CN109125196A - A kind of oil tea mouthwash and preparation method thereof - Google Patents
A kind of oil tea mouthwash and preparation method thereof Download PDFInfo
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- CN109125196A CN109125196A CN201811321486.3A CN201811321486A CN109125196A CN 109125196 A CN109125196 A CN 109125196A CN 201811321486 A CN201811321486 A CN 201811321486A CN 109125196 A CN109125196 A CN 109125196A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P11/00—Drugs for disorders of the respiratory system
- A61P11/04—Drugs for disorders of the respiratory system for throat disorders
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P35/00—Antineoplastic agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention belongs to daily use chemicals articles for washing technical fields, more particularly to a kind of oil tea mouthwash and preparation method thereof, oil tea mouthwash is mainly made by the raw material of following parts by weight: 14-20 parts of Camellia Leaves, the 13-18 parts of root barks of white mulberry, 15-19 Fen polemonium caeruleum, 3-19 parts of common averrhoa flowers, 5-7 parts of clove flower bud distillates, 8-10 parts of dewdrop Rabdosia amethystoides, 10-14 parts of Chinese artichokes, 2-6 parts of seaweed glues, oil tea leaf extract in the present invention has inhibiting effect to pathogenic bacteria and fungi, also there is antioxidation and certain antitumaous effect, and smell is unique, oil tea leaf extract it is antibacterial, antioxidant effect is also very good, it can reduce various focusing depths represented, promote canker sore healing, the effect of mitigating abscess of throat is significant, it is non-stimulated.
Description
[technical field]
The invention belongs to daily use chemicals articles for washing technical fields, and in particular to a kind of oil tea mouthwash and preparation method thereof.
[background technique]
It is previous it is believed that brushing teeth sooner or later just can reach sanitary standard, can be for oral hygiene new concept but far from
It is enough.Expert proposes: cleaning oral cavity is required as washing one's hands.But take out whenever and wherever possible toothpaste, toothbrush but it is unrealistic, mouthwash this
When can stand up and volunteer to help, take on heavy burden, anytime anywhere it can clean oral cavity for you, refuse the erosion of residue on teeth；Again
Person has meal in some occasions, containing the highly seasoned cuisines such as green onion, garlic, make you " trying to stop but cannot ", but be not without method, standby one is small
Bottle mouthwash, need to only go to time toilet, horse back ability to speak is pure and fresh, without trace, you can glut oneself with delicacies to the greatest extent；Secondly, travelling is on the way,
Water tank lacks water all often has with water is crowded, and standby bottle mouthwash, all worries one have gargled it；In addition, mouthwash will also be tooth
Old man that tooth falls off, the child that will not be brushed teeth and the optimal selection for being impatient at the dental patient's oral hygiene guarantee brushed teeth.
But the also irritant ingredient of current most of mouthwashes, oral cavity can be made not feel good after use, it is therefore desirable to one
It plants the existing bactericidal effect of mouthwash and energy mild action is in oral environment.
[summary of the invention]
In view of problem above, the present invention provides a kind of oil tea mouthwash and preparation method thereof, the existing sterilizations of the mouthwash
Energy mild action is acted on again in oral environment.
The technical problems to be solved by the invention are implemented with the following technical solutions:
A kind of oil tea mouthwash, is mainly made by the raw material of following parts by weight: 14-20 parts of Camellia Leaves, 13-18 parts of Sang Bai
Skin, 15-19 Fen polemonium caeruleum, 3-19 parts of common averrhoa flowers, 5-7 parts of clove flower bud distillates, 8-10 parts of dewdrop Rabdosia amethystoides, 10-14 parts of Chinese artichokes, 2-6 parts
Seaweed glue.
Preferably, a kind of oil tea mouthwash, is mainly made by the raw material of following parts by weight: 14 parts of Camellia Leaves, 13 parts of Sang Bai
Skin, 15 Fen polemonium caeruleums, 3 parts of common averrhoa flowers, 5 parts of clove flower bud distillates, 8 parts of dewdrop Rabdosia amethystoides, 10 parts of Chinese artichokes, 2 parts of seaweed glues.
Preferably, a kind of oil tea mouthwash, is mainly made by the raw material of following parts by weight: 16 parts of Camellia Leaves, 15 parts of Sang Bai
Skin, 17 Fen polemonium caeruleums, 5 parts of common averrhoa flowers, 6 parts of clove flower bud distillates, 9 parts of dewdrop Rabdosia amethystoides, 12 parts of Chinese artichokes, 4 parts of seaweed glues.
Preferably, a kind of oil tea mouthwash, is mainly made by the raw material of following parts by weight: 20 parts of Camellia Leaves, 18 parts of Sang Bai
Skin, 19 Fen polemonium caeruleums, 19 parts of common averrhoa flowers, 7 parts of clove flower bud distillates, 10 parts of dewdrop Rabdosia amethystoides, 14 parts of Chinese artichokes, 6 parts of seaweed glues.
A kind of oil tea mouthwash, production method include the following steps:
1) Property of Tea oil Tree Fruit, oligonerve maiden fern root, Folium rubi elliptici, clove flower bud distillates, thin,tough silk hair chrysanthemum, flacourtia rukam leaf, dalbergia wood are mixed
It is ground into the mixed powder of 130-150 mesh, places into 75% ethyl acetate and carries out ultrasonic-leaching twice, is carrying out centrifugation point
From taking upper liquid, then into carrying out vacuum freeze drying 20-24 hours, obtain stoste；
2) the resulting stoste of step 1) is put into capillary electrophoresis and is purified, with the non-coating of effective length 50cm
Fused-silica capillary column is split tunnel, and the 50mmol/L Na2B4O7 of pH9-13 is running buffer solution, separation voltage
20kV, obtains two not good liquors by 25 DEG C of capillary column temperature；
3) by the resulting two not good liquors temperature of step 2) be maintained at 46 DEG C~50 DEG C 5.5% panthenols of addition weight percentage,
Weight percentage 2.4-2.8% hydrolytic collagen, 0.55~0.6% cation guar gum of weight percentage, add rape
Seed oil stirs 20 minutes, obtains oil tea mouthwash.
By adopting the above-described technical solution, the invention has the following advantages: oil tea leaf extract in the present invention
There is inhibiting effect to pathogenic bacteria and fungi, also there is antioxidation and certain antitumaous effect, and smell is unique, oil tea
The antibacterial of leaf extract, antioxidant effect are also very good, are widely used in toothpaste, and mixture has stronger anti inflammatory blood quickening
Effect, has fine inhibiting effect to the main harmful bacteria in the resident bacteria of oral cavity.The present invention combines Multiple components, except tool
Have outside the function in cleaning oral cavity of different mouthwashes, also has and treat or prevent the mouths such as periodontitis, saprodontia, halitosis and canker sore
Chamber disease brightens, is good for the effect of tooth, clearing heat for detumescence, pre- anti-cancer.Have effects that a variety of prevention and treatment mouth diseases.This mouthwash
Using natural plant composition, there is better safety than the mouthwash on existing market, can take orally, have no toxic side effect, and has
There is broad spectrum antibacterial, there is excellent sterilizing ability to many anaerobic bacterias, Non-anaerobic bactreia, can reduce various focusing depths represented, promotes oral cavity
The effect of ulcer healing, mitigation abscess of throat, is significant, non-stimulated.
[specific embodiment]
The following examples can help those skilled in the art that the present invention is more fully understood, but cannot be with any
Mode limits the present invention.
Embodiment 1
A kind of oil tea mouthwash, is mainly made by the raw material of following parts by weight: 14 parts of Camellia Leaves, 13 parts of root barks of white mulberry, 15 parts
Polemonium caeruleum, 3 parts of common averrhoa flowers, 5 parts of clove flower bud distillates, 8 parts of dewdrop Rabdosia amethystoides, 10 parts of Chinese artichokes, 2 parts of seaweed glues.
A kind of oil tea mouthwash, production method include the following steps:
1) the oil tea leaf extract the preparation method comprises the following steps: take fresh Camellia Leaves, drying is low to moisture content at 105 DEG C
It in 5%, then crushes, crosses 35 meshes；It is soaked in the ethyl alcohol that 4 times of volumetric concentrations are 70%, stirs evenly, then its temperature is mentioned
60 DEG C are raised to, starting ultrasonic cell disruptor extracts 1 hour, filtering, so repeats to extract twice, and merging filtrate twice is to close
And filtrate, obtain oil tea leaf extract；
2) that root bark of white mulberry, polemonium caeruleum, common averrhoa flower, dewdrop Rabdosia amethystoides, Chinese artichoke mixing are crushed to 80 mesh particles with pulverizer is big
It is small, it is put into ultrasonic extractor and is added the edible alcohol of 200mL95%, temperature 50 C, supersonic frequency 30KHz ultrasound are set
It extracts 1 hour, filters, filter residue, which repeats to be put into ultrasonic extractor, to be repeated to extract 2 times under the same terms, and filtering merges filter
Liquid, filtrate are concentrated to dryness at 45 DEG C with Rotary Evaporators, obtain mixture；
3) the resulting oil tea leaf extract of step 1) is mixed with the resulting mixture of step 2), adds clove flower bud distillates, 12
45% edible alcohol of part and 16 parts of sterile water, are put into high speed dispersion homogenizer and carry out homogeneous 20 minutes, homogenizing temperature 40
Degree, obtains oil tea mouthwash.
Embodiment 2
A kind of oil tea mouthwash, is mainly made by the raw material of following parts by weight: 16 parts of Camellia Leaves, 15 parts of root barks of white mulberry, 17 parts
Polemonium caeruleum, 5 parts of common averrhoa flowers, 6 parts of clove flower bud distillates, 9 parts of dewdrop Rabdosia amethystoides, 12 parts of Chinese artichokes, 4 parts of seaweed glues.
A kind of oil tea mouthwash, production method include the following steps:
1) the oil tea leaf extract the preparation method comprises the following steps: take fresh Camellia Leaves, drying is low to moisture content at 108 DEG C
It in 5%, then crushes, crosses 40 meshes；It is soaked in the ethyl alcohol that 5 times of volumetric concentrations are 70%, stirs evenly, then its temperature is mentioned
65 DEG C are raised to, starting ultrasonic cell disruptor extracts 2 hours, filtering, so repeats to extract twice, and merging filtrate twice is to close
And filtrate, obtain oil tea leaf extract；
2) that root bark of white mulberry, polemonium caeruleum, common averrhoa flower, dewdrop Rabdosia amethystoides, Chinese artichoke mixing are crushed to 80 mesh particles with pulverizer is big
It is small, it is put into ultrasonic extractor and is added the edible alcohol of 200mL95%, is arranged 55 DEG C of temperature, supersonic frequency 30KHz ultrasound
It extracts 1 hour, filters, filter residue, which repeats to be put into ultrasonic extractor, to be repeated to extract 2 times under the same terms, and filtering merges filter
Liquid, filtrate are concentrated to dryness at 45 DEG C with Rotary Evaporators, obtain mixture；
3) the resulting oil tea leaf extract of step 1) is mixed with the resulting mixture of step 2), adds clove flower bud distillates, 13
45% edible alcohol of part and 189 parts of sterile water, are put into high speed dispersion homogenizer and carry out homogeneous 22 minutes, homogenizing temperature 40
Degree, obtains oil tea mouthwash.
Embodiment 3
A kind of oil tea mouthwash, is mainly made by the raw material of following parts by weight: 20 parts of Camellia Leaves, 18 parts of root barks of white mulberry, 19 parts
Polemonium caeruleum, 19 parts of common averrhoa flowers, 7 parts of clove flower bud distillates, 10 parts of dewdrop Rabdosia amethystoides, 14 parts of Chinese artichokes, 6 parts of seaweed glues.
A kind of oil tea mouthwash, production method include the following steps:
1) the oil tea leaf extract the preparation method comprises the following steps: take fresh Camellia Leaves, drying is low to moisture content at 110 DEG C
It in 5%, then crushes, crosses 45 meshes；It is soaked in the ethyl alcohol that 6 times of volumetric concentrations are 70%, stirs evenly, then its temperature is mentioned
70 DEG C are raised to, starting ultrasonic cell disruptor extracts 3 hours, filtering, so repeats to extract twice, and merging filtrate twice is to close
And filtrate, obtain oil tea leaf extract；
2) that root bark of white mulberry, polemonium caeruleum, common averrhoa flower, dewdrop Rabdosia amethystoides, Chinese artichoke mixing are crushed to 80 mesh particles with pulverizer is big
It is small, it is put into ultrasonic extractor and is added the edible alcohol of 200mL95%, temperature 60 C, supersonic frequency 30KHz ultrasound are set
It extracts 1 hour, filters, filter residue, which repeats to be put into ultrasonic extractor, to be repeated to extract 2 times under the same terms, and filtering merges filter
Liquid, filtrate are concentrated to dryness at 45 DEG C with Rotary Evaporators, obtain mixture；
3) the resulting oil tea leaf extract of step 1) is mixed with the resulting mixture of step 2), adds clove flower bud distillates, 15
45% edible alcohol of part and 19 parts of sterile water, are put into high speed dispersion homogenizer and carry out homogeneous 25 minutes, homogenizing temperature 40
Degree, obtains oil tea mouthwash.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, fall within the scope of the claimed invention without departing from theon the basis of the spirit of the present invention.
Claims (5)
1. a kind of oil tea mouthwash, which is characterized in that be mainly made by the raw material of following parts by weight: 14-20 parts of Camellia Leaves, 13-
18 parts of root barks of white mulberry, 15-19 Fen polemonium caeruleum, 3-19 parts of common averrhoa flowers, 5-7 parts of clove flower bud distillates, 8-10 parts of dewdrop Rabdosia amethystoides, 10-14 parts of sweet dews
Son, 2-6 parts of seaweed glues.
2. a kind of oil tea mouthwash as described in claim 1, which is characterized in that be mainly made by the raw material of following parts by weight:
14 parts of Camellia Leaves, 13 parts of root barks of white mulberry, 15 Fen polemonium caeruleums, 3 parts of common averrhoa flowers, 5 parts of clove flower bud distillates, 8 parts of dewdrop Rabdosia amethystoides, 10 parts of Chinese artichokes, 2
Part seaweed glue.
3. a kind of oil tea mouthwash as described in claim 1, which is characterized in that be mainly made by the raw material of following parts by weight:
16 parts of Camellia Leaves, 15 parts of root barks of white mulberry, 17 Fen polemonium caeruleums, 5 parts of common averrhoa flowers, 6 parts of clove flower bud distillates, 9 parts of dewdrop Rabdosia amethystoides, 12 parts of Chinese artichokes, 4
Part seaweed glue.
4. a kind of oil tea mouthwash as described in claim 1, which is characterized in that be mainly made by the raw material of following parts by weight:
20 parts of Camellia Leaves, 18 parts of root barks of white mulberry, 19 Fen polemonium caeruleums, 19 parts of common averrhoa flowers, 7 parts of clove flower bud distillates, 10 parts of dewdrop Rabdosia amethystoides, 14 parts of sweet dews
Son, 6 parts of seaweed glues.
5. a kind of oil tea mouthwash as described in claim 1-4 is any, which is characterized in that its production method includes following step
It is rapid:
1) the oil tea leaf extract the preparation method comprises the following steps: take fresh Camellia Leaves, drying is low to moisture content at 105-110 DEG C
It in 5%, then crushes, crosses 35-45 mesh；Be soaked in 4-6 times of volumetric concentration be 70% ethyl alcohol in, stir evenly, then by its
Temperature is promoted to 60-70 DEG C, and starting ultrasonic cell disruptor extracts 1-3 hours, filtering, is so repeated to extract twice, be merged
Filtrate is merging filtrate twice, obtains oil tea leaf extract；
2) root bark of white mulberry, polemonium caeruleum, common averrhoa flower, dewdrop Rabdosia amethystoides, Chinese artichoke mixing are crushed to 80 mesh granular sizes with pulverizer, put
Enter in ultrasonic extractor and be added the edible alcohol of 200mL95%, is arranged 50-60 DEG C of temperature, supersonic frequency 30KHz ultrasound mentions
1 hour is taken, is filtered, filter residue, which repeats to be put into ultrasonic extractor, to be repeated to extract 2 times under the same terms, filtering, merging filtrate,
Filtrate is concentrated to dryness at 45 DEG C with Rotary Evaporators, obtains mixture；
3) the resulting oil tea leaf extract of step 1) is mixed with the resulting mixture of step 2), adds clove flower bud distillates, 12-15 part
45% edible alcohol and 16-19 parts of sterile water are put into high speed dispersion homogenizer and carry out homogeneous 20-25 minutes, homogenizing temperature
It is 40 degree, obtains oil tea mouthwash.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811321486.3A CN109125196A (en) | 2018-11-07 | 2018-11-07 | A kind of oil tea mouthwash and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811321486.3A CN109125196A (en) | 2018-11-07 | 2018-11-07 | A kind of oil tea mouthwash and preparation method thereof |
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| Publication Number | Publication Date |
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| CN109125196A true CN109125196A (en) | 2019-01-04 |
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ID=64808017
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201811321486.3A Pending CN109125196A (en) | 2018-11-07 | 2018-11-07 | A kind of oil tea mouthwash and preparation method thereof |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101167690A (en) * | 2006-10-23 | 2008-04-30 | 王俊二 | Oral cleaning composition |
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2018
- 2018-11-07 CN CN201811321486.3A patent/CN109125196A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101167690A (en) * | 2006-10-23 | 2008-04-30 | 王俊二 | Oral cleaning composition |
Non-Patent Citations (1)
| Title |
|---|
| 武通虎: "《美容食物一本通》", 31 October 2013, 中国医药科技出版社 * |
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Application publication date: 20190104 |