CN107216402A - A kind of preparation method of Polysaccharide from Portulaca oleracea - Google Patents

A kind of preparation method of Polysaccharide from Portulaca oleracea Download PDF

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Publication number
CN107216402A
CN107216402A CN201611209779.3A CN201611209779A CN107216402A CN 107216402 A CN107216402 A CN 107216402A CN 201611209779 A CN201611209779 A CN 201611209779A CN 107216402 A CN107216402 A CN 107216402A
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CN
China
Prior art keywords
polysaccharide
portulaca oleracea
preparation
purslane
portulaca
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Pending
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CN201611209779.3A
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Chinese (zh)
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不公告发明人
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Weng Shaoyu
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Weng Shaoyu
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Priority to CN201611209779.3A priority Critical patent/CN107216402A/en
Publication of CN107216402A publication Critical patent/CN107216402A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B37/00Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
    • C08B37/0003General processes for their isolation or fractionation, e.g. purification or extraction from biomass
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • Molecular Biology (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Sustainable Development (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

A kind of preparation method of Polysaccharide from Portulaca oleracea, belongs to drug preparation technique field.The present invention is using natural Chinese medicinal herb purslane as core, its effective component Polyose extraction is extracted using supersonic extracting method, its technique is simple, save cost, extracted amount is substantially increased, the polysaccharide component can be made an addition in skin care item, with the pharmacodynamic feature such as stronger anti-oxidant, anti-aging and immunity lifting.

Description

A kind of preparation method of Polysaccharide from Portulaca oleracea
Technical field
The present invention relates to technical field of traditional Chinese medicines, and in particular to a kind of preparation method of Polysaccharide from Portulaca oleracea.
Background technology
In recent years, with the change of social environment and natural environment, human diseases spectrum there occurs huge change.Become herein Under gesture, numerous traditional chemical synthetic drugs increasingly it is impossible to meet mankind's preventing and treating diseases the need for.Therefore, from enhancing machine Body inoxidizability and autoimmunity are set out, using the distinctive multicomponent of Chinese herb medicine, many effects Integrate adjustment ability to people Body anti-aging is anti-oxidant and immune system is improved, so as to reach the purpose for improving human health level, it has also become it is medical or Health care trend.Modern medicine study achievement shows that many Chinese herbal medicines contain polysaccharide, and this material is in human body by promoting machine The oxidation resistance of body, strengthens immune cell function, improves the effect such as cytokine secretion, can be achieved to each organ dysfunction of body Consolidation and lifting, the preventing and treating to disease has great significance.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of preparation method of Polysaccharide from Portulaca oleracea.
To realize the purpose of the present invention, the technical solution adopted in the present invention is:
A kind of preparation method of Polysaccharide from Portulaca oleracea, comprises the following steps:The purslane of drying and crushing is chosen, additional proportion is 1: 10-13 50-60 DEG C of distilled water, ultrasonic wave extraction 2-3 times, each 5-7min merges each extract solution, is concentrated under reduced pressure, past dense Ethanol is added in contracting liquid precipitates Polysaccharide from Portulaca oleracea, and high speed centrifugation 10-12min is precipitated, and is washed 5-6 times with acetone, low Temperature is lower to be freeze-dried, and obtains Polysaccharide from Portulaca oleracea.
Polysaccharide from Portulaca oleracea has the antioxidation more stronger than vitamin C, and research shows that Polysaccharide from Portulaca oleracea can be removed effectively The effect of various active oxygens, reduces lipid peroxidation product MDA generation, has reached anti-oxidant, the effect of anti-aging.
Concentration of alcohol in the step is 95-97%.
Low-temperature condition in the step is -50 to -55 DEG C.
The present invention is using natural Chinese medicinal herb purslane as core, using supersonic extracting method to its effective component Polyose extraction Extracted, its technique is simple, save cost, extracted amount is substantially increased, and the polysaccharide component can be made an addition in skin care item, tool There is the pharmacodynamic feature such as stronger anti-oxidant, anti-aging and immunity lifting.
Embodiment
The following implementation to the present invention is further described, so that those skilled in the art can be better understood from simultaneously Implement.
Embodiment 1
The purslane of drying and crushing is chosen, additional proportion is 1:12 55 DEG C of distilled water, ultrasonic wave extraction 3 times, each 6min is closed And each extract solution, it is concentrated under reduced pressure, 95% ethanol is added into concentrate precipitates Polysaccharide from Portulaca oleracea, and high speed centrifugation 11min is obtained Precipitation, wash 5 times with acetone, and freeze-drying, obtains Polysaccharide from Portulaca oleracea at -50 DEG C of low temperature.

Claims (3)

1. a kind of preparation method of Polysaccharide from Portulaca oleracea, it is characterised in that comprise the following steps:The purslane of drying and crushing is chosen, Additional proportion is 1:10-13 50-60 DEG C of distilled water, ultrasonic wave extraction 2-3 times, each 5-7min merges each extract solution, subtracted Pressure concentration, into concentrate, addition ethanol precipitates Polysaccharide from Portulaca oleracea, and high speed centrifugation 10-12min is precipitated, and is washed with acetone 5-6 times, it is freeze-dried at low temperature, obtains Polysaccharide from Portulaca oleracea.
2. a kind of preparation method of Polysaccharide from Portulaca oleracea according to claim 1, it is characterised in that the second in the step Determining alcohol is 95-97%.
3. the preparation method of a kind of Polysaccharide from Portulaca oleracea according to claim 1, it is characterised in that low in the step Temperature state is -50 to -55 DEG C.
CN201611209779.3A 2016-12-23 2016-12-23 A kind of preparation method of Polysaccharide from Portulaca oleracea Pending CN107216402A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611209779.3A CN107216402A (en) 2016-12-23 2016-12-23 A kind of preparation method of Polysaccharide from Portulaca oleracea

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611209779.3A CN107216402A (en) 2016-12-23 2016-12-23 A kind of preparation method of Polysaccharide from Portulaca oleracea

Publications (1)

Publication Number Publication Date
CN107216402A true CN107216402A (en) 2017-09-29

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611209779.3A Pending CN107216402A (en) 2016-12-23 2016-12-23 A kind of preparation method of Polysaccharide from Portulaca oleracea

Country Status (1)

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CN (1) CN107216402A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108814993A (en) * 2018-09-18 2018-11-16 安徽荷本化妆品有限公司 A kind of preparation method of skin whitening, moisturizing dried noodle film
CN110483655A (en) * 2019-08-30 2019-11-22 山东花物堂生物科技有限公司 A kind of Polysaccharide from Portulaca oleracea extraction process and its application in skin care item
CN116715782A (en) * 2023-05-19 2023-09-08 长春中医药大学 Purslane polysaccharide extract and preparation method and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102838682A (en) * 2011-06-22 2012-12-26 吴梦云 Extraction process of polysaccharide in purslane
CN103864943A (en) * 2012-12-18 2014-06-18 青岛中仁药业有限公司 Portulace polysaccharide ultrasonic-auxiliary extraction method
CN106220750A (en) * 2016-08-30 2016-12-14 佛山科学技术学院 The extracting method of Polysaccharide from Portulaca oleracea

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102838682A (en) * 2011-06-22 2012-12-26 吴梦云 Extraction process of polysaccharide in purslane
CN103864943A (en) * 2012-12-18 2014-06-18 青岛中仁药业有限公司 Portulace polysaccharide ultrasonic-auxiliary extraction method
CN106220750A (en) * 2016-08-30 2016-12-14 佛山科学技术学院 The extracting method of Polysaccharide from Portulaca oleracea

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108814993A (en) * 2018-09-18 2018-11-16 安徽荷本化妆品有限公司 A kind of preparation method of skin whitening, moisturizing dried noodle film
CN110483655A (en) * 2019-08-30 2019-11-22 山东花物堂生物科技有限公司 A kind of Polysaccharide from Portulaca oleracea extraction process and its application in skin care item
CN116715782A (en) * 2023-05-19 2023-09-08 长春中医药大学 Purslane polysaccharide extract and preparation method and application thereof

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Application publication date: 20170929