CN108676626A - A kind of environmentally protective sterilizing liquid detergent and preparation method thereof - Google Patents

A kind of environmentally protective sterilizing liquid detergent and preparation method thereof Download PDF

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Publication number
CN108676626A
CN108676626A CN201810664455.1A CN201810664455A CN108676626A CN 108676626 A CN108676626 A CN 108676626A CN 201810664455 A CN201810664455 A CN 201810664455A CN 108676626 A CN108676626 A CN 108676626A
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Prior art keywords
parts
leaf
liquid detergent
preparation
extract
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CN201810664455.1A
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Chinese (zh)
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路培育
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Individual
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Priority to CN201810664455.1A priority Critical patent/CN108676626A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/04Carboxylic acids or salts thereof
    • C11D1/10Amino carboxylic acids; Imino carboxylic acids; Fatty acid condensates thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/042Acids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/26Organic compounds containing nitrogen
    • C11D3/33Amino carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3746Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776Heterocyclic compounds, e.g. lactam
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/384Animal products
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Zoology (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of environmentally protective sterilizing liquid detergents and preparation method thereof, liquid detergent component includes 20 30 parts of leaf of bamboo mulberry-leaf extract in parts by weight, 10 20 parts of peppermint extracting solution, nanometer removes 39 parts of emulsifier, 26 parts of coco-nut oil fatty acid glycine potassium, 4 10 parts of soapberry fruit bark extract, 5 12 parts of fish scale zymotic fluid, 13 parts of surfactant, 26 parts of amino-acid complex copper, 28 parts of Betagen Solution, 13 parts of nano-silver ionic particle, preparation method of the present invention is simple, liquid detergent obtained has effects that sterilizing, user's skin will not be damaged simultaneously, and device emission will not pollute water quality, soil, good environmental protection.

Description

A kind of environmentally protective sterilizing liquid detergent and preparation method thereof
Technical field
The present invention relates to liquid detergent preparing technical field, specially a kind of environmentally protective sterilizing liquid detergent and its preparation Method.
Background technology
Currently, the liquid detergent of liquid detergent especially disinfection in the market is to be added to chemosterilant conduct to kill mostly Microbial inoculum, these disinfectants have strong impulse to human skin, are easy to remain on clothes, be caused centainly to human body Injury.Today of natural green environmental protection is advocated, people increasingly wish to replace chemicals using natural fungicide.
Invention content
It is above-mentioned to solve the purpose of the present invention is to provide a kind of environmentally protective sterilizing liquid detergent and preparation method thereof The problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions:A kind of environmentally protective sterilizing liquid detergent, laundry Liquid component includes 20-30 parts of leaf of bamboo mulberry-leaf extract, 10-20 parts of peppermint extracting solution, nanometer in parts by weight except emulsifier 3-9 Part, 2-6 parts of coco-nut oil fatty acid glycine potassium, 4-10 parts of soapberry fruit bark extract, 5-12 parts of fish scale zymotic fluid, surface-active 1-3 parts of agent, 2-6 parts of amino-acid complex copper, 2-8 parts of Betagen Solution, 1-3 parts of nano-silver ionic particle.
Preferably, the preferred composition proportion of liquid detergent component include 25 parts of leaf of bamboo mulberry-leaf extract, 15 parts of peppermint extracting solution, Nanometer except 6 parts of emulsifier, 4 parts of coco-nut oil fatty acid glycine potassium, 7 parts of soapberry fruit bark extract, 9 parts of fish scale zymotic fluid, 2 parts of surfactant, 4 parts of amino-acid complex copper, 5 parts of Betagen Solution, 2 parts of nano-silver ionic particle.
Preferably, preparation method includes the following steps:
A, it by leaf of bamboo mulberry-leaf extract, peppermint extracting solution, soapberry fruit bark extract, fish scale zymotic fluid, is added after mixing It is stirred in agitator tank, rate is 30-80 revs/min, and time 5min obtains mixed liquor A;
B, by nanometer except emulsifier, coco-nut oil fatty acid glycine potassium, surfactant, amino-acid complex copper, poly- dimension Heating stirring in reaction kettle is added in ketone iodine solution after mixing, stir speed (S.S.) is 100-300 revs/min, stirs middle addition after 10min Mixed liquor A continues to stir 20min, obtains mixed liquid B;
C, nano-silver ionic particle is added in mixed liquid B, after being sufficiently mixed at normal temperatures, places 4h-8h to get to washing Clothing liquid.
Preferably, heating temperature is 45 DEG C -55 DEG C in the step B, heating time 5min-10min.
Compared with prior art, the beneficial effects of the invention are as follows:Preparation method of the present invention is simple, and liquid detergent obtained has Sterilizing effect, while user's skin will not be damaged, and also device emission will not pollute water quality, soil, good environmental protection; Wherein, leaf of bamboo mulberry-leaf extract, the soapberry fruit bark extract added in the present invention has shigella dysenteriae, Escherichia coli powerful Bactericidal effect;The Betagen Solution of addition can improve bactericidal and bacteriostatic effect;The nano-silver ionic particle added in the present invention It can effectively prevent liquid detergent from oxidation, denaturalization phenomenon occur, its holding time be extended, in addition, nano-silver ionic particle is same Sample has excellent sterilizing power.
Specific implementation mode
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field The every other embodiment that art personnel are obtained without making creative work belongs to the model that the present invention protects It encloses.
The present invention provides the following technical solutions:A kind of environmentally protective sterilizing liquid detergent, liquid detergent component is by weight Number includes 20-30 parts of leaf of bamboo mulberry-leaf extract, 10-20 parts of peppermint extracting solution, nanometer except 3-9 parts of emulsifier, coconut oil fat 2-6 parts of sour glycine potassium, 4-10 parts of soapberry fruit bark extract, 5-12 parts of fish scale zymotic fluid, 1-3 parts of surfactant, amino Sour complex copper 2-6 parts, 2-8 parts of Betagen Solution, 1-3 parts of nano-silver ionic particle.
Embodiment one:
Liquid detergent component includes 20 parts of leaf of bamboo mulberry-leaf extract, 10 part, nanometer oil removing breast of peppermint extracting solution in parts by weight 3 parts of agent, 2 parts of coco-nut oil fatty acid glycine potassium, 4 parts of soapberry fruit bark extract, 5 parts of fish scale zymotic fluid, surfactant 1 Part, 2 parts of amino-acid complex copper, 2 parts of Betagen Solution, 1 part of nano-silver ionic particle.
The preparation method of the present embodiment includes the following steps:
A, it by leaf of bamboo mulberry-leaf extract, peppermint extracting solution, soapberry fruit bark extract, fish scale zymotic fluid, is added after mixing It is stirred in agitator tank, rate is 30 revs/min, and time 5min obtains mixed liquor A;
B, by nanometer except emulsifier, coco-nut oil fatty acid glycine potassium, surfactant, amino-acid complex copper, poly- dimension Heating stirring in reaction kettle is added in ketone iodine solution after mixing, stir speed (S.S.) is 100 revs/min, stirs middle addition mixing after 10min Liquid A continues to stir 20min, obtains mixed liquid B;
C, nano-silver ionic particle is added in mixed liquid B, after being sufficiently mixed at normal temperatures, places 8h to get to laundry Liquid.
In the present embodiment, heating temperature is 45 DEG C in step B, heating time 5min.
Embodiment two:
Liquid detergent component includes 30 parts of leaf of bamboo mulberry-leaf extract, 20 part, nanometer oil removing breast of peppermint extracting solution in parts by weight 9 parts of agent, 6 parts of coco-nut oil fatty acid glycine potassium, 10 parts of soapberry fruit bark extract, 12 parts of fish scale zymotic fluid, surface-active 3 parts of agent, 6 parts of amino-acid complex copper, 8 parts of Betagen Solution, 3 parts of nano-silver ionic particle.
The preparation method of the present embodiment includes the following steps:
A, it by leaf of bamboo mulberry-leaf extract, peppermint extracting solution, soapberry fruit bark extract, fish scale zymotic fluid, is added after mixing It is stirred in agitator tank, rate is 80 revs/min, and time 5min obtains mixed liquor A;
B, by nanometer except emulsifier, coco-nut oil fatty acid glycine potassium, surfactant, amino-acid complex copper, poly- dimension Heating stirring in reaction kettle is added in ketone iodine solution after mixing, stir speed (S.S.) is 300 revs/min, stirs middle addition mixing after 10min Liquid A continues to stir 20min, obtains mixed liquid B;
C, nano-silver ionic particle is added in mixed liquid B, after being sufficiently mixed at normal temperatures, places 8h to get to laundry Liquid.
In the present embodiment, heating temperature is 55 DEG C in step B, heating time 10min.
Embodiment three:
Liquid detergent component includes 22 parts of leaf of bamboo mulberry-leaf extract, 12 part, nanometer oil removing breast of peppermint extracting solution in parts by weight 4 parts of agent, 3 parts of coco-nut oil fatty acid glycine potassium, 5 parts of soapberry fruit bark extract, 7 parts of fish scale zymotic fluid, surfactant 2 Part, 3 parts of amino-acid complex copper, 3 parts of Betagen Solution, 1 part of nano-silver ionic particle.
The preparation method of the present embodiment includes the following steps:
A, it by leaf of bamboo mulberry-leaf extract, peppermint extracting solution, soapberry fruit bark extract, fish scale zymotic fluid, is added after mixing It is stirred in agitator tank, rate is 40 revs/min, and time 5min obtains mixed liquor A;
B, by nanometer except emulsifier, coco-nut oil fatty acid glycine potassium, surfactant, amino-acid complex copper, poly- dimension Heating stirring in reaction kettle is added in ketone iodine solution after mixing, stir speed (S.S.) is 150 revs/min, stirs middle addition mixing after 10min Liquid A continues to stir 20min, obtains mixed liquid B;
C, nano-silver ionic particle is added in mixed liquid B, after being sufficiently mixed at normal temperatures, places 5h to get to laundry Liquid.
In the present embodiment, heating temperature is 46 DEG C in step B, heating time 6min.
Example IV:
Liquid detergent component includes 28 parts of leaf of bamboo mulberry-leaf extract, 18 part, nanometer oil removing breast of peppermint extracting solution in parts by weight 8 parts of agent, 5 parts of coco-nut oil fatty acid glycine potassium, 9 parts of soapberry fruit bark extract, 10 parts of fish scale zymotic fluid, surfactant 2 parts, 5 parts of amino-acid complex copper, 7 parts of Betagen Solution, 3 parts of nano-silver ionic particle.
The preparation method of the present embodiment includes the following steps:
A, it by leaf of bamboo mulberry-leaf extract, peppermint extracting solution, soapberry fruit bark extract, fish scale zymotic fluid, is added after mixing It is stirred in agitator tank, rate is 70 revs/min, and time 5min obtains mixed liquor A;
B, by nanometer except emulsifier, coco-nut oil fatty acid glycine potassium, surfactant, amino-acid complex copper, poly- dimension Heating stirring in reaction kettle is added in ketone iodine solution after mixing, stir speed (S.S.) is 280 revs/min, stirs middle addition mixing after 10min Liquid A continues to stir 20min, obtains mixed liquid B;
C, nano-silver ionic particle is added in mixed liquid B, after being sufficiently mixed at normal temperatures, places 7h to get to laundry Liquid.
In the present embodiment, heating temperature is 52 DEG C in step B, heating time 9min.
Embodiment five:
Liquid detergent component includes 25 parts of leaf of bamboo mulberry-leaf extract, 15 part, nanometer oil removing breast of peppermint extracting solution in parts by weight 6 parts of agent, 4 parts of coco-nut oil fatty acid glycine potassium, 7 parts of soapberry fruit bark extract, 9 parts of fish scale zymotic fluid, surfactant 2 Part, 4 parts of amino-acid complex copper, 5 parts of Betagen Solution, 2 parts of nano-silver ionic particle.
The preparation method of the present embodiment includes the following steps:
A, it by leaf of bamboo mulberry-leaf extract, peppermint extracting solution, soapberry fruit bark extract, fish scale zymotic fluid, is added after mixing It is stirred in agitator tank, rate is 65 revs/min, and time 5min obtains mixed liquor A;
B, by nanometer except emulsifier, coco-nut oil fatty acid glycine potassium, surfactant, amino-acid complex copper, poly- dimension Heating stirring in reaction kettle is added in ketone iodine solution after mixing, stir speed (S.S.) is 200 revs/min, stirs middle addition mixing after 10min Liquid A continues to stir 20min, obtains mixed liquid B;
C, nano-silver ionic particle is added in mixed liquid B, after being sufficiently mixed at normal temperatures, places 6h to get to laundry Liquid.
In the present embodiment, heating temperature is 50 DEG C in step B, heating time 8min.
Test example:
It is tested for the property using liquid detergent made from various embodiments of the present invention, obtains data such as following table:
Preparation method of the present invention is simple, and liquid detergent obtained has effects that sterilizing, while will not damage user's skin Skin, and device emission will not pollute water quality, soil, good environmental protection;Wherein, the leaf of bamboo mulberry leaf extraction added in the present invention Object, soapberry fruit bark extract have shigella dysenteriae, Escherichia coli powerful bactericidal effect;The Betagen Solution of addition can Improve bactericidal and bacteriostatic effect;The nano-silver ionic particle added in the present invention can effectively prevent liquid detergent from oxidation occur, becoming Matter phenomenon extends its holding time, in addition, nano-silver ionic particle equally has excellent sterilizing power.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (4)

1. a kind of environmentally protective sterilizing liquid detergent, it is characterised in that:Liquid detergent component includes leaf of bamboo mulberry leaf in parts by weight 20-30 parts of extract, 10-20 parts of peppermint extracting solution, nanometer are except 3-9 parts of emulsifier, coco-nut oil fatty acid glycine potassium 2-6 Part, 4-10 parts of soapberry fruit bark extract, 5-12 parts of fish scale zymotic fluid, 1-3 parts of surfactant, 2-6 parts of amino-acid complex copper, 2-8 parts of Betagen Solution, 1-3 parts of nano-silver ionic particle.
2. a kind of environmentally protective sterilizing liquid detergent according to claim 1, it is characterised in that:Liquid detergent component is preferred Composition proportion include 25 parts of leaf of bamboo mulberry-leaf extract, peppermint extracting solution 15 part, nanometer except 6 parts of emulsifier, coconut oil fat 4 parts of sour glycine potassium, 7 parts of soapberry fruit bark extract, 9 parts of fish scale zymotic fluid, 2 parts of surfactant, amino-acid complex copper 4 Part, 5 parts of Betagen Solution, 2 parts of nano-silver ionic particle.
3. realizing a kind of preparation method of environmentally protective sterilizing liquid detergent described in claim 1, it is characterised in that:It is made Preparation Method includes the following steps:
A, by leaf of bamboo mulberry-leaf extract, peppermint extracting solution, soapberry fruit bark extract, fish scale zymotic fluid, stirring is added after mixing It is stirred in tank, rate is 30-80 revs/min, and time 5min obtains mixed liquor A;
B, by nanometer except emulsifier, coco-nut oil fatty acid glycine potassium, surfactant, amino-acid complex copper, povidone iodine Heating stirring in reaction kettle is added in solution after mixing, stir speed (S.S.) is 100-300 revs/min, stirs middle addition mixing after 10min Liquid A continues to stir 20min, obtains mixed liquid B;
C, nano-silver ionic particle is added in mixed liquid B, after being sufficiently mixed at normal temperatures, places 4h-8h to get to laundry Liquid.
4. a kind of preparation method of environmentally protective sterilizing liquid detergent according to claim 3, it is characterised in that:It is described Heating temperature is 45 DEG C -55 DEG C in step B, heating time 5min-10min.
CN201810664455.1A 2018-06-25 2018-06-25 A kind of environmentally protective sterilizing liquid detergent and preparation method thereof Pending CN108676626A (en)

Priority Applications (1)

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CN201810664455.1A CN108676626A (en) 2018-06-25 2018-06-25 A kind of environmentally protective sterilizing liquid detergent and preparation method thereof

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CN201810664455.1A CN108676626A (en) 2018-06-25 2018-06-25 A kind of environmentally protective sterilizing liquid detergent and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109897743A (en) * 2019-03-22 2019-06-18 阜阳市路兴公路工程监理有限公司 A kind of biology radical anion stain remover and preparation method thereof
CN111317692A (en) * 2020-02-26 2020-06-23 许明 Hand sanitizer

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107619723A (en) * 2017-09-20 2018-01-23 北京军秀咨询有限公司 A kind of sterilizing liquid detergent

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107619723A (en) * 2017-09-20 2018-01-23 北京军秀咨询有限公司 A kind of sterilizing liquid detergent

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109897743A (en) * 2019-03-22 2019-06-18 阜阳市路兴公路工程监理有限公司 A kind of biology radical anion stain remover and preparation method thereof
CN111317692A (en) * 2020-02-26 2020-06-23 许明 Hand sanitizer

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Application publication date: 20181019