CN110409173A - A kind of method of fleece fabrics anti-fluffing and anti-pilling - Google Patents
A kind of method of fleece fabrics anti-fluffing and anti-pilling Download PDFInfo
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- CN110409173A CN110409173A CN201910652336.9A CN201910652336A CN110409173A CN 110409173 A CN110409173 A CN 110409173A CN 201910652336 A CN201910652336 A CN 201910652336A CN 110409173 A CN110409173 A CN 110409173A
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- fluffing
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/02—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements ultrasonic or sonic; Corona discharge
- D06M10/025—Corona discharge or low temperature plasma
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/35—Abrasion, pilling or fibrillation resistance
Abstract
The invention discloses a kind of methods of fleece fabrics anti-fluffing and anti-pilling, cashmere is after low temperature plasma irradiates, both the scale layer of villus fiber can have been opened, fiber bodies are not damaged again, a large amount of active chemical group can also be generated, plasma irradiating treated cashmere fiber and then can make functional materials be grafted onto fiber surface in the form of chemical covalent bonds, complete lasting anti-fluffing and anti-pilling design under crosslinking agent existence condition effectively with anti-fluffing and anti-pilling substance reaction.
Description
Technical field
The present invention relates to a kind of cashmere processing method more particularly to a kind of methods of fleece fabrics anti-fluffing and anti-pilling.
Background technique
Cashmere fiber is a kind of azelon, and there is scale on surface, and the rubbing action by a variety of external force is formed along inverse friction
Poor effect leads to cashmere knit goods pilling in the process of wearing, this all originates from the special Microstructure of epidermal scale of cashmere,
The performance for improving fleece fabrics anti pilling can set about from scale layer.
Plasma technique has obtained effective application in dyeing and finishing production, after the corona treatment of different condition,
There is different degrees of physics and chemical etching and acts in the surface of cashmere fibres.Guaranteeing monofilament strength loss variation not
In the case where big, the surface shrinkproof of fiber has obtained biggish improvement, has certain anti-fluffing and anti-pilling effect.Deng from
Daughter technical treatment fabric has the advantage that dry state is handled, and many-sided can apply, short processing time, processing cost is low, not dirty
Contaminate environment.Cashmere after corona treatment has certain anti-fluffing and anti-pilling effect, but haves the defects that persistence is poor, no
It is water-fastness, repeatedly obvious fluffiness is still had after washing.
Summary of the invention
In view of problem above, the invention discloses a kind of method of fleece fabrics anti-fluffing and anti-pilling, cashmere through low temperature etc. from
After daughter irradiation, the scale layer of villus fiber can be not only opened, but also do not damage fiber bodies, a large amount of activation can also be generated
Learn group, plasma irradiating treated cashmere fiber under crosslinking agent existence condition can effectively with anti-fluffing and anti-pilling object
Qualitative response, and then functional materials can be made to be grafted onto fiber surface in the form of chemical covalent bonds, it completes lasting anti-fluffing and rises
Ball design.
In order to achieve the above object, technical scheme is as follows:
A kind of method of fleece fabrics anti-fluffing and anti-pilling, the following steps are included:
(1) by fleece fabrics nitrogen and oxygen mixed gas corona treatment, the plasma process conditions are as follows: pressure
15~25Pa, 40~60W of power, the control of processing time are 0.5~2min；
(2) it will be placed in the osmotic agent solution that concentration is 0.1~1.0g/L and be swollen by the fleece fabrics of step (1) processing；
(3) it will be placed in the solution containing Lotus Leafextract by the fleece fabrics of step (2) processing, be uniformly mixed and place
5~20min adds crosslinking agent, places 24~48h at being 25~35 DEG C in temperature；
(4) it will be air-dried after the fleece fabrics that step (3) is handled is washed with clear water.
Further, the mass ratio of nitrogen and oxygen is 4:1 in step (1), and plasma process conditions are pressure 20Pa,
Power 60W, the control of processing time are 1.5min.
Specifically, the treatment process of step (2) are as follows: the concentration of bleeding agent be 0.5g/L, bath raio 1:20, temperature be 35~
45 DEG C, the processing time is 30~60min, is washed 1~2 time after processing with 35~40 DEG C of clear water.
Specifically, in step (3) Lotus Leafextract the preparation method comprises the following steps: by lotus leaf be crushed to granularity D50 be 50um hereinafter,
Using 80% ethyl alcohol, solid-liquid ratio 1:15, the ultrasonic extraction 10min for being 100W with power obtain lotus after filtering as extracting solution
Leaf crude extract.
Further, crosslinking agent is ethylene glycol diglycidylether in step (3), and dosage is 0.5~2.0g/L.
Further, the dosage of Lotus Leafextract is 10.0~20.0g/L in step (3).
Specifically, the technique of step (3) are as follows: concentration will be placed on by the fleece fabrics of step (2) processing as 20.0g/L
Lotus Leafextract solution in, be uniformly mixed and place 20min, 2.0g/L ethylene glycol diglycidylether is added, in temperature
Degree is to place for 24 hours at 25~35 DEG C.
Specifically, the technique of step (4) are as follows: emptying solution is washing 1 ~ 2 time of 35 ~ 40 DEG C with temperature, when impregnating every time
Between be 20 ~ 30min, after cooling, cashmere goes out cylinder, the hot blast drying for being 45 ~ 60 DEG C with temperature.
In the present invention, corona treatment is first modified cashmere surface, the active particle of high-energy in plasma
Complicated physical reaction, the mainly oxygen-containing polar group with nitrogen of corrasion and introduction are generated in wool surfaces.Plasma
Cystine disulfide bond in scale layer can be aoxidized and generate sulfonic group；In addition, protein molecule main chain is oxidized and gives birth in scale layer
At hydrophilic radical；After introducing functional chemical, one layer of polymeric film is formed on cashmere fiber surface and covers scale, it is fine
Tieing up surface deposits prevents scale from interacting, to prevent fiber movement and rubbing.
After cashmere corona treatment of the invention, then under the action of crosslinking agent, grafted with Lotus Leafextract,
To play the role of anti-fluffing and anti-pilling.Lotus leaf also contains albumen other than containing compounds such as carbohydrate, lipid tannin
Matter, polysaccharide, alkaloid, Flavonoid substances and essential oil substance, Lotus Leafextract has good antioxygenic property, in lotus leaf
Alkaloid has good bacteriostasis.Lotus leaf itself has very strong waterproof and antifouling property, and Lotus Leafextract is grafted in
On cashmere fiber, have the effect of for the anti-fluffing and anti-pilling of fleece fabrics certain.
In order to which Lotus Leafextract effectively to be grafted in the surface of cashmere fiber, it is particularly significant for selecting suitable crosslinking agent
's.The effect for grafting in cashmere fiber for Lotus Leafextract to various crosslinking agents is tested.It is main currently on the market
Crosslinking agent has cumyl peroxide, benzoyl peroxide, di-tert-butyl peroxide, di-isopropylbenzene hydroperoxide etc., but by
Belong to a kind of protein, non-refractory and acid-base property in cashmere fiber, harsher, the above crosslinking agent is required for reaction condition
Reaction condition be not well positioned to meet the grafting of cashmere fiber, the effect is unsatisfactory.
Ethylene glycol diglycidylether is a kind of epoxies crosslinking agent that reaction condition is mild, can be carried out at room temperature anti-
It answers.And ethylene glycol diglycidylether biocompatibility is excellent, and nontoxic, and ethylene glycol diglycidylether is in molecule
End has by two epoxy groups of the molecular equilateral three-membered ring of three originals, the existing huge ring strain of this epoxy group itself
Assign the stronger activity of the more other ethers of ethylene glycol diglycidylether.Ethylene glycol diglycidylether itself acid or
It is easier that ring-opening reaction occurs compared to neutrallty condition under person's alkaline condition, but acid-base condition again can produce fracture cashmere itself
The destruction of stress decrease, the destruction compared to the crosslinking consolidation effect soda acid of ethylene glycol diglycidylether are more tight
Weight, therefore graft reaction is suitble to carry out in neutral conditions.
The invention has the benefit that
(1) cashmere fiber is pre-processed using low temperature plasma, utilizes the work for the polar chemical group that cashmere fiber surface generates
Property, crosslinking agent is used as reaction medium, the substance with anti-fluffing and anti-pilling is grafted in into cashmere fiber surface, makes fleece fabrics
Anti-fluffing and anti-pilling performance reaches certain persistence.
(2) using nontoxic sustainable natural plants Lotus Leafextract as the active material of grafting, have environmentally protective
The advantages of and excellent anti-fluffing and anti-pilling performance.
(3) crosslinking agent ethylene glycol diglycidylether has reaction condition mild, the good advantage of Relationship between Graft Effect.
Specific embodiment
Below by way of specific embodiment, the present invention is further described.
Embodiment 1
The dry fleece fabrics of 5g is placed in the reaction bench of plasma device by a kind of method of fleece fabrics anti-fluffing and anti-pilling
On, gas switch is opened, gas is allowed to enter reaction bench, the pressure of regulating gas is 15Pa, power 60W, is incited somebody to action after preheating 20 min
Radio-frequency signal generator is opened, and is stopped after the 0.5min that discharges, is taken out sample after closing intake valve.The gas is that nitrogen and oxygen are mixed
Gas, mass ratio 4:1 are closed, or directly uses air as plasma gas.In order to just carry out the grafting of next step,
Cashmere after corona treatment is placed in osmotic agent solution and is swollen, declines the tension on cashmere surface, is conducive to transfer
Connect the palea layer that active material enters cashmere surface.The concentration of bleeding agent is 0.1g/L, and bath raio 1:20, temperature is 35~45
DEG C, the processing time is 30min, by fleece fabrics complete wetting, and it is primary every 15min stirring, with 35~40 DEG C after processing
Clear water wash 1~2 time, remove remaining bleeding agent.Then fleece fabrics is placed on containing concentration is the extraction of 20.0g/L lotus leaf
In the solution of object, it is uniformly mixed and places 20min, bath raio 1:10 adds crosslinking agent ethylene glycol diglycidylether, dosage
It is 25~35 DEG C of placements in temperature for 0.5g/L, it is primary every 2~3h stirring, infiltrate cashmere sufficiently, after placing for 24 hours, emptying
Solution, with washing 1 ~ 2 time that temperature is 35 ~ 40 DEG C, each soaking time is 20 ~ 30min, and after cooling, cashmere goes out cylinder, uses temperature
For 45 ~ 60 DEG C of hot blast drying.
Lotus Leafextract the preparation method comprises the following steps: using lotus leaf be crushed to granularity D50 be 50um hereinafter, use 80% ethyl alcohol as
Extracting solution, solid-liquid ratio 1:15, the ultrasonic extraction 10min for being 100W with power obtain lotus leaf crude extract after filtering.
Comparative example 1
Fleece fabrics is handled using the process flow of embodiment 1, cashmere dry weight is 5g, and wherein plasma pressure is
20Pa, power 50W, processing time are 1min；It is that 0.5g/L bleeding agent is swollen with concentration after corona treatment, bath raio
For 1:20, temperature is 35~45 DEG C, and the processing time is 60min, removes remaining bleeding agent with clear water.Then fleece fabrics is put
It sets in the solution for being 10.0g/L Lotus Leafextract containing concentration, be uniformly mixed and place 20min, bath raio 1:10 is added
Concentration is to be 25~35 DEG C of placements in temperature, stir one every 2~3h in the crosslinking agent ethylene glycol diglycidylether of 1.0g/L
It is secondary, it infiltrates cashmere sufficiently, after placing 30h, empties solution, with washing 1 ~ 2 time that temperature is 35 ~ 40 DEG C, each soaking time
For 20 ~ 30min, after cooling, cashmere goes out cylinder, the hot blast drying for being 45 ~ 60 DEG C with temperature.
Comparative example 2
Fleece fabrics is handled using the process flow of embodiment 1, cashmere dry weight is 5g, and wherein plasma pressure is
20Pa, power 60W, processing time are 0.5min；It is that 0.6g/L bleeding agent is swollen with concentration after corona treatment, bath
Than for 1:20, temperature is 35~45 DEG C, the processing time is 60min, with the remaining bleeding agent of clear water removing.Then by fleece fabrics
Be placed on be containing concentration be uniformly mixed in the solution of 15.0g/L Lotus Leafextract and place 20min, bath raio 1:10, then plus
Enter in the crosslinking agent ethylene glycol diglycidylether that concentration is 1.2g/L, is 25~35 DEG C of placements in temperature, is stirred every 2~3h
Once, it infiltrates cashmere sufficiently, after placing 30h, empties solution, be washing 1 ~ 2 time of 35 ~ 40 DEG C with temperature, when impregnating every time
Between be 20 ~ 30min, after cooling, cashmere goes out cylinder, the hot blast drying for being 45 ~ 60 DEG C with temperature.
Comparative example 3
Fleece fabrics is handled using the process flow of embodiment 1, cashmere dry weight is 5g, and wherein plasma pressure is
20Pa, power 50W, processing time are 1.5min；It is that 0.8g/L bleeding agent is swollen with concentration after corona treatment, bath
Than for 1:20, temperature is 35~45 DEG C, the processing time is 60min, with the remaining bleeding agent of clear water removing.Then by fleece fabrics
Be placed on be containing concentration be uniformly mixed in the solution of 20.0g/L Lotus Leafextract and place 20min, bath raio 1:10, then plus
Enter in the crosslinking agent ethylene glycol diglycidylether that concentration is 1.5g/L, is 25~35 DEG C of placements in temperature, is stirred every 2~3h
Once, it infiltrates cashmere sufficiently, after placing 30h, empties solution, be washing 1 ~ 2 time of 35 ~ 40 DEG C with temperature, when impregnating every time
Between be 20 ~ 30min, after cooling, cashmere goes out cylinder, the hot blast drying for being 45 ~ 60 DEG C with temperature.
Comparative example 4
Fleece fabrics is handled using the process flow of embodiment 1, cashmere dry weight is 5g, and wherein plasma pressure is
20Pa, power 50W, processing time are 1.5min；It is that 1.0g/L bleeding agent is swollen with concentration after corona treatment, bath
Than for 1:20, temperature is 35~45 DEG C, the processing time is 60min, with the remaining bleeding agent of clear water removing.Then by fleece fabrics
Be placed on be containing concentration be uniformly mixed in the solution of 20.0g/L Lotus Leafextract and place 20min, bath raio 1:10, then plus
Enter in the crosslinking agent ethylene glycol diglycidylether that concentration is 2.0g/L, is 25~35 DEG C of placements in temperature, is stirred every 2~3h
Once, it infiltrates cashmere sufficiently, after placing 30h, empties solution, be washing 1 ~ 2 time of 35 ~ 40 DEG C with temperature, when impregnating every time
Between be 20 ~ 30min, after cooling, cashmere goes out cylinder, the hot blast drying for being 45 ~ 60 DEG C with temperature.
Embodiment 2
By the fleece fabrics that above embodiments and comparative example are handled, to fleece fabrics in the state of drying respectively to grafting before
It weighs with after grafting, judges the effect of grafting.
The Lotus Leafextract Relationship between Graft Effect of 1 fleece fabrics of table at different conditions
It can be concluded that, the lotus leaf after grafting has weight gain phenomenon from upper table, illustrates have grafting to achieve effect.Crosslinking agent and lotus leaf
The concentration of extract has large effect to Relationship between Graft Effect, with the increase of Lotus Leafextract and crosslinker concentration, Relationship between Graft Effect
It is promoted.
Embodiment 3
Test can be carried out to the anti-pilling of the fleece fabrics in untreated fleece fabrics and implementation.By GB/T
The regulation of 4802.3-2008 standard measures the anti-fluffing and anti-pilling grade of fleece fabrics, stirs 7200 turns.
The anti-pilling property of 2 fleece fabrics of table compares
The weight that fleece fabrics anti pilling row performance after it can be seen that grafting in above table is significantly improved, and grafts
Bigger, anti-pilling property is about obvious.
Claims (8)
1. a kind of method of fleece fabrics anti-fluffing and anti-pilling, which comprises the following steps:
By fleece fabrics nitrogen and oxygen mixed gas corona treatment, the plasma process conditions are as follows: pressure 15
~25Pa, 40~60W of power, the control of processing time are 0.5~2min；
It is swollen being placed in the osmotic agent solution that concentration is 0.1~1.0g/L by the fleece fabrics of step (1) processing；
It will be placed in the solution containing Lotus Leafextract by the fleece fabrics of step (2) processing, be uniformly mixed and place 5~
20min adds crosslinking agent, places 24~48h at being 25~35 DEG C in temperature；
It will be air-dried after the fleece fabrics that step (3) is handled is washed with clear water.
2. a kind of method of fleece fabrics anti-fluffing and anti-pilling according to claim 1, which is characterized in that the step (1)
The mass ratio of middle nitrogen and oxygen is 4:1, and plasma process conditions are pressure 20Pa, power 60W, and the control of processing time is
1.5min。
3. a kind of method of fleece fabrics anti-fluffing and anti-pilling according to claim 1, which is characterized in that the step (2)
Treatment process are as follows: the concentration of bleeding agent be 0.5g/L, bath raio 1:20, temperature be 35~45 DEG C, processing the time be 30~
60min is washed 1~2 time after processing with 35~40 DEG C of clear water.
4. a kind of method of fleece fabrics anti-fluffing and anti-pilling according to claim 1, which is characterized in that the step (3)
Middle Lotus Leafextract the preparation method comprises the following steps: it is 50um hereinafter, using 80% ethyl alcohol as extracting solution that lotus leaf, which is crushed to granularity D50,
Solid-liquid ratio is 1:15, and the ultrasonic extraction 10min for being 100W with power obtains lotus leaf crude extract after filtering.
5. a kind of method of fleece fabrics anti-fluffing and anti-pilling according to claim 1, which is characterized in that the step (3)
Middle crosslinking agent is ethylene glycol diglycidylether, and dosage is 0.5~2.0g/L.
6. a kind of method of fleece fabrics anti-fluffing and anti-pilling according to claim 1, which is characterized in that the step (3)
The dosage of middle Lotus Leafextract is 10.0~20.0g/L.
7. a kind of method of fleece fabrics anti-fluffing and anti-pilling according to claim 1, which is characterized in that the step (3)
Technique are as follows: will by step (2) processing fleece fabrics be placed on concentration be 20.0g/L Lotus Leafextract solution in,
It is uniformly mixed and is placed 20min, adds 2.0g/L ethylene glycol diglycidylether, is placed for 24 hours at being 25~35 DEG C in temperature.
8. a kind of method of fleece fabrics anti-fluffing and anti-pilling according to claim 1, which is characterized in that the step (4)
Technique are as follows: emptying solution is washing 1 ~ 2 time of 35 ~ 40 DEG C with temperature, and each soaking time is 20 ~ 30min, after cooling, sheep
Suede goes out cylinder, the hot blast drying for being 45 ~ 60 DEG C with temperature.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910652336.9A CN110409173A (en) | 2019-07-19 | 2019-07-19 | A kind of method of fleece fabrics anti-fluffing and anti-pilling |
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| CN201910652336.9A CN110409173A (en) | 2019-07-19 | 2019-07-19 | A kind of method of fleece fabrics anti-fluffing and anti-pilling |
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| CN113550138A (en) * | 2020-04-24 | 2021-10-26 | 香港纺织及成衣研发中心 | Treatment method for reducing fluffing and pilling of animal textiles |
| CN115094620A (en) * | 2022-07-29 | 2022-09-23 | 湖州珍贝羊绒制品有限公司 | Method for treating cashmere fabric by low-temperature plasma |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113550138A (en) * | 2020-04-24 | 2021-10-26 | 香港纺织及成衣研发中心 | Treatment method for reducing fluffing and pilling of animal textiles |
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| CN115094620A (en) * | 2022-07-29 | 2022-09-23 | 湖州珍贝羊绒制品有限公司 | Method for treating cashmere fabric by low-temperature plasma |
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