CN104983612A - Plant tooth health care product and preparing method thereof - Google Patents
Plant tooth health care product and preparing method thereof Download PDFInfo
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- CN104983612A CN104983612A CN201510342434.4A CN201510342434A CN104983612A CN 104983612 A CN104983612 A CN 104983612A CN 201510342434 A CN201510342434 A CN 201510342434A CN 104983612 A CN104983612 A CN 104983612A
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Abstract
The invention relates to a plant tooth health care product and a preparing method thereof and belongs to the technical field of oral cleaning and caring products. The plant tooth health care product comprises, by weight, 20.0%-60.0% of soapnut saponins, 10.0%-30.0% of moisturizing agents, 1.0%-3.0% of foaming agents, 1.2%-3.0% of thickening agents, 0.8%-1.5% of xylitol, 0.4%-0.8% of mint extracts, 0.15%-0.6% of preservatives and the balance water. The plant tooth health care product is free of fluoride, saccharin sodium salt, chemical disinfectant and silica gel; active additives of a pure plant source are particularly added, germ breeding can be effectively inhibited, gingivitis is eliminated, the damaged mucosal tissue wounds are repaired, and gingival immunity is enhanced. The plant tooth health care product is safe, mild and not stimulating, people feel cool and fresh after using the product, mouth smell can be effectively removed, and dental ulcer, swelling, aching of gingiva and tooth bleeding are relieved.
Description
Technical field
The present invention relates to oral cleaning nursing article technical field, in particular to kind of plant dental care product and preparation method thereof.
Background technology
Along with the raising of human living standard, the safety consciousness of people to oral cavity series products such as toothpaste improves constantly, and drops into increasing concern to the toxic and side effects of oral cavity products material.
Existing market common toothpaste many interpolations sodium fluoride prevents dental caries, and can sodium fluoride be a kind of chronic noxious substance, fluorine participate in metabolism in vivo, can accumulate in vivo always, when fluorine intake is too much, can cause osteofluorosis.
In addition, common toothpaste is using saccharin sodium as sweeting agent, and the raw material of glucide mainly contains toluene, chlorosulfonic acid, ortho-aminotoluene etc., is petrochemicals.Toluene is volatile and burn, and even sets off an explosion, and can cause acute poisoning after a large amount of absorption human body, larger to human health damage; In addition, common toothpaste also adds silicon dioxide as abrasivus, adds chemical bactericide oral mucosa, soft tissue being had to strong stimulation, CBA, chemical pigment etc.; Silicon dioxide can be caused silicosis by human body suction for a long time; And chemical bactericide, CBA, the chemical pigment zest to body is larger.Therefore, this type of toothpaste of life-time service is very big to human health damage.
In view of this, special proposition the present invention.
Summary of the invention
An object of the present invention is to provide kind of plant dental care product, and these plant dental care product do not add fluoride, saccharin sodium, do not add chemical bactericide, silica gel; The active additive of special interpolation pure plant origin, effective anti-bacteria grows, and eliminates gingivitis, repairs damage mucosal tissue wound surface, strengthens gingiva immunity.Gentle to oral cavity safety, do not stimulate, uses after cool and sweet-smelling, effectively can remove implication, alleviate oral ulcer, gingival swelling and pain, dental hemorrhage.
Two of object of the present invention is to provide a kind of preparation method of described plant dental care product, and this preparation method achieves the preparation of plant dental care product by operations such as mixing, dispersions, and operation is simple, and condition is easy to control.
In order to realize above object, spy of the present invention by the following technical solutions:
One kind of plant dental care product, according to percent by weight, comprising:
Soapberry extract 30.0 ~ 50.0%, wetting agent 15.0 ~ 26.0%, foaming agent 1.2 ~ 2.5%, thickening agent 1.2% ~ 3.0%, xylitol 0.5 ~ 1.5%, Folium Menthae extract 0.2 ~ 1.2%, antiseptic 0.15 ~ 0.4%, water surplus.
This novel plant dental care product do not add fluoride, saccharin sodium, do not add chemical bactericide, CBA, chemical pigment, do not add silica gel, special active additive-soapberry extract of adding pure plant origin; Soapberry extract is a kind of active additive of pure natural.Containing triterpene saponin, catechin tea polyphenol, chlorogenic acid, ferulic acid in soapberry extract, the compositions such as alkaloid, anthraquinone, flavonoid, organic acid, aminoacid, protein, vitamin B2; Wherein, triterpene saponin, catechin tea polyphenol, chlorogenic acid, ferulic acid, alkaloid, anthraquinone have the pathogenic bacteria in multiple harm oral cavity, virus significantly to be killed and inhibitory action.
In addition, contained vitamin B2 and the compound of triterpene saponin such as Hederagenin, oleanolic acid derivate also have the effect for the treatment of oral ulcer; By itself and wetting agent, thickening agent and foaming agent etc. according to the dental care product made after set part by weight compatibility, it can effectively grow by anti-bacteria, eliminates gingivitis, repairs damage mucosal tissue wound surface, strengthens gingiva immunity.Gentle to oral cavity safety, do not stimulate, uses after cool and sweet-smelling, effectively can remove implication, alleviate oral ulcer, gingival swelling and pain, dental hemorrhage.
Preferably, according to percent by weight, comprising:
Soapberry extract 30.0 ~ 50.0%, wetting agent 15.0 ~ 26.0%, foaming agent 1.2 ~ 2.5%, thickening agent 1.2% ~ 3.0%, xylitol 0.5 ~ 1.5%, Folium Menthae extract 0.2 ~ 1.2%, antiseptic 0.15 ~ 0.4%, water surplus.
Preferably, described wetting agent comprises one or more in sorbitol, propylene glycol, glycerol.
Sorbitol, propylene glycol, glycerol its not only moistening effect is obvious, use safety, and it is also easy to and the mixing of the liquid charging stock such as soapberry extract and antiseptic, dispersion.
Preferably, described foaming agent comprises one or more in lauroyl Herba bromi japonici amino acid sodium, sodium lauroyl sarcosine, sodium cocoyl glycinate, sodium cocoyl glutamate, sodium lauroyl glutamate.
Above-mentioned lifted several foaming agent, are synthesized by biotechnology by natural amino acid, saccharide, Petiolus Trachycarpi wet goods, have good soil release performance, foaming characteristic, wettability, to human-body safety, environmentally friendly, have good affinity with enamel.Compared with traditional CBA, the foaming agent contact opening transmucosal of the type is safe, gentle, to oral mucosa, soft tissue fanout free region, stimulation.
Preferably, described thickening agent comprises one or more in xanthan gum, sodium carboxymethyl cellulose, guar gum, carrageenan.
Preferably, described antiseptic comprises one or more in phenoxyethanol, sodium benzoate, potassium sorbate.
Phenoxyethanol, sodium benzoate, potassium sorbate all have good antibacterial, antiseptic effect, microbial growth and breeding can be suppressed, especially after itself and Folium Menthae extract and soapberry extract mixture, antiseptic effect is more obvious, a large amount of microbial growths and breeding can be suppressed, while making dental care product have good antiseptic effect, also there is elimination gingivitis, reparation damaging mucosal organizes the effects such as wound surface, oral ulcer, gingival swelling and pain, dental hemorrhage.
Prepare a method for plant dental care product, comprise the steps:
1), by water, soapberry extract, wetting agent and antiseptic mix, obtain fluid mix; Thickening agent, foaming agent and xylitol are mixed, obtains powder mixture;
2), by described powder mixture join in described fluid mix, and carry out dispersed with stirring, obtain first product, and redispersion add Folium Menthae extract in described first product after, obtain plant dental care product.
This preparation method, utilize the physical property classification mixing of raw material, obtain fluid mix and powder mixture (without sequencing) respectively, and then by fluid mix and powder mixture mixing, carry out stirring, disperseing, make the mixing of all materials, emulsifying abundant, and obtain the first product of paste, in first product, now add the Folium Menthae extract with salubrious and fungistatic effect, carry out redispersion, the plant dental care product of the application can be obtained.This preparation method, device simple used, and also operating process is easy to control, and has cost low, is convenient to the effect realized.
Preferably, in step 1) in, the preparation method of described soapberry extract comprises:
A), by Fructus Sapindi Mukouossi fruit peel off, the fruit peel powder obtained is broken to 20 ~ 80 order granularities, and adds 5 times wherein to the distilled water of peel of Fructus Sapindi Mukouossi quality; Stirring extraction 2 hours is carried out under 53 ~ 62 DEG C, 2000 ~ 4000 revs/min;
B), step a) in Aqueous extracts leave standstill 5 minutes except after precipitation and cross macroporous adsorptive resins, gained precipitation extracts 2 ~ 3 times again, and the extracting solution again obtained is crossed described macroporous adsorptive resins;
C) macroporous adsorptive resins described in 4 ~ 6 times of distillation moisture eluting to peel of Fructus Sapindi Mukouossi quality 1 ~ 4 time, is first used, use macroporous adsorptive resins described in 6 ~ 8 times of 80 ~ 90% ethanol water eluting to peel of Fructus Sapindi Mukouossi quality 4 ~ 6 times again, collect ethanol elution, distilling under reduced pressure, except after ethanol, obtains soapberry extract.
Further preferably, Fructus Sapindi Mukouossi fruit is dried after cleaning, then peels off, and the operation of pulverizing adopts electric crusher to carry out, and to realize fast-crushing, reduces the effect that effective ingredient destroys and runs off.
By repeatedly extracting, adsorbing and the operation such as eluting, soapberry extract can be obtained; In the preparation method of this soapberry extract, because the Selecting parameter such as Extracting temperature, rotating speed is proper, and carried out repeatedly extracting, active component extracts completely, and the adsorption effect of macroporous adsorbent resin is good, a large amount of organic extracts in extracting solution optionally can be adsorbed, through 6 ~ 8 times after 80 ~ 90% ethanol water eluting of peel of Fructus Sapindi Mukouossi quality, the soapberry extract meeting preparation and require can be obtained.
Preferably, in step 2) in: described operation utilizes colloid mill to complete.
Colloid mill can collect pulverizing, dispersion, emulsifying, and homogenizing and stirring etc. are operating as one, can fast and effeciently disperse to stir ground effect, and all materials are fully mixed.
Preferably, the time of described dispersed with stirring is 50-70 minute, and the time of described redispersion is 20-40 minute; And/or after redispersion, after disperseing, material is by 70-90 order metre filter, obtains plant dental care product.
By specifically selecting the time of dispersed with stirring and redispersion, but also filter the material after redispersion, thus the dental care product made constantly have the effects such as safe, antibacterial, gentle and antiinflammatory, also make its profile excellent performance, neither too hard, nor too soft, delicate mouthfeel.
Compared with prior art, technique effect of the present invention comprises the following aspects:
1), plant dental care product provided by the invention do not add fluoride, saccharin sodium, do not add chemical bactericide, CBA, chemical pigment, do not add silica gel.The set percentage by weight of special interpolation, and the active additive and the Folium Menthae extract that are pure plant origin; Be equipped with antiseptic and foaming agent again, give the effective anti-bacteria of dental care product to grow, eliminate gingivitis, repair damage mucosal tissue wound surface, strengthen the effect of gingiva immunity, and gentle to oral cavity safety, do not stimulate, use cool and sweet-smelling afterwards, effectively remove implication, alleviate oral ulcer, gingival swelling and pain, dental hemorrhage.
2), foaming agent is synthesized by biotechnology by natural amino acid, saccharide, Petiolus Trachycarpi wet goods, there is good soil release performance, foaming characteristic, wettability, to human-body safety and environmentally friendly, there is good affinity with enamel, injury non-stimulated to oral mucosa, soft tissue.
3), soapberry extract is a kind of active additive of pure natural, containing triterpene saponin, catechin tea polyphenol, chlorogenic acid, ferulic acid, and the compositions such as alkaloid, anthraquinone, flavonoid, organic acid, aminoacid, protein, vitamin B2; Have the pathogenic bacteria in multiple harm oral cavity, virus and significantly kill and inhibitory action, also there is the effect for the treatment of oral ulcer.
4), the preparation method of plant dental care product is simple, and operation is easy to control.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but it will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting the scope of the invention.Unreceipted actual conditions person in embodiment, the condition of conveniently conditioned disjunction manufacturer suggestion is carried out.Agents useful for same or the unreceipted preparation manufacturer person of instrument, be and can buy by commercially available the conventional products obtained.
Before describing embodiments of the invention, make following explanation to the preparation method spy of soapberry extract provided by the invention, particularly, the preparation method of soapberry extract provided by the invention comprises:
S1: by Fructus Sapindi Mukouossi fruit clean, dry after peel off, the peel electric crusher obtained is crushed to 20 ~ 80 order granularities, and add 5 times wherein to the distilled water of peel of Fructus Sapindi Mukouossi quality, under 53 ~ 62 DEG C, 2000 ~ 4000 revs/min, carry out stirring extraction 2 hours;
S2: the Aqueous extracts in step S1 crosses macroporous adsorptive resins except after precipitation in standing 5 minutes, gained precipitates (slag after extraction) and extracts 2 ~ 3 times again, and the extracting solution again obtained is crossed described macroporous adsorptive resins;
S3: first use macroporous adsorptive resins described in 4 ~ 6 times of distillation moisture eluting to peel of Fructus Sapindi Mukouossi quality 1 ~ 4 time, use macroporous adsorptive resins described in 6 ~ 8 times of 80 ~ 90% ethanol water eluting to peel of Fructus Sapindi Mukouossi quality 4 ~ 6 times again, collect ethanol elution, distilling under reduced pressure, except after ethanol, obtains soapberry extract.
Next specific embodiment is once enumerated to plant dental care product of the present invention and preparation method thereof, it is pointed out that the soapberry extract in following examples obtains by above method.
Embodiment 1
By 42.65 kilograms, water, soapberry extract 20 kilograms, sorbitol 10 kilograms, propylene glycol 10 kilograms, glycerol 10 kilograms and sodium benzoate 0.15 kilogram mixing, obtain fluid mix;
By xanthan gum 0.7 kilogram, sodium carboxymethyl cellulose 0.9 kilogram, guar gum 0.5 kilogram, carrageenan 0.2 kilogram, sodium cocoyl glycinate 1 kilogram, sodium cocoyl glutamate 1 kilogram, lauroyl Herba bromi japonici amino acid sodium 0.6 kilogram and xylitol 1.5 kilograms mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 65 minutes, obtain first product, and redispersion 30 minutes add Folium Menthae extract 0.8 kilogram in first product after, through 80 order filter dischargings, obtain plant dental care product.
Embodiment 2
By 41.1 kilograms, water, soapberry extract 25 kilograms, sorbitol 15 kilograms, propylene glycol 11 kilograms and potassium sorbate 0.2 kilogram mixing, obtain fluid mix;
By sodium carboxymethyl cellulose 2.1 kilograms, carrageenan 0.9 kilogram, sodium lauroyl glutamate 1.2 kilograms, sodium lauroyl sarcosine 1.8 kilograms and xylitol 1.3 kilograms mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 70 minutes, obtain first product, and redispersion 40 minutes add Folium Menthae extract 0.4 kilogram in first product after, through 80 order filter dischargings, obtain plant dental care product.
Embodiment 3
By 40.3 kilograms, water, soapberry extract 30 kilograms, sorbitol 12 kilograms, glycerol 11 kilograms and phenoxyethanol 0.6 kilogram mixing, obtain fluid mix;
By sodium carboxymethyl cellulose 0.5 kilogram, guar gum 1.3 kilograms, sodium cocoyl glycinate 0.5 kilogram, sodium lauroyl glutamate 0.6 kilogram, sodium lauroyl sarcosine 0.4 kilogram, lauroyl Herba bromi japonici amino acid sodium 0.8 kilogram and xylitol 1 kilogram mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 60 minutes, obtain first product, and redispersion 30 minutes add Folium Menthae extract 1 kilogram in first product after, through 80 order filter dischargings, obtain plant dental care product.
Embodiment 4
By 39.5 kilograms, water, soapberry extract 35 kilograms, propylene glycol 9 kilograms, glycerol 12 kilograms and sodium benzoate 0.1 kilogram, phenoxyethanol 0.3 kilogram mixing, obtain fluid mix;
By xanthan gum 1.2 kilograms, sodium lauroyl glutamate 0.9 kilogram, lauroyl Herba bromi japonici amino acid sodium 1.3 kilograms and xylitol 0.5 kilogram mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 65 minutes, obtain first product, and redispersion 30 minutes add Folium Menthae extract 0.2 kilogram in first product after, through 80 order filter dischargings, obtain plant dental care product.
Embodiment 5
By 36.6 kilograms, water, soapberry extract 40 kilograms, glycerol 18 kilograms and potassium sorbate 0.2 kilogram mixing, obtain fluid mix;
By sodium carboxymethyl cellulose 0.3 kilogram, carrageenan 1.2 kilograms, sodium cocoyl glutamate 0.8 kilogram, sodium lauroyl glutamate 0.9 kilogram and xylitol 0.8 kilogram mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 70 minutes, obtain first product, and redispersion 35 minutes add Folium Menthae extract 1.2 kilograms in first product after, through 70 order filter dischargings, obtain plant dental care product.
Embodiment 6
By 34.8 kilograms, water, soapberry extract 40 kilograms, propylene glycol 15 kilograms and sodium benzoate 0.1, potassium sorbate 0.1 kilogram mixing, obtain fluid mix;
By guar gum 1.8 kilograms, sodium cocoyl glycinate 1.5 kilograms and xylitol 1.1 kilograms mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 60 minutes, obtain first product, and redispersion 30 minutes add Folium Menthae extract 0.6 kilogram in first product after, through 90 order filter dischargings, obtain plant dental care product.
Embodiment 7
By 33.6 kilograms, water, soapberry extract 50 kilograms, sorbitol 10 kilograms and phenoxyethanol 0.4 kilogram, potassium sorbate 0.1 kilogram mixing, obtain fluid mix;
By xanthan gum 0.8 kilogram, sodium carboxymethyl cellulose 1.6 kilograms, guar gum 0.4 kilogram, sodium lauroyl sarcosine 1 kilogram and xylitol 1.4 kilograms mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 60 minutes, obtain first product, and redispersion 30 minutes add Folium Menthae extract 0.7 kilogram in first product after, through 70 order filter dischargings, obtain plant dental care product.
Embodiment 8
By water 23.25, soapberry extract 60 kilograms, sorbitol 7 kilograms, glycerol 5 kilograms and sodium benzoate 0.15 kilogram mixing, obtain fluid mix;
By xanthan gum 1 kilogram, sodium carboxymethyl cellulose 1.2 kilograms, sodium cocoyl glycinate 0.6 kilogram, sodium cocoyl glutamate 0.6 kilogram and xylitol 0.7 kilogram mixing, obtain powder mixture;
Described powder mixture is joined in described fluid mix, and carries out dispersed with stirring 60 minutes, obtain first product, and redispersion 30 minutes add Folium Menthae extract 0.5 kilogram in first product after, through 80 order filter dischargings, obtain plant dental care product.
Test example 1 plant of the present invention dental care product are to the safe mildness of human body
The plant dental care product sample using above-described embodiment 1-8 to make carries out clinical trial, method of testing is brushed teeth, tested object is divided into 2 groups, one group is the child of 5 ~ 10 years old, one group is 30 ~ 60 years old adult, sooner or later uses every day the plant dental care product sample of above-described embodiment to brush teeth twice, a week on probation, the safety of test and appraisal novel plant dental care product sample, result of the test is in table 1 and table 2:
The plant dental care product of each embodiment of table 1 are to the test result of 5 ~ 10 years old child
The plant dental care product of each embodiment of table 2 are to the test result of 30 ~ 60 years old (adult)
Test example 2 is tested novel plant dental care product and is removed halitosis, alleviates oral ulcer, the effect of gingival swelling and pain, dental hemorrhage
The plant dental care product sample using above-described embodiment 1-8 to make carries out clinical trial, and method of testing is brushed teeth, and tested object is divided into 3 groups, and one group is the volunteer having halitosis; One group is the volunteer of oral ulcer; One group be toothache, dental hemorrhage volunteer.Sooner or later use every day the plant dental care product sample of above-described embodiment to brush teeth twice, one month on probation, test and appraisal trier oral problem improves situation, and result of the test is in Table 3-table 5.
The plant dental care product of each embodiment of table 3 are to the test result of halitosis person
The plant dental care product of each embodiment of table 4 are to the test result of oral ulcer person
The plant dental care product of each embodiment of table 5 are to the test result of toothache, dental hemorrhage patient
In sum, these kind of plant dental care product provided by the invention, soapberry extract has the pathogenic bacteria in multiple harm oral cavity, virus significantly to be killed and inhibitory action; After itself and Folium Menthae extract and vegetalitas foaming agent mixture, also there is the effect for the treatment of oral ulcer; And foaming agent is synthesized by biotechnology by natural amino acid, saccharide, Petiolus Trachycarpi wet goods, there is good soil release performance, foaming characteristic, wettability, to human-body safety and environmentally friendly, good affinity is had with enamel, and then it is safe to oral cavity, gentle to give plant dental care product, do not stimulate, use rear cool and sweet-smelling, effectively remove halitosis; Oral ulcer can be alleviated significantly, gingival swelling and pain, dental hemorrhage; Help eliminate gingivitis, repair damaging mucosal and organize wound surface, strengthen the effect of gingiva immunity.
Although illustrate and describe the present invention with specific embodiment, however it will be appreciated that can to make when not deviating from the spirit and scope of the present invention many other change and amendment.Therefore, this means to comprise all such changes and modifications belonged in the scope of the invention in the following claims.
Claims (10)
1. kind of plant dental care product, is characterized in that, according to percent by weight, comprising:
Soapberry extract 20.0 ~ 60.0%, wetting agent 10.0 ~ 30.0%, foaming agent 1.0 ~ 3.0%, thickening agent 1.2% ~ 3.0%, xylitol 0.8 ~ 1.5%, Folium Menthae extract 0.4 ~ 0.8%, antiseptic 0.15 ~ 0.6%, water surplus.
2. plant dental care product as claimed in claim 1, is characterized in that, according to percent by weight, comprising:
Soapberry extract 30.0 ~ 50.0%, wetting agent 15.0 ~ 26.0%, foaming agent 1.2 ~ 2.5%, thickening agent 1.2% ~ 3.0%, xylitol 0.5 ~ 1.5%, Folium Menthae extract 0.2 ~ 1.2%, antiseptic 0.15 ~ 0.4%, water surplus.
3. plant dental care product as claimed in claim 1 or 2, is characterized in that, described wetting agent comprise in sorbitol, propylene glycol, glycerol one or more.
4. plant dental care product as claimed in claim 3, is characterized in that, described foaming agent comprise in lauroyl Herba bromi japonici amino acid sodium, sodium lauroyl sarcosine, sodium cocoyl glycinate, sodium cocoyl glutamate, sodium lauroyl glutamate one or more.
5. plant dental care product as claimed in claim 4, is characterized in that, described thickening agent comprise in xanthan gum, sodium carboxymethyl cellulose, guar gum, carrageenan one or more.
6. plant dental care product as claimed in claim 5, is characterized in that, described antiseptic comprise in phenoxyethanol, sodium benzoate, potassium sorbate one or more.
7. prepare a method for plant dental care product, it is characterized in that, comprise the steps:
1), by water, soapberry extract, wetting agent and antiseptic mix, obtain fluid mix; Thickening agent, foaming agent and xylitol are mixed, obtains powder mixture;
2), by described powder mixture join in described fluid mix, and carry out dispersed with stirring, obtain first product, and redispersion add Folium Menthae extract in described first product after, obtain plant dental care product.
8. prepare the method for plant dental care product as claimed in claim 7, it is characterized in that, in step 1) in, the preparation method of described soapberry extract comprises:
A), by Fructus Sapindi Mukouossi fruit peel off, the fruit peel powder obtained is broken to 20 ~ 80 order granularities, and adds 5 times wherein to the distilled water of peel of Fructus Sapindi Mukouossi quality; Stirring extraction 2 hours is carried out under 53 ~ 62 DEG C, 2000 ~ 4000 revs/min;
B), step a) in Aqueous extracts leave standstill 5 minutes except after precipitation and cross macroporous adsorptive resins, gained precipitation extracts 2 ~ 3 times again, and the extracting solution again obtained is crossed described macroporous adsorptive resins;
C) macroporous adsorptive resins described in 4 ~ 6 times of distillation moisture eluting to peel of Fructus Sapindi Mukouossi quality 1 ~ 4 time, is first used, use macroporous adsorptive resins described in 6 ~ 8 times of 80 ~ 90% ethanol water eluting to peel of Fructus Sapindi Mukouossi quality 4 ~ 6 times again, collect ethanol elution, distilling under reduced pressure, except after ethanol, obtains soapberry extract.
9. prepare the method for plant dental care product as claimed in claim 8, it is characterized in that, in step 2) in: described operation utilizes colloid mill to complete.
10. the method preparing plant dental care product as described in any one of claim 7-9, is characterized in that, in step 2) in:
The time of described dispersed with stirring is 50-70 minute, and the time of described redispersion is 20-40 minute;
And/or;
After redispersion, after disperseing, material is by 70-90 order metre filter, obtains plant dental care product.
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| CN201510342434.4A CN104983612A (en) | 2015-06-18 | 2015-06-18 | Plant tooth health care product and preparing method thereof |
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| CN201510342434.4A CN104983612A (en) | 2015-06-18 | 2015-06-18 | Plant tooth health care product and preparing method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106236640A (en) * | 2016-08-24 | 2016-12-21 | 马南行 | A kind of natural mousse foam compositions and preparation method thereof that cleans one's teeth |
| CN108042420A (en) * | 2017-12-20 | 2018-05-18 | 弘美制药（中国）有限公司 | A kind of composition and its application for oral health |
| CN111686044A (en) * | 2020-04-22 | 2020-09-22 | 颜克顺 | Preparation method of soapberry toothpaste |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02262510A (en) * | 1987-08-11 | 1990-10-25 | Inahata Koryo Kk | Dentifrice composition |
| KR20120054297A (en) * | 2010-11-19 | 2012-05-30 | (주)아모레퍼시픽 | Oral composition containing extract of sapindus mukurossi gaertn |
| CN103961275A (en) * | 2013-02-03 | 2014-08-06 | 广州无患子生物科技有限公司 | Daily necessities containing all-natural source surfactant and preparation method thereof |
-
2015
- 2015-06-18 CN CN201510342434.4A patent/CN104983612A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02262510A (en) * | 1987-08-11 | 1990-10-25 | Inahata Koryo Kk | Dentifrice composition |
| KR20120054297A (en) * | 2010-11-19 | 2012-05-30 | (주)아모레퍼시픽 | Oral composition containing extract of sapindus mukurossi gaertn |
| CN103961275A (en) * | 2013-02-03 | 2014-08-06 | 广州无患子生物科技有限公司 | Daily necessities containing all-natural source surfactant and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106236640A (en) * | 2016-08-24 | 2016-12-21 | 马南行 | A kind of natural mousse foam compositions and preparation method thereof that cleans one's teeth |
| CN108042420A (en) * | 2017-12-20 | 2018-05-18 | 弘美制药（中国）有限公司 | A kind of composition and its application for oral health |
| CN111686044A (en) * | 2020-04-22 | 2020-09-22 | 颜克顺 | Preparation method of soapberry toothpaste |
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