CN111494263A - Plant tea-flavored oral cavity atomized liquid and preparation method thereof - Google Patents
Plant tea-flavored oral cavity atomized liquid and preparation method thereof Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
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- A—HUMAN NECESSITIES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/34—Alcohols
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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Abstract
The invention discloses a plant tea flavor oral cavity atomized liquid and a preparation method thereof, wherein the plant tea flavor oral cavity atomized liquid comprises the following components in percentage by mass: deionized water: 50-60%, sorbitol: 1-3%, peppermint oil: 7-9%, ethanol: 2-5%, Tieguanyin tea: 8-10%, methylparaben: 1-2%, sucralose: 5-7%, thymol: 6-8% of eucalyptol: 5-7%, methyl salicylate: 4-7 percent. The invention has the beneficial effects that: the plant tea-flavored oral cavity atomized liquid has a simple preparation process, and can clean and protect the oral cavity while freshening the breath.
Description
Technical Field
The invention relates to the technical field of oral protection, in particular to a plant tea-flavored oral atomized liquid and a preparation method thereof.
Background
The halitosis is odor emitted from the oral cavity or other cavities filled with air, such as the nose, the paranasal sinuses and the pharynx, which seriously affects social interaction and mental health of people, causes of halitosis formation are related to oral hygiene, and halitosis is easily formed because food is remained in the oral cavity and bacteria are easily bred, so that the halitosis is usually eliminated by chewing gum and the like at present.
However, the chewing time of the chewing gum is too long, which can cause adverse effects on intestines and stomach, and simultaneously can not protect the oral cavity, so that a plant tea flavor oral cavity atomized liquid and a preparation method thereof are provided.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a plant tea flavor oral cavity atomized liquid and a preparation method thereof.
The invention provides a plant tea-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: deionized water: 50-60%, sorbitol: 1-3%, peppermint oil: 7-9%, ethanol: 2-5%, Tieguanyin tea: 8-10%, methylparaben: 1-2%, sucralose: 5-7%, thymol: 6-8% of eucalyptol: 5-7%, methyl salicylate: 4-7 percent.
Preferably, the composition comprises the following components in percentage by mass: deionized water: 53%, sorbitol: 2%, peppermint oil: 8% and ethanol: 3% and Tieguanyin tea: 6%, methylparaben: 1% and sucralose: 6%, thymol: 7%, eucalyptol: 6%, methyl salicylate: 5 percent.
The preparation method comprises the following steps:
s1: selecting raw materials: deionized water, sorbitol, oleum Menthae Dementholatum, ethanol, Tieguanyin tea, methyl hydroxybenzoate, sucralose, thymol, eucalyptol, and methyl salicylate with high quality are purchased from regular markets.
S2: preparing raw materials: and in an aseptic environment, weighing the raw materials in the step S1 one by using an electronic scale according to a required proportion, and ensuring the accuracy of the used amount of the raw materials.
S3: boiling the deionized water of S2, brewing Tieguanyin tea, filtering the tea after 1 hour to obtain tea water, sequentially pouring the tea water, sorbitol, peppermint oil, ethanol, methyl hydroxybenzoate and sucralose into a full-automatic liquid medicine stirring pot, and then stirring uniformly to obtain an original base liquid A;
s4: preparing a finished product liquid: and after S3 is finished, sequentially adding the weighed thymol, eucalyptol and methyl salicylate in S2 into the original base solution A, and stirring uniformly to obtain the finished tea flavor refreshing sterilizing solution B.
S5: and (4) inspecting a finished product: and (5) extracting the finished product tea flavor refreshing sterilizing liquid B in the step (S4), and then sending the extracted sample to a detection room for safety detection and oral sterilization detection.
S6: and (4) storing the finished liquid: and (5) after S5 is finished and the detection result is qualified, pouring the finished product of the tea flavor refreshing and sterilizing liquid B obtained in the step (S4) into an atomization bottle for sealing, and then placing the atomization bottle in a shady and cool place for storage.
Preferably, in the S2, the electronic scale is L Q-C5001, and the precision is 0.01 g.
Preferably, in S3, the model of the automatic liquid medicine stirring pot is MYJ-50, and the temperature in the pot is controlled at 20-25 deg.C and the stirring time is 4-5min during the preparation of the base liquid.
Preferably, in S4, the stirring is continued for 10min after the addition of the raw material is completed.
Preferably, in S5, the extraction amount of the fresh tea flavor sterilizing solution B is 5-10ml, and the detection result needs to satisfy the requirement of the microbial indicator of the antibacterial agent and the requirement of the microbial indicator for sterilization specified in "specification for sterilization 2002 edition".
Preferably, in the step S6, the environment temperature for storing the finished product tea flavor refreshing and sterilizing liquid B in a dark place is 10-15 ℃.
Discussion of the formulation:
the mint has special cool fragrance, can play a role in refreshing brain and relieving fatigue, has strong bactericidal and antibacterial effects, and can prevent viral influenza and oral diseases and refresh breath; sorbitol can play a moisture-retaining role in the atomized liquid, and meanwhile, the taste of the atomized liquid is increased; the ethanol can play a role in disinfection; the sucralose is added into the tea water brewed by the Tie Guanyin tea, so that the atomized liquid has a strong tea fragrance, the taste of the atomized liquid is enhanced, and the atomized liquid is more easily accepted; the methyl hydroxybenzoate is mainly used for the corrosion prevention of the atomized liquid, and the storage time of the atomized liquid is prolonged; thymol mainly aims at bacteria on oral mucosa and can protect the oral cavity; the eucalyptol can reduce oral bacteria, has cool taste, and can relieve halitosis; the methyl salicylate can clean oral cavity.
The invention has the beneficial effects that: the plant tea-flavored oral cavity atomized liquid disclosed by the invention is simple in preparation process, has a strong tea flavor, and can clean and protect the oral cavity while refreshing the breath.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
Example one
The embodiment provides a plant tea-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: deionized water: 54%, sorbitol: 1%, peppermint oil: 8% and ethanol: 4%, Tieguanyin tea: 7%, methylparaben: 1% and sucralose: 7%, thymol: 7%, eucalyptol: 6%, methyl salicylate: 5 percent;
the manufacturing method comprises the following steps:
s1: selecting raw materials: deionized water, sorbitol, oleum Menthae Dementholatum, ethanol, Tieguanyin tea, methyl hydroxybenzoate, sucralose, thymol, eucalyptol, and methyl salicylate with high quality are purchased from regular markets.
S2: preparing raw materials: and in an aseptic environment, weighing the raw materials in the step S1 one by using an electronic scale according to a required proportion, and ensuring the accuracy of the used amount of the raw materials.
S3: preparing a base liquid: preparing a base liquid: boiling the deionized water of S2, brewing Tieguanyin tea, filtering the tea after 1 hour to obtain tea water, sequentially pouring the tea water, sorbitol, peppermint oil, ethanol, methyl hydroxybenzoate and sucralose into a full-automatic liquid medicine stirring pot, and then stirring uniformly to obtain an original base liquid A;
s4: preparing a finished product liquid: and after S3 is finished, sequentially adding the weighed thymol, eucalyptol and methyl salicylate in S2 into the original base solution A, and stirring uniformly to obtain the finished tea flavor refreshing sterilizing solution B.
S5: and (4) inspecting a finished product: and (5) extracting the finished product tea flavor refreshing sterilizing liquid B in the step (S4), and then sending the extracted sample to a detection room for safety detection and oral sterilization detection.
S6: and (4) storing the finished liquid: and (5) after S5 is finished and the detection result is qualified, pouring the finished product of the tea flavor refreshing and sterilizing liquid B obtained in the step (S4) into an atomization bottle for sealing, and then placing the atomization bottle in a shady and cool place for storage.
In S2, the model of an electronic scale is L Q-C5001, the precision is 0.01g, in S3, the model of a liquid medicine full-automatic stirring pot is MYJ-50, the temperature in the pot is controlled to be 20-25 ℃ when base liquid is prepared, the stirring time is 4-5min, in S4, after the raw materials are added, the continuous stirring time is 10min, in S5, the extraction amount of tea flavor fresh sterilizing liquid B is 5-10ml, the detection result needs to meet the microbial indicator and microbe killing indicator requirements of an antibacterial agent specified in the technical specification 2002 edition of disinfection, and in S6, the environment temperature for storing the finished tea flavor fresh sterilizing liquid B in a dark place is 10-15 ℃.
Example two
The embodiment provides a plant tea-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: 54%, sorbitol: 2%, peppermint oil: 7%, ethanol: 4%, Tieguanyin tea: 8%, methylparaben: 1% and sucralose: 7%, thymol: 6% and eucalyptol: 7%, methyl salicylate: 4 percent;
the manufacturing method comprises the following steps:
s1: selecting raw materials: deionized water, sorbitol, oleum Menthae Dementholatum, ethanol, Tieguanyin tea, methyl hydroxybenzoate, sucralose, thymol, eucalyptol, and methyl salicylate with high quality are purchased from regular markets.
S2: preparing raw materials: and in an aseptic environment, weighing the raw materials in the step S1 one by using an electronic scale according to a required proportion, and ensuring the accuracy of the used amount of the raw materials.
S3: preparing a base liquid: boiling the deionized water of S2, brewing Tieguanyin tea, filtering the tea after 1 hour to obtain tea water, sequentially pouring the tea water, sorbitol, peppermint oil, ethanol, methyl hydroxybenzoate and sucralose into a full-automatic liquid medicine stirring pot, and then stirring uniformly to obtain an original base liquid A;
s4: preparing a finished product liquid: and after S3 is finished, sequentially adding the weighed thymol, eucalyptol and methyl salicylate in S2 into the original base solution A, and stirring uniformly to obtain the finished tea flavor refreshing sterilizing solution B.
S5: and (4) inspecting a finished product: and (5) extracting the finished product tea flavor refreshing sterilizing liquid B in the step (S4), and then sending the extracted sample to a detection room for safety detection and oral sterilization detection.
S6: and (4) storing the finished liquid: and (5) after S5 is finished and the detection result is qualified, pouring the finished product of the tea flavor refreshing and sterilizing liquid B obtained in the step (S4) into an atomization bottle for sealing, and then placing the atomization bottle in a shady and cool place for storage.
In S2, the model of an electronic scale is L Q-C5001, the precision is 0.01g, in S3, the model of a liquid medicine full-automatic stirring pot is MYJ-50, the temperature in the pot is controlled to be 20-25 ℃ during preparation of base liquid, the stirring time is 4-5min, in S4, after the raw materials are added, the continuous stirring time is 10min, in S5, the extraction amount of the tea flavor fresh sterilizing liquid B is 5-10ml, and the detection result needs to meet the microbial indicator and microbial indicator killing requirement of an antibacterial agent specified in the disinfection technical specification 2002 edition, and in S6, the environment temperature for storing the finished tea flavor fresh sterilizing liquid B in a dark place is 10-15 ℃.
EXAMPLE III
The embodiment provides a plant tea-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: deionized water: 56%, sorbitol: 1%, peppermint oil: 6% and ethanol: 3% and Tieguanyin tea: 7%, methylparaben: 1% and sucralose: 7%, thymol: 8% and eucalyptol: 6%, methyl salicylate: 5 percent;
the manufacturing method comprises the following steps:
s1: selecting raw materials: deionized water, sorbitol, oleum Menthae Dementholatum, ethanol, Tieguanyin tea, methyl hydroxybenzoate, sucralose, thymol, eucalyptol, and methyl salicylate with high quality are purchased from regular markets.
S2: preparing raw materials: and in an aseptic environment, weighing the raw materials in the step S1 one by using an electronic scale according to a required proportion, and ensuring the accuracy of the used amount of the raw materials.
S3: preparing a base liquid: preparing a base liquid: boiling the deionized water of S2, brewing Tieguanyin tea, filtering the tea after 1 hour to obtain tea water, sequentially pouring the tea water, sorbitol, peppermint oil, ethanol, methyl hydroxybenzoate and sucralose into a full-automatic liquid medicine stirring pot, and then stirring uniformly to obtain an original base liquid A;
s4: preparing a finished product liquid: and after S3 is finished, sequentially adding the weighed thymol, eucalyptol and methyl salicylate in S2 into the original base solution A, and stirring uniformly to obtain the finished tea flavor refreshing sterilizing solution B.
S5: and (4) inspecting a finished product: and (5) extracting the finished product tea flavor refreshing sterilizing liquid B in the step (S4), and then sending the extracted sample to a detection room for safety detection and oral sterilization detection.
S6: and (4) storing the finished liquid: and (5) after S5 is finished and the detection result is qualified, pouring the finished product of the tea flavor refreshing and sterilizing liquid B obtained in the step (S4) into an atomization bottle for sealing, and then placing the atomization bottle in a shady and cool place for storage.
In S2, the model of an electronic scale is L Q-C5001, the precision is 0.01g, in S3, the model of a liquid medicine full-automatic stirring pot is MYJ-50, the temperature in the pot is controlled to be 20-25 ℃ during preparation of base liquid, the stirring time is 4-5min, in S4, after the raw materials are added, the continuous stirring time is 10min, in S5, the extraction amount of the tea flavor fresh sterilizing liquid B is 5-10ml, and the detection result needs to meet the microbial indicator and microbial indicator killing requirement of an antibacterial agent specified in the disinfection technical specification 2002 edition, and in S6, the environment temperature for storing the finished tea flavor fresh sterilizing liquid B in a dark place is 10-15 ℃.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (8)
1. The plant tea-flavored oral atomized liquid is characterized by comprising the following components in percentage by mass: deionized water: 50-60%, sorbitol: 1-3%, peppermint oil: 7-9%, ethanol: 2-5%, Tieguanyin tea: 8-10%, methylparaben: 1-2%, sucralose: 5-7%, thymol: 6-8% of eucalyptol: 5-7%, methyl salicylate: 4-7 percent.
2. The plant tea flavor oral cavity atomized liquid as claimed in claim 1, which comprises the following components by mass percent: deionized water: 53%, sorbitol: 2%, peppermint oil: 7%, ethanol: 4%, Tieguanyin tea: 8%, methylparaben: 1% and sucralose: 7%, thymol: 7%, eucalyptol: 6%, methyl salicylate: 5 percent.
3. A preparation method of plant tea flavor oral cavity atomized liquid is characterized by comprising the following steps:
s1: selecting raw materials: purchasing high-quality deionized water, sorbitol, oleum Menthae Dementholatum, ethanol, Tieguanyin tea, methyl hydroxybenzoate, sucralose, thymol, eucalyptol and methyl salicylate from regular market;
s2: preparing raw materials: in an aseptic environment, the raw materials in S1 are weighed one by using an electronic scale according to a required proportion, so that the accuracy of the used amount of the raw materials is ensured;
s3: preparing a base liquid: boiling the deionized water of S2, brewing Tieguanyin tea, filtering the tea after 1 hour to obtain tea water, sequentially pouring the tea water, sorbitol, peppermint oil, ethanol, methyl hydroxybenzoate and sucralose into a full-automatic liquid medicine stirring pot, and then stirring uniformly to obtain an original base liquid A;
s4: preparing a finished product liquid: after S3 is finished, sequentially adding the weighed thymol, eucalyptol and methyl salicylate in S2 into the original base solution A, and stirring uniformly to obtain a finished product tea flavor refreshing sterilizing solution B;
s5: and (4) inspecting a finished product: extracting the finished product tea flavor refreshing sterilizing liquid B in the step S4, and then sending the extracted sample to a detection room for safety detection and oral sterilization detection;
s6: and (4) storing the finished liquid: and (5) after S5 is finished and the detection result is qualified, pouring the finished product of the tea flavor refreshing and sterilizing liquid B obtained in the step (S4) into an atomization bottle for sealing, and then placing the atomization bottle in a shady and cool place for storage.
4. The method for preparing the plant tea flavor oral cavity atomizing liquid as claimed in claim 3, wherein in S2, an electronic scale is L Q-C5001, and the precision is 0.01 g.
5. The method of claim 3, wherein in S3, the type of the automatic stirring pot for medicinal liquid is MYJ-50, and the temperature in the pot is controlled at 20-25 deg.C and the stirring time is 4-5 min.
6. The method for preparing the plant tea flavor oral cavity atomizing liquid as claimed in claim 3, wherein in the step S4, after the raw materials are added, the stirring is continued for 10 min.
7. The method for preparing the plant tea flavor oral cavity atomized liquid as claimed in claim 3, wherein in S5, the extraction amount of the tea flavor fresh sterilizing liquid B is 5-10ml, and the detection result needs to meet the requirement of microbial indexes of antibacterial agents and microbe killing indexes specified in the technical Specification for disinfection 2002 edition.
8. The method for preparing the plant tea flavor oral cavity atomized liquid as claimed in claim 3, wherein in S6, the ambient temperature for storing the finished product tea flavor fresh sterilizing liquid B in dark is 10-15 ℃.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114306141A (en) * | 2021-12-31 | 2022-04-12 | 赣南医学院 | Active composition for mouthwash, mouthwash and preparation method of active composition |
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2020
- 2020-04-30 CN CN202010360705.XA patent/CN111494263A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106163491A (en) * | 2014-03-27 | 2016-11-23 | 烧津水产化学工业株式会社 | Oral cavity bacterium antiblastic |
| CN105232781A (en) * | 2015-11-05 | 2016-01-13 | 周菊香 | Spray for removing bad breath, and preparation method thereof |
| CN107007688A (en) * | 2017-05-03 | 2017-08-04 | 沈阳恒泽医药技术有限公司 | Treat medicinal herb spray of oral inflammation and preparation method thereof |
| CN107714530A (en) * | 2017-09-26 | 2018-02-23 | 西安罗格斯生物科技有限公司 | It is a kind of to be used to remove removing abnormal flavor in oral cavity, antibacterial, fresh breath oral hygiene spray |
| CN107875243A (en) * | 2017-11-24 | 2018-04-06 | 张龙兵 | Spray liquid for fresh breath |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114306141A (en) * | 2021-12-31 | 2022-04-12 | 赣南医学院 | Active composition for mouthwash, mouthwash and preparation method of active composition |
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Application publication date: 20200807 |