WO2021244004A1 - Zeolite energy mask and preparation method therefor - Google Patents

Abstract

A zeolite energy mask and a preparation method therefor, relating to the technical field of mask preparation, for use in solving the problem that effective disinfection and inflammation diminishing cannot be performed in a mask. The zeolite energy mask comprises the following component in percentage by weight: 30% of zeolite. The preparation method for the zeolite energy mask comprises the following steps: preparing raw materials in percentage by mass; stirring and mixing squalane and sodium carbomer, and then adding a proper amount of deionized water, butanediol, and propylene glycol. By adding zeolite, the mask can absorb many allergens, has strong adsorption and removal effects on heavy metals, toxic and harmful substances, and various waste and toxins, and also has adsorption and removal effects on some toxic radioactive chemical substances and harmful toxins causing serious contamination, so that the bacteria adsorption capacity and the disinfection rate of the mask are both remarkably improved, various toxins, harmful substances, and impurities on the face can be removed, and effects of disinfection, sterilization, and bacteriostasis are achieved.

Description

Zeolite energy facial mask and preparation method thereof Technical field

The invention relates to the technical field of facial mask preparation, in particular to a zeolite energy facial mask and a preparation method thereof.

Background technique

Facial mask is a multi-purpose cosmetic that integrates cleansing, skin care and beauty. Its function is to be applied to the facial skin. After a certain period of time is dried, a film is formed on the skin. The film is peeled off or After washing off, it can achieve the purpose of cleansing, skin care and beauty. Due to the adsorption of the mask, the secretion activity of the skin is vigorous. When the mask is peeled off or washed off, the skin secretions, dander, dirt, etc. When the mask is removed together, the skin looks abnormally clean and achieves a satisfactory cleansing effect; and because the mask covers the surface of the skin, it inhibits the evaporation of water, so as to soften the stratum corneum, expand the pores and sweat glands, and increase the skin surface temperature and promote Blood circulation enables the skin to effectively absorb the active nutrients in the mask and play a good skin care effect; as the mask is formed and dried, the tension generated increases the tension of the skin, causing the loose skin to tighten. Conducive to eliminating and reducing facial wrinkles, resulting in a cosmetic effect.

After searching, the Chinese patent application number CN201811632094.9 discloses a face mask treasure. The face mask treasure is provided with a plurality of coated bumps on the side in contact with the mask. The coated bumps include the following weights Component parts: 25-35 parts by weight of far-infrared stone; 7-12 parts by weight of Beitouite; 8-12 parts by weight of magnetite; 15-25 parts by weight of anion powder; 13-17 parts by weight of zeolite. The facial mask in the above patent has the following shortcomings: it cannot effectively sterilize and reduce inflammation for damaged skin such as acne-prone skin and dull skin.

Summary of the invention

The purpose of the present invention is to solve the shortcomings existing in the prior art, and proposes a zeolite energy mask and a preparation method thereof.

In order to achieve the above objectives, the present invention adopts the following technical solutions:

A zeolite energy mask, comprising the following components by weight: 30% zeolite, 10% dentamine extract, 2% butanediol, 3% propylene glycol, 3% carbomer sodium, 3% triethanolamine, nicotinamide stock solution, Squalane is 2%, the balance is water.

Preferably: the method for preparing the zeolite includes the following steps:

S11: After pulverizing clinoptilolite, pass a 100-mesh sieve to obtain a pulverized product;

S12: Put the obtained pulverized product into a muffle furnace, activate it at 480°C for 4 hours to obtain product A, and place product A in a desiccator for later use;

S13: Add formic acid solution to product A, and perform acid treatment under constant temperature shaking water bath conditions to obtain product B;

S14: After filtering product B with quantitative filter paper, the filter residue is repeatedly washed with deionized water until the filtrate is neutral, and the precipitate is taken;

S15: Dry the precipitate to a constant weight at 60°C to obtain the product.

Preferably: the solid-to-liquid ratio of the formic acid solution in S13 is 1 g/10 mL, and the concentration of the formic acid solution is 3 mol/L.

Preferably: the temperature of the water bath of the acid treatment in S13 is 60° C., and the time of the acid treatment is 3 hours.

Preferably: the preparation method of the purpurin extract includes the following steps:

S21: Take fresh denticles, wash them, add water 12 times their weight, and beat them to obtain a slurry;

S22: Put the slurry into a magnetic field with a magnetic field strength of 3600Gs, and perform magnetization at 45°C for 20 minutes to obtain a magnetized slurry;

S23: Microwave extraction of the magnetized slurry at a power of 600 W and a temperature of 55° C. for 30 s to obtain a dentate extract.

Preferably: the preparation method of squalane includes the following steps:

S31: Crush the washed and dried fresh camellia seeds and put them in the extraction tank;

S32: Add 85% ethanol of 5 times the weight of Camellia oleifera seeds, heat and boil for 2 hours, filter out the extract, then add 85% ethanol of the original ethanol to the residue in the tank, heat and boil for 2 hours, filter out the extract , Combine the two extracts and set aside;

S33: heating and concentrating the extract obtained in S32, recovering ethanol, and obtaining a concentrated extract for later use;

S34: Add 0.4mol/L potassium hydroxide-methanol solution, which accounts for 10% of its volume, to the concentrated extract, then place it in a water bath at 70°C under the protection of nitrogen for 4 hours. After cooling, the methyl ester After the chemical is completed, filter out the mixed liquid for later use;

S35: The mixed solution is subjected to a 0.01mol/L complexing agent-borax reaction, and separated and purified by macroporous resin chromatography, collecting 55% ethanol eluate, and then heating and concentrating to recover ethanol to obtain an ethanol-free concentrate;

S36: Add 1.5 times the volume of the ethanol-free concentrated liquid to the concentrated extract in step S33, extract for 0.5 hours at room temperature, filter the extract, and then add 1.5 times the petroleum ether to the concentrated liquid in the tank, and extract at room temperature For 0.5 hour, filter out the extract and combine the two extracts for later use;

S37: Wash the extract with water for 2-3 times. After washing, collect the supernatant, then heat and concentrate to recover petroleum ether to obtain crude squalane oil.

S38: The crude squalane oil is extracted with supercritical carbon dioxide to obtain squalane essential oil with a squalane content ≥80%.

Preferably: the preparation method of the nicotinamide stock solution includes the following steps:

S41: Add 3 parts of propylene glycol and 70 parts of water into the tempered pot, heat to 80°C, keep it warm for 30 minutes, and sterilize;

S42: When the temperature is lowered to 40°C, add 6 parts of nicotinamide, 3 parts of hydrolyzed silk, 0.08 parts of oligopeptide-1, 0.9 parts of palmitoyl pentapeptide-5, and 3 parts of Liuwei Zhenbai and mix and stir;

S43: After stirring uniformly, add 0.5 to 2 parts of 1,2-hexanediol, pass through 400 mesh filter cloth after stirring well, and then age for 2 hours to obtain nicotinamide stock solution.

A preparation method of zeolite energy facial mask includes the following steps:

S1: Prepare materials according to the above-mentioned mass percentage;

S2: Stir and mix squalane and carbomer sodium, and then add an appropriate amount of deionized water, butanediol, and propylene glycol. After stirring and mixing, let it stand for 20 hours;

S3: Add triethanolamine to adjust the pH to 7, and centrifuge at 2000r/min for 15min to obtain mixture A;

S4: Add nicotinamide stock solution to mixture A, stir evenly under 10R/S conditions, then stir while adding zeolite, and stir for 20 minutes;

S5: Finally, add the hordeum extract and the remaining deionized water, stir evenly, let it stand in the dark for 20 minutes, and centrifuge at 2000r/min for 15 minutes to obtain an energy cream mask containing zeolite.

The beneficial effects of the present invention are:

1. By adding zeolite to the mask, it can absorb a lot of allergens, heavy metals, toxic and hazardous substances, and various waste toxins. It has a strong adsorption and removal effect, and it has a strong effect on some toxic radioactive chemical substances and harmful toxins that have serious pollution. It also has the function of adsorption and removal, so that the bacteria adsorption capacity and sterilization rate of the mask have been significantly improved, and it can remove various toxins and harmful garbage and impurities on the face to achieve the effects of sterilization, sterilization and antibacterial.

2. By adding Purimi extract and nicotinamide stock solution, it has antibacterial and anti-inflammatory effects on facial acne, acne, dermatitis, etc. It has certain anti-oxidant properties on oils, effectively reducing skin dullness, and whitening at the same time. , Moisturizing and anti-aging.

3. By adding squalane to strengthen the repair of the epidermis, it can effectively form a natural protective film, help the balance between the skin and sebum, inhibit the peroxidation of skin lipids, can effectively penetrate into the skin, and promote the proliferation of skin basal cells, which can delay Skin aging, improvement and elimination of chloasma have obvious physiological effects. It can also open skin pores, promote blood microcirculation, increase cell metabolism, and help repair damaged cells.

Description of the drawings

Fig. 1 is a schematic diagram of the flow structure of a zeolite energy mask and its preparation method proposed by the present invention.

detailed description

The technical solution of this patent will be described in further detail below in conjunction with specific implementations.

The embodiments of this patent are described in detail below. Examples of the embodiments are shown in the accompanying drawings, in which the same or similar reference numerals indicate the same or similar elements or elements with the same or similar functions. The embodiments described below with reference to the drawings are exemplary, and are only used to explain the patent, and cannot be understood as a limitation to the patent.

In the description of this patent, it should be understood that the terms "center", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", The orientation or positional relationship indicated by "top", "bottom", "inner", "outer", etc. are based on the orientation or positional relationship shown in the drawings, and are only for the convenience of describing the patent and simplifying the description, rather than indicating or implying The device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation of this patent.

In the description of this patent, it should be noted that the terms "installation", "connection", "connection", and "setting" should be understood in a broad sense, unless clearly stipulated and limited otherwise. For example, they can be fixed connection, setting It can also be detachably connected and arranged, or integrally connected and arranged. For those of ordinary skill in the art, the specific meanings of the above-mentioned terms in this patent can be understood according to specific circumstances.

Example 1:

A zeolite energy facial mask and its preparation method, as shown in Figure 1, includes the following weight components: 30% zeolite, 10% dentamine extract, 2% butanediol, 3% propylene glycol, and 3% carbomer sodium , Triethanolamine 3%, Nicotinamide stock solution, Squalane 2%, the balance is water.

The preparation method of the zeolite includes the following steps:

S11: After pulverizing clinoptilolite, pass a 100-mesh sieve to obtain a pulverized product;

S12: Put the obtained pulverized product into a muffle furnace, activate it at 480°C for 4 hours to obtain product A, and place product A in a desiccator for later use;

S13: Add formic acid solution to product A, and perform acid treatment under constant temperature shaking water bath conditions to obtain product B;

S14: After filtering product B with quantitative filter paper, the filter residue is repeatedly washed with deionized water until the filtrate is neutral, and the precipitate is taken;

S15: Dry the precipitate to a constant weight at 60°C to obtain the product.

Further, the solid-to-liquid ratio of the formic acid solution in S13 is 1 g/10 mL, and the concentration of the formic acid solution is 3 mol/L.

Further, the temperature of the water bath of the acid treatment in S13 is 60° C., and the time of the acid treatment is 3 hours.

The preparation method of the purpurin extract includes the following steps:

S21: Take fresh denticles, wash them, add water 12 times their weight, and beat them to obtain a slurry;

S22: Put the slurry into a magnetic field with a magnetic field strength of 3600Gs, and perform magnetization at 45°C for 20 minutes to obtain a magnetized slurry;

S23: Microwave extraction of the magnetized slurry at a power of 600 W and a temperature of 55° C. for 30 s to obtain a dentate extract.

The preparation method of squalane includes the following steps:

S31: Crush the washed and dried fresh camellia seeds and put them in the extraction tank;

S32: Add 85% ethanol of 5 times the weight of Camellia oleifera seeds, heat and boil for 2 hours, filter out the extract, then add 85% ethanol of the original ethanol to the residue in the tank, heat and boil for 2 hours, filter out the extract , Combine the two extracts and set aside;

S33: heating and concentrating the extract obtained in S32, recovering ethanol, and obtaining a concentrated extract for later use;

S34: Add 0.4mol/L potassium hydroxide-methanol solution, which accounts for 10% of its volume, to the concentrated extract, then place it in a water bath at 70°C under the protection of nitrogen for 4 hours. After cooling, the methyl ester After the chemical is completed, filter out the mixed liquid for later use;

S35: The mixed solution is subjected to a 0.01mol/L complexing agent-borax reaction, and separated and purified by macroporous resin chromatography, collecting 55% ethanol eluent, and then heating and concentrating to recover ethanol to obtain an ethanol-free concentrate;

S36: Add 1.5 times the volume of the ethanol-free concentrated liquid to the concentrated extract in step S33, extract for 0.5 hours at room temperature, filter the extract, and then add 1.5 times the petroleum ether to the concentrated liquid in the tank, and extract at room temperature For 0.5 hour, filter out the extract and combine the two extracts for later use;

S37: Wash the extract with water for 2-3 times. After washing, collect the supernatant, then heat and concentrate to recover petroleum ether to obtain crude squalane oil.

S38: The crude squalane oil is extracted with supercritical carbon dioxide to obtain squalane essential oil with a squalane content ≥80%.

The preparation method of the nicotinamide stock solution includes the following steps:

S41: Add 3 parts of propylene glycol and 70 parts of water into the tempered pot, heat to 80°C, keep it warm for 30 minutes, and sterilize;

S42: When the temperature is lowered to 40°C, add 6 parts of nicotinamide, 3 parts of hydrolyzed silk, 0.08 parts of oligopeptide-1, 0.9 parts of palmitoyl pentapeptide-5, and 3 parts of Liuwei Zhenbai and mix and stir;

S43: After stirring uniformly, add 0.5 to 2 parts of 1,2-hexanediol, pass through 400 mesh filter cloth after stirring well, and then age for 2 hours to obtain nicotinamide stock solution.

Further, the mixing and stirring time in S42 is 20 minutes.

A preparation method of zeolite energy facial mask includes the following steps:

S1: Prepare materials according to the above-mentioned mass percentage;

S2: Stir and mix squalane and carbomer sodium, and then add an appropriate amount of deionized water, butylene glycol, and propylene glycol. After stirring and mixing, let it stand for 20 hours;

S3: Add triethanolamine to adjust the pH to 7, and centrifuge at 2000r/min for 15min to obtain mixture A;

S4: Add nicotinamide stock solution to mixture A, stir evenly under 10R/S conditions, then stir while adding zeolite, and stir for 20 minutes;

S5: Finally, add the hordeum extract and the remaining deionized water, stir evenly, let it stand in the dark for 20 minutes, and centrifuge at 2000r/min for 15 minutes to obtain an energy cream mask containing zeolite.

When this embodiment is used, by adding zeolite to the mask, it can absorb a lot of allergens, heavy metals, toxic and hazardous substances, and various waste toxins. It has a strong adsorption and removal effect, and it has a strong effect on some toxic radioactive chemical substances and their harmful effects. Severely polluted harmful toxins also have the effect of adsorption and removal, so that the bacteria adsorption capacity and sterilization rate of the mask have been significantly improved. It can remove all kinds of toxins and harmful garbage and impurities on the face to achieve the effects of sterilization, sterilization and antibacterial. Purimi extract has antibacterial and anti-inflammatory effects on facial acne, acne, dermatitis, etc. It has certain antioxidant properties on oils. Squalane strengthens and repairs the epidermis, effectively forming a natural protective film, helping skin and sebum. The balance can inhibit the peroxidation of skin lipids, can effectively penetrate into the skin, and promote the proliferation of skin basal cells, have obvious physiological effects on delaying skin aging, improving and eliminating chloasma, and can also open skin pores , Promote blood microcirculation, increase cell metabolism, and help repair damaged cells.

Example 2:

A zeolite energy mask and its preparation method, as shown in Figure 1, the following weight composition: zeolite 30%, dentamine extract 10%, butanediol 2%, propylene glycol 3%, carbomer sodium 3%, Triethanolamine 3%, nicotinamide stock solution, squalane 2%, and the balance is water.

The preparation method of the zeolite includes the following steps:

S11: After pulverizing clinoptilolite, pass a 200-mesh sieve to obtain a pulverized product;

S12: Put the prepared pulverized material into a muffle furnace, activate it at 500°C for 4 hours to obtain product A, and place product A in a desiccator for later use;

S13: Add formic acid solution to product A, and perform acid treatment under constant temperature shaking water bath conditions to obtain product B;

S14: After filtering product B with quantitative filter paper, the filter residue is repeatedly washed with deionized water until the filtrate is neutral, and the precipitate is taken;

S15: Dry the precipitate to a constant weight at 70°C to obtain the product.

Further, the solid-to-liquid ratio of the formic acid solution in S13 is 1 g/10 mL, and the concentration of the formic acid solution is 3 mol/L.

Further, the temperature of the water bath of the acid treatment in S13 is 60° C., and the time of the acid treatment is 3 hours.

The preparation method of the purpurin extract includes the following steps:

S21: Take fresh denticles, wash them, add water 12 times their weight, and beat them to obtain a slurry;

S22: Put the slurry into a magnetic field with a magnetic field strength of 3600Gs, and perform magnetization at 50°C for 25 minutes to obtain a magnetized slurry;

S23: Microwave extraction of the magnetized slurry at a power of 600 W and a temperature of 55° C. for 30 s to obtain a dentate extract.

The preparation method of squalane includes the following steps:

S31: Crush the washed and dried fresh camellia seeds and put them in the extraction tank;

S32: Add 85% ethanol of 5 times the weight of camellia seeds, heat and boil for 2.5 hours, filter out the extract, then add 85% ethanol of the original ethanol to the residue in the tank, heat and boil for 2.5 hours, filter out the extract , Combine the two extracts and set aside;

S33: heating and concentrating the extract obtained in S32, recovering ethanol, and obtaining a concentrated extract for later use;

S34: Add 0.4mol/L potassium hydroxide-methanol solution, which accounts for 10% of its volume, to the concentrated extract, then place it in a water bath at 80°C under the protection of nitrogen for 4 hours. After cooling, the methyl ester After the chemical is completed, filter out the mixed liquid for later use;

S35: The mixed solution is subjected to a 0.01mol/L complexing agent-borax reaction, and separated and purified by macroporous resin chromatography, collecting 55% ethanol eluent, and then heating and concentrating to recover ethanol to obtain an ethanol-free concentrate;

S36: Add 1.5 times the volume of the ethanol-free concentrated liquid to the concentrated extract in step S33, extract for 1 hour at room temperature, filter out the extract, then add 2 times the petroleum ether to the concentrated liquid in the tank, and extract at room temperature 1 hour, filter out the extract, combine the two extracts for later use;

S37: Wash the extract with water for 2-3 times. After washing, collect the supernatant, then heat and concentrate to recover petroleum ether to obtain crude squalane oil.

S38: The crude squalane oil is extracted with supercritical carbon dioxide to obtain squalane essential oil with a squalane content ≥80%.

The preparation method of the nicotinamide stock solution includes the following steps:

S41: Add 4 parts of propylene glycol and 70 parts of water into the tempered pot, heat to 80°C, keep it warm for 40 minutes, and sterilize;

S42: When the temperature is lowered to 40°C, add 5 parts of nicotinamide, 4 parts of hydrolyzed silk, 0.1 part of oligopeptide-1, 1 part of palmitoyl pentapeptide-5, and 5 parts of Liuwei Zhenbai and mix and stir;

S43: After stirring uniformly, add 0.5 to 2 parts of 1,2-hexanediol, pass through 400 mesh filter cloth after stirring well, and then age for 1.5 hours to obtain nicotinamide stock solution.

Further, the mixing and stirring time in S42 is 15 minutes.

A preparation method of zeolite energy facial mask includes the following steps:

S1: Prepare materials according to the above-mentioned mass percentage;

S2: Stir and mix squalane and carbomer sodium, and then add an appropriate amount of deionized water, butylene glycol, and propylene glycol. After stirring and mixing, let it stand for 30 hours;

S3: Add triethanolamine to adjust the pH to 7, and centrifuge at 2000r/min for 20min to obtain mixture A;

S4: Add nicotinamide stock solution to mixture A, stir evenly under 10R/S conditions, then stir while adding zeolite, and stir for 25min;

S5: Finally, add the hornet extract and the remaining deionized water, stir evenly, let it stand in the dark for 25 minutes, and centrifuge at 2000r/min for 20 minutes to obtain an energy cream mask containing zeolite.

The above are only the preferred specific embodiments of the present invention, but the protection scope of the present invention is not limited to this. Anyone familiar with the technical field within the technical scope disclosed by the present invention, according to the technical solution of the present invention Equivalent replacements or changes to its inventive concept should all fall within the protection scope of the present invention.

Claims (8)

1. A zeolite energy mask, which is characterized in that it comprises the following components by weight: 30% zeolite, 10% dentamine extract, 2% butanediol, 3% propylene glycol, 3% carbomer sodium, 3% triethanolamine, Nicotinamide stock solution, squalane 2%, the balance is water.
2. The zeolite energy mask according to claim 1, wherein the preparation method of the zeolite comprises the following steps:

   S11: After pulverizing clinoptilolite, pass a 100-mesh sieve to obtain a pulverized product;

   S12: Put the obtained pulverized product into a muffle furnace, activate it at 480°C for 4 hours to obtain product A, and place product A in a desiccator for later use;

   S13: Add formic acid solution to product A, and perform acid treatment under constant temperature shaking water bath conditions to obtain product B;

   S14: After filtering product B with quantitative filter paper, the filter residue is repeatedly washed with deionized water until the filtrate is neutral, and the precipitate is taken;

   S15: Dry the precipitate to a constant weight at 60°C to obtain the product.
3. The zeolite energy mask according to claim 2, wherein the solid-to-liquid ratio of the formic acid solution in S13 is 1 g/10 mL, and the concentration of the formic acid solution is 3 mol/L.
4. The zeolite energy mask according to claim 3, wherein the temperature of the water bath of the acid treatment in S13 is 60° C., and the time of the acid treatment is 3 hours.
5. A zeolite energy mask according to claim 1, characterized in that the preparation method of the purpurin extract comprises the following steps:

   S21: Take fresh denticles, wash them, add water 12 times their weight, and beat them to obtain a slurry;

   S22: Put the slurry into a magnetic field with a magnetic field strength of 3600Gs, and perform magnetization at 45°C for 20 minutes to obtain a magnetized slurry;

   S23: Microwave extraction of the magnetized slurry at a power of 600 W and a temperature of 55° C. for 30 s to obtain a dentate extract.
6. A zeolite energy mask according to claim 5, wherein the preparation method of squalane comprises the following steps:

   S31: Crush the washed and dried fresh camellia seeds and put them in the extraction tank;

   S32: Add 85% ethanol of 5 times the weight of camellia seeds, heat and boil for 2 hours, filter out the extract, then add 85% of the original ethanol to the residue in the tank, heat and boil for 2 hours, filter out the extract , Combine the two extracts and set aside;

   S33: heating and concentrating the extract obtained in S32, and recovering ethanol to obtain a concentrated extract for later use;

   S34: Add 0.4mol/L potassium hydroxide-methanol solution, which accounts for 10% of its volume, to the concentrated extract, then place it in a 70°C water bath and heat it for 4 hours under the protection of nitrogen. After cooling, the methyl ester After the chemical is completed, filter out the mixed solution for later use;

   S35: The mixed solution is subjected to a 0.01mol/L complexing agent-borax reaction, and separated and purified by macroporous resin chromatography, collecting 55% ethanol eluent, and then heating and concentrating to recover ethanol to obtain an ethanol-free concentrate;

   S36: Add 1.5 times the volume of the ethanol-free concentrated liquid to the concentrated extract in step S33, extract at room temperature for 0.5 hours, filter out the extract, then add 1.5 times the petroleum ether to the concentrated liquid in the tank, and extract at room temperature For 0.5 hour, filter out the extract and combine the two extracts for later use;

   S37: Wash the extract with water for 2-3 times. After washing, collect the supernatant, then heat and concentrate to recover petroleum ether to obtain crude squalane oil.

   S38: The crude squalane oil is extracted with supercritical carbon dioxide to obtain squalane essential oil with a squalane content ≥80%.
7. A zeolite energy mask according to claim 6, wherein the preparation method of the nicotinamide stock solution comprises the following steps:

   S41: Add 3 parts of propylene glycol and 70 parts of water into the tempered pot, heat to 80°C, keep it warm for 30 minutes, and sterilize;

   S42: When the temperature is lowered to 40°C, add 6 parts of nicotinamide, 3 parts of hydrolyzed silk, 0.08 parts of oligopeptide-1, 0.9 parts of palmitoyl pentapeptide-5, and 3 parts of Liuwei Zhenbai and mix and stir;

   S43: After stirring uniformly, add 0.5 to 2 parts of 1,2-hexanediol, pass through 400 mesh filter cloth after stirring well, and then age for 2 hours to obtain nicotinamide stock solution.
8. A method for preparing a zeolite energy mask, which is characterized in that it comprises the following steps:

   S1: Prepare materials according to the above-mentioned mass percentage;

   S2: Stir and mix squalane and carbomer sodium, and then add an appropriate amount of deionized water, butylene glycol, and propylene glycol. After stirring and mixing, let it stand for 20 hours;

   S3: Add triethanolamine to adjust the pH to 7, and centrifuge at 2000r/min for 15min to obtain mixture A;

   S4: Add nicotinamide stock solution to mixture A, stir evenly under 10R/S conditions, then stir while adding zeolite, and stir for 20 minutes;

   S5: Finally, add the hornet extract and the remaining deionized water, stir evenly, let it stand in the dark for 20 minutes, and centrifuge at 2000r/min for 15 minutes to obtain an energy cream mask containing zeolite.

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