CN109730955A - Toothpaste containing lacquer tree leaf extract - Google Patents
Toothpaste containing lacquer tree leaf extract Download PDFInfo
- Publication number
- CN109730955A CN109730955A CN201910161866.3A CN201910161866A CN109730955A CN 109730955 A CN109730955 A CN 109730955A CN 201910161866 A CN201910161866 A CN 201910161866A CN 109730955 A CN109730955 A CN 109730955A
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- lacquer tree
- leaf extract
- tree leaf
- extract
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- 239000000284 extract Substances 0.000 title claims abstract description 94
- 244000044283 Toxicodendron succedaneum Species 0.000 title claims abstract description 80
- 229940034610 toothpaste Drugs 0.000 title claims abstract description 61
- 239000000606 toothpaste Substances 0.000 title claims abstract description 61
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 44
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 39
- 241000244987 Daiswa polyphylla Species 0.000 claims abstract description 35
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000019502 Orange oil Nutrition 0.000 claims abstract description 15
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 15
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000010502 orange oil Substances 0.000 claims abstract description 15
- 239000000811 xylitol Substances 0.000 claims abstract description 15
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 15
- 235000010447 xylitol Nutrition 0.000 claims abstract description 15
- 229960002675 xylitol Drugs 0.000 claims abstract description 15
- 239000008367 deionised water Substances 0.000 claims abstract description 14
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 14
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 claims abstract description 13
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims abstract description 13
- 235000019799 monosodium phosphate Nutrition 0.000 claims abstract description 13
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims abstract description 13
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims abstract description 10
- RRLOOYQHUHGIRJ-UHFFFAOYSA-M sodium;ethyl sulfate Chemical compound [Na+].CCOS([O-])(=O)=O RRLOOYQHUHGIRJ-UHFFFAOYSA-M 0.000 claims abstract description 10
- 239000004615 ingredient Substances 0.000 claims abstract description 8
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 3
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 3
- 229960004029 silicic acid Drugs 0.000 claims abstract description 3
- 238000000605 extraction Methods 0.000 claims description 20
- 239000000706 filtrate Substances 0.000 claims description 19
- 235000019441 ethanol Nutrition 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 11
- 238000001035 drying Methods 0.000 claims description 9
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- 239000011780 sodium chloride Substances 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 108090000790 Enzymes Proteins 0.000 claims description 5
- 102000004190 Enzymes Human genes 0.000 claims description 5
- 229940088598 enzyme Drugs 0.000 claims description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 108010059892 Cellulase Proteins 0.000 claims description 3
- 239000001273 butane Substances 0.000 claims description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 3
- 229940106157 cellulase Drugs 0.000 claims description 3
- 238000007654 immersion Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 claims description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- 239000001294 propane Substances 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
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- 239000001569 carbon dioxide Substances 0.000 claims description 2
- 238000002137 ultrasound extraction Methods 0.000 claims description 2
- 235000019700 dicalcium phosphate Nutrition 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 11
- 238000004140 cleaning Methods 0.000 abstract description 7
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- 201000001245 periodontitis Diseases 0.000 abstract description 4
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- 208000025157 Oral disease Diseases 0.000 abstract 1
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- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 14
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- 229940068918 polyethylene glycol 400 Drugs 0.000 description 10
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- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
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- 241000208225 Rhus Species 0.000 description 7
- 210000000214 mouth Anatomy 0.000 description 7
- 239000000377 silicon dioxide Substances 0.000 description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
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- 229910052710 silicon Inorganic materials 0.000 description 6
- 239000010703 silicon Substances 0.000 description 6
- 239000004575 stone Substances 0.000 description 6
- 235000014220 Rhus chinensis Nutrition 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- 239000000084 colloidal system Substances 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 5
- 230000001954 sterilising effect Effects 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
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- 239000003814 drug Substances 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 4
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- 239000000126 substance Substances 0.000 description 4
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- 239000000463 material Substances 0.000 description 3
- 230000001151 other effect Effects 0.000 description 3
- WTVHAMTYZJGJLJ-UHFFFAOYSA-N (+)-(4S,8R)-8-epi-beta-bisabolol Natural products CC(C)=CCCC(C)C1(O)CCC(C)=CC1 WTVHAMTYZJGJLJ-UHFFFAOYSA-N 0.000 description 2
- RGZSQWQPBWRIAQ-CABCVRRESA-N (-)-alpha-Bisabolol Chemical compound CC(C)=CCC[C@](C)(O)[C@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-CABCVRRESA-N 0.000 description 2
- DXRKLUVKXMAMOV-UHFFFAOYSA-N 3-heptadecylcatechol Chemical compound CCCCCCCCCCCCCCCCCC1=CC=CC(O)=C1O DXRKLUVKXMAMOV-UHFFFAOYSA-N 0.000 description 2
- CCOQPGVQAWPUPE-UHFFFAOYSA-N 4-tert-butylcyclohexan-1-ol Chemical compound CC(C)(C)C1CCC(O)CC1 CCOQPGVQAWPUPE-UHFFFAOYSA-N 0.000 description 2
- 241000208223 Anacardiaceae Species 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 240000001008 Dimocarpus longan Species 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 235000000235 Euphoria longan Nutrition 0.000 description 2
- 241000628997 Flos Species 0.000 description 2
- 241000202807 Glycyrrhiza Species 0.000 description 2
- 235000001453 Glycyrrhiza echinata Nutrition 0.000 description 2
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 description 2
- 235000017382 Glycyrrhiza lepidota Nutrition 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 2
- 235000006679 Mentha X verticillata Nutrition 0.000 description 2
- 235000002899 Mentha suaveolens Nutrition 0.000 description 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 2
- 239000004909 Moisturizer Substances 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 229910021536 Zeolite Inorganic materials 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- RGZSQWQPBWRIAQ-LSDHHAIUSA-N alpha-Bisabolol Natural products CC(C)=CCC[C@@](C)(O)[C@@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-LSDHHAIUSA-N 0.000 description 2
- 239000002260 anti-inflammatory agent Substances 0.000 description 2
- 230000001741 anti-phlogistic effect Effects 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 230000003078 antioxidant effect Effects 0.000 description 2
- 235000006708 antioxidants Nutrition 0.000 description 2
- 230000003385 bacteriostatic effect Effects 0.000 description 2
- 229940036350 bisabolol Drugs 0.000 description 2
- HHGZABIIYIWLGA-UHFFFAOYSA-N bisabolol Natural products CC1CCC(C(C)(O)CCC=C(C)C)CC1 HHGZABIIYIWLGA-UHFFFAOYSA-N 0.000 description 2
- 208000020670 canker sore Diseases 0.000 description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000001877 deodorizing effect Effects 0.000 description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 description 2
- 229940043264 dodecyl sulfate Drugs 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 235000003599 food sweetener Nutrition 0.000 description 2
- 229910052588 hydroxylapatite Inorganic materials 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 229940010454 licorice Drugs 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- AHADSRNLHOHMQK-UHFFFAOYSA-N methylidenecopper Chemical compound [Cu].[C] AHADSRNLHOHMQK-UHFFFAOYSA-N 0.000 description 2
- 230000001333 moisturizer Effects 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 description 2
- WCVRQHFDJLLWFE-UHFFFAOYSA-N pentane-1,2-diol Chemical compound CCCC(O)CO WCVRQHFDJLLWFE-UHFFFAOYSA-N 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- 230000002335 preservative effect Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 2
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 239000003765 sweetening agent Substances 0.000 description 2
- 239000000230 xanthan gum Substances 0.000 description 2
- 229920001285 xanthan gum Polymers 0.000 description 2
- 229940082509 xanthan gum Drugs 0.000 description 2
- 235000010493 xanthan gum Nutrition 0.000 description 2
- 239000010457 zeolite Substances 0.000 description 2
- 239000001243 zingiber officinale rosc. root absolute Substances 0.000 description 2
- 240000001371 Chamaedaphne calyculata Species 0.000 description 1
- 235000013691 Chamaedaphne calyculata var. angustifolia Nutrition 0.000 description 1
- 235000013685 Chamaedaphne calyculata var. latifolia Nutrition 0.000 description 1
- 235000013687 Chamaedaphne calyculata var. nana Nutrition 0.000 description 1
- 241000206575 Chondrus crispus Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 108010029541 Laccase Proteins 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 241000159241 Toxicodendron Species 0.000 description 1
- 235000011756 Vitis shuttleworthii Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 206010003246 arthritis Diseases 0.000 description 1
- 150000001545 azulenes Chemical class 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
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- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
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- 239000004922 lacquer Substances 0.000 description 1
- 238000013332 literature search Methods 0.000 description 1
- 230000007721 medicinal effect Effects 0.000 description 1
- 150000002729 menthone derivatives Chemical class 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
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- 230000000474 nursing effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
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- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
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- 239000002994 raw material Substances 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- GEYJUFBPCGDENK-UHFFFAOYSA-M sodium;3,8-dimethyl-5-propan-2-ylazulene-1-sulfonate Chemical compound [Na+].CC(C)C1=CC=C(C)C2=C(S([O-])(=O)=O)C=C(C)C2=C1 GEYJUFBPCGDENK-UHFFFAOYSA-M 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
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- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Abstract
Toothpaste containing lacquer tree leaf extract, it include following ingredients as unit of parts by weight: 10~25 parts of lacquer tree leaf extract, 1~3 part of paris polyphylla extract, 8~10 parts of glycerol, 8~10 parts of sorbierite, 2~5 parts of laruyl alcohol sodium sulfovinate, 1~3 part of xylitol, 1~3 part of sodium cellulose glycolate, 1~2 part of sodium dihydrogen phosphate, 10~20 parts of two water object of calcium monohydrogen phosphate, 3~8 parts of orange oil, 3~6 parts of polyethylene glycol 400,8~15 parts of hydrated silica, 0.2~0.5 part of essence, 60~90 parts of deionized water.The present invention has refreshing and detoxicating, breath freshening by toothpaste prepared by lacquer tree leaf extract, inhibits microbial growth, anti-inflammatory, the effect of dispelling oral peculiar smell, effectively kill germ and control periodontitis.There are significant prevention and remission effect to common oral disease, it can long-acting holding oral cleaning health.
Description
Technical field
The invention belongs to forest chemical fields and natural extracts antimicrobial technology field.It is painted in particular it relates to containing
The toothpaste of leaf extract is lacquer tree comprehensive utilization technique, and extract is a kind of novel, natural antibacterial activity in Folium toxicodendri verniciflni
Substance.
Background technique
With economic development and improvement of living standards, people are higher and higher to the attention degree of mouth disease.Oral cavity
If disease not from source radical cure can along with cause some diseases, a large number of studies show that, diabetes, heart disease, arthritis, kidney
Disease, eye disease, enterogastric diseases, cranial vascular disease, respiratory disease etc. all have stronger correlation with mouth disease.And these diseases
Disease be mostly by bacterium, pathogenic bacteria, toxin oral cavity sprawling caused by etc. it is related, therefore develop have antibacterial efficacy drug pair
The health in oral cavity just becomes to be even more important.
Toothpaste is the cleaning oral cavity and optimal daily necessities of tooth, protects tooth in addition to having to clean one's teeth, removes removing abnormal flavor in oral cavity and stain dirt
Function outside, more and more functions are by demand, such as: inhibiting the growth of oral cavity harmful bacteria, assisting sterilisation anti-inflammatory, heat-clearing drop
Fire, breath freshening etc..At present there are many effect type toothpaste, such as anti-hypersensitive dentin, stain whitening, odor type, medicated toothpaste are removed,
But some chemical synthetic materials are all added in effect toothpaste, this will cause potential threat to people's health.Therefore,
The exploitation of toothpaste of the effect of to natural health becomes more urgent.
In patent CN201711430017.0, a kind of sterilization toothpaste is disclosed, in parts by weight includes following components:
3.0~4.5 parts of acrylic acid polymer；1.5~3.5 parts of Cocoamidopropyl betaine；28~40 parts of moisturizer；Sweetener
0.2~0.5 part；0.3~0.7 part of thickener；30~50 parts of rubbing agent；10~25 parts of deionized water；0.7~1.5 part of azulenes；
The rubbing agent is longan seed powder.The present invention, which has passed through, uses longan seed powder both effectively to drive away tooth as the rubbing agent of toothpaste
Tooth dirt, and it is avoided that the phenomenon that therefore friction leads to bleeding gums, and without adding new hemostatic compositions, to reduce
The production cost of toothpaste.
In patent CN201511011005.5, a kind of toothpaste of deodorizing sterilizing, including following weight percent are disclosed
Component: natural marble dust 10%, silica 1 0%, propylene glycol 28%, sldium lauryl sulfate 2%, xanthan gum 0.8%, xylitol
0.25%, Mint Essence 1%, hydroxyapatite 6%, Flos Chrysanthemi Indici extract 2%, licorice 1%, preservative 0.1%, water surplus.
Wherein: natural marble dust, silica are used as rubbing agent, and propylene glycol is used as moisturizer, sldium lauryl sulfate conduct
Surfactant uses, and xanthan gum is used as adhesive, and xylitol is used as sweetener, and Mint Essence makes as essence
With hydroxyapatite, Flos Chrysanthemi Indici extract, licorice are used as functional component.Toothpaste safe and non-toxic of the invention,
Have the effect of good antibacterial, antibacterial, deodorizing sterilizing.
In patent CN108904416A, a kind of reparation toothpaste is disclosed, comprising as following formula: copper carbon composite
0.01%-1%；Zeolite 0.1%-1%；Bisabolol 0.1%-0.5%；Ginger-root extract 0.1%-0.5%；1,2- pentanediol
Or 4- tert. butyl cyclohexanol 0.1%-0.5%；Sodium azulenesulfonate 0.3%-1%；Silica 1 0%-25%；Sorbierite 40%-
65%；Laruyl alcohol sodium sulfovinate 1.8%-2.5%；Carragheen 0.1%-0.5%；Hydroxymethyl cellulose 0.4%-0.8%；Poly- second
Glycol 1%-3%；Tertiary sodium phosphate 0.1%-0.3%；Essence 0.6%-1.5%；Titanium dioxide 0.1%-0.8%；Menthones
0.1%-0.5%；Surplus is water, compound by the basis of conventional toothpaste, being added to copper carbon by the improvement of above-mentioned formula
Material, zeolite, bisabolol, ginger-root extract, 1,2- pentanediol or 4- tert. butyl cyclohexanol, sodium sulfonate, so that toothpaste is simultaneously
Have the function that antibacterial, anti-inflammatory, Shu Min and targeting are repaired, has filled up the market vacancy.
Lacquer tree leaf extract is used to play the effect of its nursing health in toothpaste currently, having not been reported.Lacquer tree leaf extract
With anti-oxidant, bactericidal antiphlogistic, breath freshening and other effects.Lacquer tree leaf extract is used in toothpaste, developing, there is sterilization to disappear
Inflammation, natural more effect toothpaste of breath freshening are necessary.
Summary of the invention
Toothpaste containing lacquer tree leaf extract in toothpaste of the present invention protects tooth, removes removing abnormal flavor in oral cavity except having to clean one's teeth
Outside the basic function of the toothpaste such as stain dirt, additionally it is possible to effectively inhibit Buccodental harmful bacteria to breed, bactericidal antiphlogistic, anti-oxidant,
Breath freshening and other effects.
Lacquer tree refers to a kind of plant of Anacardiaceae (Anacardiaceae) Rhus (Toxico-dendron), is subordinate to
Belong to subtropical zone fauna, the 3rd ancient few survivors tree species of discipline of the Cenozoic, are China Important Economic tree species.Lacquer tree belongs to more than 20 entirely, mainly
Distribution east Asia and North America to Central America, India, Korea, Japan are also distributed.Chinese Rhus plant shares 15 kinds,
It is distributed in each provinces and regions of south China.It in the characteristics of being widely distributed for Yunnan, Yunnan lacquer tree is had from only 8 meters
Multiple types of the dungarunga to the megaphanerophyte for being up to 18 meters or more.The leaflet number of odd number leatherleaf has as little as 1, also has more to
21, it is in the majority with 9~15 types；It is leaf less than normal, mostly in narrow oval.Kind is real rich full.In addition to taping a lacquer tree, Chang Youti
The value of wax oil expression.The phenology of lacquer tree is also different in Yunnan various regions, and front and back differs 2 ~ 3 climates and other natural phenomena of a season.Yunnan lacquer tree is changeable, tall and big
Feature is inseparable with its habitat.The 84% of Yunnan landform is mountainous region.From 800~2000 meters of height above sea level of Northeast Yunnan, China, NW YUNNAN is arrived
2100~2800 meters between have lacquer tree distribution.
Leaf sumac is the leaf of Anacardiaceae lacquer tree platymiscium lacquer tree, and leaf sumac can be used as medicine, and sees ancient prescription " leaf sumac blueness is glutinous to be dissipated " earliest,
Compendium of Material Medica carry its warm-natured acrid flavour, it is slightly poisonous, cure mainly five corpse labor diseases, desinsection.It is few common medicine in Traditional Chinese Medicine, but
Lacquer tree producing region and Popular Utilization are extensive, and truly have curative effect.Modern science studies have shown that the effect of leaf sumac it is very important, currently,
There are many report in terms of lacquer tree afforestation, raw lacquer production, the application study of laccol laccase class compound, but answer leaf sumac in lacquer tree
Research report with rare research and report, in terms of rarely seen minority botany and pharmacognosy.
By literature search, for yet there are no with lacquer tree extract for the toothpaste of anti-inflammation and sterilization or its additive
Document report.
Toothpaste of the present invention containing lacquer tree leaf extract, in the lacquer tree leaf extract containing lacquer tree leaf or its
Extract.
Folium toxicodendri verniciflni of the present invention is mainly great Ye paint, small lacquer tree, sharp leaf Folium toxicodendri verniciflni.
Toothpaste of the present invention containing lacquer tree leaf extract includes following ingredients as unit of parts by weight: lacquer tree
10~25 parts of leaf extract, 1~3 part of paris polyphylla extract, 8~10 parts of glycerol, 8~10 parts of sorbierite, laruyl alcohol sodium sulfovinate 2
~5 parts, 1~3 part of xylitol, 1~3 part of sodium cellulose glycolate, 1~2 part of sodium dihydrogen phosphate, two water object 10~20 of calcium monohydrogen phosphate
Part, 3~8 parts of orange oil, 3~6 parts of polyethylene glycol 400,8~15 parts of hydrated silica, 0.2~0.5 part of essence, deionized water 60~
90 parts.
The extract extracting method of Folium toxicodendri verniciflni of the present invention, can be used Conventional solvents extraction method, ultrasonic extraction,
Supercritical extract and subcritical abstraction method.
Toothpaste of the present invention containing lacquer tree leaf extract, used Extraction solvent be n-butanol, ethyl acetate,
Water, ethyl alcohol, acetone, liquid carbon dioxide, dimethyl ether, propane, butane.
The extract of Folium toxicodendri verniciflni of the present invention can be one or more Folium toxicodendri verniciflnis.
The extract extracting method of Folium toxicodendri verniciflni of the present invention can be used and crush, extract after mixing various Folium toxicodendri verniciflnis.
Paris polyphylla method for preparing extractive of the present invention, comprising the following steps:
(1) paris polyphylla is placed in drying box with clear water washes clean and is dried to moisture < 5%, drying temperature is set
It is 80~90 DEG C；
(2) paris polyphylla after drying is crushed, is then transferred in grinder again and is pulverized to obtain paris polyphylla fine powder,
Fineness is > 100 mesh, spare；
(3) clear water will be added in resulting paris polyphylla fine powder, and complex enzyme is added thereto, be warming up to 25~35 DEG C, and constantly
Stirring, speed of agitator are 300~500r/min, and soaking time is 80~120min, and mixed component is obtained after immersion；
(4) a certain amount of sodium chloride is added into mixed component, the additional amount of sodium chloride is the 10~15% of mixed component quality,
80~100 DEG C are warming up to after being uniformly mixed, and simultaneously be stirred by ultrasonic 40~60min, after stirring keep the temperature 30~
50min；
(5) processing is filtered to the resulting mixed component of step 4), discards filter residue, retain filtrate；
(6) filtrate obtained in step 5) is mixed evenly with carclazyte, the mass ratio of carclazyte and filtrate is 1:2~3, then
It is filtered by mixture of the Suction filtration device to resulting carclazyte and filtrate, the filtrate after being decolourized；
(7) filtrate after decolourizing obtained in step 6) is transferred in spray drying device, is spray-dried, obtained solid powder
End is paris polyphylla extract.
Complex enzyme is cellulase and pectase in heretofore described paris polyphylla method for preparing extractive step 3)
Equal mass mixings object.The enzymolysis efficiency of cellulase and pectase is high, can digest the cell wall of paris polyphylla fine powder.
Heretofore described paris polyphylla extract not only have treatment because periodontitis cause various focusing depths represented, swelling it is medicinal
Effect, but also have the function of antibacterial bacteriostatic.
Heretofore described orange oil can effectively treat canker sore or gum maintenance health care.
The heretofore described toothpaste containing lacquer tree leaf extract, does not occur also in the market at present.
The present invention provides the toothpaste containing lacquer tree leaf extract, further enriches for the prior art and product
Folium toxicodendri verniciflni is processed as a kind of high value-added product, extends paint by the diversity of existing antibacterial anti-inflammatory product or its additive
The industrial chain of tree.
Compared with prior art, technological merit of the invention is:
(1) toothpaste of the invention containing lacquer tree leaf extract is Folium toxicodendri verniciflni comprehensive utilization technique, as a kind of novel, natural
Antibacterial substance.
(2) toothpaste of the invention containing lacquer tree leaf extract is because itself there is strong antibiotic property that can effectively improve guaranteeing the quality for toothpaste
Time limit.
(3) there is apparent fungistatic effect containing lacquer tree leaf extract in the present invention, can also inhibits to generate in toothpaste thin
Bacterium reduces the dosage of preservative in toothpaste.
(4) toothpaste containing lacquer tree leaf extract, which is used for a long time, to be had treatment periodontitis, reduces plaque, keeps breath freshening
And other effects.
(5) product of the invention improves the lacquer tree output value, expands lacquer tree industrial chain, improves the economic effect of plantation lacquer tree
Benefit.
(6) paris polyphylla extract of the invention not only has treatment because periodontitis causes the medicinal function of various focusing depths represented, swelling
Effect, but also have the function of antibacterial bacteriostatic.
(7) orange oil of the invention can effectively treat canker sore or gum maintenance health care.
The present invention will be described in detail based on the embodiment of the present invention below, but the present invention is not limited to this.
Specific embodiment
Embodiment 1
Toothpaste containing lacquer tree leaf extract described in the present embodiment includes following ingredients as unit of parts by weight: Folium toxicodendri verniciflni
10 parts of extract, 1 part of paris polyphylla extract, 8 parts of glycerol, 8 parts of sorbierite, 2 parts of laruyl alcohol sodium sulfovinate, 1 part of xylitol, hydroxyl first
1 part of base sodium cellulosate, 1 part of sodium dihydrogen phosphate, 10 parts of two water object of calcium monohydrogen phosphate, 3 parts of orange oil, 3 parts of polyethylene glycol 400, hydration silicon
8 parts of stone, 0.2 part of essence, 60 parts of deionized water.
The toothpaste that the present embodiment contains lacquer tree leaf extract can be prepared completely using the conventional method of this field.Specifically
, the preparation step that the present embodiment contains the toothpaste of lacquer tree leaf extract is as follows:
(1) it picks lacquer tree leaf and is cleaned with clear water；
(2) Folium toxicodendri verniciflni that surface moisture is air-dried after cleaning is crushed to 0.1~1mm；
(3) paris polyphylla extract, glycerol, sorbierite, laruyl alcohol sulfuric acid will be added in the Folium toxicodendri verniciflni crushed material obtained in step (2)
Ester sodium, xylitol, sodium cellulose glycolate, sodium dihydrogen phosphate, two water object of calcium monohydrogen phosphate, orange oil, polyethylene glycol 400, hydration silicon
Stone, essence, deionized water.It stirs 20min to mix, homogeneous can obtain the toothpaste containing lacquer tree leaf extract after crossing colloid mill.
Embodiment 2
Toothpaste containing lacquer tree leaf extract described in the present embodiment includes following ingredients as unit of parts by weight: Folium toxicodendri verniciflni
25 parts of extract, 3 parts of paris polyphylla extract, 10 parts of glycerol, 10 parts of sorbierite, 5 parts of laruyl alcohol sodium sulfovinate, 3 parts of xylitol, hydroxyl
3 parts of sodium carboxymethylcellulose pyce, 2 parts of sodium dihydrogen phosphate, 20 parts of two water object of calcium monohydrogen phosphate, 8 parts of orange oil, 6 parts of polyethylene glycol 400, hydration
15 parts of silica, 0.5 part of essence, 90 parts of deionized water.
The toothpaste that the present embodiment contains lacquer tree leaf extract can be prepared completely using the conventional method of this field.Specifically
, the preparation step that the present embodiment contains the toothpaste of lacquer tree leaf extract is as follows:
(1) it picks lacquer tree leaf and is cleaned with clear water；
(2) Folium toxicodendri verniciflni after cleaning is cut into pieces, is then extracted again, extraction process is the ratio for being 1:8 by g:g solid-to-liquid ratio
Water is added in example, and 60min is stirred at 45 DEG C, 100r/min and is extracted twice, filtering and merging filtrate after extraction, for use；
(3) paris polyphylla extract, glycerol, sorbierite, laruyl alcohol sulfuric acid is added in the lacquer tree leaf extract obtained in step (2)
Ester sodium, xylitol, sodium cellulose glycolate, sodium dihydrogen phosphate, two water object of calcium monohydrogen phosphate, orange oil, polyethylene glycol 400, hydration silicon
Stone, essence, deionized water.It stirs 40min to mix, homogeneous can obtain the toothpaste for containing lacquer tree leaf extract after crossing colloid mill.
Embodiment 3
Toothpaste containing lacquer tree leaf extract described in the present embodiment includes following ingredients as unit of parts by weight: Folium toxicodendri verniciflni
15 parts of extract, 2 parts of paris polyphylla extract, 8 parts of glycerol, 8 parts of sorbierite, 3 parts of laruyl alcohol sodium sulfovinate, 2 parts of xylitol, hydroxyl first
2 parts of base sodium cellulosate, 1 part of sodium dihydrogen phosphate, 15 parts of two water object of calcium monohydrogen phosphate, 5 parts of orange oil, 5 parts of polyethylene glycol 400, hydration silicon
10 parts of stone, 0.3 part of essence, 70 parts of deionized water.
The toothpaste that the present embodiment contains lacquer tree leaf extract can be prepared completely using the conventional method of this field.Specifically
, the preparation step that the present embodiment contains the toothpaste of lacquer tree leaf extract is as follows:
(1) lacquer tree tender shoots and leaf are picked and is cleaned with clear water；
(2) Folium toxicodendri verniciflni after cleaning is cut into pieces, then carries out supercritical CO again2Extraction extraction, extraction process are extraction
35 DEG C of kettle temperature degree, pressure 12MPa, I pressure of separating still, 5. 0 MPa, separating still II pressure 4.6MPa, 40 DEG C of separation temperature,
CO210 L h of gas flow-1, 1. 5 h of extraction time can be obtained the lacquer tree leaf extract；
(3) paris polyphylla extract, glycerol, sorbierite, laruyl alcohol sulfuric acid is added in the lacquer tree leaf extract obtained in step (2)
Ester sodium, xylitol, sodium cellulose glycolate, sodium dihydrogen phosphate, two water object of calcium monohydrogen phosphate, orange oil, polyethylene glycol 400, hydration silicon
Stone, essence, deionized water.It stirs 40min to mix, homogeneous can be obtained the tooth for containing lacquer tree leaf extract after crossing colloid mill
Cream.
Embodiment 4
Toothpaste containing lacquer tree leaf extract described in the present embodiment includes following ingredients as unit of parts by weight: Folium toxicodendri verniciflni
15 parts of extract, 2 parts of paris polyphylla extract, 10 parts of glycerol, 10 parts of sorbierite, 4 parts of laruyl alcohol sodium sulfovinate, 2 parts of xylitol, hydroxyl
1 part of sodium carboxymethylcellulose pyce, 2 parts of sodium dihydrogen phosphate, 12 parts of two water object of calcium monohydrogen phosphate, 4 parts of orange oil, 5 parts of polyethylene glycol 400, hydration
12 parts of silica, 0.2 part of essence, 70 parts of deionized water.
The toothpaste that the present embodiment contains lacquer tree leaf extract can be prepared completely using the conventional method of this field.Specifically
, the preparation step that the present embodiment contains the toothpaste of lacquer tree leaf extract is as follows:
(1) it picks lacquer tree tender shoots and is cleaned with clear water；
(2) Folium toxicodendri verniciflni after cleaning is crushed to 20~50 mesh, then carries out subcritical abstraction method extraction, extractant 4 again
Number solvent naphtha, main component are liquefied propane, butane.Extraction process is 0. 5 h of extraction time, is extracted 2 times, extractor adds
Temperature is to 45 DEG C, and for pressure in 0.4 MPa, raw material and solvent ratios are that (g:ml) 1:12 can be obtained this after extraction finishes separation
Lacquer tree leaf extract.
(3) paris polyphylla extract, glycerol, sorbierite, laruyl alcohol is added in the lacquer tree leaf extract obtained in step (2)
Sodium sulfovinate, xylitol, sodium cellulose glycolate, sodium dihydrogen phosphate, two water object of calcium monohydrogen phosphate, orange oil, polyethylene glycol 400, water
Close silica, essence, deionized water.It stirs 40min to mix, can be obtained this after homogeneous, mistake colloid mill and contain lacquer tree leaf extract
Toothpaste.
Embodiment 5
Toothpaste containing lacquer tree leaf extract described in the present embodiment includes following ingredients as unit of parts by weight: Folium toxicodendri verniciflni
18 parts of extract, 3 parts of paris polyphylla extract, 8 parts of glycerol, 8 parts of sorbierite, 3 parts of laruyl alcohol sodium sulfovinate, 1 part of xylitol, hydroxyl first
1 part of base sodium cellulosate, 1 part of sodium dihydrogen phosphate, 12 parts of two water object of calcium monohydrogen phosphate, 6 parts of orange oil, 4 parts of polyethylene glycol 400, hydration silicon
11 parts of stone, 65 parts of deionized water.
The toothpaste that the present embodiment contains lacquer tree leaf extract can be prepared completely using the conventional method of this field.Specifically
, the preparation step that the present embodiment contains the toothpaste of lacquer tree leaf extract is as follows:
(1) it picks lacquer tree leaf and is cleaned with clear water；
(2) Folium toxicodendri verniciflni after cleaning is crushed to 20~50 mesh, then carries out subcritical abstraction method extraction, extractant two again
Methyl ether.Extraction process is that smashed Folium toxicodendri verniciflni is fitted into extraction kettle, the air in starting vacuum pump abstraction extraction kettle, will be molten
Agent dimethyl ether presses Folium toxicodendri verniciflni: solvent=1: 15 weight ratio is added in Folium toxicodendri verniciflni, is 50 DEG C in temperature, pressure is 0.45MPa's
Under process conditions, continuous to extract three times, then each extraction time 30min isolates extract again；
(3) the lacquer tree leaf extract obtained in step (2) takes middle addition paris polyphylla extract, glycerol, sorbierite, laruyl alcohol sulphur
Acid esters sodium, xylitol, sodium cellulose glycolate, sodium dihydrogen phosphate, two water object of calcium monohydrogen phosphate, orange oil, polyethylene glycol 400, hydration
Silica, deionized water, stirring 30min are mixed, and homogeneous can obtain the toothpaste for containing lacquer tree leaf extract after crossing colloid mill.
Paris polyphylla method for preparing extractive in above-described embodiment, comprising the following steps:
(1) paris polyphylla is placed in drying box with clear water washes clean and is dried to moisture content < 5%, drying temperature is set
It is 85 DEG C；
(2) paris polyphylla after drying is crushed, is then transferred in grinder again and is pulverized to obtain paris polyphylla fine powder,
Fineness is > 100 mesh, spare；
(3) clear water will be added in resulting paris polyphylla fine powder, and complex enzyme is added thereto, be warming up to 30 DEG C, and be stirred continuously,
Speed of agitator is 400r/min, soaking time 100min, and mixed component is obtained after immersion；
(4) a certain amount of sodium chloride is added into mixed component, the additional amount of sodium chloride is the 10% of mixed component quality, stirring
It is warming up to 80 DEG C after mixing, and 40min is stirred by ultrasonic simultaneously, 30min is kept the temperature after stirring；
(5) processing is filtered to the resulting mixed component of step 4), discards filter residue, retain filtrate；
(6) filtrate obtained in step 5) is mixed evenly with carclazyte, the mass ratio of carclazyte and filtrate is 1:2, is then led to
It crosses Suction filtration device to filter the mixture of resulting carclazyte and filtrate, the filtrate after being decolourized；
(7) filtrate after decolourizing obtained in step 6) is transferred in spray drying device, is spray-dried, obtained solid powder
End is paris polyphylla extract.
Claims (6)
1. the toothpaste containing lacquer tree leaf extract, which is characterized in that the lacquer tree leaf extract is great Ye lacquer tree, small lacquer tree, point
Leaf lacquer tree leaf extract.
2. the toothpaste containing lacquer tree leaf extract, which is characterized in that include following ingredients as unit of parts by weight: Folium toxicodendri verniciflni
10~25 parts of extract, 1~3 part of paris polyphylla extract, 8~10 parts of glycerol, 8~10 parts of sorbierite, laruyl alcohol sodium sulfovinate 2~
5 parts, 1~3 part of xylitol, 1~3 part of sodium cellulose glycolate, 1~2 part of sodium dihydrogen phosphate, two water object 10~20 of calcium monohydrogen phosphate
Part, 3~8 parts of orange oil, 3~6 parts of polyethylene glycol 400,8~15 parts of hydrated silica, 0.2~0.5 part of essence, deionized water 60~
90 parts.
3. the toothpaste according to claim 2 containing lacquer tree leaf extract, which is characterized in that the lacquer tree leaf extract
Conventional solvents extraction method, ultrasonic extraction, supercritical extract and subcritical abstraction method can be used in extracting method.
4. the toothpaste according to claim 3 containing lacquer tree leaf extract, which is characterized in that used Extraction solvent is positive
Butanol, ethyl acetate, water, ethyl alcohol, acetone, liquid carbon dioxide, dimethyl ether, propane, butane.
5. the toothpaste according to claim 2 containing lacquer tree leaf extract, which is characterized in that the paris polyphylla extract system
Preparation Method, comprising the following steps:
(1) paris polyphylla is placed in drying box with clear water washes clean and is dried to moisture < 5%, drying temperature is set
It is 80~90 DEG C；
(2) paris polyphylla after drying is crushed, is then transferred in grinder again and is pulverized to obtain paris polyphylla fine powder,
Fineness is > 100 mesh, spare；
(3) clear water will be added in resulting paris polyphylla fine powder, and complex enzyme is added thereto, be warming up to 25~35 DEG C, and constantly
Stirring, speed of agitator are 300~500r/min, and soaking time is 80~120min, and mixed component is obtained after immersion；
(4) a certain amount of sodium chloride is added into mixed component, the additional amount of sodium chloride is the 10~15% of mixed component quality,
80~100 DEG C are warming up to after being uniformly mixed, and simultaneously be stirred by ultrasonic 40~60min, after stirring keep the temperature 30~
50min；
(5) processing is filtered to the resulting mixed component of step 4), discards filter residue, retain filtrate；
(6) filtrate obtained in step 5) is mixed evenly with carclazyte, the mass ratio of carclazyte and filtrate is 1:2~3, then
It is filtered by mixture of the Suction filtration device to resulting carclazyte and filtrate, the filtrate after being decolourized；
(7) filtrate after decolourizing obtained in step 6) is transferred in spray drying device, is spray-dried, obtained solid powder
End is paris polyphylla extract.
6. the toothpaste according to claim 5 containing lacquer tree leaf extract, which is characterized in that complex enzyme in the step 3)
For the equal mass mixings object of cellulase and pectase.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115969025A (en) * | 2022-12-28 | 2023-04-18 | 祝雪良 | Compound polysaccharide seasoning for improving freshness |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1183036A (en) * | 1995-03-10 | 1998-05-27 | 卫材株式会社 | Dentifrice composition |
| KR20120112929A (en) * | 2011-04-04 | 2012-10-12 | (주)에스에이치제약 | Oral composition comprising rhus verniciflua extracts and hinokitiol |
| CN108531318A (en) * | 2018-07-21 | 2018-09-14 | 安溪县凤城建金产品外观设计服务中心 | A kind of preparation process of the soap containing paris polyphylla extract |
-
2019
- 2019-03-04 CN CN201910161866.3A patent/CN109730955A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1183036A (en) * | 1995-03-10 | 1998-05-27 | 卫材株式会社 | Dentifrice composition |
| KR20120112929A (en) * | 2011-04-04 | 2012-10-12 | (주)에스에이치제약 | Oral composition comprising rhus verniciflua extracts and hinokitiol |
| CN108531318A (en) * | 2018-07-21 | 2018-09-14 | 安溪县凤城建金产品外观设计服务中心 | A kind of preparation process of the soap containing paris polyphylla extract |
Non-Patent Citations (3)
| Title |
|---|
| MATHEW ATTOKARAN: "橙油", 《天然食用香料与色素》 * |
| 徐洁: "滇重楼", 《芳香植物研究与应用》 * |
| 陈虹霞: "漆树黄酮提取物的化学特征及生物活性研究", 《中国博士学位论文全文数据库工程科技Ⅰ辑》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115969025A (en) * | 2022-12-28 | 2023-04-18 | 祝雪良 | Compound polysaccharide seasoning for improving freshness |
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Application publication date: 20190510 |