CN112641643A - Activated zinc-loaded zeolite facial mask and preparation method thereof - Google Patents
Activated zinc-loaded zeolite facial mask and preparation method thereof Download PDFInfo
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- CN112641643A CN112641643A CN202110016277.3A CN202110016277A CN112641643A CN 112641643 A CN112641643 A CN 112641643A CN 202110016277 A CN202110016277 A CN 202110016277A CN 112641643 A CN112641643 A CN 112641643A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention relates to a preparation method of an activated zinc-loaded zeolite facial mask and a facial mask product, which mainly comprise the following steps: processing natural zeolite into zeolite powder; roasting the zeolite powder, dredging zeolite channels and removing organic impurities; mixing the roasted zeolite powder with water to form ore pulp, adding zinc salt into the ore pulp, adjusting the pH value to be 4.5-6.5, heating and controlling the temperature to be 40-90 ℃ for reaction, and preparing the ore pulp after the reaction into a filter cake; drying and crushing the filter cake to obtain zinc-loaded zeolite; activating the zinc-loaded zeolite to obtain activated zinc-loaded zeolite; mixing water with other raw materials, heating, stirring and dissolving uniformly, and sequentially adding the activated zinc-loaded zeolite and the toner color paste pigment; and continuously stirring the mixture evenly when the temperature of the water phase is reduced to obtain the activated zinc-loaded zeolite mask. The product has the function of deeply cleaning heavy metal residues on the skin; has strong antibacterial property and has antibacterial and acarid killing effects.
Description
The technical field is as follows:
the application belongs to the technical field of cosmetics, and particularly relates to an activated zeolite facial mask and a preparation method thereof.
Background art:
the inorganic antibacterial agent takes inorganic non-metallic ore as a carrier, fully utilizes the adsorbability ion exchange property of the inorganic non-metallic ore, wherein zinc ions are one of three antibacterial ions with safety recognized all over the world, has broad-spectrum antibacterial property and does not generate drug resistance; the antibacterial principle of the zinc-loaded zeolite is as follows: the zinc ions with positive charges and the microbial cell membranes with negative charges are firmly adsorbed and destroyed under the action of coulomb force, so that bacteria are killed.
Zinc ion is an essential trace element of the skin, and zinc is involved in the activity of many enzymes associated with human health and skin health. There are 55 zinc-containing Ingredients in the International Cosmetic materials catalog (INCI) Dictionary and Handbook. Of these, 7 are classified by FDA into OTC management due to safety and functional diversity, and these functions also include effects on the skin such as astringency, bacteriostasis, dandruff removal, protection, and the like. Among these functions, the known effects are basically the role of the divalent ion of Zn. With the progress of zincs in recent years, Zinc ions are known to be involved in the activities of over 300 enzymes and the actions of several transcription factors. For example, the demand for Zinc ions is greatly increased during the wound healing process.
There is a fresh record in the prior art of the application of zinc-loaded zeolite or similar inorganic antibacterial agents to facial masks and skin care products.
The invention content is as follows:
the application aims to provide an activated zinc-loaded zeolite facial mask, and the characteristics of the zinc-loaded zeolite such as antibiosis and harmful substance adsorption are applied to a facial mask product. And provides an efficient and reliable preparation process of the facial mask.
The technical scheme of the application comprises a preparation method of the activated zinc-loaded zeolite facial mask, which comprises the following steps,
processing natural zeolite into zeolite powder;
roasting the zeolite powder, dredging zeolite channels and removing organic impurities;
mixing the roasted zeolite powder with water to form ore pulp, adding zinc salt into the ore pulp, adjusting the pH value to be 4.5-6.5, heating and controlling the temperature to be 40-90 ℃ for reaction, and preparing the ore pulp after the reaction into a filter cake;
drying and crushing the filter cake to obtain zinc-loaded zeolite;
activating the zinc-loaded zeolite to obtain activated zinc-loaded zeolite;
mixing water with an emollient, an emulsifier, a thickener, a humectant, a preservative, an aromatizing agent and a regulator, heating to 80-85 ℃, stirring at the rotating speed of 2600-3000 r/min for uniform dissolution, and sequentially adding the activated zinc-loaded zeolite and a toner color paste pigment; and uniformly stirring when the temperature of the water phase is reduced to 60-50 ℃ to obtain the activated zinc-loaded zeolite facial mask.
Preferably, the zinc salt is any one or more of zinc chloride, zinc nitrate and zinc sulfate, or a hydrate thereof.
Preferably, the roasting temperature is 450-550 ℃, and the roasting time is 1-4 hours.
Preferably, the activation treatment is to bake the zinc-loaded zeolite in a high-temperature kiln for 1-10 hours.
The preferred ingredients for each of the raw materials described above are as follows:
the emollient includes: white oil, dimethicone and/or argan;
the emulsifier comprises: polyoxyethylene stearyl ether and/or oil-in-water emulsifiers;
the toner color paste pigment comprises chlorite mud powder;
the thickener comprises magnesium aluminum silicate;
the humectant includes: glycerol and/or 1-3 butanediol;
the regulator comprises disodium edetate.
The technical scheme of the application also comprises an activated zinc-loaded zeolite mask product prepared by the preparation method.
Preferably, the content of the activated zinc-loaded zeolite in the activated zinc-loaded zeolite mask is 5% -7%, the content of silicon dioxide in the activated zinc-loaded zeolite is more than 60%, and the content of aluminum oxide in the activated zinc-loaded zeolite is more than 11%; the pH value of the activated zinc-loaded zeolite mask is 6.5-7.0.
Preferably, the activated zinc-loaded zeolite mask further comprises one or more of the following components:
titanium dioxide, allantoin, vitamin E acetate, and cherry extract.
Preferably, the zinc-loaded zeolite in the activated zinc-loaded zeolite mask is in a 1250 mesh powder form.
The technical scheme of the application has the following advantages:
the facial mask contains zinc ions, has broad-spectrum sterilization effect, does not generate drug resistance, and does not generate side effects of skin injury, skin irritation and the like during sterilization. In addition, zinc ions participate in epithelial tissue differentiation, participate in transport and storage of metallothionein, have anti-inflammatory effects, can reduce ultraviolet-induced cell and gene damage, and can improve the tolerance of skin fibroblast cells to oxidative stress. Can improve skin elasticity and reduce wrinkle.
The zeolite as the zinc ion carrier has adsorbability, and after being combined with other components in the mask, the mask can adsorb aflatoxin, escherichia coli, ammonia nitrogen and hydrogen sulfide gas, heavy metals and other substances harmful to the skin, and has the function of deeply cleaning heavy metal residues on the skin.
The formula of the product also has good functions of nourishing, repairing and controlling oil, is blended with high-efficiency moisture-keeping components, and can solve the problems of fine lines, darkness, large pores and the like caused by dryness.
In the aspect of the preparation method, the control of the temperature can improve the emulsification degree of the raw materials including the zinc-loaded zeolite, simultaneously avoid the destruction of zinc ions in the mask and ensure the efficacy of the mask product.
The specific implementation mode is as follows:
the technical idea of the application is that the zinc-loaded zeolite is added into the facial mask, the zinc ions in the zinc-loaded zeolite play roles of resisting bacteria and protecting skin, and the zeolite plays a role of cleaning harmful substances such as heavy metals on the skin, and has conventional functions of nourishing, repairing, controlling oil and moisturizing. On the other hand, the application provides a preparation method specially suitable for the products, which is different from the conventional means, and the technical characteristics in the method can promote the emulsification effect of the raw materials such as the zinc-loaded zeolite and the like, and prevent the zinc ions from being damaged.
The examples of the application are as follows:
a preparation method of an activated zinc-loaded zeolite facial mask comprises the following steps,
processing natural zeolite into zeolite powder; this step is intended to prepare for subsequent processing.
Roasting the zeolite powder, preferably for 1-4 hours, dredging zeolite channels and removing organic impurities; meanwhile, the microporous structure of the zeolite is opened, so that zinc ions can be better loaded, and the adsorption performance of the zeolite is enhanced.
The calcined zeolite powder is mixed with water to form a slurry, preferably in the ratio zeolite powder to water 1: 10, adding the mixture into a reaction kettle, adding zinc salt into the ore pulp, adjusting the pH value to be 4.5-6.5, heating and controlling the temperature to be 40-90 ℃ for reaction, wherein the reaction time is 1-10 hours. Preparing the ore pulp after the reaction into a filter cake; control of temperature and ph is used to avoid destruction of zinc ions.
Drying and crushing the filter cake to obtain zinc-loaded zeolite;
activating the zinc-loaded zeolite to obtain activated zinc-loaded zeolite; specifically, the activation treatment can be to roast the zinc-loaded zeolite in a high-temperature kiln for 1-10 hours to enhance the adsorption performance and the ion exchange performance of the zinc-loaded zeolite. Making it into fine powder.
Mixing water with an emollient, an emulsifier, a thickener, a humectant, a preservative, an aromatizing agent and a regulator, heating to 80-85 ℃, stirring at the rotating speed of 2600-3000 r/min for uniform dissolution, and sequentially adding the activated zinc-loaded zeolite and a toner color paste pigment; and uniformly stirring when the temperature of the water phase is reduced to 60-50 ℃ to obtain the activated zinc-loaded zeolite facial mask. In the process of preparing the facial mask from the zeolite and other raw materials, the principle of firstly emulsifying and then stirring the zinc-loaded zeolite is followed, the temperature is controlled to be 80-85 ℃, the raw materials in various facial masks are added, the temperature can better promote the emulsification, the raw materials are uniformly stirred at a proper speed, at the moment, the temperature is reduced, the zeolite is added, the raw materials are stirred when the temperature is reduced to 60-50 ℃, the zinc ions in the zeolite can be prevented from being damaged by high temperature on the basis of not reducing the production efficiency, and the equipment does not need secondary heating.
Preferably, the zinc salt is any one or more of zinc chloride, zinc nitrate and zinc sulfate, or a hydrate thereof. The zinc salt is added in an amount of 5% by weight of the zeolite powder.
Preferably, the roasting temperature is 450-550 ℃, and the roasting time is 1-4 hours.
Preferably, the activation treatment is to bake the zinc-loaded zeolite in a high-temperature kiln for 1-10 hours.
The preferred ingredients for each of the raw materials described above are as follows:
the emollient includes: white oil, dimethicone and/or argan;
the emulsifier comprises: polyoxyethylene stearyl ether and/or oil-in-water emulsifiers;
the toner color paste pigment comprises chlorite mud powder;
the thickener comprises magnesium aluminum silicate;
the humectant includes: glycerol and/or 1-3 butanediol;
the regulator comprises disodium edetate.
The various materials and their functions are similar to those of the prior art and are not described in detail herein.
The technical scheme of the application also comprises an activated zinc-loaded zeolite mask product prepared by the preparation method.
Preferably, the content of the activated zinc-loaded zeolite in the activated zinc-loaded zeolite mask is 5% -7%, the content of silicon dioxide in the activated zinc-loaded zeolite is more than 60%, and the content of aluminum oxide in the activated zinc-loaded zeolite is more than 11%; the pH value of the activated zinc-loaded zeolite mask is 6.5-7.0. Through experiments, the zinc-loaded zeolite is safe when being used for the mask, and the zinc ions with positive charges and the microbial cell membranes with negative charges are firmly adsorbed and destroyed under the action of coulomb force, so that bacteria are killed; in addition, the zeolite can adsorb aflatoxin and escherichia coli, ammonia nitrogen and hydrogen sulfide gas and heavy metal.
Preferably, the activated zinc-loaded zeolite mask further comprises one or more of the following components:
titanium dioxide, allantoin, vitamin E acetate, and cherry extract.
Preferably, the zinc-loaded zeolite in the activated zinc-loaded zeolite mask is in a 1250 mesh powder form.
The following is a list of components and their content ratios for one example of the present application:
TABLE 1
The effective components in the above examples include water, 26# white oil, dimethicone, wacker DM350 silicone oil, Morocco glycerin, polyoxyethylene stearyl ether, oil-in-water emulsifier, 1250 mesh calcined zinc-loaded zeolite, TiO2 USP BC 3328, chlorite mud powder (volcanic mud), magnesium aluminum silicate, glycerin, 1-3 butanediol, allantoin, vitamin E acetate, cherry extract, preservative, flavoring agent, disodium edetate, and activated zinc-loaded zeolite. The product prepared according to the formula proportion has good functions of nourishing, repairing and controlling oil, and can solve the problems of fine lines, darkness, large pores and the like caused by drying. The present invention uses zeolite from Liaoning. Has the following advantages: has the function of deeply cleaning the heavy metal residue on the skin; has strong antibacterial property and has antibacterial and acarid killing effects. The prepared facial mask has the advantages that efficient moisture-retaining components are blended into a formula system, so that the facial mask has good functions of nourishing, repairing and controlling oil.
The above description is only exemplary of the present application and should not be taken as limiting the present application, as any modification, equivalent replacement, or improvement made within the spirit and principle of the present application should be included in the protection scope of the present application.
Claims (9)
1. A preparation method of an activated zinc-loaded zeolite facial mask, which is characterized in that,
processing natural zeolite into zeolite powder;
roasting the zeolite powder, dredging zeolite channels and removing organic impurities;
mixing the roasted zeolite powder with water to form ore pulp, adding zinc salt into the ore pulp, adjusting the pH value to be 4.5-6.5, heating and controlling the temperature to be 40-90 ℃ for reaction, and preparing the ore pulp after the reaction into a filter cake;
drying and crushing the filter cake to obtain zinc-loaded zeolite;
activating the zinc-loaded zeolite to obtain activated zinc-loaded zeolite;
mixing water with an emollient, an emulsifier, a thickener, a humectant, a preservative, an aromatizing agent and a regulator, heating to 80-85 ℃, stirring at the rotating speed of 2600-3000 r/min for uniform dissolution, and sequentially adding the activated zinc-loaded zeolite and a toner color paste pigment; and uniformly stirring when the temperature of the water phase is reduced to 60-50 ℃ to obtain the activated zinc-loaded zeolite facial mask.
2. The preparation method of the activated zinc-loaded zeolite facial mask as claimed in claim 1, wherein the zinc salt is any one or more of zinc chloride, zinc nitrate, zinc sulfate or their mixture or their hydrate.
3. The preparation method of the activated zinc-loaded zeolite facial mask according to claim 1, wherein the roasting temperature is 450-550 ℃ and the roasting time is 1-4 hours.
4. The preparation method of the activated zinc-loaded zeolite facial mask according to claim 1, wherein the activation treatment is baking the zinc-loaded zeolite in a high-temperature kiln for 1-10 hours.
5. The method for preparing an activated zinc-loaded zeolite mask as claimed in claim 1, wherein,
the emollient includes: white oil, dimethicone and/or argan;
the emulsifier comprises: polyoxyethylene stearyl ether and/or oil-in-water emulsifiers;
the toner color paste pigment comprises chlorite mud powder;
the thickener comprises magnesium aluminum silicate;
the humectant includes: glycerol and/or 1-3 butanediol;
the regulator comprises disodium edetate.
6. An activated zinc-loaded zeolite facial mask prepared by the preparation method of any one of claims 1 to 5.
7. The activated zinc-loaded zeolite mask of claim 6, wherein the activated zinc-loaded zeolite comprises 5% to 7% of the activated zinc-loaded zeolite mask, wherein the activated zinc-loaded zeolite comprises greater than 60% silica and greater than 11% alumina; the pH value of the activated zinc-loaded zeolite mask is 6.5-7.0.
8. The activated zinc-loaded zeolite mask of claim 6, further comprising one or more of the following ingredients:
titanium dioxide, allantoin, vitamin E acetate, and cherry extract.
9. The activated zinc-loaded zeolite mask of claim 6, wherein said zinc-loaded zeolite in said activated zinc-loaded zeolite mask is in the form of a 1250 mesh powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110016277.3A CN112641643A (en) | 2021-01-07 | 2021-01-07 | Activated zinc-loaded zeolite facial mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110016277.3A CN112641643A (en) | 2021-01-07 | 2021-01-07 | Activated zinc-loaded zeolite facial mask and preparation method thereof |
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| CN112641643A true CN112641643A (en) | 2021-04-13 |
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| CN202110016277.3A Pending CN112641643A (en) | 2021-01-07 | 2021-01-07 | Activated zinc-loaded zeolite facial mask and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113576989A (en) * | 2021-08-02 | 2021-11-02 | 辽宁工程技术大学 | Zeolite-loaded aloe vera gel for treating acne and preparation method thereof |
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| US20060099161A1 (en) * | 2002-10-25 | 2006-05-11 | Toshihiko Nakane | Skin preparations for external use |
| KR20090112138A (en) * | 2008-04-23 | 2009-10-28 | 손준형 | Zeolite mask pack composition for treating acnes or whitening skins, and preparation thereof |
| CN107875069A (en) * | 2017-12-22 | 2018-04-06 | 广州环亚化妆品科技有限公司 | A kind of mineral clay mask and preparation method thereof |
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2021
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060099161A1 (en) * | 2002-10-25 | 2006-05-11 | Toshihiko Nakane | Skin preparations for external use |
| CN1738589A (en) * | 2003-01-16 | 2006-02-22 | 科蒂股份有限公司 | Self-heating cosmetic products |
| KR20090112138A (en) * | 2008-04-23 | 2009-10-28 | 손준형 | Zeolite mask pack composition for treating acnes or whitening skins, and preparation thereof |
| CN107875069A (en) * | 2017-12-22 | 2018-04-06 | 广州环亚化妆品科技有限公司 | A kind of mineral clay mask and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113576989A (en) * | 2021-08-02 | 2021-11-02 | 辽宁工程技术大学 | Zeolite-loaded aloe vera gel for treating acne and preparation method thereof |
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Application publication date: 20210413 |