CN108729271B - Multi-color-register printing fabric adopting digital jet printing and preparation method thereof - Google Patents
Multi-color-register printing fabric adopting digital jet printing and preparation method thereof Download PDFInfo
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- CN108729271B CN108729271B CN201810711124.9A CN201810711124A CN108729271B CN 108729271 B CN108729271 B CN 108729271B CN 201810711124 A CN201810711124 A CN 201810711124A CN 108729271 B CN108729271 B CN 108729271B
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Abstract
The invention discloses a multi-color-register printing fabric adopting digital jet printing and a preparation method thereof, wherein the fabric is prepared by adopting a multi-color-register printing method of natural dye, the multi-component characteristic and the acid-base color development characteristic of the natural dye are utilized, and the processes of plasma pretreatment, alkaline protein pulp printing, dyeing, post-treatment and the like are carried out, so that the color 1 obtained by dyeing a non-printing part, the color 2 at an alkaline protein printing outline part and the color 3 at the alkaline protein printing part can be realized on the fabric by only using one natural dye, namely, the printing effect with the working stroke outline characteristic of three color sets is realized; the invention reduces the variety of required dyes, does not need plate making, has simple process and low cost, the pattern has the effect of imitating the artificial strokes, and the auxiliary agent is ecological and environment-friendly, thereby meeting the requirements of energy conservation and emission reduction in processing and ecological safety of products.
Description
The application is application number: 201710151660.3, filing date: 2017-03-15, name: the divisional application of 'multi-color process printing method of natural dye'.
Technical Field
The invention relates to a multi-color-register printing method of natural dye.
Background
The natural dye multi-color printing overcomes the monotonous appearance of single color of dyed fabrics, the expressive force of pattern patterns is richer, visual impact of people is stronger, consumers are more attracted, the market prospect is wide, the printing is carried out by adopting a cationic modifier, then the fabrics are dyed by adopting natural dyes, the effects of deep light and light colors are not changed, only the fabrics are treated by adopting a deep light and light color mordant, and the fabrics are subjected to a multi-step dyeing process by adopting two or more than two sets of mordant dyes, wherein the three or more than two sets of mordant dyes are used for carrying out a multi-step dyeing process for dyeing on the fabrics, and the multi-color mordant dyeing process is not used for carrying out a multi-step dyeing process for dyeing on the fabrics.
Disclosure of Invention
The invention aims to provide a multi-color-register printing method using only one natural dye (plant extract), which reduces the variety of the required dye, does not need plate making, has simple process and low cost, has the effect of imitating the effect of a Chinese character 'gong' pattern, is ecological and environment-friendly as an auxiliary agent, and meets the requirements of energy conservation and emission reduction in processing and ecological safety of products.
The technical solution of the invention is as follows:
a multi-color process printing method of natural dye is characterized in that: sequentially comprises the following steps:
(1) low-temperature plasma pretreatment: the power is 5-10 kilowatts, the vehicle speed is 5-10 m/min, and the atmosphere is as follows: air;
(2) and (3) carrying out alkaline protein pulp printing on the fabric: the printing paste comprises the following components: lime, bean flour, water, the proportion of 1: 3-4: 5-6; uniformly mixing the printing paste, and carrying out spray printing on the patterns under the control of a computer through a digital printing nozzle;
(3) drying at the low temperature of 60-90 ℃;
(4) preparing natural dye solution, namely adding acetic acid or hydrochloric acid into 60-100 g/L of extracted natural dye to adjust the pH value to 3-6;
(5) putting the dried printed fabric into a dye solution for dyeing, wherein the dyeing temperature is 80-90 ℃, and the dyeing time is 10-30 min;
(6) putting the dyed fabric into a post-treatment solution, wherein the treatment temperature is 30-50 ℃, the treatment time is 10-20 min, the concentration of the post-treatment agent is 2-10 g/L, and the pH value is 6-10;
(7) taking out, ultrasonic washing with ultrasonic power of 60-100W, frequency of 40-80Hz, temperature of 50 deg.C, and time of 5-20 min.
The natural dye is extracted from one of lignum sappan, radix Rubiae or folium Bambusae.
The post-treatment agent is ferrous sulfate, copper sulfate or plant ash. The fabric is made of one or more of cotton, hemp, real silk, wool, cashmere, chinlon, acrylic fiber, spandex, bamboo fiber, viscose, tencel, modal, polylactic acid fiber and acetate fiber.
The invention provides a method for realizing three-color printing by using only one natural dye by utilizing the multi-component characteristic and the acid-base color development characteristic of the dye extracted from natural plants through the processes of plasma pretreatment, alkaline protein pulp printing, dyeing, post-treatment and the like. The method reduces the variety of required dyes, does not need plate making, has simple process and low cost, ensures that the pattern has the effect of imitating the artificial strokes, is ecological and environment-friendly as an auxiliary agent, and meets the requirements of energy conservation and emission reduction in processing and ecological safety of products.
The plasma treatment aims at improving the adhesion of the alkaline protein printing paste to the fabric, and the continuous plasma treatment equipment is used, has an air atmosphere, is efficient to operate and is low in cost.
The physical and chemical actions of the basic protein printing paste on subsequent natural dyes are utilized, namely, the subsequent dyeing and post-treatment processing are carried out, due to the acid-base difference (the alkalinity of the printing part and the weak acidity of the dyeing part) of the printing part and the action of protein in the printing paste, the dyeing liquid is firstly blocked, neutralized and separated by the basic protein paste at the outline part at the printing part except for dyeing at the non-printing part, the separated part of the dye enters the printing part to dye fibers, and the outline part is another separated dye component. Therefore, the color 1 obtained by dyeing at a non-printing position, the color 2 at the outline of the basic protein printing and the color 3 of the basic protein printing part are generated on the fabric, namely, the printing effect with the outline characteristic of the strongbox of three-color register is generated.
The present invention will be further described with reference to the following examples.
Detailed Description
Example 1:
a multi-color process printing method of natural dye comprises the following steps in sequence:
(1) low-temperature plasma pretreatment: the power is 5-10 kilowatts, the vehicle speed is 5-10 m/min, and the atmosphere is as follows: air;
(2) the fabric is printed by alkaline protein paste, and the printing paste comprises the following components: lime, bean flour, water, the proportion of 1: 3-4: 5-6. Uniformly blending, and carrying out spray printing on the patterns through a digital printing nozzle under the control of a computer;
(3) low temperature drying (60 ℃ -90 ℃ C.)
(4) Preparing natural dye liquor, namely extracting 80 g/L of the dye liquor, and adding hydrochloric acid to adjust the pH value to 5.
The dye is extracted from traditional Chinese medicine sappan wood, and the extraction method comprises the following steps:
adding water into 8 parts of sappan wood, 2 parts of sodium hydroxide and 100 parts of water, adding the sodium hydroxide into the sappan wood, soaking for a period of time, boiling for 30min, and filtering to prepare 80 g/L of sappan wood extract.
(5) And (3) putting the dried printed fabric into a dye liquor for dyeing at the temperature of 80-90 ℃ for 10-30 min.
(6) The dyed fabric is put into the post-treatment liquid, the temperature is 30-50 ℃, the time is 10-20 min, the concentration of the post-treatment agent is 2-10 g/L, the pH value is 6-10, and the post-treatment agent is ferrous sulfate.
(7) Taking out and ultrasonically washing. Ultrasonic power is 60-100W, frequency is 40-80Hz, temperature is 50 ℃, and time is 5-20 min.
The fabric is made of one or more of cotton, hemp, real silk, wool, cashmere, chinlon, acrylic fiber, spandex, bamboo fiber, viscose, tencel, modal, polylactic acid fiber and acetate fiber.
Example 2:
(1) low-temperature plasma pretreatment: the power is 5-10 kilowatts, the vehicle speed is 5-10 m/min, and the atmosphere is as follows: air;
(2) the fabric is printed by alkaline protein paste, and the printing paste comprises the following components: lime, bean flour, water, the proportion of 1: 3-4: 5-6. Uniformly blending, and carrying out spray printing by controlling the pattern through a digital printing nozzle by a computer.
(3) Low temperature drying (60 ℃ -90 ℃ C.)
(4) Preparing a natural dye liquor, namely extracting 60 g/L of the dye liquor, and adding hydrochloric acid to adjust the pH value to 3.
The dye is extracted from traditional Chinese medicine madder, and the extraction method comprises the following steps:
6 parts of madder, 3 parts of sodium carbonate and 100 parts of water, adding water into the madder, adding the sodium carbonate into the madder, soaking the madder for a period of time, boiling the mixture for 30min, and filtering the mixture to prepare 60 g/L of an extracting solution of the madder.
(5) And (3) putting the dried printed fabric into a dye liquor for dyeing at the temperature of 80-90 ℃ for 10-30 min.
(6) Putting the dyed fabric into the post-treatment liquid, wherein the temperature is 30-50 ℃, the time is 10-20 min, the concentration of the post-treatment agent is 2-10 g/L, the pH value is 6-10, and the post-treatment agent is plant ash.
(7) Taking out and ultrasonically washing. Ultrasonic power is 60-100W, frequency is 40-80Hz, temperature is 50 ℃, and time is 5-20 min.
The fabric is made of one or more of cotton, hemp, real silk, wool, cashmere, chinlon, acrylic fiber, spandex, bamboo fiber, viscose, tencel, modal, polylactic acid fiber and acetate fiber.
Example 3:
(1) low-temperature plasma pretreatment: the power is 5-10 kilowatts, the vehicle speed is 5-10 m/min, and the atmosphere is as follows: air;
(2) the fabric is printed by alkaline protein paste, and the printing paste comprises the following components: lime, bean flour, water, the proportion of 1: 3-4: 5-6. Uniformly blending, and carrying out spray printing by controlling the pattern through a digital printing nozzle by a computer.
(3) Low temperature drying (60 ℃ -90 ℃ C.)
(4) Preparing natural dye liquor, namely extracting the dye liquor with the concentration of 100 g/L, and adding acetic acid to adjust the pH value to 6.
The dye is extracted from traditional Chinese medicine lophatherum gracile, and the extraction method comprises the following steps:
10 parts of lophatherum gracile, 2 parts of sodium hydroxide and 100 parts of water, wherein the water and the sodium hydroxide are added into the lophatherum gracile, the water and the sodium hydroxide are soaked for a period of time, and then the 100 g/L of lophatherum gracile extract is prepared by boiling for 30min and filtering.
(5) And (3) putting the dried printed fabric into a dye liquor for dyeing at the temperature of 80-90 ℃ for 10-30 min.
(6) The dyed fabric is put into the post-treatment liquid, the temperature is 30-50 ℃, the time is 10-20 min, the concentration of the post-treatment agent is 2-10 g/L, the pH value is 6-10, and the post-treatment agent is copper sulfate.
(7) Taking out and ultrasonically washing. Ultrasonic power is 60-100W, frequency is 40-80Hz, temperature is 50 ℃, and time is 5-20 min.
The fabric is made of one or more of cotton, hemp, real silk, wool, cashmere, chinlon, acrylic fiber, spandex, bamboo fiber, viscose, tencel, modal, polylactic acid fiber and acetate fiber.
Claims (2)
1. A multi-color-register printing fabric adopting digital jet printing is characterized in that: the fabric is made of one or more of cotton, hemp, real silk, wool, cashmere, chinlon, acrylic fiber, spandex, bamboo fiber, viscose, tencel, modal, polylactic acid fiber and acetate fiber;
the multi-color-set printing method of the natural dye is prepared by adopting the multi-color-set printing method of the natural dye, and the multi-color-set printing method of the natural dye sequentially comprises the following steps:
(1) low-temperature plasma pretreatment: the power is 5-10 kilowatts, the vehicle speed is 5-10 m/min, and the atmosphere is as follows: air;
(2) and (3) carrying out alkaline protein pulp printing on the fabric: the printing paste comprises the following components: lime, bean flour, water, the proportion of 1: 3-4: 5-6; uniformly mixing the printing paste, and carrying out spray printing on the patterns under the control of a computer through a digital printing nozzle;
(3) drying at the low temperature of 60-90 ℃;
(4) preparing a natural dye solution, namely adding hydrochloric acid into the extracted dye solution of 60 g/L to adjust the pH value to 3;
the dye is extracted from traditional Chinese medicine madder, and the extraction method comprises the following steps:
6 parts of madder, 3 parts of sodium carbonate and 100 parts of water, adding water into the madder, adding the sodium carbonate, soaking for a period of time, boiling for 30min, and filtering to prepare 60 g/L of an extract of the madder;
(5) putting the dried printed fabric into a dye solution for dyeing, wherein the dyeing temperature is 80-90 ℃, and the dyeing time is 10-30 min;
(6) putting the dyed fabric into a post-treatment solution, wherein the treatment temperature is 30-50 ℃, the treatment time is 10-20 min, the concentration of the post-treatment agent is 2-10 g/L, and the pH value is 6-10;
(7) taking out, ultrasonic washing with ultrasonic power of 60-100W, frequency of 40-80Hz, temperature of 50 deg.C, and time of 5-20 min;
the post-treatment agent is ferrous sulfate, copper sulfate or plant ash.
2. A method for preparing a multi-color printed fabric by digital jet printing according to claim 1, which comprises the following steps: the multi-color-set printing method of the natural dye is prepared by adopting the multi-color-set printing method of the natural dye, and the multi-color-set printing method of the natural dye sequentially comprises the following steps:
(1) low-temperature plasma pretreatment: the power is 5-10 kilowatts, the vehicle speed is 5-10 m/min, and the atmosphere is as follows: air;
(2) and (3) carrying out alkaline protein pulp printing on the fabric: the printing paste comprises the following components: lime, bean flour, water, the proportion of 1: 3-4: 5-6; uniformly mixing the printing paste, and carrying out spray printing on the patterns under the control of a computer through a digital printing nozzle;
(3) drying at the low temperature of 60-90 ℃;
(4) preparing a natural dye solution, namely adding hydrochloric acid into the extracted dye solution of 60 g/L to adjust the pH value to 3;
the dye is extracted from traditional Chinese medicine madder, and the extraction method comprises the following steps:
6 parts of madder, 3 parts of sodium carbonate and 100 parts of water, adding water into the madder, adding the sodium carbonate, soaking for a period of time, boiling for 30min, and filtering to prepare 60 g/L of an extract of the madder;
(5) putting the dried printed fabric into a dye solution for dyeing, wherein the dyeing temperature is 80-90 ℃, and the dyeing time is 10-30 min;
(6) putting the dyed fabric into a post-treatment solution, wherein the treatment temperature is 30-50 ℃, the treatment time is 10-20 min, the concentration of the post-treatment agent is 2-10 g/L, and the pH value is 6-10;
(7) taking out, ultrasonic washing with ultrasonic power of 60-100W, frequency of 40-80Hz, temperature of 50 deg.C, and time of 5-20 min;
the post-treatment agent is ferrous sulfate, copper sulfate or plant ash.
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