CN108926503A - The preparation method of Skin whitening care cosmetics containing glycyrrhiza uralensis fisch extract - Google Patents
The preparation method of Skin whitening care cosmetics containing glycyrrhiza uralensis fisch extract Download PDFInfo
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- CN108926503A CN108926503A CN201710411412.8A CN201710411412A CN108926503A CN 108926503 A CN108926503 A CN 108926503A CN 201710411412 A CN201710411412 A CN 201710411412A CN 108926503 A CN108926503 A CN 108926503A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of preparation methods of Skin whitening care cosmetics containing glycyrrhiza uralensis fisch extract：The first step：With ethyl alcohol extract Radix Glycyrrhizae, Radix Notoginseng, rhizoma polygonati extract；Second step：After C18 alcohol, inositol hexaphosphate, glycerol, stearic acid heating consolute, oily phase is obtained after tert-butylhydroquinone dissolution is added；Third step：The Chinese herbal medicine extract is added after borax, glyceryl monostearate, Purified Water mix and obtains water phase；4th step：The oil is added in water phase and is emulsified, essence is added to get the skin care item with whitening effect.Skin metabolism can be improved, promote skin blood circulation, increase skin-nourishing, be effectively removed free radical, eliminate pigementation, the wrinkle and color spot that desalination skin occurs make finer and smoother, smooth, the tender white and high resilience of skin.
Description
Technical field
The present invention relates to technical field of traditional Chinese medicines, in particular to a kind of Skin whitening care cosmetics preparation sides containing licorice
Method.
Background technique
Skin-whitening class skin care item are also referred to as freckle removing and whitening class skin care item, are to be classified as caused by cosmetics for special use in China.
Whitening class skin care item occupy always considerable share in Cosmetic Market.Especially in recent years, with aesthetic medicine
The raising of development and economic level, skin-whitening class skin care item are very by the welcome of consumer.
Skin is the important component of human body, even more directly expresses the mark of human health and aging.Work as skin metabolism
Vigorous, blood circulation is unimpeded, and when full of nutrition, then skin is fine and smooth, smooth, tender, is rich in elasticity, and be less prone to wrinkle and color
Spot.When skin metabolism weakens, poor blood circulation, when nutriment is bad, then skin can become gloomy, aging, and be also easy to produce
Wrinkle and color spot.The principal element of decider skin colour difference core force is carrotene and melanin, and wherein melanin is most
Important.Melanin is synthesized in melanocyte, and adjacent angle is transferred to by the dendritic processes of melanocyte
Change in cell.Melanocyte in application on human skin is located at basal layer of epidermis, hair root portion and outer hair sheath etc., in 7-8 basal cell
There are about a melanocytes.Therefore, for the distribution density of melanocyte without ethnic group difference, the people of the various colours of skin is essentially identical,
Whole body about 2,000,000,000 altogether.Under normal condition, melanin can absorb excessive daylight light, especially ultraviolet light, protect human body, if
The melanin of generation cannot be metabolized in time and assemble, be deposited on epidermis, then can make occur freckle, chloasma or year spot on skin
Deng.It is generally acknowledged that the formation mechanism of melanin is that tyrosine is synthesized through tyrosinase catalysis in melanocyte.Tyrosine
The process for being oxidized to melanin is considerably complicated, and ultraviolet light can cause the activity and the increasing of melanocyte activity of tyrosinase
By force, because this oxidation can be promoted.
Up to the present, widely used whitening agent mainly has following several：Ascorbic acid and its derivative, kojic acid
And its derivative, hydroquinone and its derivative, a- carboxylic acid and its derivative, animal protein extract, Chinese herbal medicine extract
And sun-screening agent.
Skin care item currently on the market can not usually improve skin metabolism, promote skin blood circulation, increase skin battalion
It supports, it is even more impossible to remove the color spot of skin appearance to make fine and smooth, smooth, the tender white and springiness of skin.Therefore people couple are not able to satisfy
The skin care requirement of the whitening and anti-aging, nti-freckle of skin of face, brings inconvenience to the daily nursing of people's skin of face.
Summary of the invention
The object of the present invention is to provide a kind of main method for preparing of Skin whitening care cosmetics containing licorice, this method is made
Skin care item not only can be improved skin metabolism, promote skin blood circulation, increase skin-nourishing, but also can remove skin-color
Spot keeps skin more tender white.
The present invention is achieved by the following technical solutions：
The preparation method of Skin whitening care cosmetics containing licorice is：The first step：By 10 parts by weight of Radix Glycyrrhizae, 5 parts by weight of Radix Notoginseng,
2 parts by weight of rhizoma polygonati carry out 80 mesh sievings after being uniformly mixed crushing, 500 parts by weight quality are then added to attempt the second for being 85~90%
Alcohol carries out low temperature ultrasonic and extracts 2 hours after impregnating 24 hours under the conditions of 25 DEG C, go supernatant centrifugation, filtering, refluxing ethanol, most
By after secondary filter to get Chinese herbal medicine extract；Second step：By 1.5 parts by weight of C18 alcohol, 0.5 weight of inositol hexaphosphate
After part, 6 parts by weight of glycerol, 12 parts by weight of stearic acid are heated to 75 DEG C~85 DEG C consolutes, 0.02 weight of tert-butylhydroquinone is added
Part is measured, oily phase is obtained after dissolution；Third step：It is hard that 3 parts by weight of borax, glycerol list is added in 3 parts by weight of Chinese herbal medicine extract
Water phase is obtained after point mixing of 2 parts by weight of ester acid esters, 60 weight of Purified Water；4th step：The oil is added to 70 DEG C of the water phase
Essence is added when temperature is down to 40 DEG C~50 DEG C to get the skin care item with whitening effect in middle emulsification.
The main component of Radix Glycyrrhizae is triterpenes and flavone compound, there are also a small amount of alkaloid, lignin, cumarin and
A variety of amino acid.Radix Glycyrrhizae is common medicine simply in tcm clinical practice, has and invigorates the spleen and benefits qi, clearing heat and detoxicating, expelling phlegm and arresting coughing, emergency is stopped
Bitterly, coordinating the drug actions of a prescription function.There is good result in terms of the activity and whitening that improve skin, to myocyte, vascular endothelial cell
It is proliferated and has facilitation to the generation of -4 type of collagen, have certain inhibiting effect to melanocyte generation, it can whitening
Skin, radiate the vigour of youth beautiful elegance.
Its ingredient of Radix Notoginseng is mainly arasaponin, notoginseng polysaccharide, amino acid, panoxadiol and alkaloid and glycosides displayed
Deng.With activating blood and removing stasis, the effect of hemostasis, swelling and pain relieving.In terms of beauty can scavenging activated oxygen, enhance endogenous super oxygen
The activity of mutase reinforces body to the Scavenging activity of oxygen radical, mitigates chain reaction caused by oxygen radical, reduce in blood
The peroxidating of lipid.
Rhizoma polygonati contains steroid saponin, amino acid, compound of polysaccharide, anthraquinone analog compound, aspartic acid, homoserine, two
The ingredients such as aminobutyric acid, compound of polysaccharide.Property：Sweet and neutral, channel tropism：Returns spleen, lung, kidney channel.Major function boosting qi and nourishing yin, invigorating the spleen, profit
Lung, kidney-nourishing.Superoxide radical and hydroxyl radical free radical are eliminated, the inhibition to B-16 melanocyte activity, there is whitening
Skin, the effect of anti-aging.
Contain the various plants activity extracted by Chinese herbal medicines such as Radix Glycyrrhizae, Radix Notoginseng, rhizoma polygonatis in composite skin care product of the invention
Ingredient has very strong antioxidation, and is small-molecule substance, it is easier to penetrate into skin and be less readily available for absorption by the skin, not only may be used
To improve skin metabolism, promote skin blood circulation, increase skin-nourishing, and it can be effectively removed free radical, eliminate pigment
Precipitating, the wrinkle and color spot that desalination skin occurs, makes finer and smoother, smooth, the tender white and high resilience of skin, can meet people couple
The whitening and anti-aging of skin of face smoothes away wrinkles, the daily skin care requirement of nti-freckle, is a kind of Chinese herbal medicine skin care of great effect
Product.
Clinical application shows that the skin care item of the invention containing Radix Glycyrrhizae, Radix Notoginseng, Rhizoma Polygonati extract mainly pass through inhibition junket
The activity of propylhomoserin enzyme and dopachrome interconvertible enzyme (TRP-2), the polymerization for hindering 5,6- dihydroxy indole (DH1) interfere melanin
The intermediate of generation；Reduction can be played to melanin, prevent photooxidation, horn cell black plasmid of degrading；It can promote black
The metabolism of element, prevents melanin deposition, excretes melanin rapidly；The entrance for preventing ultraviolet light prevents due to ultraviolet light
Excessive melanin is formed, thus the effect of reaching whitening and the nti-freckle of skin.
Specific embodiment
Below with reference to embodiment and case, the present invention is further illustrated.
Embodiment 1
The first step：Accurately weigh Radix Glycyrrhizae 10Kg, Radix Notoginseng 5Kg, rhizoma polygonati 2Kg, be uniformly mixed crush after carry out 80 mesh sievings, then plus
Enter the ethyl alcohol that 500Kg mass concentration is 85%, low temperature ultrasonic is carried out after impregnating 24 hours under the conditions of 25 DEG C and is extracted 2 hours, is gone
Supernatant centrifugation, filtering, refluxing ethanol, most afterwards after secondary filter to get Chinese herbal medicine extract；Second step：By C18 alcohol 1.5Kg,
After inositol hexaphosphate 0.5Kg, glycerol 6Kg, stearic acid 12Kg are heated to 75 DEG C of consolutes, tert-butylhydroquinone is added
0.02Kg obtains oily phase after dissolution；Third step：Borax 3Kg, glyceryl monostearate is added in the Chinese herbal medicine extract 3Kg
Water phase is obtained after 2Kg, Purified Water 60Kg mixing；4th step：The oil is added in 70 DEG C of the water phase and is emulsified, dropped to temperature
Essence is added when to 40 DEG C to get the skin care item with white-skinned face function.
Embodiment 2
The first step：Accurately weigh Radix Glycyrrhizae 10Kg, Radix Notoginseng 5Kg, rhizoma polygonati 2Kg, be uniformly mixed crush after carry out 80 mesh sievings, then plus
Enter the ethyl alcohol that 500Kg mass concentration is 90%, low temperature ultrasonic is carried out after impregnating 24 hours under the conditions of 25 DEG C and is extracted 2 hours, is gone
Supernatant centrifugation, filtering, refluxing ethanol, most afterwards after secondary filter to get Chinese herbal medicine extract；Second step：By C18 alcohol 1.5Kg,
After inositol hexaphosphate 0.5Kg, glycerol 6Kg, stearic acid 12Kg are heated to 85 DEG C of consolutes, tert-butylhydroquinone is added
0.02Kg obtains oily phase after dissolution；Third step：Borax 3Kg, glyceryl monostearate is added in the Chinese herbal medicine extract 3Kg
Water phase is obtained after 2Kg, Purified Water 60Kg mixing；4th step：The oil is added in 70 DEG C of the water phase and is emulsified, dropped to temperature
Essence is added when to 50 DEG C to get the skin care item with white-skinned face function.
Embodiment 3
The first step：Accurately weigh Radix Glycyrrhizae 10Kg, Radix Notoginseng 5Kg, rhizoma polygonati 2Kg, be uniformly mixed crush after carry out 80 mesh sievings, then plus
Enter the ethyl alcohol that 500Kg mass concentration is 85%, low temperature ultrasonic is carried out after impregnating 24 hours under the conditions of 25 DEG C and is extracted 2 hours, is gone
Supernatant centrifugation, filtering, refluxing ethanol, most afterwards after secondary filter to get Chinese herbal medicine extract；Second step：By C18 alcohol 1.5Kg,
After inositol hexaphosphate 0.5Kg, glycerol 6Kg, stearic acid 12Kg are heated to 85 DEG C of consolutes, tert-butylhydroquinone is added
0.02Kg obtains oily phase after dissolution；Third step：Borax 3Kg, glyceryl monostearate is added in the Chinese herbal medicine extract 3Kg
Water phase is obtained after 2Kg, Purified Water 60Kg mixing；4th step：The oil is added in 70 DEG C of the water phase and is emulsified, dropped to temperature
Essence is added when to 45 DEG C to get the skin care item with white-skinned face function.
Embodiment 4
The first step：Accurately weigh Radix Glycyrrhizae 10Kg, Radix Notoginseng 5Kg, rhizoma polygonati 2Kg, be uniformly mixed crush after carry out 80 mesh sievings, then plus
Enter the ethyl alcohol that 500Kg mass concentration is 87%, low temperature ultrasonic is carried out after impregnating 24 hours under the conditions of 25 DEG C and is extracted 2 hours, is gone
Supernatant centrifugation, filtering, refluxing ethanol, most afterwards after secondary filter to get Chinese herbal medicine extract；Second step：By C18 alcohol 1.5Kg,
After inositol hexaphosphate 0.5Kg, glycerol 6Kg, stearic acid 12Kg are heated to 80 DEG C of consolutes, tert-butylhydroquinone is added
0.02Kg obtains oily phase after dissolution；Third step：Borax 3Kg, glyceryl monostearate is added in the Chinese herbal medicine extract 3Kg
Water phase is obtained after 2Kg, Purified Water 60Kg mixing；4th step：The oil is added in 70 DEG C of the water phase and is emulsified, dropped to temperature
Essence is added when to 47 DEG C to get the skin care item with white-skinned face function.
Human body whitening is tested a melanin content and is reduced：
Any product (cosmetics or topical drug) cannot be used within 2-3 days before measurement recipient site.Before test, subject needs to unite
One cleaning and hand inner forearm, with dry face tissue wiped clean.Measurement zone is carried out in subject's both hands inner forearm after cleaning
Field mark, should sit quietly at least 30min before official testing in standard compliant room, and forearm exposure is placed in test mode, protected
It holds and loosens.
4 × 4cm of label on the inside of left and right arm in experiment2Test area, same arm can mark multiple regions, region simultaneously
It is spaced 2cm, test product (extracting solution of various concentration) and blank control are randomly dispersed in left and right arm.It is black using skin
Pigment and ferroheme tester carry out the measurement of tested region and control zone, and each region is according to parallel determination 5 times.First measure
Then the blank value of each test zone presses 2.0 ± 0.1mg sample/cm2Dosage, using latex finger cot by sample even spread
In in trial zone.1 week, 2 weeks, 3 weeks, the dermal melanin content in 4 weeks tested regions and blank control region are measured after smearing respectively.
The test of the same volunteer is completed by the same survey crew.
The experimental result of the embodiment of the present invention 1~4：With the extension of time of measuring, melanin content reduction amount is also gradually
Increase, this illustrates that skin care item whitening active composition made from the embodiment of the present invention 1~4 persistently acts as the melanin reduction of skin
With.
Clinical trial of the present invention and result：
Experimental method：Select volunteer of the age bracket at 35 years old to 60 years old, male volunteer 50, female volunteer 50.
Cardinal symptom：Freckle, chloasma, sun spot, the colour of skin are obscure.Volunteer is randomly divided into two groups, every group of 50 people.
Test group：After daily face cleaning, facial mask prepared by embodiment 4 is spread on into 20~30min of face before sleeping, is cleaned with wet water
, other skin care item are not applied, 2~3 times weekly, experimental period one month.
Control group：After daily face cleaning, commercially available 20~30min of whitening mask is coated on facial skin before sleeping, with wet washing
It is net, other skin care item are not applied.2~3 times weekly, experimental period one month.
Respectively count primary within 3 days, 7 days, 1 month.
Evaluation criterion：Experienced by user's readme and computer compares dermatoglyph pattern identification colour of skin whitening degree and color
Spot desalinates degree.Effectively：The colour of skin highlights, color spot color dodge.In vain：It is not any change between the colour of skin and color spot and experiment.
Result on trial：3 days this products have a whitening effect for being substantially better than commercial product, and test group effective 45, effectively
Rate 90%.Control group effective 18, effective percentage 36%.After 30 days, test group effective percentage reaches 100%, and can also be obvious
Increase the glossiness of skin, skin exquisiteness is mellow and full.There is no an example reaction phenomena such as allergy, skin is uncomfortable occur.Control group is only
56%.
Claims (1)
1. the Skin whitening care cosmetics preparation method containing glycyrrhiza uralensis fisch extract, it is characterised in that：The first step：By 10 weight of Radix Glycyrrhizae
Part, 5 parts by weight of Radix Notoginseng, 2 parts by weight of rhizoma polygonati carry out 80 mesh sievings after being uniformly mixed crushing, and it is dense that 500 parts by weight quality are then added
The ethyl alcohol that degree is 85%~90% carries out low temperature ultrasonic and extracts 2 hours, goes to clear after impregnating 24 hours under the conditions of 25 DEG C
The heart, filtering, refluxing ethanol, finally to get Chinese herbal medicine extract after secondary filter；Second step：By 1.5 parts by weight of C18 alcohol,
After 0.5 parts by weight of inositol hexaphosphate, 6 parts by weight of glycerol, 12 parts by weight of stearic acid are heated to 75 DEG C~85 DEG C consolutes, it is added special
0.02 parts by weight of butylhydroquinone obtain oily phase after dissolution；Third step：By 3 parts by weight of Chinese herbal medicine extract, glycerol list
Water phase is obtained after 2 parts by weight of stearic acid ester, the mixing of 60 parts by weight of Purified Water；4th step：The oil is added to 70 DEG C of the water
It is emulsified in phase, essence is added when temperature is down to 40 DEG C~50 DEG C to get described has whitening effect skin care item.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111388544A (en) * | 2020-04-18 | 2020-07-10 | 北温草生物科技(上海)有限公司 | Chinese herbal medicine composition for removing freckles |
Citations (3)
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|---|---|---|---|---|
| KR101257641B1 (en) * | 2012-10-31 | 2013-04-29 | 노세응 | Method of manufacture a nature component cosmetics for skin-whitening and anti-wrinkle |
| CN103263364A (en) * | 2013-02-18 | 2013-08-28 | 沈惠萍 | Method for preparing whitening cosmetic containing bupleurum extract |
| CN106619345A (en) * | 2015-10-30 | 2017-05-10 | 青岛鹏通瑞德电气科技有限公司 | Hand cream |
-
2017
- 2017-05-24 CN CN201710411412.8A patent/CN108926503A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101257641B1 (en) * | 2012-10-31 | 2013-04-29 | 노세응 | Method of manufacture a nature component cosmetics for skin-whitening and anti-wrinkle |
| CN103263364A (en) * | 2013-02-18 | 2013-08-28 | 沈惠萍 | Method for preparing whitening cosmetic containing bupleurum extract |
| CN106619345A (en) * | 2015-10-30 | 2017-05-10 | 青岛鹏通瑞德电气科技有限公司 | Hand cream |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111388544A (en) * | 2020-04-18 | 2020-07-10 | 北温草生物科技(上海)有限公司 | Chinese herbal medicine composition for removing freckles |
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