CN106400173A - Preparation method of Chinese herbal medicine fragrant polyarmide fiber - Google Patents
Preparation method of Chinese herbal medicine fragrant polyarmide fiber Download PDFInfo
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- CN106400173A CN106400173A CN201610912907.4A CN201610912907A CN106400173A CN 106400173 A CN106400173 A CN 106400173A CN 201610912907 A CN201610912907 A CN 201610912907A CN 106400173 A CN106400173 A CN 106400173A
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- China
- Prior art keywords
- chinese herbal
- spinning
- herbal medicine
- preparation
- fypro
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/90—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyamides
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Cosmetics (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a preparation method of a Chinese herbal medicine fragrant polyarmide fiber and belongs to the field of textile materials. The preparation method comprises preparing an aqueous emulsion of Chinese herbal medicines, preparing a microcapsule fragrance agent, preparing a chitosan solution, mixing the aqueous emulsion of Chinese herbal medicines, the microcapsule fragrance agent, the chitosan solution and a polyamide fiber spinning solution and carrying out spinning raw material spinning, washing, drying and tube-shaped yarn formation so that finished product Chinese herbal medicine fragrant polyarmide fibers are obtained. The polyarmide fiber has good traditional Chinese medicine health effects, good drug adhesion and durability, good wearing performances, a natural aroma for masking the smell of Chinese herbal medicines and has antibacterial properties.
Description
Technical field
The invention belongs to textile material field is and in particular to a kind of preparation method of Chinese herbal medicine aroma type Fypro.
Background technology
Textile is one of most basic demand for the survival of mankind, with increasing of the size of population and carrying of quality of life
Height, the also more and more higher of the requirement to textile material.It is desirable to textile material has traditional resisting cold, the general function such as attractive in appearance
While, there is special miscellaneous function again, such as medicinal health function, fragrant performance.It is critical only that of Development of Textile Industry is new
The exploitation of product.At present, functionalization textile technology is the major trend of World Textile technology development.Using new material, new technology,
New technology development has multipurpose, high-performance, high value-added product has become the new development trend of textile, especially health care
Medicine is be combined with each other with textile, to obtain new taking and feature.But at present with regard to the research of healthcare face fabric, it need
Develop further.In recent years, the health-care textile material having had Chinese medicine improvement emerges, but difficulty has lasting best-selling product on the market
Occur, trace it to its cause and mainly have:Drug attachment and persistency are poor, and the wearability of fabric is poor, and Chinese herbal medicine abnormal smells from the patient is too heavy.
Content of the invention
In order to solve the above problems, the invention provides a kind of preparation method of Chinese herbal medicine aroma type Fypro, adopt
With the Fypro that the method is obtained, there is good Chinese medicine health-care performance, and drug attachment, persistency are good, wearability
Good, there is natural aromatic, can effectively cover the abnormal smells from the patient of Chinese herbal medicine, and there is anti-microbial property.
In order to solve the above problems, the present invention employs the following technical solutions:
A kind of preparation method of Chinese herbal medicine aroma type Fypro, comprises the following steps:
Step one:Adopt super-refinement powder body process equipment by after Radix Glycyrrhizae, the Radix Angelicae Dahuricae, Herba Dendrobii mixing, being processed into particle diameter is 30
~50 nanometers of super-refinement powder body, and powder body and dispersant are added to the water, mixing and stirring, ultrasonic disperse deaerates, and is obtained
Chinese herbal medicine aqueous emulsion;
Step 2:To in the saturated aqueous solution of beta-schardinger dextrin-add jasmin quintessence oil, with magnetic stirring apparatuss with 500r/min
Speed stir 30~50min, then stand 24 hours froth breakings, obtain jasmine microcapsule aromatic agent;
Step 3:Shitosan is dissolved in the acetic acid solution that mass concentration is 90%, is stirred at room temperature to being completely dissolved, is obtained
Chitosan solution;
Step 4:By Chinese herbal medicine aqueous emulsion, jasmine microcapsule aromatic agent, chitosan solution, Fypro spinning liquid with
Weight ratio 3~4.5:0.5~0.6:11~13:86~92 mixed grindings 3~5 hours, then through deaeration, filtration, prepared spinning
Stock solution;
Step 5:By spinning solution in spinning coagulation bath spinning moulding, spinning speed is 20~40m/min, and spinning draws
Stretch than for 60~100%, technological process is:Spinning solution-spinning-washing-drying-one-tenth cylinder-finished product, obtains Chinese herbal medicine aroma type and gathers
Nylon.
Preferably, the saturated aqueous solution temperature control of the beta-schardinger dextrin-described in step 2 is at 40 DEG C.
Preferably, the weight of the beta-schardinger dextrin-described in step 2 and jasmin quintessence oil is than for 6: 1.
Preferably, the dispersant described in step one is polyacrylic acid sodium salt.
Preferably, the weight of the powder body described in step one, dispersant, water is than for 1:0.2:4.
Preferably, in the chitosan solution described in step 3, the mass concentration of shitosan is 1.5~3%.
Preferably, the consisting of of the spinning coagulation bath described in step 5:Sulphuric acid 100~150g/L, sodium sulfate 300~
350g/L, zinc sulfate 8~10g/L, aluminum sulfate 8~10g/L;The temperature control of spinning coagulation bath is at 40~50 DEG C.
Preferably, in described step 5, drying temperature is 70~80 DEG C.
Preferably, described Fypro spinning liquid is that polyamide is obtained through dipping, squeezing, pulverizing and dissolving.
The beneficial effects of the present invention is:
1) pass through to add Chinese herbal medicine aqueous emulsion in Fypro spinning liquid, give Fypro with excellent Chinese medicine
Health-care effect.Wherein Radix Glycyrrhizae has the effects such as heat-clearing and toxic substances removing, antiallergic;The Radix Angelicae Dahuricae has the functions such as dehumidifying, promoting blood circulation and stopping pain that get rid of illness;Stone
Dry measure used in former times has functions that anticancer.
2) pass through to microcapsule aromatic agent in Fypro spinning liquid, give Fypro with natural Flos Jasmini Sambac
Perfume (or spice), can cover the abnormal smells from the patient of Chinese medicine, add chitosan solution again, improve the antibiotic property of fiber.
3) when the saturated aqueous solution temperature control of beta-schardinger dextrin-is at 40 DEG C, the weight of beta-schardinger dextrin-and jasmin quintessence oil is than for 6:
1, the prepared lasting intensity of microcapsule aromatic agent and slow-release time optimal.
4) the Chinese herbal medicine aroma type Fypro that the present invention is obtained, drug attachment, persistency, taking are good, and make
Standby process is simple is it is easy to industrialized production.
Specific embodiment
For making the object, technical solutions and advantages of the present invention clearer, below the present invention is made further to retouch in detail
State.Based on the embodiment in the present invention, those of ordinary skill in the art are obtained under the premise of not making creative work
Every other embodiment, broadly falls into the scope of protection of the invention.
Embodiment 1
A kind of preparation method of Chinese herbal medicine aroma type Fypro, comprises the following steps:
Step one:Adopt super-refinement powder body process equipment by after Radix Glycyrrhizae, the Radix Angelicae Dahuricae, Herba Dendrobii mixing, being processed into particle diameter is 30
~50 nanometers of super-refinement powder body, and powder body and dispersant are added to the water, mixing and stirring, ultrasonic disperse deaerates, and is obtained
Chinese herbal medicine aqueous emulsion;
Step 2:To in the saturated aqueous solution of beta-schardinger dextrin-add jasmin quintessence oil, with magnetic stirring apparatuss with 500r/min
Speed stirring 30min, then stand 24 hours froth breakings, obtain jasmine microcapsule aromatic agent;
Step 3:Shitosan is dissolved in the acetic acid solution that mass concentration is 90%, is stirred at room temperature to being completely dissolved, is obtained
Chitosan solution;
Step 4:By Chinese herbal medicine aqueous emulsion, jasmine microcapsule aromatic agent, chitosan solution, Fypro spinning liquid with
Weight compares 3:0.5:11:86 mixed grindings 3 hours, then through deaeration, filtration, prepared spinning solution;
Step 5:By spinning solution in spinning coagulation bath spinning moulding, spinning speed be 20m/min, spin-draw ratio
For 60%, technological process is:Spinning solution-spinning-washing-drying-one-tenth cylinder-finished product, obtains Chinese herbal medicine aroma type Fypro.
In described step 2, the saturated aqueous solution temperature control of beta-schardinger dextrin-is at 40 DEG C, the weight of beta-schardinger dextrin-and jasmin quintessence oil
Amount ratio is 6: 1.
Powder body in described step one, dispersant, the weight of water are than for 1:0.2:4;Wherein dispersant is polyacrylic acid sodium salt.
In chitosan solution in described step 3, the mass concentration of shitosan is 1.5%.
The consisting of of spinning coagulation bath in described step 5:Sulphuric acid 100g/L, sodium sulfate 300g/L, zinc sulfate 8g/L,
Aluminum sulfate 8g/L;The temperature of spinning coagulation bath is 40 DEG C;Drying temperature is 70 DEG C.
Embodiment 2
A kind of preparation method of Chinese herbal medicine aroma type Fypro, comprises the following steps:
Step one:Adopt super-refinement powder body process equipment by after Radix Glycyrrhizae, the Radix Angelicae Dahuricae, Herba Dendrobii mixing, being processed into particle diameter is 30
~50 nanometers of super-refinement powder body, and powder body and dispersant are added to the water, mixing and stirring, ultrasonic disperse deaerates, and is obtained
Chinese herbal medicine aqueous emulsion;
Step 2:To in the saturated aqueous solution of beta-schardinger dextrin-add jasmin quintessence oil, with magnetic stirring apparatuss with 500r/min
Speed stirring 40min, then stand 24 hours froth breakings, obtain jasmine microcapsule aromatic agent;
Step 3:Shitosan is dissolved in the acetic acid solution that mass concentration is 90%, is stirred at room temperature to being completely dissolved, is obtained
Chitosan solution;
Step 4:By Chinese herbal medicine aqueous emulsion, jasmine microcapsule aromatic agent, chitosan solution, Fypro spinning liquid with
Weight compares 4:0.6:12:90 mixed grindings 4 hours, then through deaeration, filtration, prepared spinning solution;
Step 5:By spinning solution in spinning coagulation bath spinning moulding, spinning speed be 30m/min, spin-draw ratio
For 80%, technological process is:Spinning solution-spinning-washing-drying-one-tenth cylinder-finished product, obtains Chinese herbal medicine aroma type Fypro.
In described step 2, the saturated aqueous solution temperature control of beta-schardinger dextrin-is at 40 DEG C, the weight of beta-schardinger dextrin-and jasmin quintessence oil
Amount ratio is 6: 1.
Powder body in described step one, dispersant, the weight of water are than for 1:0.2:4;Wherein dispersant is polyacrylic acid sodium salt.
In chitosan solution in described step 3, the mass concentration of shitosan is 2%.
The consisting of of spinning coagulation bath in described step 5:Sulphuric acid 120g/L, sodium sulfate 320g/L, zinc sulfate 9g/L,
Aluminum sulfate 9g/L;The temperature of spinning coagulation bath is 45 DEG C;Drying temperature is 75 DEG C.
Embodiment 3
A kind of preparation method of Chinese herbal medicine aroma type Fypro, comprises the following steps:
Step one:Adopt super-refinement powder body process equipment by after Radix Glycyrrhizae, the Radix Angelicae Dahuricae, Herba Dendrobii mixing, being processed into particle diameter is 30
~50 nanometers of super-refinement powder body, and powder body and dispersant are added to the water, mixing and stirring, ultrasonic disperse deaerates, and is obtained
Chinese herbal medicine aqueous emulsion;
Step 2:To in the saturated aqueous solution of beta-schardinger dextrin-add jasmin quintessence oil, with magnetic stirring apparatuss with 500r/min
Speed stirring 50min, then stand 24 hours froth breakings, obtain jasmine microcapsule aromatic agent;
Step 3:Shitosan is dissolved in the acetic acid solution that mass concentration is 90%, is stirred at room temperature to being completely dissolved, is obtained
Chitosan solution;
Step 4:By Chinese herbal medicine aqueous emulsion, jasmine microcapsule aromatic agent, chitosan solution, Fypro spinning liquid with
Weight compares 4.5:0.6:13:92 mixed grindings 5 hours, then through deaeration, filtration, prepared spinning solution;
Step 5:By spinning solution in spinning coagulation bath spinning moulding, spinning speed be 40m/min, spin-draw ratio
For 100%, technological process is:Spinning solution-spinning-washing-drying-one-tenth cylinder-finished product, obtains Chinese herbal medicine aroma type polyamide fine
Dimension.
In described step 2, the saturated aqueous solution temperature control of beta-schardinger dextrin-is at 40 DEG C, the weight of beta-schardinger dextrin-and jasmin quintessence oil
Amount ratio is 6: 1.
Powder body in described step one, dispersant, the weight of water are than for 1:0.2:4;Wherein dispersant is polyacrylic acid sodium salt.
In chitosan solution in described step 3, the mass concentration of shitosan is 3%.
The consisting of of spinning coagulation bath in described step 5:Sulphuric acid 150g/L, sodium sulfate 350g/L, zinc sulfate 10g/L,
Aluminum sulfate 10g/L;The temperature of spinning coagulation bath is 50 DEG C;Drying temperature is 80 DEG C.
Claims (8)
1. a kind of preparation method of Chinese herbal medicine aroma type Fypro is it is characterised in that comprise the following steps:
Step one:Adopt super-refinement powder body process equipment by after Radix Glycyrrhizae, the Radix Angelicae Dahuricae, Herba Dendrobii mixing, being processed into particle diameter is 30~50
The super-refinement powder body of nanometer, and powder body and dispersant are added to the water, mixing and stirring, ultrasonic disperse deaerates, prepared medium-height grass
Liquid medicine emulsion;
Step 2:To in the saturated aqueous solution of beta-schardinger dextrin-add jasmin quintessence oil, with magnetic stirring apparatuss with 500r/min speed
Degree stirring 30~50min, then stand 24 hours froth breakings, obtain jasmine microcapsule aromatic agent;
Step 3:Shitosan is dissolved in the acetic acid solution that mass concentration is 90%, is stirred at room temperature to being completely dissolved, prepared shell gathers
Sugar juice;
Step 4:By Chinese herbal medicine aqueous emulsion, jasmine microcapsule aromatic agent, chitosan solution, Fypro spinning liquid with weight
Ratio 3~4.5:0.5~0.6:11~13:86~92 mixed grindings 3~5 hours, then through deaeration, filtration, prepared spinning solution;
Step 5:By spinning solution in spinning coagulation bath spinning moulding, spinning speed be 20~40m/min, spin-draw ratio
For 60~100%, technological process is:Spinning solution-spinning-washing-drying-one-tenth cylinder-finished product, obtains Chinese herbal medicine aroma type polyamide
Fiber.
2. a kind of Chinese herbal medicine aroma type Fypro according to claim 1 preparation method it is characterised in that:Step
The saturated aqueous solution temperature control of the beta-schardinger dextrin-described in two is at 40 DEG C.
3. a kind of Chinese herbal medicine aroma type Fypro according to claim 1 preparation method it is characterised in that:Step
The weight of the beta-schardinger dextrin-described in two and jasmin quintessence oil is than for 6: 1.
4. a kind of Chinese herbal medicine aroma type Fypro according to claim 1 preparation method it is characterised in that:Step
Dispersant described in one is polyacrylic acid sodium salt.
5. a kind of Chinese herbal medicine aroma type Fypro according to claim 1 preparation method it is characterised in that:Step
Powder body described in one, dispersant, the weight of water are than for 1:0.2:4.
6. a kind of Chinese herbal medicine aroma type Fypro according to claim 1 preparation method it is characterised in that:Step
In chitosan solution described in three, the mass concentration of shitosan is 1.5~3%.
7. a kind of Chinese herbal medicine aroma type Fypro according to claim 1 preparation method it is characterised in that:Step
The consisting of of spinning coagulation bath described in five:Sulphuric acid 100~150g/L, sodium sulfate 300~350g/L, zinc sulfate 8~10g/
L, aluminum sulfate 8~10g/L;The temperature control of spinning coagulation bath is at 40~50 DEG C.
8. a kind of Chinese herbal medicine aroma type Fypro according to claim 1 preparation method it is characterised in that:Described
Step 5 in drying temperature be 70~80 DEG C.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106929940A (en) * | 2017-03-24 | 2017-07-07 | 李军 | The spinning fabric and its preparation technology of a kind of delicate fragrance antibacterial |
CN107604455A (en) * | 2017-10-31 | 2018-01-19 | 中原工学院 | A kind of preparation method of Chinese herbal medicine fiber |
CN109527673A (en) * | 2018-11-30 | 2019-03-29 | 东华大学 | A kind of chargeable Chinese medicine thermotherapy waist support |
CN111394818A (en) * | 2020-04-07 | 2020-07-10 | 江苏金太阳纺织科技股份有限公司 | Liquorice regenerated cellulose fiber and preparation method thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106929940A (en) * | 2017-03-24 | 2017-07-07 | 李军 | The spinning fabric and its preparation technology of a kind of delicate fragrance antibacterial |
CN107604455A (en) * | 2017-10-31 | 2018-01-19 | 中原工学院 | A kind of preparation method of Chinese herbal medicine fiber |
CN107604455B (en) * | 2017-10-31 | 2020-03-31 | 中原工学院 | Preparation method of Chinese herbal medicine fiber |
CN109527673A (en) * | 2018-11-30 | 2019-03-29 | 东华大学 | A kind of chargeable Chinese medicine thermotherapy waist support |
CN111394818A (en) * | 2020-04-07 | 2020-07-10 | 江苏金太阳纺织科技股份有限公司 | Liquorice regenerated cellulose fiber and preparation method thereof |
CN111394818B (en) * | 2020-04-07 | 2022-09-30 | 江苏金太阳纺织科技股份有限公司 | Liquorice regenerated cellulose fiber and preparation method thereof |
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