CN109010149A - A kind of agilawood essential oil toothpaste and preparation method thereof - Google Patents
A kind of agilawood essential oil toothpaste and preparation method thereof Download PDFInfo
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- CN109010149A CN109010149A CN201811250483.5A CN201811250483A CN109010149A CN 109010149 A CN109010149 A CN 109010149A CN 201811250483 A CN201811250483 A CN 201811250483A CN 109010149 A CN109010149 A CN 109010149A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The present invention relates to daily necessities field, in particular to a kind of agilawood essential oil toothpaste and preparation method thereof.It includes following ingredient that the present invention, which provides agilawood essential oil toothpaste: 40 ~ 70 parts of 10 ~ 20 parts of glycerol, 1 ~ 2 part of sodium carboxymethylcellulose, 30 ~ 50 parts of deionized water, 1 ~ 4 part of lauryl sodium sulfate, 0.01 ~ 0.2 part of saccharin sodium, 0.1 ~ 0.5 part of xanthan gum, calcium carbonate or silica, 0.01 ~ 0.1 part of sodium benzoate and agilawood essential oil .1 ~ 1 part, there is good antagonistic property, the stabilization of flora in oral cavity can be maintained, oral health is kept.
Description
Technical field
The present invention relates to technical field of daily necessities, in particular to a kind of agilawood essential oil toothpaste and preparation method thereof.
Background technique
Toothpaste is the necessity of people's daily life.People are used to clean tooth, keep oral hygiene, maintain implication clear
Newly.Toothpaste uses simple and convenient, becomes hygiene articles indispensable in modern life.With economic hair
Exhibition, people's living standard are continuously improved, and people have not only been satisfied with toothpaste only with cleaning efficacy, and toothpaste is by general
Logical clean type develops to efficiency health-care type.Toothpaste is as a kind of cleaning agent for mouth cavity, other than should have basic cleaning action,
Should also have anti-inflammatory antibacterial hemostasis and other effects type effect, effectively oral bacteria be inhibited to breed to guarantor's body health.Tooth
The main component of cream has a rubbing agent, moisturizer, surfactant, thickener, sweetener, preservative and pigment essence etc. press than
Example mixes[1].Developing new and effective Chinese herbal medicine formula to be added in toothpaste will be the research for having good prospect
Direction.This new and effective functional toothpaste can be accomplished to take care of one's teeth, while cannot destroy the growth of probiotics in oral cavity
Environment.The technology of innovation and excellent formula occupy an important position in the research and development of dental care product.So creative
Thinking is conducive to the rapid development of functional toothpaste research and development.In recent years, influence of the oral problem to human health be also increasingly
Greatly, thus the effect status in people's daily life of novel effect type toothpaste it is also higher and higher.
It is that raw material refines after distillation extraction that agilawood essential oil, which is by very precious agalloch eaglewood,.Agalloch eaglewood is good for human body
Health has very big influence, its health value with higher can be used for oral administration and externally, go to eliminate bad breath, the side such as hemostasis and anti-inflammation
There is surprising effect in face.This experiment determines the process recipe of agilawood essential oil toothpaste by optimization formulation of tooth-paste, sensory properties,
Determine optimization formula agilawood essential oil toothpaste.For saprodontia and periodontitis, both are disease high-incidence in oral cavity, functional form toothpaste
It comes into being.The producing cause of saprodontia is to produce acid after the bacterium in oral cavity decomposes swill, leads to calcium member in tooth
Caused by the loss of element.Periodontitis is because the gingiva tissue periodontium that factors cause such as be inflamed in part generates in tooth
Chronic disease.Brushing time is inadequate in daily life or the cleaning capacity difference of toothpaste can all lead to the production of periodontitis by people
It is raw.The oral hygiene of human body can be roughly divided into two parts greatly: first is that eliminating oral peculiar smell, inhibiting bacteria breed, to make oral cavity
Smell is clearly pleasant, is conducive to mould the interpersonal contacts of good self-image promotion；Second is that giving for certain odontopathy
It treats and prevents；Called function type toothpaste is the medicated toothpaste for targetedly treating certain odontopathy, it is added in toothpaste
Certain certain drug increases specific therapeutic effect on the basis of easy clean effect.Agilawood essential oil provided by the present application
Toothpaste has apparent fungistatic effect to oral cavity streptococcus mutans, staphylococcus aureus, Escherichia coli, staphylococcus albus.
Summary of the invention
The purpose of the present invention is to provide a kind of agilawood essential oil toothpaste with good fungistatic effect, which is characterized in that
Ingredient including following parts by weight:
10~20 parts of glycerol
1~2 part of sodium carboxymethylcellulose
30~50 parts of deionized water
1~4 part of lauryl sodium sulfate
0.01~0.2 part of saccharin sodium
0.1~0.5 part of xanthan gum
Calcium carbonate or 40~70 parts of silica
0.01~0.1 part of sodium benzoate
0.1~1 part of agilawood essential oil.
Preferably, the agilawood essential oil toothpaste includes the ingredient of following parts by weight:
12~18 parts of glycerol
1~2 part of sodium carboxymethylcellulose
30~45 parts of deionized water
1~3 part of lauryl sodium sulfate
0.01~0.2 part of saccharin sodium
0.1~0.5 part of xanthan gum
Calcium carbonate or 40~60 parts of silica
0.01~0.1 part of sodium benzoate
0.1~1 part of agilawood essential oil.
Further, the agilawood essential oil toothpaste includes the ingredient of following parts by weight:
12~18 parts of glycerol
1~2 part of sodium carboxymethylcellulose
35~45 parts of deionized water
1~2 part of lauryl sodium sulfate
0.05~0.2 part of saccharin sodium
0.2~0.4 part of xanthan gum
Calcium carbonate or 45~55 parts of silica
0.01~0.05 part of sodium benzoate
0.1~0.5 part of agilawood essential oil.
Further, the agilawood essential oil toothpaste further includes 0.1~0.5 part of fruit ferment.
Preferably, the agilawood essential oil the preparation method is as follows:
It fetches to be put into pulverizer from the agalloch eaglewood raw material of Hainan Tunchang and handle, 10~15 times of agalloch eaglewood weight of deionization is added
Water, is placed on 100 DEG C~120 DEG C of thermostatical oil bath refluxing extraction 2~10 hours, collects efflux, is extracted with anhydrous ether
Volatile oil obtains flaxen agalloch eaglewood volatile oil after dry.
The second aspect of the present invention provides a kind of preparation method of agilawood essential oil toothpaste, comprising the following steps:
A, weigh metering part glycerol and sodium carboxymethylcellulose be placed in container stir to obtain without agglomeration clear
Solution；
B, the lauryl sodium sulfate of addition metering part, saccharin sodium, Huang in clear transparent solutions is added to what step a was obtained
After mixing evenly, it is 60~70 DEG C or so that solution temperature is heated under stirring to virgin rubber, up to no solid particle state；
C, the calcium carbonate/silica and deionized water of metering part are added in the liquid obtained to step b, continues stirring extremely
It is smooth to obtain agilawood essential oil lotion of toothpaste；
D, the agilawood essential oil and sodium benzoate that metering part is added into agilawood essential oil lotion of toothpaste, through sterilization treatment after mixing
Obtain agilawood essential oil toothpaste finished product.
Preferably, the fruit ferment of metering part is also added into the step d.
The beneficial effects of the present invention are: agilawood essential oil toothpaste provided by the invention has good antagonistic property, Ke Yiwei
The stabilization of flora in oral cavity is held, oral health is kept.
Detailed description of the invention
Fig. 1 is agilawood essential oil GC-MS ion total figure
Specific embodiment
Illustrate technical solution of the present invention below by way of specific embodiment, but the scope of the present invention is not limited thereto.
Table 1: 1 experimental material of table and reagent
The fruit ferment that the fruit ferment can select Common Fruits to be prepared into.
Embodiment 1
A kind of preparation method of agilawood essential oil toothpaste, comprising the following steps:
A, weigh 15g glycerol and 1g sodium carboxymethylcellulose be placed in container stir it is molten without agglomeration clear to obtaining
Liquid；
B, into the addition clear transparent solutions that step a is obtained be added 1.5g lauryl sodium sulfate, 0.1g saccharin sodium,
After mixing evenly, it is 60~70 DEG C or so that solution temperature is heated under stirring to 0.3g xanthan gum, up to no solid particle state；
C, 50g calcium carbonate and 39g deionized water are added in the liquid obtained to step b, continues stirring and is sunk to smooth
Essential oil lotion of toothpaste；
D, 0.5g agilawood essential oil and 0.01g sodium benzoate are added into agilawood essential oil lotion of toothpaste, after mixing through sterilizing at
Reason obtains agilawood essential oil toothpaste finished product.
Embodiment 2
A kind of preparation method of agilawood essential oil toothpaste, comprising the following steps:
A, weigh 12g glycerol and 2g sodium carboxymethylcellulose be placed in container stir it is molten without agglomeration clear to obtaining
Liquid；
B, 1g lauryl sodium sulfate, 0.2g saccharin sodium, 0.4g are added into the addition clear transparent solutions that step a is obtained
After mixing evenly, it is 60~70 DEG C or so that solution temperature is heated under stirring to xanthan gum, up to no solid particle state；
C, 55g calcium carbonate and 45g deionized water are added in the liquid obtained to step b, continues stirring and is sunk to smooth
Essential oil lotion of toothpaste；
D, 0.1g agilawood essential oil, 0.5g fruit ferment and 0.03g sodium benzoate are added into agilawood essential oil lotion of toothpaste, are mixed
Agilawood essential oil toothpaste finished product is obtained through sterilization treatment after even.
Embodiment 3
A kind of preparation method of agilawood essential oil toothpaste, comprising the following steps:
A, weigh 18g glycerol and 1g sodium carboxymethylcellulose be placed in container stir it is molten without agglomeration clear to obtaining
Liquid；
B, into the addition clear transparent solutions that step a is obtained be added 2g lauryl sodium sulfate, 0.05g saccharin sodium,
After mixing evenly, it is 60~70 DEG C or so that solution temperature is heated under stirring to 0.2g xanthan gum, up to no solid particle state；
C, 45g silica and 40g deionized water are added in the liquid obtained to step b, continues stirring and is obtained to smooth
Agilawood essential oil lotion of toothpaste；
D, 0.5g agilawood essential oil, 0.5g fruit ferment and 0.02g sodium benzoate are added into agilawood essential oil lotion of toothpaste, are mixed
Agilawood essential oil toothpaste finished product is obtained through sterilization treatment after even.
Experimental example 1: the extraction process and agilawood essential oil constituent analysis of agilawood essential oil
Table 2: laboratory apparatus and reagent
It fetches to be put into pulverizer from the agalloch eaglewood raw material 100g of Hainan Tunchang and handle, the distilled water of 1200ml is added, place
Thermostatical oil bath refluxing extraction 8 hours of 110 DEG C~120 DEG C, efflux is collected, oil is will volatilize with anhydrous ether and extracts
Come, is dried by anhydrous sodium sulfate, obtains flaxen agalloch eaglewood volatile oil.
Constituent analysis is carried out to agalloch eaglewood volatile oil using gas chromatography-mass spectrum computer combination (GC-MS) method, analyzes result
It is shown in Table shown in 2 and Fig. 1.
Table 3
It is found that being divided into analysis in the volatile oil of the agalloch eaglewood extracted with the method for steam distillation from above-mentioned analysis result
45 kinds of compound out account for the 52.78% of total peak area, wherein saturated alkane 13, and cyclic alkane 2, phenolic substances 3, alcohol
Substance 10, Ester 17.The higher ingredient of content is Furadan -7- phenol (16.550%), tetramethrin II
(11.577%), 3- (2- ethylhexyl) phosphate (4.182%), Furadan (5.579%).
Experimental example 2: the physical and chemical index test of agilawood essential oil toothpaste
1. the cold-resistant heat resistance of toothpaste is tested
Each 15g of toothpaste for taking every kind of formula, is respectively charged into conical flask, is placed in constant incubator (80 ± 5 DEG C), refrigerator
It in frozen coating (- 25 DEG C), is taken out after cultivating 36h wherein, carries out character comparison with the toothpaste for being placed on room temperature, observe its lotion
Texture, color etc..
2. the centrifugation of toothpaste is tested
The toothpaste of different formulations is fitted into centrifuge tube, centrifuge tube is placed on (37 ± 1 DEG C) of constant incubator heat preservations, 1n
After put into a centrifuge, be centrifuged 40min, revolving speed 4000r/min, observation lotion of toothpaste whether there is or not laminations.Experimental result such as table 4
It is shown.
Table 4
Experimental example 3: the bacteriostatic experiment of agilawood essential oil toothpaste
1. experimental principle
Mouth disease has become one of the major chronic illnesses of puzzlement human health at present, for mouth disease
It prevents and treats extremely urgent, while also becoming the problem of scientist and ordinary populace are paid high attention to.Agilawood essential oil is good due to its own
Good medicinal efficacy and special fragrance become the optimization formula for inhibiting that bacterium excessively breeds in oral cavity, pass through comparison in experiment
The Chinese herbal toothpaste (tianqi toothpaste, mica filled polypropylene) of production and the Chinese herbal medicine essence of heterogeneity have been put on the market
Oil extract compares.Staphylococcus aureus, white Portugal are carried out to agilawood essential oil toothpaste with flat band method antibacterial test
Grape coccus, Escherichia coli, streptococcus mutans bacteriostatic test.
2. bacteriostatic experiment material and instrument
Table 5
3. bacteriostatic experiment concrete operations
Filter paper, cotton swab, tweezers, culture dish are bandaged into sterilizing, drying, spare.
With liquid nutrient broth solution 2L, it is dispensed into the conical flask of 15 250ml, stoppers plug.It is molten with liquid nutrient agar
Liquid 1L, stoppers plug.With liquid BHI brain-heart leaching extraction liquid culture medium 500mL, it is divided in 2 250mL conical flasks, fills in
Son.With liquid 1L BHI brain-heart leaching extraction agar medium, plug is stoppered.The above-mentioned culture solution prepared is put into high-temperature sterilization box,
Sterilization time is 30min, and setting sterilising temp is 121 DEG C.After temperature is cooled to the temperature that can be held, in superclean bench
On agar solution is poured into the culture dish of sterilizing, drying, the agar solution in each culture dish is in 10~15ml or so.Processing
Good agar medium, which is put into constant incubator, to be stored.
Actication of culture: the Escherichia coli, staphylococcus aureus and white Portugal of 4 DEG C of preservations in refrigerator will be deposited in
Grape coccus is transferred on fresh nutrient agar slopes, while the streptococcus mutans kept are seeded in BHI brain-heart leaching extraction fine jade
In rouge medium slant, 37 DEG C of cultures 18~for 24 hours.
The preparation of bacteria suspension: the strain on benchboard is fitted into conical flask in two times with 10ml sterile saline and is put into
It is shaken on shaking table.
The preparation of antibacterial plate: on superclean bench, 50 μ l are pipetted in the conical flask equipped with bacteria suspension with liquid-transfering gun
It is applied uniformly to nutrient agar panel, and with stick is applied.
Filter paper immerses medical fluid: on superclean bench, the toothpaste that filter paper immerses 100mg/ml difference extract being hanged
In turbid, it is put into 5 filter papers in each culture dish, and marks good number.
The agar plates placed are put into 37 DEG C of constant incubators and carry out Spawn incubation, it is antibacterial to take out observation every other day
Enclose and measured with a yardstick the diameter of inhibition zone.
4. bacteriostatic experiment result
Wherein comparative example 1 is commercially available Chinese herbal medicine tianqi toothpaste；Comparative example 2 is commercially available mica filled polypropylene.
In summary it is good antibacterial to be not difficult to find out that agilawood essential oil toothpaste has for the antibacterial result of the extract of different proportion
Characteristic can maintain the stabilization of flora in oral cavity, keep oral health.It is also just opposite to add more agilawood essential oil fungistatic effect
Preferably, best to the fungistatic effect of the streptococcus mutans for leading to saprodontia in oral cavity.Escherichia coli can also be effectively controlled simultaneously
Microflora in human body maintains stable flora, and reaching will not diseased state.The Chinese herbal toothpaste sold on the market is compared, this
The characteristic for testing the agilawood essential oil toothpaste of research and development is also very prominent, can achieve good effect in terms of inhibiting bacteria and diminishing inflammation.
Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.
Claims (7)
1. a kind of agilawood essential oil toothpaste with good fungistatic effect, which is characterized in that the ingredient including following parts by weight:
10 ~ 20 parts of glycerol
1 ~ 2 part of sodium carboxymethylcellulose
30 ~ 50 parts of deionized water
1 ~ 4 part of lauryl sodium sulfate
0.01 ~ 0.2 part of saccharin sodium
0.1 ~ 0.5 part of xanthan gum
Calcium carbonate or 40 ~ 70 parts of silica
0.01 ~ 0.1 part of sodium benzoate
0.1 ~ 1 part of agilawood essential oil.
2. agilawood essential oil toothpaste as described in claim 1, it is characterised in that the ingredient including following parts by weight:
12 ~ 18 parts of glycerol
1 ~ 2 part of sodium carboxymethylcellulose
30 ~ 45 parts of deionized water
1 ~ 3 part of lauryl sodium sulfate
0.01 ~ 0.2 part of saccharin sodium
0.1 ~ 0.5 part of xanthan gum
Calcium carbonate or 40 ~ 60 parts of silica
0.01 ~ 0.1 part of sodium benzoate
0.1 ~ 1 part of agilawood essential oil.
3. agilawood essential oil toothpaste as described in claim 1, it is characterised in that the ingredient including following parts by weight:
12 ~ 18 parts of glycerol
1 ~ 2 part of sodium carboxymethylcellulose
35 ~ 45 parts of deionized water
1 ~ 2 part of lauryl sodium sulfate
0.05 ~ 0.2 part of saccharin sodium
0.2 ~ 0.4 part of xanthan gum
Calcium carbonate or 45 ~ 55 parts of silica
0.01 ~ 0.05 part of sodium benzoate
0.1 ~ 0.5 part of agilawood essential oil.
4. such as the described in any item agilawood essential oil toothpaste of claim 1 ~ 3, which is characterized in that the agilawood essential oil toothpaste further includes
0.1 ~ 0.5 part of fruit ferment.
5. such as the described in any item agilawood essential oil toothpaste of claim 1 ~ 3, it is characterised in that the preparation method of the agilawood essential oil
It is as follows:
It takes agalloch eaglewood raw material to be put into pulverizer to handle, 10 ~ 15 times of agalloch eaglewood weight of deionized water is added, is placed on 100 DEG C ~ 120
DEG C thermostatical oil bath refluxing extraction 2 ~ 10 hours, collect efflux, extract volatile oil with anhydrous ether, obtained after dry yellowish
The agalloch eaglewood volatile oil of color.
6. a kind of prepare the preparation method such as the described in any item agilawood essential oil toothpaste of claim 1 ~ 3, comprising the following steps:
A, weigh metering part glycerol and sodium carboxymethylcellulose be placed in container stir to obtain without agglomeration clear transparent solutions；
B, the lauryl sodium sulfate of addition metering part, saccharin sodium, xanthan gum in clear transparent solutions is added to what step a was obtained
After mixing evenly, it is 60 ~ 70 DEG C or so that solution temperature is heated under stirring, up to no solid particle state；
C, the calcium carbonate/silica and deionized water of metering part are added in the liquid obtained to step b, continues to stir to smooth
Obtain agilawood essential oil lotion of toothpaste；
D, the agilawood essential oil and sodium benzoate that metering part is added into agilawood essential oil lotion of toothpaste, obtain after mixing through sterilization treatment
Agilawood essential oil toothpaste finished product.
7. the preparation method of agilawood essential oil toothpaste as claimed in claim 6, it is characterised in that be also added into meter in the step d
Measure the fruit ferment of part.
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| CN111437240A (en) * | 2020-04-30 | 2020-07-24 | 云南风联科技有限公司 | Plant agilawood-flavor oral cavity atomized liquid and preparation method thereof |
| CN112076124A (en) * | 2020-09-25 | 2020-12-15 | 海口楠脂香业有限公司 | Agilawood toothpaste and preparation method thereof |
| CN112617548A (en) * | 2020-12-25 | 2021-04-09 | 海南娜古芳沉香科技有限公司 | Kyara extract for preparing latex pillow for improving sleep, preparation method and latex pillow prepared from Kyara extract |
| CN114306151A (en) * | 2021-11-23 | 2022-04-12 | 电子科技大学中山学院 | Nano agilawood suspension, anhydrous agilawood toothpaste and preparation method of anhydrous agilawood toothpaste |
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| CN111437240A (en) * | 2020-04-30 | 2020-07-24 | 云南风联科技有限公司 | Plant agilawood-flavor oral cavity atomized liquid and preparation method thereof |
| CN112076124A (en) * | 2020-09-25 | 2020-12-15 | 海口楠脂香业有限公司 | Agilawood toothpaste and preparation method thereof |
| CN112617548A (en) * | 2020-12-25 | 2021-04-09 | 海南娜古芳沉香科技有限公司 | Kyara extract for preparing latex pillow for improving sleep, preparation method and latex pillow prepared from Kyara extract |
| CN114306151A (en) * | 2021-11-23 | 2022-04-12 | 电子科技大学中山学院 | Nano agilawood suspension, anhydrous agilawood toothpaste and preparation method of anhydrous agilawood toothpaste |
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