CN103865292A - Natural red ximei (Chinese character) dye, preparation method, and ecological dyeing thereof applied to azelon - Google Patents
Natural red ximei (Chinese character) dye, preparation method, and ecological dyeing thereof applied to azelon Download PDFInfo
- Publication number
- CN103865292A CN103865292A CN201410122603.9A CN201410122603A CN103865292A CN 103865292 A CN103865292 A CN 103865292A CN 201410122603 A CN201410122603 A CN 201410122603A CN 103865292 A CN103865292 A CN 103865292A
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- Prior art keywords
- dyeing
- plum
- thiozell
- natural dyestuff
- ecological
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Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 15
- 239000012192 staining solution Substances 0.000 claims abstract description 12
- 239000004744 fabric Substances 0.000 claims abstract description 8
- 238000005406 washing Methods 0.000 claims abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000000975 dye Substances 0.000 claims description 32
- 238000010790 dilution Methods 0.000 claims description 7
- 239000012895 dilution Substances 0.000 claims description 7
- 239000000835 fiber Substances 0.000 claims description 7
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 claims description 5
- 210000000085 cashmere Anatomy 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 210000002268 wool Anatomy 0.000 claims description 4
- 238000005516 engineering process Methods 0.000 claims description 3
- 238000009434 installation Methods 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 102000004169 proteins and genes Human genes 0.000 claims description 2
- 108090000623 proteins and genes Proteins 0.000 claims description 2
- 239000007921 spray Substances 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- -1 yarn Substances 0.000 claims description 2
- 239000000049 pigment Substances 0.000 abstract description 3
- 229910001385 heavy metal Inorganic materials 0.000 abstract description 2
- 239000002932 luster Substances 0.000 abstract description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- 238000004140 cleaning Methods 0.000 abstract 1
- 238000007865 diluting Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000007654 immersion Methods 0.000 abstract 1
- 238000010299 mechanically pulverizing process Methods 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 239000002351 wastewater Substances 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 229960000583 acetic acid Drugs 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000003085 diluting agent Substances 0.000 description 3
- 238000007598 dipping method Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 241000305492 Gastrodia Species 0.000 description 1
- 229930182559 Natural dye Natural products 0.000 description 1
- 235000011158 Prunus mume Nutrition 0.000 description 1
- 244000018795 Prunus mume Species 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000978 natural dye Substances 0.000 description 1
- 230000007170 pathology Effects 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 235000019633 pungent taste Nutrition 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
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Abstract
The invention discloses a natural red ximei (Chinese character) dye, a preparation method, and ecological dyeing thereof applied to azelon. The method comprises the following steps: cleaning and airing ximei; mechanically pulverizing, and soaking into 10-50fold water; adding 5-10g/L of sodium hydroxide and 5-10g/L of sodium chloride; filtering and removing residues after immersion treatment at 30-100 DEG C, so as to obtain a natural ximei stock staining solution; diluting the natural ximen stock staining solution and then dyeing the azelon, wherein the dyeing conditions are as follows: the bath ratio is 1:(10-50), pH is 5-7, the dyeing temperature is 80-100 DEG C and the dyeing time is 45-90 minutes; washing and baking to obtain the dyed product. By adopting the dyeing method disclosed by the invention, heavy metal does not need to be fixated, the dyed fabric is even in color and luster, the fastness can be up to 3-4, the dyeing process is simple, stable in pigment, and high in dyeing rate, a wastewater is colorless basically, the dye can be biodegraded, and the dyeing method is a pure ecological dyeing method, and is very broad in market prospect.
Description
Technical field
The present invention relates to a kind of ecological dyeing method of plum natural dyestuff to thiozell of liking, belong to fabrics printing and dyeing technical field.
Background technology
Textiles, after the dyeing of chemosynthesis, can cause pungency to skin, easily causes human body skin pathology.And the dyestuff of chemosynthesis can affect to environment in production and use procedure, does not meet the requirement of science Sustainable development.Along with going deep into of environmental protection idea, natural dyestuff is more and more subject to people's favor.Natural dyestuff refers to from the root of plant, leaf, bark, trunk, shell, flower or animal secretions, mineral substance and extracts, preparation process can not cause environmental pollution, dyeing after textiles wear safety, and natural dyestuff and ecotope consistency good, biodegradable.But natural dye dying colour fastness is low, and conventionally need heavy metal fixation, therefore, finding high color fastness natural dyestuff becomes investigator's focus.
Fruit plum is in existing more than the 3000 year history of China, aboundresources, there are altogether 205 kinds, wherein 13 of Japanese apricot classes, 95 of green plum classes, 83 of red plum classes, 14 of Introduced from Japan kinds, happiness plum belongs to the one of fruit plum, is mainly distributed in Guangdong, Taiwan, Guangxi, torrid areas, Fujian, be distributed as master with wild species, be generally used for squeezing juice.Publication number is that the Chinese invention patent of CN102746972A discloses a kind of happiness plum gastrodia liquor and preparation method thereof, has nourishing function.But have no report for research and the application of contained pigment in happiness plum at present.
Summary of the invention
The present invention utilizes happiness to contain abundant pigment in plum, and a kind of happiness plum natural dyestuff and preparation method thereof is provided, and by the happiness plum natural dyestuff obtaining for the ecological dyeing method to thiozell.Feature environmental and ecological, that dyeing product color and luster is even, fastness is good that technical scheme provided by the invention has.
What realize the object of the invention is that technical scheme is to provide a kind of preparation method who likes plum natural dyestuff, comprise that step is as follows: happiness plum is cleaned, dried, mechanical disintegration, by weight, be soaked in the water of 10～50 times, add sodium hydroxide 5～10g/L, sodium-chlor 5～10g/L, under the temperature condition of 30～100 DEG C, after dip treating, remove by filter residue, obtain liking right stock staining solution of the rainy season.
The dip treating time of the present invention is 30～100min.
Technical solution of the present invention also comprises the happiness plum natural dyestuff stoste obtaining by above-mentioned preparation method.
Happiness plum natural dyestuff of the present invention is applied to the ecological dyeing method to thiozell, step is as follows: will like right stock staining solution dilution of the rainy season, in dyeing installation to the thiozell processing of dyeing; bath raio is 1:10～50, and the pH of dye liquor is 5～7, and dyeing temperature is 80～100 DEG C; dyeing time is 45～90min; again through washing, dry, obtain a kind of red protein fiber.
Dyeing of the present invention processing comprise adopt flood, pad, spraying, spray technology.Described thiozell comprises the one in silk, wool, cashmere, or their blending product; The state of thiozell comprises bulk fibre, yarn, fabric or finished product dress ornament.
Beneficial effect of the present invention is: preparation method has that technique is simple, the feature of environmental protection and energy saving, dyeing behavior excellence; Dyeing product has the safety of taking, added value is high, to skin without advantages such as supersensitivity; It is bright-coloured that fiber color dyes in institute, and environmental protection, is particularly suitable for production next to the skin and children's fabric.The happiness plum that the present invention adopts is a kind of rose natural dyestuff of excellent property, and market outlook are very wide.
Brief description of the drawings
Fig. 1 is the photo in kind of embodiment of the present invention happiness used plum;
Fig. 2 be the happiness plum natural dyestuff dyeing silk that provides of the embodiment of the present invention 1 on dye trend map.
Embodiment
Below in conjunction with embodiment and accompanying drawing, technical scheme of the present invention is further elaborated.
Embodiment 1:
Referring to accompanying drawing 1, it is the photo in kind of the present embodiment happiness used plum.100g is liked to plum and clean, dry rear mechanical disintegration, join in the aqueous solution of 50 times and soak, add 5g/L sodium hydroxide and 5g/L sodium-chlor, at 60 DEG C of temperature dipping 60min, remove by filter after residue, obtain liking right stock staining solution of the rainy season.To like right stock staining solution of the rainy season and dilute 20 multiples, take out 100mL happiness right dye-dilution liquid of the rainy season, 10g real silk fabric is put into diluent to dye, with vinegar acid for adjusting pH be 6,100 DEG C of dyeing temperatures, dyeing time 75min, the real silk fabric after dyeing is washed oven dry, obtain bright-coloured red real silk, colour fastness after tested result referring to table 1.
Referring to accompanying drawing 2, it be the real silk fabric that makes by the present embodiment working method on dye trend map.In figure, curve B is for before dying, curve C for dye rear 10 minutes 60 DEG C, curve D for dye rear 20 minutes 80 DEG C, curve E for dye rear 30 minutes 100 DEG C, curve F is for dying latter 40 minutes, curve G is 50 minutes, curve H is for dying latter 60 minutes, and curve I is for dying latter 70 minutes, and curve J is for dying latter 75 minutes.
Embodiment 2:
100g is liked to plum and clean rear mechanical disintegration, then join in 50 times of aqueous solution and soak, add 3g/L sodium hydroxide, add 10g/L sodium-chlor, at 80 DEG C of temperature dipping 80min, remove by filter after residue, obtain liking right stock staining solution of the rainy season, will like 20 times of right stock staining solution dilutions of the rainy season, take out 100mL happiness right dye-dilution liquid of the rainy season, 10g cashmere fiber is put into diluent to dye, with vinegar acid for adjusting pH be 5,90 DEG C of dyeing temperatures, dyeing time 80min, cashmere fiber after dyeing is washed oven dry, colour fastness after tested result referring to table 1.
Embodiment 3:
100g is liked to plum and clean rear mechanical disintegration, then join in 50 times of aqueous solution and soak, add 5g/L sodium hydroxide, add 10g/L sodium-chlor, at 60 DEG C of temperature dipping 60min, remove by filter after residue, obtain liking right stock staining solution of the rainy season, will like 20 times of right stock staining solution dilutions of the rainy season, take out 100mL happiness right dye-dilution liquid of the rainy season, 10g wool yarn is put into diluent to dye, with vinegar acid for adjusting pH be 5,90 DEG C of dyeing temperatures, dyeing time 80min, wool yarn after dyeing is washed oven dry, colour fastness after tested result referring to table 1.
The colour fastness test result of the each embodiment product of table 1
Claims (7)
1. like the preparation method of plum natural dyestuff for one kind, it is characterized in that step is as follows: happiness plum is cleaned, dried, mechanical disintegration, by weight, be soaked in the water of 10～50 times, add sodium hydroxide 5～10g/L, sodium-chlor 5～10g/L, under the temperature condition of 30～100 DEG C, after dip treating, remove by filter residue, obtain liking right stock staining solution of the rainy season.
2. a kind of preparation method who likes plum natural dyestuff according to claim 1, is characterized in that: the described dip treating time is 30～100min.
3. the happiness plum natural dyestuff stoste obtaining by claim 1 preparation method.
4. a happiness plum natural dyestuff as claimed in claim 2 is applied to the ecological dyeing method to thiozell, it is characterized in that step is as follows: will like right stock staining solution dilution of the rainy season, in dyeing installation to the thiozell processing of dyeing; bath raio is 1:10～50, and the pH of dye liquor is 5～7, and dyeing temperature is 80～100 DEG C; dyeing time is 45～90min; again through washing, dry, obtain a kind of red protein fiber.
5. a kind of ecological dyeing method of plum natural dyestuff to thiozell of liking according to claim 4, is characterized in that: described dyeing processing comprise adopt flood, pad, spraying, spray technology.
6. a kind of ecological dyeing method of plum natural dyestuff to thiozell of liking according to claim 4, is characterized in that: described thiozell comprises the one in silk, wool, cashmere, or their blending product.
7. a kind of ecological dyeing method of plum natural dyestuff to thiozell of liking according to claim 4, is characterized in that: the state of thiozell comprises bulk fibre, yarn, fabric or finished product dress ornament.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410122603.9A CN103865292B (en) | 2014-03-28 | 2014-03-28 | A kind of ecological dyeing liked plum natural dyestuff, preparation method and be applied to thiozell |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410122603.9A CN103865292B (en) | 2014-03-28 | 2014-03-28 | A kind of ecological dyeing liked plum natural dyestuff, preparation method and be applied to thiozell |
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| Publication Number | Publication Date |
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| CN103865292A true CN103865292A (en) | 2014-06-18 |
| CN103865292B CN103865292B (en) | 2015-10-28 |
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| CN201410122603.9A Expired - Fee Related CN103865292B (en) | 2014-03-28 | 2014-03-28 | A kind of ecological dyeing liked plum natural dyestuff, preparation method and be applied to thiozell |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105421111A (en) * | 2015-12-22 | 2016-03-23 | 广州番禺职业技术学院 | Process of printing and dyeing animal skin with pitaya juice |
| CN106046846A (en) * | 2016-05-26 | 2016-10-26 | 惠州同富康生物科技有限公司 | Method for extracting peel pigment from green plums |
| CN107354739A (en) * | 2017-07-05 | 2017-11-17 | 苏州大学 | modified silk fabric and preparation method thereof |
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| CN1030924A (en) * | 1988-08-06 | 1989-02-08 | 陕西省微生物研究所 | The extracting method of fructus pyracanthae red pigment |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105421111A (en) * | 2015-12-22 | 2016-03-23 | 广州番禺职业技术学院 | Process of printing and dyeing animal skin with pitaya juice |
| CN106046846A (en) * | 2016-05-26 | 2016-10-26 | 惠州同富康生物科技有限公司 | Method for extracting peel pigment from green plums |
| CN107354739A (en) * | 2017-07-05 | 2017-11-17 | 苏州大学 | modified silk fabric and preparation method thereof |
| CN107354739B (en) * | 2017-07-05 | 2020-03-10 | 苏州大学 | Modified silk fabric and preparation method thereof |
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| Publication number | Publication date |
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| CN103865292B (en) | 2015-10-28 |
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Effective date of registration: 20160601 Address after: 200135 room D02, building, No. 2000, Pudong Avenue, Pudong New Area Free Trade Zone, Shanghai Patentee after: ABESS NANOTECHNOLOGY (SHANGHAI) Co.,Ltd. Address before: 215123 Suzhou City, Suzhou Province Industrial Park, No. love road, No. 199 Patentee before: Soochow University |
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Address after: 200135 room D02, building, No. 2000, Pudong Avenue, Pudong New Area Free Trade Zone, Shanghai Patentee after: ABS INTERNATIONAL Inc. Address before: 200135 room D02, building, No. 2000, Pudong Avenue, Pudong New Area Free Trade Zone, Shanghai Patentee before: ABESS NANOTECHNOLOGY (SHANGHAI) Co.,Ltd. |
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Effective date of registration: 20170308 Address after: 215138 Suzhou, Xiangcheng District Yangcheng Lake Town, Lake Road, painter, No. 13, No. Patentee after: SUZHOU HEXIANG TEXTILE CO.,LTD. Address before: 200135 room D02, building, No. 2000, Pudong Avenue, Pudong New Area Free Trade Zone, Shanghai Patentee before: ABS INTERNATIONAL Inc. |
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Address after: 215138 Suzhou, Xiangcheng District Yangcheng Lake Town, Lake Road, painter, No. 13, No. Patentee after: SUZHOU HEXIANG TEXTILE TECHNOLOGY CO.,LTD. Address before: 215138 Suzhou, Xiangcheng District Yangcheng Lake Town, Lake Road, painter, No. 13, No. Patentee before: SUZHOU HEXIANG TEXTILE CO.,LTD. |
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