CN105603788B - A kind of plasma is crosslinked composite modified high-precision cashmere digital printing process - Google Patents
A kind of plasma is crosslinked composite modified high-precision cashmere digital printing process Download PDFInfo
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- CN105603788B CN105603788B CN201510800395.8A CN201510800395A CN105603788B CN 105603788 B CN105603788 B CN 105603788B CN 201510800395 A CN201510800395 A CN 201510800395A CN 105603788 B CN105603788 B CN 105603788B
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Abstract
The invention discloses a kind of plasma to be crosslinked composite modified high-precision cashmere digital printing process, comprises the following steps：(1) fleece fabrics is through evaporating technique；(2) fleece fabrics plasma etching industrial；(3) fleece fabrics crosslinking agent photoresist coating process；(4) fleece fabrics digital decorating machine jet printing technique；(5) be heating and curing to obtain finished product.The present invention is using low temperature plasma pretreatment cashmere fiber, physical etchings and chemical oxidation occur on cashmere surface, introduce oxy radical, 3 (2 are used after assigning the excellent hydrophilic effect of cashmere, 3 the third oxygen of epoxy) propyl trimethoxy silicane processing fiber, improve the digital spray printing performance of cashmere fiber, improve cashmere fiber absorption color ink ability.Without through evaporating washing, obtaining bright-coloured clearly decorative pattern, simplifying revenue stamp process, spray printing is flexible, can meet the needs of personalized and quantitative production, small lot and fast reaction after red ink paste used for seals.
Description
Technical field
The invention belongs to digit printing field, and in particular to a kind of composite modified high-precision cashmere number of plasma-crosslinking
Code printing technology.
Background technology
Digit printing is the model that computer technology is combined with traditional textile printing technique.With energy consumption is low, blowdown is few,
Change the features such as fast, printing floral designs stereovision is strong, and color and luster change is more without plate-making, flower pattern, pattern can be adjusted at any time
Color and size, it is that conventional stamp institute is unapproachable.
Base with people to the cry more and more higher of environmental protection, green and ecological textile as textile industry sustainable development
Plinth, exploitation environmental pollution is small or free of contamination material surface modifying technique turns into a main direction of studying.Plasma
Process for modifying surface is described as " green " process technology, enjoys the very big attention of people.Low Temperature Plasma Treating textile material,
Fiber surface chemical constitution and form can be changed, but its penetrable material surface is most deep only 10 μm, and some processing thickness only 10 is received
Rice or so, about 99.8% body still fully preserves, thus after processing the chemistry of fiber with physical property without aobvious
Write change, and its dyeability can be improved significantly.
The content of the invention
Goal of the invention：The present invention provides a kind of composite modified high-precision cashmere digital printing process of plasma-crosslinking.
Technical scheme：A kind of composite modified high-precision cashmere digital printing process of plasma-crosslinking, including following step
Suddenly：(1) fleece fabrics is through evaporating technique；(2) fleece fabrics plasma etching industrial；(3) fleece fabrics crosslinking agent photoresist coating process；
(4) fleece fabrics digital decorating machine jet printing technique；(5) be heating and curing to obtain finished product；
Wherein, in described (3) fleece fabrics crosslinking agent photoresist coating process, fabric is padded in the dressing liquid of compounding crosslinking agent
Processing, liquid carrying rate 50-60, dried at a temperature of 70-80 DEG C, it is described compounding crosslinking agent dressing liquid by following parts by weight group
It is grouped into：Nano-ZnO is 1-5 parts, and citric acid/sodium citrate pH value of buffer solution is 4.2 ± 0.2, myristalkonium
Ammonium chloride antiseptic is 1-5 parts, and 3- (2,3- the third oxygen of epoxy) propyl trimethoxy silicane is 10-15 parts, and remaining is water.
As further optimization：(1) fleece fabrics is evaporated in technique, and fleece fabrics is under loose formula state, spray
0.3-0.5g/L antistatic additive SN, fiber weightening 100g/m2, fabric enters J-type gas steam box gas with 20-40 ms/min and steamed, to steam
Vapour or hot-air are that medium gas at 100-110 DEG C steams.
As further optimization：In (2) the fleece fabrics plasma etching industrial, using AtomfloTM250 type normal pressures
Plasma jet equipment, ejection form plasma jet and are modified fleece fabrics, and fleece fabrics is laid in corona treatment
On the bottom crown of equipment, atmospheric pressure plasma jet treatment condition is as follows：Medium air, power parameter 380V, frequency 1000Hz, output
Power 30-120KW, processing speed 20-60m/min, the spacing 2-3mm of shower nozzle sample.
As further optimization：In (3) the fleece fabrics crosslinking agent photoresist coating process, if fabric is for a long time after reaction completely
Without digital printing process, covered, can be preserved for a long time with polypropylene film in fabric positive and negative；Short time after reaction completely
Interior carry out digital printing process, then polypropylene film covering is not needed.
As further optimization：(4) the fleece fabrics digit printing jet printing technique is digital spray printing, drying, the print
Pattern slurry is waterborne digital coating, and 0.4g/LGoon1201 amido silicon oils are added in mill base, and drying temperature is 90-110 DEG C, when
Between be 30-180s.
Beneficial effect：The specific advantage of the present invention is as follows：
(1) in the present invention, cashmere fiber is pre-processed using low temperature plasma, assigns the extraordinary etching effect of cashmere
Afterwards, with 3- (2,3- the third oxygen of epoxy) propyl trimethoxy silicane coupling agents as crosslinking agent by bridge formation base to cashmere surface, prepare
Reactive cashmere fiber, part amido silicon oil is added in water-based color paste of printing coating, form that plasma-crosslinking is compound to be changed
Property high accuracy cashmere digital printing process.The printing technology changes the floral designs stereovision of fast printing without plate-making, flower pattern
By force, color and luster changes more, antibacterial, anti-felting, softness.Meet demand and following textile techniques of the modern society people to personalization
Development trend.
(2) in the present invention, cashmere can obtain extraordinary ink absorption after Low Temperature Plasma Treating, be carried for industrialization
For fabulous pre-treatment effect, acted on by the Ou Lian of 3- (2,3- the third oxygen of epoxy) propyl trimethoxy silicane antiseptic is organic
Involvement cashmere fiber in so that fiber strength is also partly lifted, fleece fabrics antibacterial, keep fabric it is smooth, improve fabric obtain
Colo(u)r specification, prevent color ink imbibition from improving flower pattern fineness.With energy consumption is low, blowdown is few, need not plate-making, flower pattern compared with Conventional decal
The features such as change is fast, the floral designs stereovision of printing is strong, and color and luster change is more, can adjust the color and size of pattern at any time, be
Conventional stamp institute is unapproachable.
(3) in the present invention, under loose formula state, spray antistatic additive gas steams fleece fabrics, improves cashmere fiber wetability
Can, soften cashmere fiber surface scale Rotating fields, be advantageous to rear road plasma etching, improve etching effect.
(4) in the present invention, pretreatment is performed etching to cashmere fiber using low temperature plasma, destroys surface scale, is prevented
Only cashmere felting, fiber surface is produced segment polarity group, increase cashmere surface hydrophilicity and reactivity, while do not lose
Cashmere fiber strength.
(5) in the present invention, using the fleece fabrics crosslinking agent photoresist coating process equivalent to the fleece fabrics progress to etching
Build bridge, antimicrobial treatment, nano-ZnO, myristyl benzyl dimethyl chlorination ammonium antimicrobial agent provide cashmere antibacterial effect, 3- (2,3-
The oxygen of epoxy third) for propyl trimethoxy silicane to be crosslinked coupling agent, holding fabric is smooth, and fabric tinctorial yield is improved, prevents color ink from oozing
Change and improve flower pattern fineness, while digital printing color ink range of choice expands.
(6) in the present invention, digit printing uses coating, avoids the defect of water droplet circle caused by being steamed with road gas after acid dyes
Point, while spray printing speed greatly promotes, colour system range of choice expands, and improves fabric tinctorial yield, prevents color ink imbibition from improving flower pattern
Fineness.The feel that 20ml Goon1201 amido silicon oils (0.4g/L) are favorably improved fleece fabrics, filling are added in mill base
Gap in fiber, prevent fleece fabrics felting.
Embodiment
With reference to specific embodiment, the present invention will be described in detail.
Specific embodiment one：
A kind of composite modified high-precision cashmere digital printing process of plasma-crosslinking, comprise the following steps：
(1) fleece fabrics is through evaporating technique：Fleece fabrics sprays 0.3g/L antistatic additive SN, fiber under loose formula state
Increase weight 100g/m2, fabric enters J-type gas steam box gas with 20 ms/min and steams, using steam or hot-air as medium the gas at 100 DEG C
Steam；
Under loose formula state, spray antistatic additive gas steams fleece fabrics, improves cashmere fiber wettability, softens Cashmere fiber
Dimension table face Microstructure of epidermal scale, be advantageous to rear road plasma etching, improve etching effect.
(2) fleece fabrics plasma etching industrial：Using AtomfloTM250 type atmospheric plasma jet apparatus, spray
Form plasma jet and be modified fleece fabrics, fleece fabrics is laid on the bottom crown of apparatus for processing plasma, normal pressure etc.
Gas ions treatment conditions are as follows：Medium air, power parameter 380V, frequency 1000Hz, power output 30KW, processing speed 20m/
Min, the spacing 2mm of shower nozzle sample；
Pretreatment is performed etching to cashmere fiber using low temperature plasma, surface scale is destroyed, prevents cashmere felting, make
Fiber surface produces segment polarity group, increases cashmere surface hydrophilicity and reactivity, while does not lose cashmere fiber strength.
(3) fleece fabrics crosslinking agent photoresist coating process：Fabric is padded into processing, liquid carrying rate in the dressing liquid of compounding crosslinking agent
For 50, dried at a temperature of 70 DEG C, the dressing liquid of the compounding crosslinking agent is made up of the component of following parts by weight：Nano-ZnO is 1
Part, citric acid/sodium citrate pH value of buffer solution is 4.0, and myristyl benzyl dimethyl chlorination ammonium antimicrobial agent is 1 part, 3- (2,
The oxygen of 3- epoxies third) propyl trimethoxy silicane be 10 parts, remaining is water；
If fabric is covered for a long time without digital printing process in fabric positive and negative with polypropylene film after reaction completely
Lid, can be preserved for a long time；Digital printing process are carried out after reaction completely in short time, then do not need polypropylene film covering；
Built bridge, at antibacterial equivalent to the fleece fabrics to etching using the fleece fabrics crosslinking agent photoresist coating process
Reason, nano-ZnO, myristyl benzyl dimethyl chlorination ammonium antimicrobial agent provide cashmere antibacterial effect, 3- (2,3- the third oxygen of epoxy) third
Base trimethoxy silane is crosslinking coupling agent, keeps fabric smooth, improves fabric tinctorial yield, prevents color ink imbibition from improving flower pattern essence
Fineness, while digital printing color ink range of choice expands.
(4) fleece fabrics digital decorating machine jet printing technique：The print paste is waterborne digital coating, is added in mill base
0.4g/L Goon1201 amido silicon oils, drying temperature are 90 DEG C, time 30s；
Digit printing uses coating, avoids the fault of water droplet circle caused by being steamed with road gas after acid dyes, while spray printing
Speed greatly promotes, and colour system range of choice expands, and improves fabric tinctorial yield, prevents color ink imbibition from improving flower pattern fineness.In color
20ml Goon1201 amido silicon oils (0.4g/L) are added in slurry and are favorably improved the feel of fleece fabrics, gap in fiberfill fibers,
Prevent fleece fabrics felting.
(5) be heating and curing to obtain finished product.
Specific embodiment two：
A kind of composite modified high-precision cashmere digital printing process of plasma-crosslinking, comprise the following steps：
(1) fleece fabrics is through evaporating technique：Fleece fabrics sprays 0.5g/L antistatic additive SN, fiber under loose formula state
Increase weight 100g/m2, fabric enters J-type gas steam box gas with 40 ms/min and steams, using steam or hot-air as medium the gas at 110 DEG C
Steam；
Under loose formula state, spray antistatic additive gas steams fleece fabrics, improves cashmere fiber wettability, softens Cashmere fiber
Dimension table face Microstructure of epidermal scale, be advantageous to rear road plasma etching, improve etching effect.
(2) fleece fabrics plasma etching industrial：Using AtomfloTM250 type atmospheric plasma jet apparatus, spray
Form plasma jet and be modified fleece fabrics, fleece fabrics is laid on the bottom crown of apparatus for processing plasma, normal pressure etc.
Gas ions treatment conditions are as follows：Medium air, power parameter 380V, frequency 1000Hz, power output 120KW, processing speed
60m/min, the spacing 3mm of shower nozzle sample；
Pretreatment is performed etching to cashmere fiber using low temperature plasma, surface scale is destroyed, prevents cashmere felting, make
Fiber surface produces segment polarity group, increases cashmere surface hydrophilicity and reactivity, while does not lose cashmere fiber strength.
(3) fleece fabrics crosslinking agent photoresist coating process：Fabric is padded into processing, liquid carrying rate in the dressing liquid of compounding crosslinking agent
For 60, dried at a temperature of 80 DEG C, the dressing liquid of the compounding crosslinking agent is made up of the component of following parts by weight：Nano-ZnO is 5
Part, citric acid/sodium citrate pH value of buffer solution is 4.4, and myristyl benzyl dimethyl chlorination ammonium antimicrobial agent is 5 parts, 3- (2,
The oxygen of 3- epoxies third) propyl trimethoxy silicane be 15 parts, remaining is water；
If fabric is covered for a long time without digital printing process in fabric positive and negative with polypropylene film after reaction completely
Lid, can be preserved for a long time；Digital printing process are carried out after reaction completely in short time, then do not need polypropylene film covering；
Built bridge, at antibacterial equivalent to the fleece fabrics to etching using the fleece fabrics crosslinking agent photoresist coating process
Reason, nano-ZnO, myristyl benzyl dimethyl chlorination ammonium antimicrobial agent provide cashmere antibacterial effect, 3- (2,3- the third oxygen of epoxy) third
Base trimethoxy silane is crosslinking coupling agent, keeps fabric smooth, improves fabric tinctorial yield, prevents color ink imbibition from improving flower pattern essence
Fineness, while digital printing color ink range of choice expands.
(4) fleece fabrics digital decorating machine jet printing technique：The print paste is waterborne digital coating, is added in mill base
0.4g/L Goon1201 amido silicon oils, drying temperature are 110 DEG C, time 180s；
Digit printing uses coating, avoids the fault of water droplet circle caused by being steamed with road gas after acid dyes, while spray printing
Speed greatly promotes, and colour system range of choice expands, and improves fabric tinctorial yield, prevents color ink imbibition from improving flower pattern fineness.In color
20ml Goon1201 amido silicon oils (0.4g/L) are added in slurry and are favorably improved the feel of fleece fabrics, gap in fiberfill fibers,
Prevent fleece fabrics felting.
(5) be heating and curing to obtain finished product.
Specific embodiment three：
A kind of composite modified high-precision cashmere digital printing process of plasma-crosslinking, comprise the following steps：
(1) fleece fabrics is through evaporating technique：Fleece fabrics sprays 0.4g/L antistatic additive SN, fiber under loose formula state
Increase weight 100g/m2, fabric enters J-type gas steam box gas with 30 ms/min and steams, using steam or hot-air as medium the gas at 105 DEG C
Steam；
Under loose formula state, spray antistatic additive gas steams fleece fabrics, improves cashmere fiber wettability, softens Cashmere fiber
Dimension table face Microstructure of epidermal scale, be advantageous to rear road plasma etching, improve etching effect.
(2) fleece fabrics plasma etching industrial：Using AtomfloTM250 type atmospheric plasma jet apparatus, spray
Form plasma jet and be modified fleece fabrics, fleece fabrics is laid on the bottom crown of apparatus for processing plasma, normal pressure etc.
Gas ions treatment conditions are as follows：Medium air, power parameter 380V, frequency 1000Hz, power output 80KW, processing speed 40m/
Min, the spacing 2.4mm of shower nozzle sample；
Pretreatment is performed etching to cashmere fiber using low temperature plasma, surface scale is destroyed, prevents cashmere felting, make
Fiber surface produces segment polarity group, increases cashmere surface hydrophilicity and reactivity, while does not lose cashmere fiber strength.
(3) fleece fabrics crosslinking agent photoresist coating process：Fabric is padded into processing, liquid carrying rate in the dressing liquid of compounding crosslinking agent
For 54, dried at a temperature of 76 DEG C, the dressing liquid of the compounding crosslinking agent is made up of the component of following parts by weight：Nano-ZnO is 3
Part, citric acid/sodium citrate pH value of buffer solution is 4.2, and myristyl benzyl dimethyl chlorination ammonium antimicrobial agent is 3 parts, 3- (2,
The oxygen of 3- epoxies third) propyl trimethoxy silicane be 13 parts, remaining is water；
If fabric is covered for a long time without digital printing process in fabric positive and negative with polypropylene film after reaction completely
Lid, can be preserved for a long time；Digital printing process are carried out after reaction completely in short time, then do not need polypropylene film covering；
Built bridge, at antibacterial equivalent to the fleece fabrics to etching using the fleece fabrics crosslinking agent photoresist coating process
Reason, nano-ZnO, myristyl benzyl dimethyl chlorination ammonium antimicrobial agent provide cashmere antibacterial effect, 3- (2,3- the third oxygen of epoxy) third
Base trimethoxy silane is crosslinking coupling agent, keeps fabric smooth, improves fabric tinctorial yield, prevents color ink imbibition from improving flower pattern essence
Fineness, while digital printing color ink range of choice expands.
(4) fleece fabrics digital decorating machine jet printing technique：The print paste is waterborne digital coating, is added in mill base
0.4g/L Goon1201 amido silicon oils, drying temperature are 100 DEG C, time 130s；
Digit printing uses coating, avoids the fault of water droplet circle caused by being steamed with road gas after acid dyes, while spray printing
Speed greatly promotes, and colour system range of choice expands, and improves fabric tinctorial yield, prevents color ink imbibition from improving flower pattern fineness.In color
20ml Goon1201 amido silicon oils (0.4g/L) are added in slurry and are favorably improved the feel of fleece fabrics, gap in fiberfill fibers,
Prevent fleece fabrics felting.
(5) be heating and curing to obtain finished product.
The present invention is not limited to above-mentioned preferred forms, and anyone can show that other are various under the enlightenment of the present invention
The product of form, however, make any change in its shape or structure, it is every that there is skill identical or similar to the present application
Art scheme, is within the scope of the present invention.
Claims (1)
- A kind of 1. composite modified high-precision cashmere digital printing process of plasma-crosslinking, it is characterised in that：Including following step Suddenly：(1) fleece fabrics is through evaporating technique；(2) fleece fabrics plasma etching industrial；(3) fleece fabrics crosslinking agent photoresist coating process； (4) fleece fabrics digital decorating machine jet printing technique；(5) be heating and curing to obtain finished product；Wherein, in described (3) fleece fabrics crosslinking agent photoresist coating process, fabric is padded into place in the dressing liquid of compounding crosslinking agent Reason, liquid carrying rate 50-60%, dried at a temperature of 70-80 DEG C, it is described compounding crosslinking agent dressing liquid by following parts by weight group It is grouped into：Nano-ZnO is 1-5 parts, and citric acid/sodium citrate pH value of buffer solution is 4.2 ± 0.2, myristalkonium Ammonium chloride antiseptic is 1-5 parts, and 3- (2,3- the third oxygen of epoxy) propyl trimethoxy silicane is 10-15 parts, and remaining is water；(1) fleece fabrics is evaporated in technique, and fleece fabrics sprays 0.3-0.5g/L antistatic additive SN under loose formula state, Fiber weightening 100g/m2, fabric entered J-type gas steam box gas with 20-40 ms/min and steamed, existed using steam or hot-air as medium Gas steams at 100-110 DEG C；In (2) the fleece fabrics plasma etching industrial, using AtomfloTM250 type atmospheric plasma jet apparatus, spray Go out to be formed plasma jet and be modified fleece fabrics, fleece fabrics is laid on the bottom crown of apparatus for processing plasma, normal pressure Plasma process conditions are as follows：Medium air, power parameter 380V, frequency 1000Hz, power output 30-120KW, processing speed Spend 20-60m/min, the spacing 2-3mm of shower nozzle sample；In (3) the fleece fabrics crosslinking agent photoresist coating process, if fabric is for a long time without digital printing process after reaction completely, Covered, can be preserved for a long time with polypropylene film in fabric positive and negative；Digital printing process are carried out after reaction completely in short time, Polypropylene film covering is not needed then；(4) the fleece fabrics digit printing jet printing technique is digital spray printing, drying, and the print paste applies for waterborne digital Material, 0.4g/L Goon1201 amido silicon oils are added in mill base, drying temperature is 90-110 DEG C, time 30-180s.
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| CN106120200B (en) * | 2016-06-22 | 2018-10-19 | 武汉纺织大学 | A kind of the hydrophilic of single side wool fabric, antistatic finish device and method for sorting |
| CN108729271B (en) * | 2017-03-15 | 2020-07-31 | 南通大学 | Multi-color-register printing fabric adopting digital jet printing and preparation method thereof |
| CN108642650A (en) * | 2018-05-09 | 2018-10-12 | 内蒙古鄂尔多斯资源股份有限公司 | The two-sided digital printing method and cashmere product of cashmere tatting product |
| CN109112856B (en) * | 2018-07-17 | 2021-01-15 | 嘉兴学院 | Digital printing process for cotton fabric |
| CN110409173A (en) * | 2019-07-19 | 2019-11-05 | 浙江玛戈利亚羊绒世家有限公司 | A kind of method of fleece fabrics anti-fluffing and anti-pilling |
| CN116815521B (en) * | 2023-08-23 | 2024-01-09 | 杭州帛阳新材料科技有限公司 | Anhydrous digital printing method |
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| CN101100808A (en) * | 2007-07-23 | 2008-01-09 | 江南大学 | Normal-pressure low-temperature plasma preprocessing technique of textile for digital inking printing |
| CN101602299A (en) * | 2008-06-10 | 2009-12-16 | 冷博 | Plasma on-line real-time pretreating printing system |
| CN103437225A (en) * | 2013-09-03 | 2013-12-11 | 福建省华奇环保印花有限公司 | Direct printing method of low-temperature plasma processed fabric |
| CN103485163A (en) * | 2013-09-11 | 2014-01-01 | 昆山市万丰制衣有限责任公司 | Finishing method of antibacterial anti-felting wool |
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