cocamide DEA, 1% of lemon essence and 1% of phenoxyethanol;
phase E: 0.8 percent of taurine.
The preparation method of the ice crystal amino acid shower gel comprises the following steps:
(1) adding the phase A component into a stirring kettle, heating to 90 ℃, and stirring until the phase A component is completely dissolved;
(2) adding the phase B component, and stirring until the phase B component is completely dissolved;
(3) cooling to 60 deg.C, adding C phase component, and stirring to transparent;
(4) cooling to 50 ℃, adding the phase D component, and uniformly stirring;
(5) adding the phase E component, stirring for 6 minutes, stopping stirring, and standing to obtain the ice crystal amino acid shower gel.
Example 3
The ice crystal amino acid shower gel comprises the following components in percentage by weight:
phase A: 10% of glycerol, 20% of sodium laureth sulfate, 5% of sodium lauroyl sarcosinate, 5% of disodium laureth sulfosuccinate and the balance of deionized water;
phase B: 15% of taurine, 2% of a kelp extract and 3% of a ginger root extract;
and C phase: 10% of acrylic acid (ester) copolymer, 10% of deionized water and 0.5% of sodium hydroxide;
phase D: 3% of cocamide DEA, 2% of rose essence and 2% of phenoxyethanol;
phase E: 0.5 percent of taurine.
The preparation method of the ice crystal amino acid shower gel comprises the following steps:
(1) adding the phase A component into a stirring kettle, heating to 85 ℃, and stirring until the phase A component is completely dissolved;
(2) adding the phase B component, and stirring until the phase B component is completely dissolved;
(3) cooling to 62 ℃, adding the C phase component, and uniformly stirring until the mixture is transparent;
(4) cooling to 48 ℃, adding the phase D component, and uniformly stirring;
(5) adding the phase E component, stirring for 5 minutes, stopping stirring, and standing to obtain the ice crystal amino acid shower gel.
Comparative example 1
Compared with example 3, the composition of the composite surfactant used in the body wash was: 20% of potassium dodecyl phosphate, 5% of sodium lauryl amphoacetate and 5% of hydroxysulfobetaine.
Comparative example 2
Compared with example 3, the composition of the composite surfactant used in the body wash was: 20% of N-acyl-N-methyl sodium taurate, 5% of disodium citrate monoester and 5% of disodium cocoyl glutamate.
Comparative example 3
In contrast to example 3, hydroxyethyl cellulose was used as a suspension stabilizer in the body wash instead of the acrylic copolymer.
Comparative example 4
In contrast to example 3, guar gum was used as a suspension stabilizer in the body wash instead of the acrylic copolymer.
Comparative example 5
Compared with example 3, the natural plant extracts used in the body wash were 15% taurine and 5% kelp extract.
Comparative example 6
Compared with example 3, the natural plant extracts used in the body wash were 15% taurine and 5% ginger root extract.
Appearance test of ice crystal shower gel
Comparing the appearances of the shower gels prepared in example 3 and comparative examples 1 to 4, it can be seen that taurine crystals (shown in the attached figures 1 to 2) having a unique shape are present in the shower gel of example 3, giving a refreshing and comfortable feeling to people, and having good stability; the shower gels of comparative examples 1 to 4 were free from precipitated crystals of taurine. The results show that the specific compound surfactant and suspension stabilizer can promote the precipitation and uniform distribution of taurine crystals, so that the taurine crystals can be formed into different shapes, and the appearance property of the ice crystal shower gel is improved.
Irritation test for Ice Crystal shower gel
5ml of the ice crystal bath cream in the examples 1-3 is uniformly smeared on the back of hands of volunteers (20-30 years old, 50 people in total), and is observed for half an hour to judge whether symptoms such as red swelling, itching, eruption and the like appear. The results show that all volunteers have no adverse reaction within half an hour, and the ice crystal shower gel disclosed by the invention has no stimulation to the skin and is good in safety.
Use efficacy test of ice crystal shower gel
The test subjects were 60 female volunteers with healthy skin between 20-30 years of age, and the 60 test subjects were randomly divided into three groups, designated as group a, group B and group C, with 20 persons per group. The test area was determined on the left and right anterior arms of female volunteers and was approximately 5cm by 5 cm. Group a volunteers used the shower gel of example 3, group B volunteers used the shower gel of comparative example 5, and group C volunteers used the shower gel of comparative example 6. The application is continued for 5 days, and 1 time per day. The skin condition before and after use was measured by an SEM575 type skin elasticity tester, and the skin elasticity (%) and skin firmness (%) were calculated. The results of the experiment are shown in table 1.
From the experimental results in table 1, it can be seen that the addition of the zostera marina extract and the ginger root extract in a specific ratio to the ice crystal shower gel can improve the skin activity, enhance the skin elasticity and firmness, and further generate the skin care effects of moisturizing the skin and resisting skin aging, compared with the addition of only a single type of natural plant extract.
In conclusion, the ice crystal amino acid shower gel disclosed by the invention has the appearance characteristics of a unique ice crystal pattern by using the composite surfactant, the suspension stabilizer and the natural plant extract which are specially composed, is strong in moisturizing capability and moist but not greasy, and also has the excellent effects of good safety, mildness, cleanness, moistening, skin care and the like.
The above description is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, several modifications or equivalents may be made to the technical solution without departing from the principle of the present invention, and these modifications or equivalents should also be regarded as the protection scope of the present invention.
Claims (8)
1. The ice crystal amino acid shower gel is characterized by comprising the following components in percentage by weight:
phase A: 5-15% of glycerol, 17-45% of composite surfactant and the balance of deionized water;
phase B: 5-25% of taurine and 3-7% of natural plant extract;
and C phase: 3-20% of acrylic acid (ester) copolymer, 6-15% of deionized water and 0-1% of sodium hydroxide;
phase D: 1-5% of cocamide DEA, a proper amount of essence and 1-3% of preservative;
phase E: 0.1 to 1 percent of taurine.
2. The ice crystal amino acid shower gel of claim 1, wherein the shower gel is composed of the following components in percentage by weight:
phase A: 8-12% of glycerol, 25-35% of composite surfactant and the balance of deionized water;
phase B: 12-18% of taurine and 4-6% of natural plant extract;
and C phase: 8-12% of acrylic acid (ester) copolymer, 8-12% of deionized water and 0.2-0.8% of sodium hydroxide;
phase D: 2-4% of cocamide DEA, a proper amount of essence and 1.5-2.5% of preservative;
phase E: 0.2 to 0.8 percent of taurine.
3. The ice crystal amino acid shower gel of claim 2, wherein the shower gel is composed of the following components in percentage by weight:
phase A: 10% of glycerol, 30% of composite surfactant and the balance of deionized water;
phase B: 15% of taurine and 5% of natural plant extract;
and C phase: 10% of acrylic acid (ester) copolymer, 10% of deionized water and 0.5% of sodium hydroxide;
phase D: 3% of cocamide DEA, a proper amount of essence and 2% of preservative;
phase E: 0.5 percent of taurine.
4. The ice crystal amino acid shower gel of claim 1, wherein the complex surfactant in phase a consists of: 15-25% of sodium laureth sulfate, 1-10% of sodium lauroyl sarcosinate and 1-10% of disodium laureth sulfosuccinate.
5. The ice crystal amino acid shower gel of claim 1, wherein the natural plant extract in phase B consists of: 1-3% of seaweed extract and 2-4% of ginger root extract.
6. An ice crystal amino acid shower gel according to any one of claims 1 to 5 wherein the flavour in phase D is selected from mint flavour, lemon flavour or rose flavour.
7. An ice crystal amino acid shower gel according to any one of claims 1 to 5 wherein the preservative in phase D is phenoxyethanol.
8. The preparation method of ice crystal amino acid shower gel according to any one of claims 1 to 7, comprising the steps of:
(1) adding the phase A component into a stirring kettle, heating to 80-90 ℃, and stirring until the phase A component is completely dissolved;
(2) adding the phase B component, and stirring until the phase B component is completely dissolved;
(3) cooling to 60-65 deg.C, adding C phase component, and stirring to transparent;
(4) cooling to 45-50 deg.C, adding phase D component, and stirring;
(5) adding the phase E component, stirring for 4-6 minutes, stopping stirring, and standing to obtain the ice crystal amino acid shower gel.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113633560A (en) * | 2021-09-28 | 2021-11-12 | 美丽链接生物科技研究院(广东)有限公司 | Needle-shaped amino acid crystal face-cleaning gel and preparation method thereof |
| CN114053172A (en) * | 2021-11-23 | 2022-02-18 | 广州锦同生物科技有限公司 | Ice crystal amino acid crystallization composition and preparation method thereof |
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| CN114053172B (en) * | 2021-11-23 | 2022-06-28 | 广州锦同生物科技有限公司 | Ice crystal amino acid crystallization composition and preparation method thereof |
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