CN112779104A - A soap solution and soap with antibacterial effect, and its preparation method - Google Patents
A soap solution and soap with antibacterial effect, and its preparation method Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
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Abstract
The invention provides a soap solution and soap with antibacterial function and a preparation method thereof. The soap with the antibacterial function is prepared by the following method: adding alkali liquor into base oil containing Prinsepia utilis Royle oil and the like to perform saponification reaction to prepare soap liquid; adding rhizoma paridis powder, rhizoma paridis stem and leaf extract, rhizoma paridis root extract, or other plant additives into the above soap solution, mixing, and curing. The product of the invention has antibacterial effect, is natural and pollution-free, can remove dirt mildly, and has no irritation to skin; the paris polyphylla stem and leaf extract is added into the soap liquid, so that the soap liquid has a good antibacterial effect, the utilization of waste plant resources is increased, the cost is low, and the application value and the prospect are good. In addition, the invention lays a certain foundation for the application of folk plant resources, and has the advantages of simple preparation method, easy implementation and very good application prospect.
Description
Technical Field
The invention belongs to the technical field of daily chemicals, and particularly relates to non-transparent/transparent soap liquid and soap with an antibacterial function and containing paris polyphylla powder, paris polyphylla root extracts, paris polyphylla stem and leaf extracts and prinsepia utilis royle oil and a preparation method thereof.
Background
The soap is a daily chemical product which is most widely used, and the main component of the soap is a surfactant. The soap and soap have no difference in main components, and are high-grade fatty acid soaps, which are generally prepared by saponification of fats and oils (mutton fat, coconut oil, olive oil, palm oil or other fats and oils) and alkali under heating. However, the perfumed soap is usually added with essence, bacteriostatic components and the like to achieve the effects of cleaning, bacteriostasis, skin moistening and the like, and meanwhile, the perfumed soap has fragrant smell, is mainly contacted with the skin, and the acceptance degree of the skin needs to be considered. The soap has relatively simple process, the main component is metal stearate, and the irritation is far greater than that of the soap, so the soap is mainly used for washing clothes. However, the toilet soaps on the market are mainly added with chemical essence and chemical raw materials to achieve the disinfection and antibiosis effects, the toilet soaps can cause great damage to the skin after being used for a long time, and chemical substances cannot be thoroughly cleaned in the using process and enter the deep layer of the skin or enter the mouth through hands to cause deep damage to human bodies. With the development of economic society, the living conditions of people are improved, so that more and more people select more healthy and original ecological products. The paris polyphylla serving as a folk prescription has the effects of sterilization and disinfection when being used in folk. Prinsepia utilis Royle oil, produced from fruit pits of Prinsepia utilis Royle ex Fr, has a history of thousands of years in the minority of Lijiang, and has the effects of good safety, no irritation, strong permeability, inflammation diminishing, bacteria inhibiting, ultraviolet ray resisting, circulation improving, aging resisting, anoxia resisting, arteriosclerosis resisting and the like according to the research of the authorities of the national ministry of health, Beijing university, south China university, Yunnan pharmaceutical research institute and the like.
Paris genus plant, which is a perennial herb belonging to the family trillioniaceae, has 26 species and 14 varieties [ reference 1: the pharmaceutical value and the chemical substance basis of the plants of the paris genus, China journal of Chinese materia medica, 2015,40(5), 833-containing cost 839 ], and the types of the steroidal saponin compounds contained in different paris plants are different [ reference 2: wei JC, Gao WY, Yan XD, Wang Y, lacing SS, Xiao PG, chemical Constitutes of Plants from the Genus Paris, chem, biological conversion, 2014,11(9), 1277-containing 1297 ], 94 total steroidal saponin compounds are separated and identified in the Paris plant. Steroid saponin is the most important component in Paris plant, and the 2020 pharmacopoeia uses steroid saponin as quality control standard, and specifies that the total amount of Paris saponin I, saponin II and saponin VII in Paris is not less than 0.60%. The content of steroid saponins in Paris plants is influenced by many factors (such as the production area, harvest season, growth period, etc.) [ reference 1 ]. Therefore, different species of steroid saponin compounds contained in different species of paris plants are different in type and content. The steroid saponin is an oligomeric glycoside derived from spirostane compounds, and from the current research results and folk application investigation, the use effects of the steroid saponin mainly include antibacterial, hemostatic, anticancer and other effects. The stems and leaves of the paris polyphylla plant are basically directly discarded after the seeds are harvested every year, and few reports of the paris polyphylla plant are used in daily chemicals and other fields, so that the resource is greatly wasted. The rhizoma paridis extract used in the patent is the root extract of rhizoma paridis Yunnanensis and the stem and leaf extract of rhizoma paridis.
The Prinsepia utilis Royle is a Prinsepia utilis Royle (Prinsepia Royle) plant of Rosaceae (Rosae) Prinsepia genus, also called Prinsepia utilis Role (Chinese plant), Ribes portulaca (Qujing), semen oleaginis, fructus Plumeriae Acutissimae (Pu' er), anacis (Nasika), 1-5 m high shrubs, thick and grey green old branches, cylindrical branches in green or with grey green, with ribs, and with brown short and soft hairs or nearly hairless hairs, and the plant has the remarkable characteristics of longer branches and longer length reaching 3.5 cm, and leaves and nearly hairless hairs are grown on the branches. The fertilizer is distributed in mountains, wastelands, valleys or roadside places in Yunnan, Guizhou, Sichuan and Tibet of China. The drupes pseudolaricis is long round or inverted egg long round, the length is 1-1.5 cm, the width is about 8 mm, and the drupes pseudocerasus is purple brown or black purple, smooth and unhairing and is white powder; the stone was smooth and purplish red. The flowering period is 4-5 months, and the fruit ripening period is 8-9 months. The Prinsepia utilis Royle seeds are rich in oil, the oil yield is about 30 percent generally, the oil is dark brown yellow, clear and transparent, and is white like lard oil after solidification. At present, the utilization reports of the prinsepia utilis royle seeds are few, the prinsepia utilis royle seeds are generally eaten and used for skin care in folk use, reports of the prinsepia utilis royle seeds used in other fields are not found, and the resource waste is large.
Disclosure of Invention
The invention aims to solve the defects of the toilet soap in the prior art, and provides the toilet soap with an antibacterial function and no harm to human skin and a preparation method thereof by adding a paris polyphylla extract and prinsepia utilis royle oil on the basis of national folk application and scientific research. Provides a non-transparent/transparent soap solution and soap with antibacterial function and containing rhizoma paridis powder, rhizoma paridis root extract, rhizoma paridis stem and leaf extract, and Prinsepia utilis oil, and its preparation method.
The purpose of the invention is realized by the following technical scheme:
a soap solution and a perfumed soap with antibacterial function comprise a transparent soap solution and a non-transparent soap solution, wherein the non-transparent soap solution and the perfumed soap are prepared by the following method:
(1) heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature;
(2) slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs;
(3) after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the non-transparent soap.
A soap solution and a perfumed soap with antibacterial function comprise a transparent soap solution and a non-transparent soap solution, wherein the transparent soap solution and the perfumed soap are prepared according to the following method:
(1) taking 50 parts of non-transparent soap solution with an antibacterial function, and keeping the constant temperature to a set saponification temperature;
(2) adding 25-35 parts of absolute ethyl alcohol into the soap solution in the step (1), and stirring for reaction for 120-240 minutes until the reactant is changed from the opaque dope to a transparent solution;
(3) adding 20-40 parts of 50% sucrose solution and 10-13 parts of glycerol into the reaction solution in the step (2), and reacting for 20-60 minutes to obtain transparent soap solution with an antibacterial function;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the transparent soap with the antibacterial function;
the preparation method of the non-transparent soap liquid with the antibacterial function comprises the following steps: heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature; slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs; after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution.
The soap solution and the soap with the antibacterial function are characterized in that the base oil is one or more of mutton fat, prinsepia utilis royle oil, olive oil, coconut oil, palm oil and castor oil.
According to the soap solution and the perfumed soap with the antibacterial function, the alkali liquor is a sodium hydroxide aqueous solution, the dosage of the sodium hydroxide is determined by the type and the mass ratio of basic oil, namely the sum of the product of the weight of each oil and the saponification value of each oil; the amount of water is 2.1-3.2 times of the mass of sodium hydroxide.
According to the soap solution and the soap with the antibacterial function, the temperature of the saponification reaction is 30-80 ℃.
The soap solution and the soap with the antibacterial function have the advantages that the saponification reaction time is 30-180 minutes.
According to the soap solution and the soap with the antibacterial function, the paris polyphylla additive is one or more of paris polyphylla root powder, paris polyphylla root extract and paris polyphylla stem and leaf extract, the paris polyphylla root powder is prepared by grinding dry paris polyphylla root blocks into powder by a grinder, a grinder and other machines, and sieving the powder by a 40-80-mesh sieve; the rhizoma paridis root extract is an extraction product which takes rhizoma paridis root powder as a raw material and ethanol as a solvent; the paris polyphylla stem and leaf extract is an extraction product which takes dry paris polyphylla stem and leaf as a raw material and takes ethanol as a solvent.
According to the soap solution and the soap with the antibacterial function, the plant additive is one or more of rose essential oil, lavender essential oil, rose extract, safflower powder and lithospermum.
The invention also provides a preparation method of the non-transparent soap liquid and the soap with the antibacterial function, which comprises the following steps:
(1) heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature;
(2) slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs;
(3) after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the non-transparent soap.
The invention also provides a preparation method of the transparent soap liquid and the soap with the antibacterial function, which comprises the following steps:
firstly, preparing non-transparent soap solution with antibacterial function, which comprises the following steps: heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature; slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs; after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution;
then, the preparation method comprises the following steps:
(1) taking 50 parts of the non-transparent soap solution with the antibacterial function obtained in the step, and keeping the temperature to a set saponification temperature;
(2) adding 25-35 parts of absolute ethyl alcohol into the soap solution in the step (1), and stirring for reaction for 120-240 minutes until the reactant is changed from the opaque dope to a transparent solution;
(3) adding 20-40 parts of 50% sucrose solution and 10-13 parts of glycerol into the reaction solution in the step (2), and reacting for 20-60 minutes to obtain transparent soap solution with an antibacterial function;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the transparent soap with the antibacterial function.
The Prinsepia utilis Royle oil, the rhizoma paridis root powder, the rhizoma paridis stem and leaf extract and the rhizoma paridis root extract added in the invention contain a large amount of active substances, and have the effects of antibiosis and health. The invention provides a new application of paris polyphylla stems and leaves and prinsepia utilis royle seeds in preparing soap, avoids waste of national folk plant resources, and expands the types of soap products. Secondly, the soap solution and the soap with the antibacterial function have good antibacterial effect, are natural and pollution-free, have no irritation to skin, are simple and easy to implement in the preparation method, have good application prospects, and simultaneously expand the industrial application of national folk plants.
Drawings
Fig. 1 is a diagram showing the bacteriostatic effect of the soap of the invention on staphylococcus aureus.
Detailed Description
The invention will be further elucidated with reference to specific embodiments of the invention in the following description, in conjunction with the appended drawings. It should be understood that the embodiments described herein are only for explaining the present invention, and are not intended to limit the technical solutions of the present invention.
Example 1
A soap solution and soap with antibacterial function and a preparation method thereof comprise the following steps:
(1) base grease mixture: 15g of castor oil, 15g of coconut oil, 15g of palm oil and 5g of prinsepia utilis royle oil, heating, dissolving and mixing uniformly, and keeping the temperature to 70 ℃ (saponification temperature);
(2) calculating the using amount of sodium hydroxide and water:
the calculation method comprises the following steps: the dosage of the sodium hydroxide is the sum of the product of the weight of each grease and the saponification value of each grease; the amount of water is equal to the amount of sodium hydroxide (2.1-3.2);
the amount of sodium hydroxide is (15 × 0.128) + (15 × 0.190) + (15 × 0.141) + (5 × 0.121) ═ 7.49 g;
the amount of water used was 7.49g × 3 g 22.47g (the amount of water used in this example was 3 times the amount of sodium hydroxide);
(3) preparation of sodium hydroxide aqueous solution:
weighing sodium hydroxide particles in the mass in the step (2), dissolving the sodium hydroxide particles in water in the mass in the step (2), stirring to release heat, and cooling to a specified saponification temperature;
(4) at the set saponification temperature, the alkali liquor is slowly poured into the base oil mixture, and the reaction is stirred for 30 minutes (set saponification time). Detecting whether the grease is completely reacted or not as required, and if the grease is not completely reacted, continuously heating the grease to be completely reacted as required;
(5) after the saponification reaction is completed, 0.1g of rhizoma paridis root powder is added to obtain the non-transparent soap solution with the antibacterial function;
(6) pouring the soap liquid in the step (5) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the soap.
Example 2
A soap solution and soap with antibacterial function and a preparation method thereof comprise the following steps:
(1) base grease: heating, dissolving and uniformly mixing 50g of mutton fat, and keeping the temperature to 40 ℃ (saponification temperature);
(2) preparation of sodium hydroxide aqueous solution:
weighing 6.91g (mutton fat saponification value is 0.1382) of sodium hydroxide particles, dissolving in 17.9g of water, stirring to release heat, and cooling to the specified saponification temperature;
(3) at the set saponification temperature, the alkali liquor is slowly poured into the base oil and stirred for reaction for 30 minutes (set saponification time). Detecting whether the grease is completely reacted or not as required, and if the grease is not completely reacted, continuously heating the grease to be completely reacted as required;
(4) after the saponification reaction is completed, 0.05g of paris polyphylla root extract is added to obtain the non-transparent soap solution with the antibacterial function;
(5) pouring the soap liquid in the step (4) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the soap.
Example 3
A soap solution and soap with antibacterial function and a preparation method thereof comprise the following steps:
(1) base grease mixture: 15g of coconut oil, 15g of palm oil, 15g of olive oil and 5g of prinsepia utilis royle oil, heating, dissolving and mixing uniformly, and keeping the temperature to 80 ℃ (saponification temperature);
(2) preparation of sodium hydroxide aqueous solution:
weighing 7.58g of sodium hydroxide particles, dissolving in 15.9g of water, stirring to release heat, and cooling to a specified saponification temperature;
(3) at the set saponification temperature, the alkali liquor is slowly poured into the base oil mixture, and the reaction is stirred for 90 minutes (set saponification time). Detecting whether the grease is completely reacted or not as required, and if the grease is not completely reacted, continuously heating the grease to be completely reacted as required;
(4) after the saponification reaction is completed, 0.1g of paris polyphylla stem and leaf extract is added to obtain the non-transparent soap solution with the antibacterial function;
(5) adding 35mL of absolute ethyl alcohol into the soap solution in the step (4), and stirring and reacting for 160 minutes until the reactant is changed from the opaque viscous substance to a transparent solution;
(6) adding 22.5g of 50% sucrose solution and 11.5g of glycerol into the reaction solution in the step (5), and reacting for 40 minutes to obtain the transparent soap solution with the antibacterial function;
(7) pouring the soap liquid in the step (6) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the soap.
Example 4
A soap solution and soap with antibacterial function and a preparation method thereof comprise the following steps:
(1) base grease mixture: 5g of olive oil, 15g of coconut oil, 15g of palm oil and 15g of prinsepia utilis royle oil, heating, dissolving and mixing uniformly, and keeping the temperature to 40 ℃ (saponification temperature);
(2) preparation of sodium hydroxide aqueous solution:
weighing 7.46g of sodium hydroxide particles, dissolving in 23.87g of water, stirring to release heat, and cooling to a specified saponification temperature;
(3) at the set saponification temperature, the alkali liquor is slowly poured into the base oil mixture, and the reaction is stirred for 60 minutes (set saponification time). Detecting whether the grease is completely reacted or not as required, and if the grease is not completely reacted, continuously heating the grease to be completely reacted as required;
(4) after the saponification reaction is completed, respectively adding 0.1g of paris polyphylla extract and 0.5g of rose essential oil to obtain the non-transparent soap solution with the antibacterial function;
(5) pouring the soap liquid in the step (4) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the soap.
Example 5
A soap solution and soap with antibacterial function and a preparation method thereof comprise the following steps:
(1) preparing a lithospermum extract: soaking 5g radix Arnebiae in 30g oleum Olivarum for 7 days;
(2) base grease mixture: heating, dissolving and mixing 15g of olive oil, 15g of coconut oil, 10g of palm oil and 10g of prinsepia utilis royle oil soaked in lithospermum uniformly, and keeping the temperature to 30 ℃ (saponification temperature);
(3) preparation of sodium hydroxide aqueous solution:
weighing 7.48g of sodium hydroxide particles, dissolving in 22.45g of water, stirring to release heat, and cooling to a specified saponification temperature;
(4) at the set saponification temperature, the alkali liquor is slowly poured into the base oil mixture, and the reaction is stirred for 70 minutes (set saponification time). Detecting whether the grease is completely reacted or not as required, and if the grease is not completely reacted, continuously heating the grease to be completely reacted as required;
(5) after the saponification reaction is completed, 0.1g of rhizoma paridis root powder is respectively added to obtain the non-transparent soap solution with the antibacterial function;
(6) pouring the soap liquid in the step (5) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the soap.
Example 6
The soap solution and the soap with antibacterial function have the antibacterial effect on staphylococcus aureus.
Test subjects: selecting handmade soap containing 20% of rhizoma paridis extract and Prinsepia utilis Royle oil, and using water, soap base without antibacterial component, and Penicillin-Streptomycin solution (double-antibody, Penicillin Streptomycin, concentration of the two is respectively 10000U/mL, and Streptomycin: 10000 μ g/mL, available from BIOEXPLORER Life Sciences) as control group; the test bacterium is Staphylococcus aureus (ATCC 6538) provided by Beiner's Association of Biotechnology, Inc. The test method is the bacteriostatic loop method.
TABLE 1 bacteriostatic effect of perfumed soap on staphylococcus aureus
As can be seen from Table 1 and FIG. 1, the product of the present invention has a significant inhibitory effect on Staphylococcus aureus, as compared with the control group. The antibacterial soap conforms to the definition of the common antibacterial soap in the national standard GB 19877.3-2005 special soap: the special toilet soap can completely inhibit the growth of staphylococcus aureus (ATCC 6538). Therefore, the product of the invention has obvious bacteriostatic action and is bacteriostatic perfumed soap. The water in the invention is distilled water or deionized water.
Claims (10)
1. A non-transparent soap solution and soap with antibacterial function is characterized by being prepared according to the following method:
(1) heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature;
(2) slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs;
(3) after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the non-transparent soap.
2. A transparent soap solution and soap with antibacterial function is characterized by being prepared according to the following method:
firstly, preparing a non-transparent soap solution with an antibacterial function: heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature; slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs; after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution;
then preparing transparent soap liquid and soap according to the following steps:
(1) taking 50 parts of non-transparent soap solution with an antibacterial function, and keeping the constant temperature to a set saponification temperature;
(2) adding 25-35 parts of absolute ethyl alcohol into the soap solution in the step (1), and stirring for reaction for 120-240 minutes until the reactant is changed from the opaque dope to a transparent solution;
(3) adding 20-40 parts of 50% sucrose solution and 10-13 parts of glycerol into the reaction solution in the step (2), and reacting for 20-60 minutes to obtain transparent soap solution with an antibacterial function;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the transparent soap with the antibacterial function.
3. The non-transparent/transparent soap solution and soap with antibacterial function according to claim 1 or 2, wherein the base oil is one or more of mutton fat, prinsepia utilis royle oil, olive oil, coconut oil, palm oil and castor oil.
4. The non-transparent/transparent soap solution and soap with antibacterial function according to claim 1 or 2, wherein the alkali solution is sodium hydroxide aqueous solution, and the amount of sodium hydroxide is determined by the type and mass ratio of basic oil, i.e. the sum of the product of the weight of each oil and the saponification valence of each oil; the amount of water is 2.1-3.2 times of the mass of sodium hydroxide.
5. The non-transparent/transparent soap solution and soap having antibacterial function according to claim 1 or 2, wherein the saponification reaction temperature is 30-80 ℃.
6. The non-transparent/transparent soap solution and soap having antibacterial function according to claim 1 or 2, wherein the saponification reaction time is 30 to 180 minutes.
7. The non-transparent/transparent soap solution and soap with antibacterial function according to claim 1 or 2, wherein the rhizoma paridis additive is one or more of rhizoma paridis root powder, rhizoma paridis root extract, and rhizoma paridis stem and leaf extract, the rhizoma paridis root powder is dry rhizoma paridis root tuber of Yunnan, and is pulverized by a pulverizer, a grinder, etc., and sieved with a 40-80 mesh sieve; the rhizoma paridis root extract is an extraction product which takes rhizoma paridis root powder as a raw material and ethanol as a solvent; the paris polyphylla stem and leaf extract is an extraction product which takes dry paris polyphylla stem and leaf as a raw material and takes ethanol as a solvent.
8. The non-transparent/transparent soap solution and soap with antibacterial function according to claim 1 or 2, wherein the plant additive is one or more of rose essential oil, lavender essential oil, rose extract, safflower powder and lithospermum.
9. A method for preparing non-transparent soap liquid and soap with antibacterial function comprises the following steps:
(1) heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature;
(2) slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs;
(3) after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the non-transparent soap.
10. A method for preparing transparent soap liquid and soap with antibacterial function comprises the following steps:
firstly, preparing non-transparent soap solution with antibacterial function, which comprises the following steps: heating, dissolving and uniformly mixing a base grease mixture prepared according to the mass ratio, and keeping the temperature to the corresponding saponification temperature; slowly pouring alkali liquor into the basic oil mixture at a set saponification temperature, stirring for a set saponification time, detecting whether the oil is completely reacted or not, and if the oil is not completely reacted, continuously heating to completely react according to needs; after the saponification reaction is completed, 50 parts of soap solution are respectively added with 0.01-0.2 part of paris polyphylla additive and 0.005-0.5 part of plant additive to obtain non-transparent soap solution;
then, the preparation method comprises the following steps:
(1) taking 50 parts of the non-transparent soap solution with the antibacterial function obtained in the step, and keeping the temperature to a set saponification temperature;
(2) adding 25-35 parts of absolute ethyl alcohol into the soap solution in the step (1), and stirring for reaction for 120-240 minutes until the reactant is changed from the opaque dope to a transparent solution;
(3) adding 20-40 parts of 50% sucrose solution and 10-13 parts of glycerol into the reaction solution in the step (2), and reacting for 20-60 minutes to obtain transparent soap solution with an antibacterial function;
(4) pouring the soap liquid in the step (3) into a mould, cooling at room temperature, and demoulding after 24-48 hours to obtain the transparent soap with the antibacterial function.
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| CN105219552A (en) * | 2015-09-08 | 2016-01-06 | 桂林盛兴电子科技有限公司 | A kind of herbal medicine whitening soap and preparation method thereof |
| CN108531318A (en) * | 2018-07-21 | 2018-09-14 | 安溪县凤城建金产品外观设计服务中心 | A kind of preparation process of the soap containing paris polyphylla extract |
| CN109837148A (en) * | 2017-11-27 | 2019-06-04 | 沈阳华企力拓企业服务有限公司 | A kind of whitening goldleaf perfumed soap and preparation method thereof |
| CN111518639A (en) * | 2020-03-20 | 2020-08-11 | 王信 | Soap for inhibiting pityrosporum orbiculare |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105219552A (en) * | 2015-09-08 | 2016-01-06 | 桂林盛兴电子科技有限公司 | A kind of herbal medicine whitening soap and preparation method thereof |
| CN109837148A (en) * | 2017-11-27 | 2019-06-04 | 沈阳华企力拓企业服务有限公司 | A kind of whitening goldleaf perfumed soap and preparation method thereof |
| CN108531318A (en) * | 2018-07-21 | 2018-09-14 | 安溪县凤城建金产品外观设计服务中心 | A kind of preparation process of the soap containing paris polyphylla extract |
| CN111518639A (en) * | 2020-03-20 | 2020-08-11 | 王信 | Soap for inhibiting pityrosporum orbiculare |
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