CN105603788A - Plasma-crosslinking composite modified high-precision cashmere digital printing technology - Google Patents
Plasma-crosslinking composite modified high-precision cashmere digital printing technology Download PDFInfo
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- CN105603788A CN105603788A CN201510800395.8A CN201510800395A CN105603788A CN 105603788 A CN105603788 A CN 105603788A CN 201510800395 A CN201510800395 A CN 201510800395A CN 105603788 A CN105603788 A CN 105603788A
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Abstract
The invention discloses a plasma-crosslinking composite modified high-precision cashmere digital printing technology including the following steps: (1) a cashmere fabric ageing process; (2) a cashmere fabric plasma etching process; (3) a cashmere fabric crosslinking agent gluing process; (4) a cashmere fabric digital printing machine spray printing process; and (5) heating curing and product obtaining. Cashmere fibers are pre-treated by low temperature plasma, physical etching and chemical oxidation are carried out on the surface of cashmere, and oxygen-containing groups are introduced; after the cashmere is endowed with excellent hydrophilic effect, 3-(2,3-epoxy propoxy)propyl trimethoxy silane is used for treating the fibers, so that the digital spray printing performance of the cashmere fibers is improved, and the color ink adsorption capacity of the cashmere fibers is improved. After color printing, ageing and waster washing are not required, clear and bright patterns are obtained, the printing process is simplified, spray printing is flexible, and the needs of personalized and quantitative production, small batch and rapid response can be met.
Description
Technical field
The invention belongs to digit printing field, be specifically related to a kind of plasma-crosslinked compound changingProperty high accuracy cashmere digit printing technique.
Background technology
Digit printing is the model that computer technology is combined with traditional textile printing technique. HaveEnergy consumption is low, blowdown is few, it is strong to change floral designs stereovision fast, that print without plate-making, flower type,Color and luster changes the features such as many, can adjust at any time color and the size of pattern, is a conventional stamp difficultyWith what reach.
Along with people are more and more higher to the cry of environmental protection, green and ecological textile becomes textile industryThe basis of sustainable development, the little or free of contamination material surface modifying technique of exploitation environmental pollutionBecome a main direction of studying. Plasma surface modification technology is described as " green " and addsWork technology, enjoys people's very big attention. Low Temperature Plasma Treating textile material, can changeFiber surface chemical constitution and form, but deeply the most only 10 μ m of its penetrable material surface haveProcess only 10 nanometer left and right of thickness, approximately 99.8% body still preserves in good condition, because ofChemistry of fiber and physical property are without marked change after treatment for this, and its dyeability can obtainTo obviously improving.
Summary of the invention
Goal of the invention: the invention provides a kind of plasma-crosslinked composite modified high accuracy cashmereDigit printing technique.
Technical scheme: a kind of plasma-crosslinked composite modified high accuracy cashmere digit printing workSkill, comprises the steps: that (1) fleece fabrics is through evaporating technique; (2) fleece fabrics plasmaEtching technics; (3) fleece fabrics crosslinking agent photoresist coating process; (4) fleece fabrics digital decorating machineJet printing technique; (5) finished product that is heating and curing to obtain;
Wherein, in described (3) fleece fabrics crosslinking agent photoresist coating process, by fabric in composite friendshipIn the dressing liquid of connection agent, pad processing, liquid carrying rate is 50-60, at 70-80 DEG C of temperature, dry,The dressing liquid of described composite crosslinking agent is made up of the component of following weight portion: nano-ZnO is 1-5Part, citric acid/sodium citrate pH value of buffer solution is 4.2 ± 0.2, myristyl dimethylBenzyl ammonium chloride antiseptic is 1-5 part, 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicaneFor 10-15 part, all the other are water.
As further optimization: described (1) fleece fabrics evaporates in technique, and fleece fabrics existsUnder pine formula state, spray 0.3-0.5g/L antistatic additive SN, fiber weightening finish 100g/m2, knitThing enters J type gas steam box gas with 20-40 m/min and steams, and exists taking steam or hot-air as mediumAt 100-110 DEG C, gas steams.
As further optimization: in described (2) fleece fabrics plasma etching industrial, adoptAtomfloTM250 type atmospheric plasma jet apparatus, ejection forms plasma jet and changesProperty fleece fabrics, fleece fabrics is laid on the bottom crown of apparatus for processing plasma, normal pressure etc.Gas ions treatment conditions are as follows: medium air, and power parameter 380V, frequency 1000Hz, defeatedGo out power 30-120KW, processing speed 20-60m/min, the spacing 2-3mm of shower nozzle sample.
As further optimization: in described (3) fleece fabrics crosslinking agent photoresist coating process, reactionIf fabric does not carry out digit printing technique for a long time completely, thin with polypropylene at fabric positive and negativeFilm covers, and can preserve for a long time; After reacting completely, in the short time, carry out digit printing technique,Do not need polypropylene film to cover.
As further optimization: described (4) fleece fabrics digit printing jet printing technique is, numberCode spray printing, oven dry, described print paste is waterborne digital coating, adds 0.4g/L in mill baseGoon1201 amido silicon oil, bake out temperature is 90-110 DEG C, the time is 30-180s.
Beneficial effect: concrete advantage of the present invention is as follows:
(1) in the present invention, adopt low temperature plasma pretreatment cashmere fiber, give cashmereAfter extraordinary etching effect, with 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane couplingAgent as crosslinking agent by bridge formation base to cashmere surface, prepared reactive cashmere fiber, in water-basedIn color paste of printing coating, add part amido silicon oil, form plasma-crosslinked composite modified heightPrecision cashmere digit printing technique. This printing technology changes fast, printing without plate-making, flower typeFloral designs stereovision is strong, and color and luster changes many, antibacterial, anti-feltings, softness. Meet modern societyPeople are to personalized demand and the development trend of following textile techniques in meeting.
(2), in the present invention, cashmere can obtain extraordinary suction after Low Temperature Plasma TreatingPerformance of ink, for industrialization provides fabulous pre-treatment effect, by 3-(2,3-epoxy the third oxygen)The Ou Lian effect of propyl trimethoxy silicane organically incorporates antiseptic in cashmere fiber, makesFiber strength also part promotes, and fleece fabrics is antibacterial, keeps fabric smooth, improves fabric Dry SackAmount, prevents that the imbibition of look China ink from improving flower type fineness. With traditional stamp relatively have energy consumption low, rowDirt less, without making a plate, spending, type changes soon, the floral designs stereovision of printing is strong, color and luster variationThe features such as many, can adjust color and the size of pattern at any time, are that conventional stamp institute is unapproachable.
(3) in the present invention, fleece fabrics is under loose formula state, and spray antistatic additive gas steams,Improve cashmere fiber wettability, softening cashmere fiber surface Microstructure of epidermal scale, is conducive to rear roadPlasma etching, improves etching effect.
(4), in the present invention, adopt low temperature plasma to carry out etching pretreatment to cashmere fiber,Deface scale, prevents cashmere felting, makes fiber surface generating portion polar group, increasesCashmere surface hydrophilicity and reactivity, do not lose cashmere fiber brute force simultaneously.
(5), in the present invention, adopt described fleece fabrics crosslinking agent photoresist coating process to be equivalent to quarterThe fleece fabrics of erosion is built bridge, antimicrobial treatment, nano-ZnO, myristyl dimethyl benzylAmmonium chloride antiseptic provides cashmere antibacterial effect, 3-(2,3-epoxy the third oxygen) propyl trimethoxySilane is crosslinked coupling agent, keeps fabric smooth, improves fabric tinctorial yield, prevents the imbibition of look China inkImprove flower type fineness, digital printing look China ink range of choice expands simultaneously.
(6), in the present invention, digit printing adopts coating, has avoided with road gas after acid dyesThe fault of the water droplet circle that steaming causes, spray printing speed promotes greatly simultaneously, and colour system range of choice expands,Improve fabric tinctorial yield, prevent that the imbibition of look China ink from improving flower type fineness. In mill base, add 20mlGoon1201 amido silicon oil (0.4g/L) contributes to improve the feel of fleece fabrics, fiberfill fibersInterior gap, prevents fleece fabrics felting.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be described in detail.
Specific embodiment one:
A kind of plasma-crosslinked composite modified high accuracy cashmere digit printing technique, comprises as followsStep:
(1) fleece fabrics is through evaporating technique: fleece fabrics, under loose formula state, sprays 0.3g/LAntistatic additive SN, fiber weightening finish 100g/m2, fabric enters J type gas steam box with 20 ms/minGas steams, and taking steam or hot-air as medium, at 100 DEG C, gas steams;
Fleece fabrics is under loose formula state, and spray antistatic additive gas steams, and improves cashmere fiber wettingPerformance, softening cashmere fiber surface Microstructure of epidermal scale, is conducive to rear road plasma etching, improvesEtching effect.
(2) fleece fabrics plasma etching industrial: adopt AtomfloTM250 type normal pressure etc. fromDaughter jet apparatus, ejection forms plasma jet modification fleece fabrics, fleece fabrics tilingOn the bottom crown of apparatus for processing plasma, atmospheric plasma treatment conditions are as follows: mediumAir, power parameter 380V, frequency 1000Hz, power output 30KW, processing speed 20m/min,The spacing 2mm of shower nozzle sample;
Adopt low temperature plasma to carry out etching pretreatment to cashmere fiber, deface scale,Prevent cashmere felting, make fiber surface generating portion polar group, increase cashmere surface hydrophilicityAnd reactivity, do not lose cashmere fiber brute force simultaneously.
(3) fleece fabrics crosslinking agent photoresist coating process: the dressing liquid by fabric at composite crosslinking agentIn pad processing, liquid carrying rate is 50, at 70 DEG C of temperature, dry, described composite crosslinking agentDressing liquid is made up of the component of following weight portion: nano-ZnO is 1 part, citric acid/citric acidSodium pH value of buffer solution is 4.0, and myristyl dimethyl benzyl ammonium chloride antiseptic is 1 part,3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane is 10 parts, and all the other are water;
If fabric does not carry out digit printing technique for a long time after reacting completely, use at fabric positive and negativePolypropylene film covers, and can preserve for a long time; After reacting completely, in the short time, carry out digit printingTechnique, does not need polypropylene film to cover;
Adopt described fleece fabrics crosslinking agent photoresist coating process to be equivalent to enter to the fleece fabrics of etchingRow is built bridge, antimicrobial treatment, and nano-ZnO, myristyl dimethyl benzyl ammonium chloride antiseptic are carriedFor cashmere antibacterial effect, 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane is crosslinked couplingAgent, keeps fabric smooth, improves fabric tinctorial yield, prevents that the imbibition of look China ink from improving flower type fineness,Digital printing look China ink range of choice expands simultaneously.
(4) fleece fabrics digital decorating machine jet printing technique: described print paste is waterborne digitalCoating adds 0.4g/LGoon1201 amido silicon oil in mill base, and bake out temperature is 90 DEG C,Time is 30s;
Digit printing adopts coating, avoided steaming with road gas after acid dyes the water droplet circle that causesFault, spray printing speed promotes greatly simultaneously, and colour system range of choice expands, and improves fabric tinctorial yield,Prevent that the imbibition of look China ink from improving flower type fineness. In mill base, add the amino silicon of 20mlGoon1201Oil (0.4g/L) contributes to improve the feel of fleece fabrics, and gap in fiberfill fibers, prevents cashmereFabric felting.
(5) finished product that is heating and curing to obtain.
Specific embodiment two:
A kind of plasma-crosslinked composite modified high accuracy cashmere digit printing technique, comprises as followsStep:
(1) fleece fabrics is through evaporating technique: fleece fabrics, under loose formula state, sprays 0.5g/LAntistatic additive SN, fiber weightening finish 100g/m2, fabric enters J type gas steam box with 40 ms/minGas steams, and taking steam or hot-air as medium, at 110 DEG C, gas steams;
Fleece fabrics is under loose formula state, and spray antistatic additive gas steams, and improves cashmere fiber wettingPerformance, softening cashmere fiber surface Microstructure of epidermal scale, is conducive to rear road plasma etching, improvesEtching effect.
(2) fleece fabrics plasma etching industrial: adopt AtomfloTM250 type normal pressure etc. fromDaughter jet apparatus, ejection forms plasma jet modification fleece fabrics, fleece fabrics tilingOn the bottom crown of apparatus for processing plasma, atmospheric plasma treatment conditions are as follows: mediumAir, power parameter 380V, frequency 1000Hz, power output 120KW, processing speed60m/min, the spacing 3mm of shower nozzle sample;
Adopt low temperature plasma to carry out etching pretreatment to cashmere fiber, deface scale,Prevent cashmere felting, make fiber surface generating portion polar group, increase cashmere surface hydrophilicityAnd reactivity, do not lose cashmere fiber brute force simultaneously.
(3) fleece fabrics crosslinking agent photoresist coating process: the dressing liquid by fabric at composite crosslinking agentIn pad processing, liquid carrying rate is 60, at 80 DEG C of temperature, dry, described composite crosslinking agentDressing liquid is made up of the component of following weight portion: nano-ZnO is 5 parts, citric acid/citric acidSodium pH value of buffer solution is 4.4, and myristyl dimethyl benzyl ammonium chloride antiseptic is 5 parts,3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane is 15 parts, and all the other are water;
If fabric does not carry out digit printing technique for a long time after reacting completely, use at fabric positive and negativePolypropylene film covers, and can preserve for a long time; After reacting completely, in the short time, carry out digit printingTechnique, does not need polypropylene film to cover;
Adopt described fleece fabrics crosslinking agent photoresist coating process to be equivalent to enter to the fleece fabrics of etchingRow is built bridge, antimicrobial treatment, and nano-ZnO, myristyl dimethyl benzyl ammonium chloride antiseptic are carriedFor cashmere antibacterial effect, 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane is crosslinked couplingAgent, keeps fabric smooth, improves fabric tinctorial yield, prevents that the imbibition of look China ink from improving flower type fineness,Digital printing look China ink range of choice expands simultaneously.
(4) fleece fabrics digital decorating machine jet printing technique: described print paste is waterborne digitalCoating adds 0.4g/LGoon1201 amido silicon oil in mill base, and bake out temperature is 110 DEG C,Time is 180s;
Digit printing adopts coating, avoided steaming with road gas after acid dyes the water droplet circle that causesFault, spray printing speed promotes greatly simultaneously, and colour system range of choice expands, and improves fabric tinctorial yield,Prevent that the imbibition of look China ink from improving flower type fineness. In mill base, add the amino silicon of 20mlGoon1201Oil (0.4g/L) contributes to improve the feel of fleece fabrics, and gap in fiberfill fibers, prevents cashmereFabric felting.
(5) finished product that is heating and curing to obtain.
Specific embodiment three:
A kind of plasma-crosslinked composite modified high accuracy cashmere digit printing technique, comprises as followsStep:
(1) fleece fabrics is through evaporating technique: fleece fabrics, under loose formula state, sprays 0.4g/LAntistatic additive SN, fiber weightening finish 100g/m2, fabric enters J type gas steam box with 30 ms/minGas steams, and taking steam or hot-air as medium, at 105 DEG C, gas steams;
Fleece fabrics is under loose formula state, and spray antistatic additive gas steams, and improves cashmere fiber wettingPerformance, softening cashmere fiber surface Microstructure of epidermal scale, is conducive to rear road plasma etching, improvesEtching effect.
(2) fleece fabrics plasma etching industrial: adopt AtomfloTM250 type normal pressure etc. fromDaughter jet apparatus, ejection forms plasma jet modification fleece fabrics, fleece fabrics tilingOn the bottom crown of apparatus for processing plasma, atmospheric plasma treatment conditions are as follows: mediumAir, power parameter 380V, frequency 1000Hz, power output 80KW, processing speed 40m/min,The spacing 2.4mm of shower nozzle sample;
Adopt low temperature plasma to carry out etching pretreatment to cashmere fiber, deface scale,Prevent cashmere felting, make fiber surface generating portion polar group, increase cashmere surface hydrophilicityAnd reactivity, do not lose cashmere fiber brute force simultaneously.
(3) fleece fabrics crosslinking agent photoresist coating process: the dressing liquid by fabric at composite crosslinking agentIn pad processing, liquid carrying rate is 54, at 76 DEG C of temperature, dry, described composite crosslinking agentDressing liquid is made up of the component of following weight portion: nano-ZnO is 3 parts, citric acid/citric acidSodium pH value of buffer solution is 4.2, and myristyl dimethyl benzyl ammonium chloride antiseptic is 3 parts,3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane is 13 parts, and all the other are water;
If fabric does not carry out digit printing technique for a long time after reacting completely, use at fabric positive and negativePolypropylene film covers, and can preserve for a long time; After reacting completely, in the short time, carry out digit printingTechnique, does not need polypropylene film to cover;
Adopt described fleece fabrics crosslinking agent photoresist coating process to be equivalent to enter to the fleece fabrics of etchingRow is built bridge, antimicrobial treatment, and nano-ZnO, myristyl dimethyl benzyl ammonium chloride antiseptic are carriedFor cashmere antibacterial effect, 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane is crosslinked couplingAgent, keeps fabric smooth, improves fabric tinctorial yield, prevents that the imbibition of look China ink from improving flower type fineness,Digital printing look China ink range of choice expands simultaneously.
(4) fleece fabrics digital decorating machine jet printing technique: described print paste is waterborne digitalCoating adds 0.4g/LGoon1201 amido silicon oil in mill base, and bake out temperature is 100 DEG C,Time is 130s;
Digit printing adopts coating, avoided steaming with road gas after acid dyes the water droplet circle that causesFault, spray printing speed promotes greatly simultaneously, and colour system range of choice expands, and improves fabric tinctorial yield,Prevent that the imbibition of look China ink from improving flower type fineness. In mill base, add the amino silicon of 20mlGoon1201Oil (0.4g/L) contributes to improve the feel of fleece fabrics, and gap in fiberfill fibers, prevents cashmereFabric felting.
(5) finished product that is heating and curing to obtain.
The present invention is not limited to above-mentioned preferred forms, anyone under enlightenment of the present invention allCan draw other various forms of products, no matter but in its shape or structure, do any variation,Every have identical with a application or akin technical scheme, all drops on protection model of the present inventionWithin enclosing.
Claims (5)
1. plasma-crosslinked composite modified high accuracy cashmere digit printing technique, its feature existsIn: comprise the steps: that (1) fleece fabrics is through evaporating technique; (2) fleece fabrics plasmaEtching technics; (3) fleece fabrics crosslinking agent photoresist coating process; (4) fleece fabrics digital decorating machineJet printing technique; (5) finished product that is heating and curing to obtain;
Wherein, in described (3) fleece fabrics crosslinking agent photoresist coating process, by fabric in composite friendshipIn the dressing liquid of connection agent, pad processing, liquid carrying rate is 50-60, at 70-80 DEG C of temperature, dry,The dressing liquid of described composite crosslinking agent is made up of the component of following weight portion: nano-ZnO is 1-5Part, citric acid/sodium citrate pH value of buffer solution is 4.2 ± 0.2, myristyl dimethylBenzyl ammonium chloride antiseptic is 1-5 part, 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicaneFor 10-15 part, all the other are water.
2. plasma according to claim 1-crosslinked composite modified high accuracy cashmere is digital to be printedFlower process, its characteristic is: described (1) fleece fabrics evaporates in technique, and fleece fabrics existsUnder pine formula state, spray 0.3-0.5g/L antistatic additive SN, fiber weightening finish 100g/m2, knitThing enters J type gas steam box gas with 20-40 m/min and steams, and exists taking steam or hot-air as mediumAt 100-110 DEG C, gas steams.
3. plasma according to claim 1-crosslinked composite modified high accuracy cashmere is digital to be printedFlower process, its characteristic is: in described (2) fleece fabrics plasma etching industrial, adoptAtomfloTM250 type atmospheric plasma jet apparatus, ejection forms plasma jet and changesProperty fleece fabrics, fleece fabrics is laid on the bottom crown of apparatus for processing plasma, normal pressure etc.Gas ions treatment conditions are as follows: medium air, and power parameter 380V, frequency 1000Hz, defeatedGo out power 30-120KW, processing speed 20-60m/min, the spacing 2-3mm of shower nozzle sample.
4. plasma according to claim 1-crosslinked composite modified high accuracy cashmere is digital to be printedFlower process, its characteristic is: in described (3) fleece fabrics crosslinking agent photoresist coating process, reactionIf fabric does not carry out digit printing technique for a long time completely, thin with polypropylene at fabric positive and negativeFilm covers, and can preserve for a long time; After reacting completely, in the short time, carry out digit printing technique,Do not need polypropylene film to cover.
5. plasma according to claim 1-crosslinked composite modified high accuracy cashmere is digital to be printedFlower process, its characteristic is: described (4) fleece fabrics digit printing jet printing technique is to countCode spray printing, oven dry, described print paste is waterborne digital coating, adds 0.4g/L in mill baseGoon1201 amido silicon oil, bake out temperature is 90-110 DEG C, the time is 30-180s.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106120200A (en) * | 2016-06-22 | 2016-11-16 | 武汉纺织大学 | Hydrophilic, the antistatic finish device of a kind of one side wool fabric and method for sorting |
| CN106978735A (en) * | 2017-03-15 | 2017-07-25 | 南通大学 | Many topping printing methods of natural dye |
| CN108642650A (en) * | 2018-05-09 | 2018-10-12 | 内蒙古鄂尔多斯资源股份有限公司 | The two-sided digital printing method and cashmere product of cashmere tatting product |
| CN109112856A (en) * | 2018-07-17 | 2019-01-01 | 嘉兴学院 | Cotton fabric digital printing process |
| CN110409173A (en) * | 2019-07-19 | 2019-11-05 | 浙江玛戈利亚羊绒世家有限公司 | A kind of method of fleece fabrics anti-fluffing and anti-pilling |
| CN116815521A (en) * | 2023-08-23 | 2023-09-29 | 南通新世纪布业有限公司 | Anhydrous digital printing method |
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| CN108642650A (en) * | 2018-05-09 | 2018-10-12 | 内蒙古鄂尔多斯资源股份有限公司 | The two-sided digital printing method and cashmere product of cashmere tatting product |
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| CN110409173A (en) * | 2019-07-19 | 2019-11-05 | 浙江玛戈利亚羊绒世家有限公司 | A kind of method of fleece fabrics anti-fluffing and anti-pilling |
| CN116815521A (en) * | 2023-08-23 | 2023-09-29 | 南通新世纪布业有限公司 | Anhydrous digital printing method |
| CN116815521B (en) * | 2023-08-23 | 2024-01-09 | 杭州帛阳新材料科技有限公司 | Anhydrous digital printing method |
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