CN108531318A - A kind of preparation process of the soap containing paris polyphylla extract - Google Patents
A kind of preparation process of the soap containing paris polyphylla extract Download PDFInfo
- Publication number
- CN108531318A CN108531318A CN201810807711.8A CN201810807711A CN108531318A CN 108531318 A CN108531318 A CN 108531318A CN 201810807711 A CN201810807711 A CN 201810807711A CN 108531318 A CN108531318 A CN 108531318A
- Authority
- CN
- China
- Prior art keywords
- paris polyphylla
- soap
- blending ingredients
- gained
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Animal Behavior & Ethology (AREA)
- Medicinal Chemistry (AREA)
- Veterinary Medicine (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- General Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Dermatology (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Epidemiology (AREA)
- Pain & Pain Management (AREA)
- Rheumatology (AREA)
- Communicable Diseases (AREA)
- Oncology (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to soap preparing technical fields, and in particular to a kind of preparation process of the soap containing paris polyphylla extract；The paris polyphylla extract contained in soap not only has the medicinal efficacy for the treatment of carbuncle swells, but also has the function of antibacterial bacteriostatic.By the way that cellulase and pectase are added into the solution containing paris polyphylla fine powder, and temperature is set as 27 35 DEG C；The cell wall of paris polyphylla fine powder can be digested, obtain blending ingredients by the enzymolysis efficiency higher of cellulase and pectase under the conditions of this；Then a certain amount of sodium chloride is added into blending ingredients, and is stirred by ultrasonic simultaneously；Wherein sodium chloride can increase the membrane passage of the paris polyphylla cell after enzymolysis, so that the intracellular active ingredient of paris polyphylla fully flows out, the outflow for the active ingredient that paris polyphylla can be accelerated intracellular is stirred by ultrasonic, so that the active ingredient of paris polyphylla is flow in soap to greatest extent, enhance soap treatment malignant boil swell carbuncle swells, anti-inflammatory and antibacterial bacteriostatic the effect of.
Description
Technical field
The present invention relates to soap preparing technical fields, and in particular to a kind of preparation work of the soap containing paris polyphylla extract
Skill.
Background technology
Soap is the general name of fatty acid metal salts.General formula is RCOOM, and RCOO is fatty acid radical in formula, and M is metal ion.
Aliphatic acid carbon number in daily soap is generally 10-18, and metal is mainly the alkali metal such as sodium or potassium, also useful ammonia and certain organic
Specific use soap is made in alkali such as ethanol amine, triethanolamine etc..Broadly, grease, wax, rosin or aliphatic acid etc. and bases rise
Fatty acid salt obtained by saponification or neutralization reaction, all can be described as soap.Soap can be dissolved in water, there is washing decontamination.Soap
It is all kinds of to have perfumed soap, also known as wash one's hands and face soap, metallic soap and compound soap.Soap is the general name of fatty acid metal salts, the fat in daily soap
Fat acid carbon number is generally 10-18, and metal is mainly the alkali metal such as sodium or potassium, also useful ammonia and certain organic bases such as ethanol amine, three
Specific use soap is made in ethanol amine etc..Soap includes laundry soap, perfumed soap, metallic soap, liquid soap, also Related product fat
Acid, fixed oil, glycerine etc..The ingredient of soap：The sodium salt R-CO2Na of carboxylic acid, it is synthetic dyestuff, synthetic perfume, preservative, anti-oxidant
Agent, foaming agent, curing agent, adhesion agent, synthesis interfacial agent.The main component R-CO2Na of soap, wherein R group are usually
Different, it is various alkyl.R- is hydrophobic group, and carboxyl is hydrophilic group.
Soap has many uses, and other than the familiar clothes that are used for doing washing, is also widely used for textile industry.Usually
It is with the most use with the sodium salt of higher fatty acids, generally referred to as hard soap；Its sylvite is called green soap, is chiefly used in hair washing and shaves.
Its ammonium salt is then commonly used to make toilet cream.According to the ingredient of soap, consider from fatty acid part, the big aliphatic acid of saturation degree is made
The soap obtained is harder；Conversely, the soap obtained by the larger aliphatic acid of degree of unsaturation is relatively soft.The primary raw material of soap is molten
The higher grease of point.
A kind of soap preparation method is provided in the patent document application No. is CN201711452016.6.It includes following
Step：In 150ml beakers, the alcohol of 6 grams of lard and 5ml95% is contained, then adds the NaOH solution of 10ml40%, is stirred with glass rod
It mixes；Beaker is placed on asbestos gauge, is heated with small fire, and is constantly held in both hands and is stirred with glass；Stick takes out a few drop samples and is put into test tube,
Distilled water 5-6ml is added in test tube, heating oscillation when standing, has grease to separate, illustrates that saponification is incomplete, can be added dropwise lye after
Continuous saponification；The distilled water of 20ml heat is slowly added in the complete viscous fluid of saponification, stirring makes them dissolve each other, then that this is sticky
Liquid slowly pours into the saturated common salt solution for containing 150ml heat, stirring while adding, and after standing, soap is just saltoutd floating, waits for soap
It is all precipitated, can be taken out with glass rod after solidification, soap is made.
Although soap prepared by above-mentioned patent document has many advantages, such as that alkalinity is weak, irritation is not strong and use scope is wide,
It is that it does not have the medicinal efficacy for the treatment of carbuncle swells and antibacterial bacteriostatic, is based on such situation, a kind of fertilizer with medicinal efficacy is provided
Soap becomes this field urgent problem to be solved！
Invention content
In view of the deficiencies of the prior art, the present invention provides a kind of preparation process of the soap containing paris polyphylla extract,
For solving the technical issues of background technology is proposed.
The present invention is achieved by the following technical programs：
A kind of preparation process of the soap containing paris polyphylla extract, includes the following steps：
(1) preparation of paris polyphylla extract：
A, by paris polyphylla clear water washes clean, then a certain amount of paris polyphylla of precise, spare；
B, the paris polyphylla of washes clean is placed in drying box and processing is dried, drying temperature is set as 80-90 DEG C；
C, the paris polyphylla after drying is transferred in pulverizer and is crushed, be then transferred in grinder again and be ground into powder
Paris polyphylla fine powder is obtained, is saved backup；
D, the paris polyphylla fine powder of gained is transferred in clear water, and complex enzyme is added thereto, be warming up to 27-35 DEG C, not
Disconnected stirring, soaking time 90-120min, gained are denoted as blending ingredients；
E, and then into blending ingredients a certain amount of sodium chloride is added, is warming up to 80-100 DEG C after being uniformly mixed, and
40-60min is stirred by ultrasonic simultaneously；30-50min is kept the temperature after stirring；
F, processing is filtered to the blending ingredients obtained by step e, discards filter residue, retain filtrate；
G, the filtrate of gained in step f is mixed evenly with carclazyte, then the carclazyte as Suction filtration device to obtained by
It is filtered with the mixture of filtrate, the filtrate after being decolourized；
H, the filtrate after the decoloration of gained in step g is transferred in spray drying device, is spray-dried, obtained solid
Powder is paris polyphylla extract；
(2) preparation of the soap containing paris polyphylla extract：
S1：40-55 points of soap fat is accurately weighed according to mass percent, and is heated to thawing and stirs, and gained is denoted as
Blending ingredients A；
S2：3.4-4.6 parts of organic base, 5-8 parts of deionized water and paris polyphylla extract 0.8- are added into blending ingredients A
After 1.4 parts are mixed, blending ingredients B is obtained, blending ingredients B is transferred in ultrasonic agitation machine and is stirred by ultrasonic, is set to soap lye
At thick；
S3：The thick soap lye of gained in step S2 is squeezed into vacuum drying cabinet, then through squeezing, cutting into neat soap,
The soap finished product containing paris polyphylla extract is made through molding, stripping and slicing again.
Preferably, it is 4-6% that paris polyphylla, which is dried to moisture, in the step a.
Preferably, the fineness of paris polyphylla fine powder is 100-200 mesh in the step c.
Preferably, complex enzyme is formed by mass mixings such as cellulase and pectases in the step d.
Preferably, in the step e sodium chloride addition be blending ingredients quality 10-16%.
Preferably, carclazyte and the mass ratio of filtrate are 1 in the step g:2-3.
Preferably, the mixing speed in the step S1 is 450-650r/min.
Beneficial effects of the present invention are：
The present invention provides a kind of preparation process of the soap containing paris polyphylla extract, the paris polyphylla contained in soap carries
Taking object not only has the medicinal efficacy for the treatment of carbuncle swells, but also has the function of antibacterial bacteriostatic.By to containing paris polyphylla fine powder
Solution in cellulase and pectase is added, and temperature is set as 27-35 DEG C；The enzyme of cellulase and pectase under the conditions of this
It solves more efficient, the cell wall of paris polyphylla fine powder can be digested, obtain blending ingredients.Then it is added into blending ingredients a certain amount of
Sodium chloride, and be stirred by ultrasonic simultaneously.Wherein sodium chloride can increase the membrane passage of the paris polyphylla cell after enzymolysis, make
It obtains the intracellular active ingredient of paris polyphylla fully to flow out, the outflow for the active ingredient that paris polyphylla can be accelerated intracellular is stirred by ultrasonic,
So that the active ingredient of paris polyphylla is flow in soap to greatest extent, enhance the swollen carbuncle swells for the treatment of malignant boil, the suppression of anti-inflammatory and antibacterial of soap
The effect of bacterium.Bacterium is decreased the phenomenon that soap surface is grown simultaneously, protects the cleaning on soap surface.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, shall fall within the protection scope of the present invention.
Embodiment 1：
A kind of preparation process of the soap containing paris polyphylla extract, includes the following steps：
(1) preparation of paris polyphylla extract：
A, by paris polyphylla clear water washes clean, then a certain amount of paris polyphylla of precise, spare；
B, the paris polyphylla of washes clean is placed in drying box and processing is dried, drying temperature is set as 80 DEG C；
C, the paris polyphylla after drying is transferred in pulverizer and is crushed, be then transferred in grinder again and be ground into powder
Paris polyphylla fine powder is obtained, is saved backup；
D, the paris polyphylla fine powder of gained is transferred in clear water, and complex enzyme is added thereto, be warming up to 27 DEG C, and constantly stir
It mixes, soaking time 90min, gained is denoted as blending ingredients；
E, and then into blending ingredients a certain amount of sodium chloride is added, 80 DEG C are warming up to after being uniformly mixed, and simultaneously
40min is stirred by ultrasonic；30min is kept the temperature after stirring；
F, processing is filtered to the blending ingredients obtained by step e, discards filter residue, retain filtrate；
G, the filtrate of gained in step f is mixed evenly with carclazyte, then the carclazyte as Suction filtration device to obtained by
It is filtered with the mixture of filtrate, the filtrate after being decolourized；
H, the filtrate after the decoloration of gained in step g is transferred in spray drying device, is spray-dried, obtained solid
Powder is paris polyphylla extract；
(2) preparation of the soap containing paris polyphylla extract：
S1：Soap fat 40 is accurately weighed according to mass percent to divide, and is heated to thawing and stirs, and gained is denoted as mixing
Component A；
S2：3.4 parts of organic base is added into blending ingredients A, 5 parts of deionized water and the 0.8 part of mixing of paris polyphylla extract are stirred
After mixing, blending ingredients B is obtained, blending ingredients B is transferred in ultrasonic agitation machine and is stirred by ultrasonic, is set to soap lye at thick；
S3：The thick soap lye of gained in step S2 is squeezed into vacuum drying cabinet, then through squeezing, cutting into neat soap,
The soap finished product containing paris polyphylla extract is made through molding, stripping and slicing again.
It is 4% that paris polyphylla, which is dried to moisture, in step a.
The fineness of paris polyphylla fine powder is 100 mesh in step c.
The addition of sodium chloride is the 10% of blending ingredients quality in step e.
Carclazyte and the mass ratio of filtrate are 1 in step g:2.
Mixing speed in step S1 is 450r/min.
Embodiment 2：
A kind of preparation process of the soap containing paris polyphylla extract, includes the following steps：
(1) preparation of paris polyphylla extract：
A, by paris polyphylla clear water washes clean, then a certain amount of paris polyphylla of precise, spare；
B, the paris polyphylla of washes clean is placed in drying box and processing is dried, drying temperature is set as 85 DEG C；
C, the paris polyphylla after drying is transferred in pulverizer and is crushed, be then transferred in grinder again and be ground into powder
Paris polyphylla fine powder is obtained, is saved backup；
D, the paris polyphylla fine powder of gained is transferred in clear water, and complex enzyme is added thereto, be warming up to 30 DEG C, and constantly stir
It mixes, soaking time 100min, gained is denoted as blending ingredients；
E, and then into blending ingredients a certain amount of sodium chloride is added, 85 DEG C are warming up to after being uniformly mixed, and simultaneously
45min is stirred by ultrasonic；35min is kept the temperature after stirring；
F, processing is filtered to the blending ingredients obtained by step e, discards filter residue, retain filtrate；
G, the filtrate of gained in step f is mixed evenly with carclazyte, then the carclazyte as Suction filtration device to obtained by
It is filtered with the mixture of filtrate, the filtrate after being decolourized；
H, the filtrate after the decoloration of gained in step g is transferred in spray drying device, is spray-dried, obtained solid
Powder is paris polyphylla extract；
(2) preparation of the soap containing paris polyphylla extract：
S1：Soap fat 45 is accurately weighed according to mass percent to divide, and is heated to thawing and stirs, and gained is denoted as mixing
Component A；
S2：3.8 parts of organic base is added into blending ingredients A, 6 parts of deionized water and the 1.0 parts of mixing of paris polyphylla extract are stirred
After mixing, blending ingredients B is obtained, blending ingredients B is transferred in ultrasonic agitation machine and is stirred by ultrasonic, is set to soap lye at thick；
S3：The thick soap lye of gained in step S2 is squeezed into vacuum drying cabinet, then through squeezing, cutting into neat soap,
The soap finished product containing paris polyphylla extract is made through molding, stripping and slicing again.
It is 4.5% that paris polyphylla, which is dried to moisture, in step a.
The fineness of paris polyphylla fine powder is 150 mesh in step c.
The addition of sodium chloride is the 12% of blending ingredients quality in step e.
Carclazyte and the mass ratio of filtrate are 1 in step g:2.5.
Mixing speed in step S1 is 500r/min.
Embodiment 3：
A kind of preparation process of the soap containing paris polyphylla extract, includes the following steps：
(1) preparation of paris polyphylla extract：
A, by paris polyphylla clear water washes clean, then a certain amount of paris polyphylla of precise, spare；
B, the paris polyphylla of washes clean is placed in drying box and processing is dried, drying temperature is set as 88 DEG C；
C, the paris polyphylla after drying is transferred in pulverizer and is crushed, be then transferred in grinder again and be ground into powder
Paris polyphylla fine powder is obtained, is saved backup；
D, the paris polyphylla fine powder of gained is transferred in clear water, and complex enzyme is added thereto, be warming up to 32 DEG C, and constantly stir
It mixes, soaking time 110min, gained is denoted as blending ingredients；
E, and then into blending ingredients a certain amount of sodium chloride is added, 95 DEG C are warming up to after being uniformly mixed, and simultaneously
55min is stirred by ultrasonic；45min is kept the temperature after stirring；
F, processing is filtered to the blending ingredients obtained by step e, discards filter residue, retain filtrate；
G, the filtrate of gained in step f is mixed evenly with carclazyte, then the carclazyte as Suction filtration device to obtained by
It is filtered with the mixture of filtrate, the filtrate after being decolourized；
H, the filtrate after the decoloration of gained in step g is transferred in spray drying device, is spray-dried, obtained solid
Powder is paris polyphylla extract；
(2) preparation of the soap containing paris polyphylla extract：
S1：Soap fat 50 is accurately weighed according to mass percent to divide, and is heated to thawing and stirs, and gained is denoted as mixing
Component A；
S2：4.2 parts of organic base is added into blending ingredients A, 7 parts of deionized water and the 1.2 parts of mixing of paris polyphylla extract are stirred
After mixing, blending ingredients B is obtained, blending ingredients B is transferred in ultrasonic agitation machine and is stirred by ultrasonic, is set to soap lye at thick；
S3：The thick soap lye of gained in step S2 is squeezed into vacuum drying cabinet, then through squeezing, cutting into neat soap,
The soap finished product containing paris polyphylla extract is made through molding, stripping and slicing again.
It is 5.5% that paris polyphylla, which is dried to moisture, in step a.
The fineness of paris polyphylla fine powder is 170 mesh in step c.
The addition of sodium chloride is the 14% of blending ingredients quality in step e.
Carclazyte and the mass ratio of filtrate are 1 in step g:2.8.
Mixing speed in step S1 is 550r/min.
Embodiment 4：
A kind of preparation process of the soap containing paris polyphylla extract, includes the following steps：
(1) preparation of paris polyphylla extract：
A, by paris polyphylla clear water washes clean, then a certain amount of paris polyphylla of precise, spare；
B, the paris polyphylla of washes clean is placed in drying box and processing is dried, drying temperature is set as 90 DEG C；
C, the paris polyphylla after drying is transferred in pulverizer and is crushed, be then transferred in grinder again and be ground into powder
Paris polyphylla fine powder is obtained, is saved backup；
D, the paris polyphylla fine powder of gained is transferred in clear water, and complex enzyme is added thereto, be warming up to 35 DEG C, and constantly stir
It mixes, soaking time 120min, gained is denoted as blending ingredients；
E, and then into blending ingredients a certain amount of sodium chloride is added, 100 DEG C are warming up to after being uniformly mixed, and simultaneously
60min is stirred by ultrasonic；50min is kept the temperature after stirring；
F, processing is filtered to the blending ingredients obtained by step e, discards filter residue, retain filtrate；
G, the filtrate of gained in step f is mixed evenly with carclazyte, then the carclazyte as Suction filtration device to obtained by
It is filtered with the mixture of filtrate, the filtrate after being decolourized；
H, the filtrate after the decoloration of gained in step g is transferred in spray drying device, is spray-dried, obtained solid
Powder is paris polyphylla extract；
(2) preparation of the soap containing paris polyphylla extract：
S1：Soap fat 55 is accurately weighed according to mass percent to divide, and is heated to thawing and stirs, and gained is denoted as mixing
Component A；
S2：4.6 parts of organic base is added into blending ingredients A, 8 parts of deionized water and the 1.4 parts of mixing of paris polyphylla extract are stirred
After mixing, blending ingredients B is obtained, blending ingredients B is transferred in ultrasonic agitation machine and is stirred by ultrasonic, is set to soap lye at thick；
S3：The thick soap lye of gained in step S2 is squeezed into vacuum drying cabinet, then through squeezing, cutting into neat soap,
The soap finished product containing paris polyphylla extract is made through molding, stripping and slicing again.
It is 6% that paris polyphylla, which is dried to moisture, in step a.
The fineness of paris polyphylla fine powder is 200 mesh in step c.
The addition of sodium chloride is the 16% of blending ingredients quality in step e.
Carclazyte and the mass ratio of filtrate are 1 in step g:3.
Mixing speed in step S1 is 650r/min.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, it will be understood by those of ordinary skill in the art that：It still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features；And these modification or
It replaces, the spirit and scope for various embodiments of the present invention technical solution that it does not separate the essence of the corresponding technical solution.
Claims (7)
1. a kind of preparation process of the soap containing paris polyphylla extract, which is characterized in that include the following steps：
(1) preparation of paris polyphylla extract：
A, by paris polyphylla clear water washes clean, then a certain amount of paris polyphylla of precise, spare；
B, the paris polyphylla of washes clean is placed in drying box and processing is dried, drying temperature is set as 80-90 DEG C；
C, the paris polyphylla after drying is transferred in pulverizer and is crushed, be then transferred to again in grinder and be ground into powder and obtain
Paris polyphylla fine powder, saves backup；
D, the paris polyphylla fine powder of gained is transferred in clear water, and complex enzyme is added thereto, be warming up to 27-35 DEG C, and constantly stir
It mixes, soaking time 90-120min, gained is denoted as blending ingredients；
E, and then into blending ingredients a certain amount of sodium chloride is added, 80-100 DEG C is warming up to after being uniformly mixed, and simultaneously
40-60min is stirred by ultrasonic；30-50min is kept the temperature after stirring；
F, processing is filtered to the blending ingredients obtained by step e, discards filter residue, retain filtrate；
G, the filtrate of gained in step f is mixed evenly with carclazyte, the then carclazyte as Suction filtration device to obtained by and filter
The mixture of liquid is filtered, the filtrate after being decolourized；
H, the filtrate after the decoloration of gained in step g is transferred in spray drying device, is spray-dried, obtained solid powder
As paris polyphylla extract；
(2) preparation of the soap containing paris polyphylla extract：
S1：40-55 points of soap fat is accurately weighed according to mass percent, and is heated to thawing and stirs, and gained is denoted as mixing
Component A；
S2：0.8-1.4 parts of 3.4-4.6 parts of organic base, 5-8 parts of deionized water and paris polyphylla extract are added into blending ingredients A
After mixing, blending ingredients B is obtained, blending ingredients B is transferred in ultrasonic agitation machine and is stirred by ultrasonic, is set to soap lye at sticky
Shape；
S3：The thick soap lye of gained in step S2 is squeezed into vacuum drying cabinet, then through squeezing, cut into neat soap, then is passed through
The soap finished product containing paris polyphylla extract is made in molding, stripping and slicing.
2. a kind of preparation process of the soap containing paris polyphylla extract according to claim 1, it is characterised in that：The step
It is 4-6% that paris polyphylla, which is dried to moisture, in rapid a.
3. a kind of preparation process of the soap containing paris polyphylla extract according to claim 1, it is characterised in that：The step
The fineness of paris polyphylla fine powder is 100-200 mesh in rapid c.
4. a kind of preparation process of the soap containing paris polyphylla extract according to claim 1, it is characterised in that：The step
Complex enzyme is formed by mass mixings such as cellulase and pectases in rapid d.
5. a kind of preparation process of the soap containing paris polyphylla extract according to claim 1, it is characterised in that：The step
The addition of sodium chloride is the 10-16% of blending ingredients quality in rapid e.
6. a kind of preparation process of the soap containing paris polyphylla extract according to claim 1, it is characterised in that：The step
Carclazyte and the mass ratio of filtrate are 1 in rapid g:2-3.
7. a kind of preparation process of the soap containing paris polyphylla extract according to claim 1, it is characterised in that：The step
Mixing speed in rapid S1 is 450-650r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810807711.8A CN108531318A (en) | 2018-07-21 | 2018-07-21 | A kind of preparation process of the soap containing paris polyphylla extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810807711.8A CN108531318A (en) | 2018-07-21 | 2018-07-21 | A kind of preparation process of the soap containing paris polyphylla extract |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108531318A true CN108531318A (en) | 2018-09-14 |
Family
ID=63488101
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810807711.8A Pending CN108531318A (en) | 2018-07-21 | 2018-07-21 | A kind of preparation process of the soap containing paris polyphylla extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108531318A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109730955A (en) * | 2019-03-04 | 2019-05-10 | 王忠良 | Toothpaste containing lacquer tree leaf extract |
| CN112779104A (en) * | 2021-01-06 | 2021-05-11 | 中国科学院昆明植物研究所 | A soap solution and soap with antibacterial effect, and its preparation method |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1490413A (en) * | 2003-08-11 | 2004-04-21 | 云南白药集团天然药物研究院 | Method of leaching pairs polyphylla saponin |
| CN102234307A (en) * | 2011-05-06 | 2011-11-09 | 南京泽朗医药科技有限公司 | Method for extracting and separating pardifomoside from Lysimachia paridiformis |
| CN105219552A (en) * | 2015-09-08 | 2016-01-06 | 桂林盛兴电子科技有限公司 | A kind of herbal medicine whitening soap and preparation method thereof |
| CN105602768A (en) * | 2016-02-18 | 2016-05-25 | 李金明 | Prinsepia utilis royle soap and preparation method thereof |
| CN105963479A (en) * | 2016-06-17 | 2016-09-28 | 广州中大南沙科技创新产业园有限公司 | Method for extracting paris polyphylla saponin |
| CN107440992A (en) * | 2017-08-22 | 2017-12-08 | 安徽省中日农业环保科技有限公司 | A kind of preparation method of the anti-acne essence containing Rhizoma Paridis extract |
| CN107502488A (en) * | 2017-08-07 | 2017-12-22 | 上海纳米技术及应用国家工程研究中心有限公司 | Preparation method of antibiotic skin-care soap and products thereof |
-
2018
- 2018-07-21 CN CN201810807711.8A patent/CN108531318A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1490413A (en) * | 2003-08-11 | 2004-04-21 | 云南白药集团天然药物研究院 | Method of leaching pairs polyphylla saponin |
| CN102234307A (en) * | 2011-05-06 | 2011-11-09 | 南京泽朗医药科技有限公司 | Method for extracting and separating pardifomoside from Lysimachia paridiformis |
| CN105219552A (en) * | 2015-09-08 | 2016-01-06 | 桂林盛兴电子科技有限公司 | A kind of herbal medicine whitening soap and preparation method thereof |
| CN105602768A (en) * | 2016-02-18 | 2016-05-25 | 李金明 | Prinsepia utilis royle soap and preparation method thereof |
| CN105963479A (en) * | 2016-06-17 | 2016-09-28 | 广州中大南沙科技创新产业园有限公司 | Method for extracting paris polyphylla saponin |
| CN107502488A (en) * | 2017-08-07 | 2017-12-22 | 上海纳米技术及应用国家工程研究中心有限公司 | Preparation method of antibiotic skin-care soap and products thereof |
| CN107440992A (en) * | 2017-08-22 | 2017-12-08 | 安徽省中日农业环保科技有限公司 | A kind of preparation method of the anti-acne essence containing Rhizoma Paridis extract |
Non-Patent Citations (2)
| Title |
|---|
| 刘文英: "《植物逆境与基因》", 31 May 2015, 北京：北京理工大学出版社 * |
| 童立雷等: "酶法提取重楼中总皂苷工艺研究", 《农产品加工 学刊》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109730955A (en) * | 2019-03-04 | 2019-05-10 | 王忠良 | Toothpaste containing lacquer tree leaf extract |
| CN112779104A (en) * | 2021-01-06 | 2021-05-11 | 中国科学院昆明植物研究所 | A soap solution and soap with antibacterial effect, and its preparation method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101857824B (en) | Detergent using sodium alcohol ether carboxylate as main raw material | |
| CN106047539A (en) | Camellia seed handmade soap and preparation method thereof | |
| CN108531318A (en) | A kind of preparation process of the soap containing paris polyphylla extract | |
| CN106893644A (en) | A kind of Wax removal water and its application, preparation, paraffin removal method | |
| CN102399643B (en) | Efficient cleaning paste and preparation method thereof | |
| CN108822976A (en) | A kind of preparation method of the compound bio dish washing liquid containing paratoluenesulfonic acid sodium salt | |
| CN105012209A (en) | Marine fish oil bath lotion and preparation method thereof | |
| CN104312786A (en) | Natural botanical soap and preparation method thereof | |
| CN111073766A (en) | Underwear laundry detergent and preparation method thereof | |
| CN110016390A (en) | A kind of liquid detergent and preparation method thereof removing formaldehyde | |
| US2352021A (en) | Detergent composition | |
| CN106753866B (en) | A kind of laundry sheet and preparation method thereof that solubility property is good | |
| US6380153B1 (en) | Methods for producing surfactants with cellulose compositions | |
| CN109055034A (en) | Liquid detergent | |
| CN108277118A (en) | A kind of biomass-based surfactant and preparation method thereof containing trench oil extract | |
| CN108865494A (en) | A kind of highly-efficient glass cleaning agent and preparation method thereof | |
| CN110373286B (en) | Laundry soap powder and preparation method thereof | |
| CN108004066A (en) | It is a kind of suitable for soap of sensitiveness skin and preparation method thereof | |
| CN106520414A (en) | Method for production of natural green perfumed soap from tea saponin and beeswax | |
| CN112080354A (en) | Baby laundry detergent containing silver ion bacteriostatic agent and preparation method thereof | |
| CN105624709A (en) | Method for preparing environment-friendly composite metal cleaning agent based on waste vegetables | |
| CN110257198A (en) | A method of facial soap is prepared with natural sericin stoste | |
| CN110982645A (en) | Formula and production process of laundry soap solution | |
| CN104987958B (en) | For preparing the fatty alcohol of cleaning solution and the preparation method of the fatty alcohol | |
| CN101717701B (en) | Attapulgite kitchen oil stain cleaning cream |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180914 |
|
| WD01 | Invention patent application deemed withdrawn after publication |