CN111437240A - Plant agilawood-flavor oral cavity atomized liquid and preparation method thereof - Google Patents
Plant agilawood-flavor oral cavity atomized liquid and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/43—Guanidines
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
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- A61K8/988—Honey; Royal jelly, Propolis
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- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
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- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
The invention discloses a plant agilawood-flavor oral cavity atomized liquid which comprises the following components in percentage by mass: agilawood essential oil: 7-9%, deionized water: 67-76%, peppermint oil: 2-4%, absolute ethyl alcohol: 2-4% and watermelon frost: 1-1.5%, sodium benzoate: 0.3-0.5%, honey: 7-9%, borneol: 2-3%, chlorhexidine gluconate: 0.15-0.2% and 2-3% of emulsifier. The plant agilawood-flavor oral cavity atomized liquid has a sterilization effect, can kill various bacteria in the oral cavity, contains watermelon frost, borneol and peppermint oil, can play a good role in diminishing inflammation and healing ulcer in the oral cavity, has a strong quality effect on pathological ozostomia caused by oral ulcer and gingivitis, is agilawood-flavor, has strong and long-lasting fragrance, has a good covering effect on the ozostomia, is fresh and sweet when being taken, and has the advantages of convenience in carrying and use.
Description
Technical Field
The invention relates to the technical field of breath freshening products, in particular to a plant agilawood-flavor oral cavity atomized liquid and a preparation method thereof.
Background
Along with the continuous development of economy in China, the living standard of people is greatly improved, the social image of people is more and more emphasized, halitosis can be caused due to the problems of smoking, staying up all night, eating and the like, and when the halitosis problem occurs, people usually chew chewing gum to eliminate halitosis, so that the influence on other people is avoided.
However, chewing gum can only block the odor of physiological halitosis caused by eating onion, garlic and the like, but does not have the sterilization effect, so that the chewing gum has no effect on pathological halitosis caused by gingivitis, canker sore and the like, and chewing gum or xylitol and the like in the prior art are mostly fruity and have monotonous odor, so that a plant agilawood-flavor type oral cavity atomized liquid is provided.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides the plant agilawood-flavor oral cavity atomized liquid.
The invention provides a plant agilawood-flavor oral cavity atomized liquid which comprises the following components in percentage by mass: agilawood essential oil: 7-9%, deionized water: 67-76%, peppermint oil: 2-4%, absolute ethyl alcohol: 2-4% and watermelon frost: 1-1.5%, sodium benzoate: 0.3-0.5%, honey: 7-9%, borneol: 2-3%, chlorhexidine gluconate: 0.15-0.2% and 2-3% of emulsifier.
Preferably, the composition comprises the following components in percentage by mass: peppermint oil: 8%, polyvinylpyrrolidone: agilawood essential oil: 8% and deionized water: 70.72%, peppermint oil: 3%, absolute ethyl alcohol: 3.5% and watermelon frost: 1.2%, sodium benzoate: 0.4%, honey: 8% and borneol: 2.5%, chlorhexidine gluconate: 0.18 percent and 2.5 percent of emulsifier.
The preparation method comprises the following steps:
t1: preparing raw materials: the preparation method comprises the steps of purchasing agilawood essential oil, deionized water, peppermint oil, absolute ethyl alcohol, watermelon crystal, sodium benzoate, honey, borneol and chlorhexidine gluconate with high quality from a regular market, and weighing the components by using an electronic scale according to the required amount of the components.
T2: preparing a base liquid: and putting the weighed deionized water, the agilawood essential oil, the emulsifier and the peppermint oil into a reaction kettle, stirring for 20-30min, continuously heating during stirring, setting the heating temperature at 60-70 ℃, and obtaining the agilawood base liquid A after stirring.
T3: fusing borneol: putting the weighed absolute ethyl alcohol of T1 into a clean vessel, then pouring borneol into the vessel, and stirring by using a stirring rod until the borneol is completely fused in the absolute ethyl alcohol to obtain borneol fusion liquid B;
t4: preparing a semi-finished product: after the agilawood base liquid A described by T2 is cooled to a certain temperature, the borneol fusion liquid B described by T3 is poured into the agilawood base liquid A, a stirring motor of a reaction kettle is started to stir, 2-3min later, the weighed watermelon frost, sodium benzoate, honey and chlorhexidine gluconate described by T1 are sequentially put into the reaction kettle, and after all the components are added, the semi-finished agilawood atomized liquid C can be obtained after continuous stirring for a period of time.
T5: and (3) sterilization treatment: and (3) sterilizing the semi-finished agilawood atomized liquid A obtained in the step T4 by a pasteurization machine for two times, controlling the sterilization temperature at 62-65 ℃ each time, and keeping the sterilization temperature for 30min to obtain a finished agilawood atomized liquid D after the sterilization is finished.
T6: filling and packaging: and after T5, filling the finished product agilawood atomized liquid D into the spray bottle through a spray filling machine, and after filling, packaging the spray bottle filled with the finished product agilawood atomized liquid D by using a packaging machine.
Preferably, in the T1, the electronic scale is I2000, and the specification is 3Kg/0.1 g.
Preferably, in the T2, the model of the reaction kettle is S212-10L, and the rotating speed of the motor is set at 600r/min in the stirring process.
Preferably, in the T4, the motor rotation speed is 180-300r/min, and after all the components are added, the continuous stirring time is 15-20 r/min.
Preferably, in T5, before sterilization, floating foam on the upper layer of the semi-finished product of the agilawood atomized liquid C needs to be removed in advance, and then the semi-finished product of the agilawood atomized liquid C is filtered by using a filtering device to remove impurities that may also exist in the liquid.
Preferably, in the T6, before filling, the spray bottle used for filling needs to be subjected to vacuum sterilization treatment.
The invention has the beneficial effects that: the plant agilawood-flavor oral cavity atomized liquid disclosed by the invention is simple in preparation process, the contained chlorhexidine gluconate has a broad-spectrum sterilization effect and can kill various bacteria in the oral cavity, the contained watermelon frost, borneol and mint oil can play a good anti-inflammation and healing role on ulcer parts in the oral cavity, the osmotic force is strong, the atomized liquid has a strong quality effect on pathological halitosis caused by oral ulcer and gingivitis, the atomized liquid is agilawood-flavor, the fragrance is strong and long-lasting, the halitosis masking effect is good, the mint oil and honey are added, so that the spray is fresh and sweet when entering the mouth, and the atomized liquid is sprayed by adopting an atomizing agent bottle, so that the plant agilawood-flavor oral cavity atomized liquid has the advantages of convenience in carrying and use.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
Example one
The embodiment provides a plant agilawood oral cavity atomized liquid which comprises the following components in percentage by mass: agilawood essential oil: 8% and deionized water: 70.72%, peppermint oil: 3%, absolute ethyl alcohol: 3.5% and watermelon frost: 1.2%, sodium benzoate: 0.4%, honey: 8% and borneol: 2.5%, chlorhexidine gluconate: 0.18 percent of emulsifier and 2.5 percent of emulsifier;
the manufacturing method comprises the following steps:
t1: preparing raw materials: the preparation method comprises the steps of purchasing agilawood essential oil, deionized water, peppermint oil, absolute ethyl alcohol, watermelon crystal, sodium benzoate, honey, borneol and chlorhexidine gluconate with high quality from a regular market, and weighing the components by using an electronic scale according to the required amount of the components.
T2: preparing a base liquid: and putting the weighed deionized water, the agilawood essential oil, the emulsifier and the peppermint oil into a reaction kettle, stirring for 25min, continuously heating during stirring, setting the heating temperature at 68 ℃, and obtaining the agilawood base liquid A after stirring.
T3: fusing borneol: putting the weighed absolute ethyl alcohol of T1 into a clean vessel, then pouring borneol into the vessel, and stirring by using a stirring rod until the borneol is completely fused in the absolute ethyl alcohol to obtain borneol fusion liquid B;
t4: preparing a semi-finished product: after the agilawood base liquid A of T2 is cooled to a certain temperature, the borneol fusion liquid B of T3 is poured into the agilawood base liquid A, a stirring motor of a reaction kettle is started to stir, after 3min, the weighed watermelon frost, sodium benzoate, honey and chlorhexidine gluconate of T1 are sequentially poured into the reaction kettle, and after all the components are added, the semi-finished agilawood atomized liquid C can be obtained after continuous stirring for a period of time.
T5: and (3) sterilization treatment: and (3) sterilizing the semi-finished agilawood atomized liquid A obtained in the step T4 by a pasteurization machine twice, controlling the sterilization temperature at 65 ℃ each time, and keeping the sterilization temperature for 30min to obtain a finished agilawood atomized liquid D after sterilization.
T6: filling and packaging: and after T5, filling the finished product agilawood atomized liquid D into the spray bottle through a spray filling machine, and after filling, packaging the spray bottle filled with the finished product agilawood atomized liquid D by using a packaging machine.
The method comprises the following steps of performing vacuum sterilization on an aerosol bottle used for filling in T6, wherein the model of an electronic scale in T1 is I2000, the specification is 3Kg/0.1g, the model of a reaction kettle in T2 is S212-10L, the rotating speed of a motor in the stirring process is set at 600r/min, the rotating speed of the motor in T4 is 180r/min, the continuous stirring time is 15min after all components are added, floating foam on the upper layer of a semi-finished product agilawood atomized liquid C needs to be removed in advance before sterilization in T5, then the semi-finished product atomized liquid C is filtered by using a filtering device, impurities which can also exist in the liquid are removed, and the vacuum sterilization is performed on the aerosol bottle used for filling in T6 before filling.
Example two
The embodiment provides a plant agilawood oral cavity atomized liquid which comprises the following components in percentage by mass: agilawood essential oil: 8.5%, deionized water: 69.3%, peppermint oil: 3.5%, absolute ethyl alcohol: 3.5% and watermelon frost: 1.5%, sodium benzoate: 0.5%, honey: 9% and borneol: 2%, chlorhexidine gluconate: 0.2 percent of emulsifier and 2 percent of emulsifier;
the manufacturing method comprises the following steps:
t1: preparing raw materials: the preparation method comprises the steps of purchasing agilawood essential oil, deionized water, peppermint oil, absolute ethyl alcohol, watermelon crystal, sodium benzoate, honey, borneol and chlorhexidine gluconate with high quality from a regular market, and weighing the components by using an electronic scale according to the required amount of the components.
T2: preparing a base liquid: and putting the weighed deionized water, the agilawood essential oil, the emulsifier and the peppermint oil into a reaction kettle, stirring for 25min, continuously heating during stirring, setting the heating temperature at 68 ℃, and obtaining the agilawood base liquid A after stirring.
T3: fusing borneol: putting the weighed absolute ethyl alcohol of T1 into a clean vessel, then pouring borneol into the vessel, and stirring by using a stirring rod until the borneol is completely fused in the absolute ethyl alcohol to obtain borneol fusion liquid B;
t4: preparing a semi-finished product: after the agilawood base liquid A of T2 is cooled to a certain temperature, the borneol fusion liquid B of T3 is poured into the agilawood base liquid A, a stirring motor of a reaction kettle is started to stir, after 3min, the weighed watermelon frost, sodium benzoate, honey and chlorhexidine gluconate of T1 are sequentially poured into the reaction kettle, and after all the components are added, the semi-finished agilawood atomized liquid C can be obtained after continuous stirring for a period of time.
T5: and (3) sterilization treatment: and (3) sterilizing the semi-finished agilawood atomized liquid A obtained in the step T4 by a pasteurization machine twice, controlling the sterilization temperature at 65 ℃ each time, and keeping the sterilization temperature for 30min to obtain a finished agilawood atomized liquid D after sterilization.
T6: filling and packaging: and after T5, filling the finished product agilawood atomized liquid D into the spray bottle through a spray filling machine, and after filling, packaging the spray bottle filled with the finished product agilawood atomized liquid D by using a packaging machine.
The method comprises the following steps of performing vacuum sterilization on an aerosol bottle used for filling in T6, wherein the model of an electronic scale in T1 is I2000, the specification is 3Kg/0.1g, the model of a reaction kettle in T2 is S212-10L, the rotating speed of a motor in the stirring process is set at 450r/min, the rotating speed of the motor in T4 is 180r/min, the continuous stirring time is 15min after all components are added, floating foam on the upper layer of a semi-finished product agilawood atomized liquid C needs to be removed in advance before sterilization in T5, then the semi-finished product atomized liquid C is filtered by using a filtering device, impurities which can also exist in the liquid are removed, and the vacuum sterilization is performed on the aerosol bottle used for filling in T6 before filling.
EXAMPLE III
The embodiment provides a plant agilawood oral cavity atomized liquid which comprises the following components in percentage by mass: agilawood essential oil: 9% and deionized water: 71.45%, peppermint oil: 2%, absolute ethyl alcohol: 3% and watermelon frost: 1.3%, sodium benzoate: 0.5%, honey: 7% and borneol: 2.8%, chlorhexidine gluconate: 0.15 percent of emulsifier and 2.8 percent of emulsifier;
the manufacturing method comprises the following steps:
t1: preparing raw materials: the preparation method comprises the steps of purchasing agilawood essential oil, deionized water, peppermint oil, absolute ethyl alcohol, watermelon crystal, sodium benzoate, honey, borneol and chlorhexidine gluconate with high quality from a regular market, and weighing the components by using an electronic scale according to the required amount of the components.
T2: preparing a base liquid: and putting the weighed deionized water, the agilawood essential oil, the emulsifier and the peppermint oil into a reaction kettle, stirring for 30min, continuously heating during stirring, setting the heating temperature at 62 ℃, and obtaining the agilawood base liquid A after stirring.
T3: fusing borneol: putting the weighed absolute ethyl alcohol of T1 into a clean vessel, then pouring borneol into the vessel, and stirring by using a stirring rod until the borneol is completely fused in the absolute ethyl alcohol to obtain borneol fusion liquid B;
t4: preparing a semi-finished product: after the agilawood base liquid A of T2 is cooled to a certain temperature, the borneol fusion liquid B of T3 is poured into the agilawood base liquid A, a stirring motor of a reaction kettle is started to stir, after 3min, the weighed watermelon frost, sodium benzoate, honey and chlorhexidine gluconate of T1 are sequentially poured into the reaction kettle, and after all the components are added, the semi-finished agilawood atomized liquid C can be obtained after continuous stirring for a period of time.
T5: and (3) sterilization treatment: and (3) sterilizing the semi-finished agilawood atomized liquid A obtained in the step T4 by a pasteurization machine twice, controlling the sterilization temperature at 63 ℃ each time, and keeping the sterilization temperature for 30min to obtain a finished agilawood atomized liquid D after sterilization.
T6: filling and packaging: and after T5, filling the finished product agilawood atomized liquid D into the spray bottle through a spray filling machine, and after filling, packaging the spray bottle filled with the finished product agilawood atomized liquid D by using a packaging machine.
The method comprises the following steps of performing vacuum sterilization on an aerosol bottle used for filling in T6, wherein the model of an electronic scale in T1 is I2000, the specification is 3Kg/0.1g, the model of a reaction kettle in T2 is S212-10L, the rotating speed of a motor in the stirring process is set at 600r/min, the rotating speed of the motor in T4 is 300r/min, the continuous stirring time is 18min after all components are added, floating foam on the upper layer of a semi-finished product agilawood atomized liquid C needs to be removed in advance before sterilization in T5, then the semi-finished product atomized liquid C is filtered by using a filtering device, impurities which can also exist in the liquid are removed, and the vacuum sterilization is performed on the aerosol bottle used for filling in T6 before filling.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (8)
1. The plant agilawood oral cavity atomized liquid is characterized by comprising the following components in percentage by mass: agilawood essential oil: 7-9%, deionized water: 67-76%, peppermint oil: 2-4%, absolute ethyl alcohol: 2-4% and watermelon frost: 1-1.5%, sodium benzoate: 0.3-0.5%, honey: 7-9%, borneol: 2-3%, chlorhexidine gluconate: 0.15-0.2% and 2-3% of emulsifier.
2. The plant agilawood-flavor oral cavity atomizing liquid as claimed in claim 1, which is characterized by comprising the following components in percentage by mass: agilawood essential oil: 8% and deionized water: 70.72%, peppermint oil: 3%, absolute ethyl alcohol: 3.5% and watermelon frost: 1.2%, sodium benzoate: 0.4%, honey: 8% and borneol: 2.5%, chlorhexidine gluconate: 0.18 percent and 2.5 percent of emulsifier.
3. A preparation method of plant agilawood-flavor oral cavity atomized liquid is characterized by comprising the following steps:
t1: preparing raw materials: purchasing agilawood essential oil, deionized water, peppermint oil, absolute ethyl alcohol, watermelon crystal, sodium benzoate, honey, borneol and chlorhexidine gluconate with higher quality from a regular market, and weighing each component by using an electronic scale according to the required amount of each component;
t2: preparing a base liquid: putting the weighed deionized water, agilawood essential oil, emulsifier and peppermint oil into a reaction kettle, stirring for 20-30min, continuously heating during stirring, setting the heating temperature at 60-70 ℃, and obtaining agilawood base liquid A after stirring;
t3: fusing borneol: putting the weighed absolute ethyl alcohol of T1 into a clean vessel, then pouring borneol into the vessel, and stirring by using a stirring rod until the borneol is completely fused in the absolute ethyl alcohol to obtain borneol fusion liquid B;
t4: preparing a semi-finished product: after the agilawood base liquid A of T2 is cooled to a certain temperature, firstly pouring the borneol fusion liquid B of T3 into the agilawood base liquid A, starting a stirring motor of a reaction kettle to stir for 2-3min, then sequentially putting the weighed watermelon frost, sodium benzoate, honey and chlorhexidine gluconate of T1 into the reaction kettle, and after all the components are added, continuously stirring for a period of time to obtain a semi-finished agilawood atomized liquid C;
t5: and (3) sterilization treatment: sterilizing the semi-finished product agilawood atomized liquid A described in T4 by a pasteurization machine twice, controlling the sterilization temperature at 62-65 ℃ each time, and keeping the sterilization temperature for 30min to obtain a finished product agilawood atomized liquid D;
t6: filling and packaging: and after T5, filling the finished product agilawood atomized liquid D into the spray bottle through a spray filling machine, and after filling, packaging the spray bottle filled with the finished product agilawood atomized liquid D by using a packaging machine.
4. The method for preparing the plant agilawood-flavor oral cavity atomizing liquid as claimed in claim 3, wherein in T1, an electronic scale is I2000, and the specification is 3Kg/0.1 g.
5. The method for preparing the plant agilawood-flavor oral cavity atomizing liquid as claimed in claim 3, wherein in T2, the model of the reaction kettle is S212-10L, and the rotation speed of the motor is set at 600r/min during stirring.
6. The method as claimed in claim 3, wherein the motor speed is 180-300r/min in T4, and the stirring time is 15-20min after all the components are added.
7. The method according to claim 3, wherein said T5 is prepared by removing the floating foam on the upper layer of the semi-finished product of lignum Aquilariae Resinatum atomized liquid C before sterilization, and then filtering the semi-finished product of lignum Aquilariae Resinatum atomized liquid C with a filter to remove impurities.
8. The method for preparing the plant agilawood-flavor oral cavity atomizing liquid as claimed in claim 3, wherein in T6, a spray bottle used for filling needs to be subjected to vacuum sterilization treatment before filling.
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