CN108968172A - A kind of preparation method of health care underwear - Google Patents
A kind of preparation method of health care underwear Download PDFInfo
- Publication number
- CN108968172A CN108968172A CN201810625334.6A CN201810625334A CN108968172A CN 108968172 A CN108968172 A CN 108968172A CN 201810625334 A CN201810625334 A CN 201810625334A CN 108968172 A CN108968172 A CN 108968172A
- Authority
- CN
- China
- Prior art keywords
- health care
- solution
- preparation
- fiber
- chitosan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B17/00—Selection of special materials for underwear
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B9/00—Undergarments
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D1/00—Garments
- A41D1/04—Vests, jerseys, sweaters or the like
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D31/00—Materials specially adapted for outerwear
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
- A41B2400/20—Air permeability; Ventilation
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
- A41B2400/34—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass antimicrobial or antibacterial
Abstract
The present invention relates to a kind of preparation methods of health care underwear.Sodium hyaluronate, vitamin and collagen are encapsulated in chitosan microcapsules first with microencapsulation to prepare chitosan microcapsules powder by the preparation method；Then fiber spinning solution is prepared in nano-cellulose, chitosan microcapsules powder, natural, water, spin finish aid after mixing, dry the health fiber after electrostatic spinning is handled；Finally by the cotton fiber of health fiber and hydrophobically modified carry out it is blended after to get health fiber fabric, after clipped sewing health care underwear.Not only there is antibiotic health care function through health care underwear prepared by the present invention, and have both that skin-friendly is good, sucting wet air permeability it is strong wear experience sense.
Description
Technical field
The present invention relates to underwear preparation technical field, specially a kind of preparation method of health care underwear.
Background technique
With the improvement of living standards, people are also more next to the comfortableness and security requirement of the underwear product worn next to the skin
It is higher.In recent years, domestic many areas all have launched the underwear of many new varieties and new pattern, and some of them have function
Property, dicoration and comfort underwear product, it is such as various can the underwear of body shaping, aloe underwear, water bag underwear, remote red
Outer underwear, bamboo charcoal underwear, antibacterial and deodorizing underwear and all kinds of cold-proof underwears etc..
Nowadays, as people's lives pressure is increasing and the high speed development of electronic product, so that people rest
Deficiency, many human bodies are in sub-health state, therefore the underwear product for developing healthcare function will have great importance.
Summary of the invention
In order to meet the health care energy requirement of underwear, consumer is solved because life stress is big and ignores asking for itself health care
Topic, the present invention provides a kind of health care underwears.
To solve the above-mentioned problems, the preparation method for a kind of health care underwear that this hair provides, which is characterized in that including following
Step:
(1) after chitosan being dissolved in acetum under the mixing speed of 600-1000rpm/min, anhydrous calcium chloride is added, stirs
It mixes dissolution and prepares chitosan calcium chloride solution；
(2) sodium hyaluronate, vitamin and collagen are dissolved in the Arabic gum aqueous solution prepared, will contain sodium hyaluronate,
The Arabic gum aqueous solution of vitamin and collagen is slowly dropped in isometric chitosan calcium chloride solution, in 40-
In 55 DEG C of water-baths, after stirring 10-20min under the conditions of 400-600rpm/min, add the distilled water of 1-2 times of volume cold after mixing
But, pH value is adjusted to 7 after adding glutaraldehyde solution to solidify 90min, continues stirring 20-40 min and obtains microcapsule solution, by microcapsule solution
After being centrifuged 15 min under the conditions of 3000-4000rpm/min, supernatant is abandoned, precipitating is freeze-dried after being washed with water 2-3 times to be contained to obtain the final product
The chitosan microcapsules powder of sodium hyaluronate, vitamin and collagen；
(3) nano-cellulose, chitosan microcapsules powder, natural, water, spin finish aid are prepared after mixing
Fiber spinning solution, dry the health fiber after electrostatic spinning is handled；
(4) by the cotton fiber of health fiber and hydrophobically modified carry out it is blended after to get health fiber fabric, after clipped sewing
Health care underwear.
Preferably, the concentration of acetum as described in step (1) is 1-2%.
Preferably, in chitosan calcium chloride solution as described in step (1) chitosan concentration be 1-3%, calcium chloride it is dense
Degree is 0.1-0.5%.
Preferably, the concentration of Arabic gum is 5-8% in Arabic gum aqueous solution described in step (2)；Described contains glass
The concentration of sodium hyaluronate, vitamin and collagen is successively in the Arabic gum aqueous solution of uric acid, vitamin and collagen
For 2-5%, 3-5%, 5-10%.
Preferably, the concentration of glutaraldehyde is 25-45%, the addition matter of glutaraldehyde in glutaraldehyde solution described in step (2)
Amount is 0.1-0.2 times of chitosan.
Preferably, natural described in step (3) is vine polyphenol extract, tea polyphenols and gallic acid
One of；The spin finish aid is one of polyacrylamide, polycarbonate.
Preferably, nano-cellulose described in step (3), chitosan microcapsules powder, natural, water, spinning
Auxiliary agent is figured by mass parts and is followed successively by: 20-35 parts, 1-2 parts, 0.5-1 parts, 65-85 parts, 5-8 parts.
Preferably, the mass ratio when cotton fiber of health fiber described in step (4) and hydrophobically modified is blended is 1:
0.5-0.8。
Compared with prior art, a kind of preparation method of health care underwear of the present invention has the advantages that this
Sodium hyaluronate, vitamin and collagen are added in underwear by invention, so that underwear, which has, improves function of joint, remove skin
Surface free radical, promotion local metabolic and other effects；The present invention uses chitosan microcapsules technology by sodium hyaluronate, vitamin and glue
Former albumen is encapsulated in micro-capsule, not only be can be reduced its loss when preparing underwear and be can guarantee the slow release of active constituent；
The chitosan of addition makes fabric have good antibacterial effect；It is blended using the cotton fiber of health fiber and hydrophobically modified so that
Fabric skin-friendly is good, and sucting wet air permeability is strong.Not only there is antibiotic health care function through health care underwear prepared by the present invention, and have both pro-skin
Property is good, sucting wet air permeability it is strong wear experience sense.
Specific embodiment
[embodiment 1]
A kind of preparation method of health care underwear, which comprises the following steps:
(1) after chitosan being dissolved in 2% acetum under the mixing speed of 600rpm/min, anhydrous calcium chloride, stirring is added
Dissolution preparation contains 1.5% chitosan and 0.2% calcium chloride mixed solution；
(2) sodium hyaluronate, vitamin and collagen are dissolved in the aqueous solution containing 7% Arabic gum prepared, will be contained
4% sodium hyaluronate, 3% vitamin and the 8% Arabic gum aqueous solution of collagen are slowly dropped to isometric step
(1) in resulting chitosan calcium chloride solution, in 45 DEG C of water-baths, after stirring 20min under the conditions of 500rpm/min, add 2 times of bodies
Long-pending distilled water cools down after mixing, is adjusted to pH value after adding the glutaraldehyde solution of 0.15 times of chitosan mass to solidify 90min
7, continue 30 min of stirring and obtain microcapsule solution, after microcapsule solution is centrifuged 15 min under the conditions of 4000rpm/min, abandons supernatant
Liquid, precipitating are freeze-dried up to the chitosan microcapsules powder containing sodium hyaluronate, vitamin and collagen after being washed with water 3 times；
(3) 20 parts of nano-celluloses, 1.5 parts of chitosan microcapsules powder, 0.5 part of vine polyphenol extract, 73 parts of water, 5 parts are gathered
Fiber spinning solution is prepared in acrylamide after mixing, dry the health fiber after electrostatic spinning is handled；
(4) to get health fiber face after the mass ratio progress for the cotton fiber of health fiber and hydrophobically modified being pressed 1:0.6 is blended
Material obtains health care underwear after clipped sewing.
[embodiment 2]
A kind of preparation method of health care underwear, which comprises the following steps:
(1) after chitosan being dissolved in 2.5% acetum under the mixing speed of 800rpm/min, anhydrous calcium chloride is added, stirs
Dissolution preparation is mixed containing 2% chitosan and 0.3% calcium chloride mixed solution；
(2) sodium hyaluronate, vitamin and collagen are dissolved in the aqueous solution containing 7% Arabic gum prepared, will be contained
4.5% sodium hyaluronate, 3.5% vitamin and the 6% Arabic gum aqueous solution of collagen are slowly dropped to isometric step
Suddenly in (1) resulting chitosan calcium chloride solution, in 45 DEG C of water-baths, after stirring 20min under the conditions of 600rpm/min, add 2 times
The distilled water of volume cools down after mixing, is adjusted to pH value after adding the glutaraldehyde solution of 0.2 times of chitosan mass to solidify 90min
7, continue 30 min of stirring and obtain microcapsule solution, after microcapsule solution is centrifuged 15 min under the conditions of 4000rpm/min, abandons supernatant
Liquid, precipitating are freeze-dried up to the chitosan microcapsules powder containing sodium hyaluronate, vitamin and collagen after being washed with water 3 times；
(3) 22 parts of nano-celluloses, 2 parts of chitosan microcapsules powder, 1 part of gallic acid, 70 parts of water, 5 parts of polyacrylamides are mixed
Fiber spinning solution is prepared after closing uniformly, dry the health fiber after electrostatic spinning is handled；
(4) to get health fiber face after the mass ratio progress for the cotton fiber of health fiber and hydrophobically modified being pressed 1:0.7 is blended
Material obtains health care underwear after clipped sewing.
[embodiment 3]
A kind of preparation method of health care underwear, which comprises the following steps:
(1) after chitosan being dissolved in 2.5% acetum under the mixing speed of 800rpm/min, anhydrous calcium chloride is added, stirs
Dissolution preparation is mixed containing 2% chitosan and 0.3% calcium chloride mixed solution；
(2) sodium hyaluronate, vitamin and collagen are dissolved in the aqueous solution containing 7% Arabic gum prepared, will be contained
3% sodium hyaluronate, 4% vitamin and the 6% Arabic gum aqueous solution of collagen are slowly dropped to isometric step
(1) in resulting chitosan calcium chloride solution, in 50 DEG C of water-baths, after stirring 20min under the conditions of 600rpm/min, add 1 times of body
Long-pending distilled water cools down after mixing, and pH value is adjusted to 7 after adding the glutaraldehyde solution of 0.2 times of chitosan mass to solidify 90min,
Continue 30 min of stirring and obtain microcapsule solution, after microcapsule solution is centrifuged 15 min under the conditions of 4000rpm/min, abandons supernatant,
Precipitating is freeze-dried up to the chitosan microcapsules powder containing sodium hyaluronate, vitamin and collagen after being washed with water 3 times；
(3) by 25 parts of nano-celluloses, 1.5 parts of chitosan microcapsules powder, 1 part of gallic acid, 67 parts of water, 5.5 parts of polycarbonate
Fiber spinning solution is prepared after mixing, dry the health fiber after electrostatic spinning is handled；
(4) to get health fiber face after the mass ratio progress for the cotton fiber of health fiber and hydrophobically modified being pressed 1:0.7 is blended
Material obtains health care underwear after clipped sewing.
For the ordinary skill in the art, specific embodiment is only exemplarily described the present invention,
Obviously the present invention specific implementation is not subject to the restrictions described above, as long as use the inventive concept and technical scheme of the present invention into
The improvement of capable various unsubstantialities, or not improved the conception and technical scheme of the invention are directly applied to other occasions
, it is within the scope of the present invention.
Claims (8)
1. a kind of preparation method of health care underwear, which comprises the following steps:
(1) chitosan is dissolved under the mixing speed of 600-1000rpm/min acetum, anhydrous calcium chloride, stirring is added
Dissolution prepares chitosan calcium chloride solution；
(2) sodium hyaluronate, vitamin and collagen are dissolved in the Arabic gum aqueous solution prepared, will contain sodium hyaluronate,
The Arabic gum aqueous solution of vitamin and collagen is slowly dropped in isometric chitosan calcium chloride solution, in 40-
In 55 DEG C of water-baths, 10-20min is stirred under the conditions of 400-600rpm/min, adds the distilled water of 1-2 times of volume cold after mixing
But, pH value is adjusted to 7 after adding glutaraldehyde solution to solidify 90min, continues stirring 20-40 min and obtains microcapsule solution, by microcapsule solution
After being centrifuged 15 min under the conditions of 3000-4000rpm/min, supernatant is abandoned, precipitating is washed with water 2-3 times, is freeze-dried and contains to obtain the final product
The chitosan microcapsules powder of sodium hyaluronate, vitamin and collagen；
(3) nano-cellulose, chitosan microcapsules powder, natural, water, spin finish aid are prepared after mixing
Fiber spinning solution, dry the health fiber after electrostatic spinning is handled；
(4) by the cotton fiber of health fiber and hydrophobically modified carry out it is blended after to get health fiber fabric, after clipped sewing
Health care underwear.
2. a kind of preparation method of health care underwear according to claim 1, which is characterized in that vinegar as described in step (1)
The concentration of acid solution is 1-2%.
3. a kind of preparation method of health care underwear according to claim 1, which is characterized in that shell as described in step (1)
The concentration of chitosan is 1-3% in glycan calcium chloride solution, and the concentration of calcium chloride is 0.1-0.5%.
4. a kind of preparation method of health care underwear according to claim 1, which is characterized in that Ah. described in step (2)
The concentration for drawing Arabic gum in primary glue solution is 5-8%；The Arab containing sodium hyaluronate, vitamin and collagen
The concentration of sodium hyaluronate, vitamin and collagen is followed successively by 2-5%, 3-5%, 5-10% in glue solution.
5. a kind of preparation method of health care underwear according to claim 1, which is characterized in that penta described in step (2)
The concentration of glutaraldehyde is 25-45% in dialdehyde solution, and the addition quality of glutaraldehyde is 0.1-0.2 times of chitosan.
6. a kind of preparation method of health care underwear according to claim 1, which is characterized in that day described in step (3)
Right antioxidant is one of vine polyphenol extract, tea polyphenols and gallic acid；The spin finish aid is polypropylene
One of amide, polycarbonate.
7. a kind of preparation method of health care underwear according to claim 1, which is characterized in that step is received described in (3)
Rice cellulose, chitosan microcapsules powder, natural, water, spin finish aid are figured by mass parts and are followed successively by: 20-35 parts, 1-
2 parts, 0.5-1 parts, 65-85 parts, 5-8 parts.
8. a kind of preparation method of health care underwear according to claim 1, which is characterized in that guarantor described in step (4)
The mass ratio when cotton fiber of strong fiber and hydrophobically modified is blended is 1:0.5-0.8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810625334.6A CN108968172B (en) | 2018-06-18 | 2018-06-18 | Preparation method of health-care underwear |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810625334.6A CN108968172B (en) | 2018-06-18 | 2018-06-18 | Preparation method of health-care underwear |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108968172A true CN108968172A (en) | 2018-12-11 |
| CN108968172B CN108968172B (en) | 2020-09-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810625334.6A Active CN108968172B (en) | 2018-06-18 | 2018-06-18 | Preparation method of health-care underwear |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109943893A (en) * | 2019-02-27 | 2019-06-28 | 唐卫兵 | A kind of preparation method of the warming natural nano bamboo fibre/cotton fiber composite material of long acting antibiotic |
| CN112481738A (en) * | 2020-10-26 | 2021-03-12 | 杭州乐铭科技有限公司 | Hyaluronic acid fiber and production process thereof |
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Also Published As
| Publication number | Publication date |
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| CN108968172B (en) | 2020-09-04 |
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