CN108814993A - A kind of preparation method of skin whitening, moisturizing dried noodle film - Google Patents
A kind of preparation method of skin whitening, moisturizing dried noodle film Download PDFInfo
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- CN108814993A CN108814993A CN201811087387.3A CN201811087387A CN108814993A CN 108814993 A CN108814993 A CN 108814993A CN 201811087387 A CN201811087387 A CN 201811087387A CN 108814993 A CN108814993 A CN 108814993A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention belongs to dried noodle technical field of membrane, especially a kind of preparation method of skin whitening, moisturizing dried noodle film specifically includes following steps：（1）Leaf of bamboo fiber, aloe fibre and China rose fiber are cleaned, co-grinding respectively, add Hippophate flavone and erythrose alcohol solution, stirred, vacuum freeze drying, routinely spun lacing method operating process is reinforced, and facial mask shape is made, and is spray-dried, is obtained face paper；（2）Fresh strawberry leaf and fresh spinach are mixed with beating, watertight is added to place, carries out CO2Supercritical fluid extraction processing, takes extract, and Taraxacum Polysaccharides and Polysaccharide from Portulaca oleracea is added, and carries out magnetization treatment, obtains Essence；（3）Face paper is immersed in Essence, vacuum freeze drying, compresses, obtain skin whitening, moisturizing dried noodle film；With very strong anti-oxidant, removing free radical and replenishing water and preserving moisture ability, so that user's skin smooth is delicate, whitening is ruddy glossy, enhances antibacterial skin and antiallergy ability, promotes skin health.
Description
Technical field
The invention belongs to dried noodle technical field of membrane, especially a kind of preparation method of skin whitening, moisturizing dried noodle film.
Background technique
Facial mask is a kind of carrier of skin of face maintenance or cosmetics, is applied or is attached to and keeps certain time on the face,
When the benefit materials in maintenance or cosmetics be absorbed by the skin or epidermis face in the substance of harmful skin health adsorbed by facial mask
Afterwards, it is removed it by cleaning or removing, reaches facial skin quality maintenance or beautification purpose；At present facial mask product type and dosage form compared with
It is more, such as paste, pulvis, creme, lotion and with non-woven fabrics, silk, biological fiber material be rely on tearing type hygenic towelette face
Film etc., dried noodle film are also one of facial mask, but presently commercially available dried noodle film single effect, only serve the effect of face paper,
And with facial mask consumer to skin care require it is higher and higher, dried noodle film can no longer meet consumer demand, face gradually by
Superseded problem.
Summary of the invention
In view of the above-mentioned problems, the present invention is intended to provide a kind of preparation method of skin whitening, moisturizing dried noodle film.
The invention is realized by the following technical scheme：
A kind of preparation method of skin whitening, moisturizing dried noodle film, specifically includes following steps：
（1）The preparation of face paper
The China rose fiber of the leaf of bamboo fiber of 29 ~ 31 parts by weight, the aloe fibre of 9 ~ 10 parts by weight and 15 ~ 16 parts by weight is distinguished
Clean, co-grinding, be added 0.12 ~ 0.14 parts by weight Hippophate flavone and 28 ~ 30 parts by weight erythrose alcohol solution, with turn
19 ~ 21min is stirred in the blender stirring that speed is 330 ~ 350r/min clockwise, inverse with the blender that revolving speed is 430 ~ 450r/min
Hour hands stir 23 ~ 25min, and vacuum freeze drying is to no moisture under conditions of temperature is -18 ~ -16 DEG C, and routinely spun lacing method is grasped
It is reinforced as process, facial mask shape is made, spray drying obtains face paper to no moisture under conditions of temperature is 41 ~ 43 DEG C；
（2）The preparation of Essence
The fresh spinach of the fresh strawberry leaf of 8.6 ~ 9.2 parts by weight and 10 ~ 11 parts by weight is mixed with beating, 24 ~ 28 parts by weight, temperature are added
Degree stirs evenly for 61 ~ 65 DEG C of water, and constant-temperature enclosed placement, carries out row CO under conditions of temperature is 45 ~ 47 DEG C2Shooting flow
Body extraction processing takes extract, and the Taraxacum Polysaccharides of 0.13 ~ 0.15 parts by weight and the purslane of 0.20 ~ 0.22 parts by weight are added
Polysaccharide stirs evenly, and carries out magnetization treatment, obtains Essence；
（3）The preparation of dried noodle film
Face paper is immersed in 50 ~ 60min of immersion in Essence, is taken out, vacuum refrigeration under conditions of temperature is -15 ~ -13 DEG C
Dry, compression obtains skin whitening, moisturizing dried noodle film.
As invention further embodiment：Step（1）The temperature of the erythrose alcohol solution is 52 ~ 54 DEG C, quality
Score is 6% ~ 7%.
As invention further embodiment：Step（2）The CO2Supercritical fluid extraction processing is 39 ~ 41 in temperature
DEG C, pressure be 18 ~ 20MPa, flow is 44 ~ 48min of extraction processing under conditions of 8 ~ 9L/h, temperature be 49 ~ 51 DEG C, pressure be
47 ~ 49MPa, flow are 23 ~ 27min of extraction processing under conditions of 19 ~ 21L/h.
As invention further embodiment：Step（2）The magnetization treatment, in the condition that magnetic field strength is 770 ~ 810G
8 ~ 10min of lower magnetization treatment, 13 ~ 15min of magnetization treatment under conditions of magnetic field strength is 1330 ~ 1370G.
As invention further embodiment：A kind of skin whitening, moisturizing dried noodle of the preparation method preparation of skin whitening, moisturizing dried noodle film
Film.
Beneficial effects of the present invention：A kind of preparation method of skin whitening, moisturizing dried noodle film provided by the invention, using bamboo fibre,
Aloe fibre and China rose fiber and be added Hippophate flavone and erythrose alcohol solution stirring it is blended, can effectively enhance face paper
Antibacterial bacteriostatic ability, anti-inflammatory anti-itch effectively absorb epidermal cell metabolism product and accumulation oil substances, while having very
Strong load outlet capacity promotes moisture and beneficiating ingredient to penetrate into the cuticula of epidermis, so that skin becomes soft, natural light has bullet
Property；Essence obtained contains vitamin abundant and a variety of active ingredients, has very strong antioxygenic property and removes free radical
Ability, effectively enhancing skin metabolism, increase skin elasticity, delay skin aging, activating cell, eliminate dermal melanin, suppression
Melanin pigmentation processed, so that the pure white beauty of skin；Face paper is impregnated using Essence, then freeze-drying compression, it can be effective
Promote Essence effective component uniformly penetrating to each position of face paper, combines closely with facial mask paper fiber structure, effectively mention
The bioactivity of high face paper, the anti-oxidant of enhancing dried noodle film entirety, removing free radical and replenishing water and preserving moisture ability, so that user
Skin smooth is delicate, and moisture content is high, so that skin-whitening is ruddy glossy, enhances antibacterial skin and antiallergy ability, promotes
Skin health.
Specific embodiment
Illustrate the present invention with specific embodiment below, but is not limitation of the present invention.
Embodiment 1
In the embodiment of the present invention, a kind of preparation method of skin whitening, moisturizing dried noodle film specifically includes following steps：
（1）The preparation of face paper
The China rose fiber of the leaf of bamboo fiber of 29 parts by weight, the aloe fibre of 9 parts by weight and 15 parts by weight is cleaned respectively, is mixed
It crushes, the Hippophate flavone of 0.12 parts by weight and the erythrose alcohol solution of 28 parts by weight is added, is stirring for 330r/min with revolving speed
Device stirring stirring 19min clockwise is mixed, stirs 23min counterclockwise with the blender that revolving speed is 430r/min, is -18 DEG C in temperature
Under conditions of vacuum freeze drying to no moisture, routinely spun lacing method operating process is reinforced, and facial mask shape is made, and is in temperature
Spray drying obtains face paper to no moisture under conditions of 41 DEG C；
（2）The preparation of Essence
The fresh spinach of the fresh strawberry leaf of 8.6 parts by weight and 10 parts by weight is mixed with beating, 24 parts by weight are added, temperature is 61 DEG C
Water stirs evenly, and constant-temperature enclosed placement, carries out row CO under conditions of temperature is 45 DEG C2Supercritical fluid extraction processing, takes extraction
Object is taken, the Polysaccharide from Portulaca oleracea of Taraxacum Polysaccharides and 0.20 parts by weight that 0.13 parts by weight are added stirs evenly, magnetization treatment is carried out,
Obtain Essence；
（3）The preparation of dried noodle film
Face paper is immersed in Essence and impregnates 50min, is taken out, vacuum freeze drying under conditions of temperature is -15 DEG C, pressure
Contracting, obtains skin whitening, moisturizing dried noodle film.
As invention further embodiment：Step（1）The temperature of the erythrose alcohol solution is 52 DEG C, mass fraction
It is 6%.
As invention further embodiment：Step（2）The CO2Supercritical fluid extraction processing, temperature be 39 DEG C,
Extraction processing 44min under conditions of pressure is 18MPa, flow is 8L/h, temperature is 49 DEG C, pressure 47MPa, flow are
Extraction processing 23min under conditions of 19L/h.
As invention further embodiment：Step（2）The magnetization treatment, magnetic under conditions of magnetic field strength is 770G
Change processing 8min, magnetization treatment 13min under conditions of magnetic field strength is 1330G.
As invention further embodiment：A kind of skin whitening, moisturizing dried noodle of the preparation method preparation of skin whitening, moisturizing dried noodle film
Film.
Embodiment 2
In the embodiment of the present invention, a kind of preparation method of skin whitening, moisturizing dried noodle film specifically includes following steps：
（1）The preparation of face paper
The China rose fiber of the leaf of bamboo fiber of 30 parts by weight, the aloe fibre of 9.5 parts by weight and 15.5 parts by weight is cleaned respectively,
Co-grinding is added the Hippophate flavone of 0.13 parts by weight and the erythrose alcohol solution of 29 parts by weight, is 340r/min with revolving speed
Blender stirring clockwise stirring 20min, stir 24min counterclockwise with the blender that revolving speed is 440r/min, temperature be-
Vacuum freeze drying to no moisture, routinely reinforced, and facial mask shape is made, in temperature by spun lacing method operating process under conditions of 17 DEG C
Spray drying obtains face paper to no moisture under conditions of degree is 42 DEG C；
（2）The preparation of Essence
The fresh spinach of the fresh strawberry leaf of 8.9 parts by weight and 10.5 parts by weight is mixed with beating, 26 parts by weight are added, temperature is 63 DEG C
Water stir evenly, constant-temperature enclosed placement under conditions of temperature is 46 DEG C carries out row CO2Supercritical fluid extraction processing, takes
The Polysaccharide from Portulaca oleracea of extract, Taraxacum Polysaccharides and 0.21 parts by weight that 0.14 parts by weight are added stirs evenly, and carries out at magnetization
Reason, obtains Essence；
（3）The preparation of dried noodle film
Face paper is immersed in Essence and impregnates 55min, is taken out, vacuum freeze drying under conditions of temperature is -14 DEG C, pressure
Contracting, obtains skin whitening, moisturizing dried noodle film.
As invention further embodiment：Step（1）The temperature of the erythrose alcohol solution is 53 DEG C, mass fraction
It is 6.5%.
As invention further embodiment：Step（2）The CO2Supercritical fluid extraction processing, temperature be 40 DEG C,
Extraction processing 46min under conditions of pressure is 19MPa, flow is 8.5L/h, temperature is 50 DEG C, pressure 48MPa, flow are
Extraction processing 25min under conditions of 20L/h.
As invention further embodiment：Step（2）The magnetization treatment, magnetic under conditions of magnetic field strength is 790G
Change processing 9min, magnetization treatment 14min under conditions of magnetic field strength is 1350G.
As invention further embodiment：A kind of skin whitening, moisturizing dried noodle of the preparation method preparation of skin whitening, moisturizing dried noodle film
Film.
Embodiment 3
In the embodiment of the present invention, a kind of preparation method of skin whitening, moisturizing dried noodle film specifically includes following steps：
（1）The preparation of face paper
The China rose fiber of the leaf of bamboo fiber of 31 parts by weight, the aloe fibre of 10 parts by weight and 16 parts by weight is cleaned respectively, is mixed
It closes and crushes, the Hippophate flavone of 0.14 parts by weight and the erythrose alcohol solution of 30 parts by weight is added, is 350r/min's with revolving speed
21min is stirred in blender stirring clockwise, stirs 25min counterclockwise with the blender that revolving speed is 450r/min, is -16 in temperature
Vacuum freeze drying to no moisture, routinely reinforced, and facial mask shape is made, in temperature by spun lacing method operating process under conditions of DEG C
Spray drying obtains face paper to no moisture under conditions of being 43 DEG C；
（2）The preparation of Essence
The fresh spinach of the fresh strawberry leaf of 9.2 parts by weight and 11 parts by weight is mixed with beating, 28 parts by weight are added, temperature is 65 DEG C
Water stirs evenly, and constant-temperature enclosed placement, carries out row CO under conditions of temperature is 47 DEG C2Supercritical fluid extraction processing, takes extraction
Object is taken, the Polysaccharide from Portulaca oleracea of Taraxacum Polysaccharides and 0.22 parts by weight that 0.15 parts by weight are added stirs evenly, magnetization treatment is carried out,
Obtain Essence；
（3）The preparation of dried noodle film
Face paper is immersed in Essence and impregnates 60min, is taken out, vacuum freeze drying under conditions of temperature is -13 DEG C, pressure
Contracting, obtains skin whitening, moisturizing dried noodle film.
As invention further embodiment：Step（1）The temperature of the erythrose alcohol solution is 54 DEG C, mass fraction
It is 7%.
As invention further embodiment：Step（2）The CO2Supercritical fluid extraction processing, temperature be 41 DEG C,
Extraction processing 48min under conditions of pressure is 20MPa, flow is 9L/h, temperature is 51 DEG C, pressure 49MPa, flow are
Extraction processing 27min under conditions of 21L/h.
As invention further embodiment：Step（2）The magnetization treatment, magnetic under conditions of magnetic field strength is 810G
Change processing 10min, magnetization treatment 15min under conditions of magnetic field strength is 1370G.
As invention further embodiment：A kind of skin whitening, moisturizing dried noodle of the preparation method preparation of skin whitening, moisturizing dried noodle film
Film.
Comparative example 1
A kind of preparation method of skin whitening, moisturizing dried noodle film, the difference from embodiment 1 is that, by step（1）The leaf of bamboo fiber
It is replaced with aloe fibre with China rose fiber, other conditions are all the same.
Comparative example 2
A kind of preparation method of skin whitening, moisturizing dried noodle film, the difference from embodiment 1 is that, step（1）Be added without Hippophate flavone and
Erythrose alcohol solution is stirred, and other conditions are all the same.
Comparative example 3
A kind of preparation method of skin whitening, moisturizing dried noodle film, the difference from embodiment 1 is that, step（2）It is added without Taraxacum Polysaccharides
And Polysaccharide from Portulaca oleracea, other conditions are all the same.
Selection subject 60 is tested（Subject：It is included in standard:1) men and women is unlimited, and the age is facial at 20 ~ 65 years old
Skin is partially black or partially yellow or has mild macular；2) health suffers from history, recipient site without any skin or systemic disease
For face, do not smeared in test and using other any external drugs and cosmetics etc. with effect；3) it is able to cooperate this test,
Attitude is conscientious, has certain expressive faculty, can really reflect the impression after use；4) voluntary participation, and sign and read informed consent form,
The requirement that research approach can be strictly observed using product and completes follow-up by research approach requirement；Exclusion criteria：1) gestation or the food in one's mouth
Newborn phase women；2) sensitive；3) skin of face breakage or the skin patient for observing facial state that has an impact；4) face uses
Cross laser, chemical peeling, creotoxin, skin filling or facelift；5) there is sunburn in nearly 1 month；6) current or 3 nearly
Other facial clinical researches were participated in month or received dermatologist curer）, 6 groups are equally divided into, every group 10, is used
The skin whitening, moisturizing dried noodle film of embodiment and comparative example preparation, which is immersed in clear water, impregnates 2min, and expansion spreads on face, pastes every time
10min or so does not need to be cleaned with clear water after applying, daily using primary, using preceding and using detection is primary after 30 days
The keratoderma water content of subject（Use moisture tester measurement left and right face cheek position water content of stratum corneum）, skin blackness
Value（Use the blackness value of skin dark red degree tester measurement left and right face cheek position）, skin brightness value and skin yellow value degree（It uses
Minolta analysis tester measures the brightness value and yellow value degree of left and right face cheek position）, testing result such as table 1：
The effect of 1 embodiment and comparative example dried noodle film skin whitening, moisturizing of table
As it can be seen from table 1 skin whitening, moisturizing dried noodle film of the invention can effectively improve the keratoderma water content of subject
With skin brightness value, skin blackness value and skin yellow value degree, skin whitening, moisturizing significant effect are reduced.
Claims (5)
1. a kind of preparation method of skin whitening, moisturizing dried noodle film, which is characterized in that specifically include following steps：
（1）The preparation of face paper
The China rose fiber of the leaf of bamboo fiber of 29 ~ 31 parts by weight, the aloe fibre of 9 ~ 10 parts by weight and 15 ~ 16 parts by weight is distinguished
Clean, co-grinding, be added 0.12 ~ 0.14 parts by weight Hippophate flavone and 28 ~ 30 parts by weight erythrose alcohol solution, with turn
19 ~ 21min is stirred in the blender stirring that speed is 330 ~ 350r/min clockwise, inverse with the blender that revolving speed is 430 ~ 450r/min
Hour hands stir 23 ~ 25min, and vacuum freeze drying is to no moisture under conditions of temperature is -18 ~ -16 DEG C, and routinely spun lacing method is grasped
It is reinforced as process, facial mask shape is made, spray drying obtains face paper to no moisture under conditions of temperature is 41 ~ 43 DEG C；
（2）The preparation of Essence
The fresh spinach of the fresh strawberry leaf of 8.6 ~ 9.2 parts by weight and 10 ~ 11 parts by weight is mixed with beating, 24 ~ 28 parts by weight, temperature are added
Degree stirs evenly for 61 ~ 65 DEG C of water, and constant-temperature enclosed placement, carries out row CO under conditions of temperature is 45 ~ 47 DEG C2Shooting flow
Body extraction processing takes extract, and the Taraxacum Polysaccharides of 0.13 ~ 0.15 parts by weight and the purslane of 0.20 ~ 0.22 parts by weight are added
Polysaccharide stirs evenly, and carries out magnetization treatment, obtains Essence；
（3）The preparation of dried noodle film
Face paper is immersed in 50 ~ 60min of immersion in Essence, is taken out, vacuum refrigeration under conditions of temperature is -15 ~ -13 DEG C
Dry, compression obtains skin whitening, moisturizing dried noodle film.
2. the preparation method of skin whitening, moisturizing dried noodle film according to claim 1, which is characterized in that step（1）Described is red
The temperature of fresh sugar alcohol aqueous solution is 52 ~ 54 DEG C, mass fraction is 6% ~ 7%.
3. the preparation method of skin whitening, moisturizing dried noodle film according to claim 1, which is characterized in that step（2）The CO2
Supercritical fluid extraction processing, under conditions of temperature is 39 ~ 41 DEG C, pressure is 18 ~ 20MPa, flow is 8 ~ 9L/h at extraction
Manage 44 ~ 48min, under conditions of temperature is 49 ~ 51 DEG C, pressure is 47 ~ 49MPa, flow is 19 ~ 21L/h extraction processing 23 ~
27min。
4. the preparation method of skin whitening, moisturizing dried noodle film according to claim 1, which is characterized in that step（2）The magnetic
Change processing, 8 ~ 10min of magnetization treatment under conditions of magnetic field strength is 770 ~ 810G, in the item that magnetic field strength is 1330 ~ 1370G
13 ~ 15min of magnetization treatment under part.
5. the skin whitening, moisturizing dried noodle of the preparation method preparation of described in any item skin whitening, moisturizing dried noodle films according to claim 1 ~ 4
Film.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811087387.3A CN108814993A (en) | 2018-09-18 | 2018-09-18 | A kind of preparation method of skin whitening, moisturizing dried noodle film |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811087387.3A CN108814993A (en) | 2018-09-18 | 2018-09-18 | A kind of preparation method of skin whitening, moisturizing dried noodle film |
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| CN108814993A true CN108814993A (en) | 2018-11-16 |
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| CN111514044A (en) * | 2020-05-30 | 2020-08-11 | 江苏福砳生物环保科技有限公司 | Zeolite energy facial mask and preparation method thereof |
| CN111803400A (en) * | 2020-08-18 | 2020-10-23 | 黑龙江中医药大学 | Traditional Chinese medicine polysaccharide moisturizing and freckle removing mask and preparation method thereof |
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Application publication date: 20181116 |
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