CN104988773A - Dyeing method of environmentally-friendly bamboo fiber bath towel - Google Patents
Dyeing method of environmentally-friendly bamboo fiber bath towel Download PDFInfo
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Abstract
The invention relates to a dyeing method of a bamboo fiber bath towel, and especially relates to a dyeing method of an environmentally-friendly bamboo fiber bath towel. The method comprises the following steps: 1, extracting a plant color fixing agent; 2, drying the plant color fixing agent; 3, extracting a plant dyeing agent; 4, pre-processing; 5, carrying out primary color fixation; 5, dyeing; 7, carrying out secondary color fixation; and 8, dehydrating, and drying. Primary color fixation, dyeing and secondary color fixation are combined to dye the bamboo fiber bath towel, so the process is simple, the color is fastened, and a color fixation solution can be repeatedly used to save the cost; the above ultrasonic dyeing method realizes fast and uniform dyeing and softens the bamboo fiber bath towel; and plant extract products are adopted as the color fixation agent and the dyeing agent, have the characteristics of no heavy metal ions, natural plants, environmentally-friendly dyeing, weed removal, production facilitation and low cost, can clear heat, detoxify and prevent bacteria, and has a very good protection effect on skins.
Description
Technical field
The present invention relates to the colouring method of bamboo fiber, particularly relate to a kind of colouring method of Environmental-protection bamboo fiber bath towel, belong to bamboo fiber dyeing industry.
Background technology
Bamboo fiber owing to having natural antibacterial, antibacterial and anti-ultraviolet effect is widely used in the pro-skin products such as clothes, bedding, towel, chemical dyeing method is mainly adopted to dye to bamboo fiber at present, be 2011-01-05 if publication number is CN101935930A(publication number) Chinese patent, adopt pickling dirty painted very large to environment in the method pretreatment process, and usually make pro-skin product due to bamboo fiber, therefore can not ensure with the bamboo fiber after chemical dyeing method process the safety that people use.Along with the raising of people's quality of the life, increasing researcher starts trial natural dye and carries out painted, the Chinese patent being CN201210384097.1 as publication number adopts tealeaves for the dyeing of bamboo fiber, the method once dyeing after through mordant dyeing look, carrying out secondary dyeing, utilize lime and ethylenediamine tetra-acetic acid to be chemical reagent in matchmaker's dyeing course, the effect of natural environmental-protective can not be played, and the quality of chemical reagent to bamboo fiber has a certain impact.Therefore, to natural dyeing agent, further research is also needed to the technique that bamboo fiber dyes.
Bamboo fibre bath towel uses when being and taking a shower, and directly contacts skin, with chemical staining agent or color-fixing agent, easily produces stimulation well to skin, or even irritated, dyes, well can protect skin by the method for All Pure Nature to bamboo fibre bath towel.
Summary of the invention
The object of the invention is for solving the problems of the technologies described above, a kind of colouring method of Environmental-protection bamboo fiber bath towel is provided.The colouring method operation that the present invention is used for bamboo fibre bath towel is simple, and cost is low, ecological, environmental protective, the function of treated bamboo fibre bath towel not only firm coloration but also health care.
A colouring method for Environmental-protection bamboo fiber bath towel, processing step is as follows:
(1) aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian are cleaned, making beating, 120 ~ 200 orders sieve, and obtain juice;
(2) juice is carried out vacuum freeze drying, obtain plant color-fixing agent;
(3) acalypha copperleaf, lady's-grass and wartwort are cleaned, smash, supercritical carbon dioxide extracting, obtain vegetable dyeing agent, being adjusted to concentration is 5%;
(4) by the blanching in the hot water of bamboo fibre bath towel, temperature 90 ~ 100 DEG C, blanching 20 ~ 30 minutes, takes out, rinses by normal-temperature water;
(5) fixation: water bamboo fibre bath towel being put into 45 ~ 55 DEG C, add plant color-fixing agent 1 ~ 2g/L, bath raio 1:30 ~ 35, stir immersion 40 ~ 50 minutes, take out, rinse by normal-temperature water;
(6) dye: the bamboo fibre bath towel through soaking is put into vegetable dyeing agent by bath raio 1:20 ~ 25, ultrasonic wave soaks, and temperature is 50 ~ 55 DEG C, is incubated 5 ~ 10 minutes, with 1 ~ 2 DEG C/min of intensification, to 70 ~ 80 DEG C, is incubated 20 ~ 30 minutes;
(7) secondary fixation: the plant color-fixing agent bamboo fibre bath towel after dyeing being put into step 5), stirs immersion 20 ~ 30 minutes, takes out, rinses by normal-temperature water;
(8) dewater, dry.
Described supercritical carbon dioxide extracting condition is temperature 38 DEG C, pressure 36MPa.
The frequency of described Ultrasonic Dyeing is 30kHz.
Described aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian are by weight 3:0.8:1.2:2:0.6 mixing (in fresh material), and the mixing colour fixation of this ratio is good.Described acalypha copperleaf, lady's-grass and wartwort are by weight 12:4:8.5 mixing (in fresh material), and color-fixing agent and the coloring agent treatment effect of this proportioning are more natural, nondiscoloration nondiscolouring, painted easier, good stability, and have good skin care effect.
The colouring method of a kind of Environmental-protection bamboo fiber bath towel provided by the present invention; extract aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian cleaned is adopted to be plant color-fixing agent; with the extract of acalypha copperleaf, lady's-grass and wartwort as coloring agent; naturally not stimulate; can be clearing heat and detoxicating; antibacterial bacteriostatic, has good protective effect to skin.And acalypha copperleaf, lady's-grass and wartwort are ruderal, in this, as coloring agent, can reduce weeds, be beneficial to production, wide material sources, cost is low.
The present invention adopts fixation, dyeing and a secondary fixation to combine and to dye to bamboo fibre bath towel, and technique is simple, color fast, effectively improves the attachment of the molecule of colouring matter.Because after a fixation, plant color-fixing agent and bamboo fibre bath towel generation crosslinked action, bamboo fibre bath towel forms a skim; After vegetable dyeing agent dyeing, some coordinate bonds in vegetable dyeing agent and bamboo fibre and plant color-fixing agent react, and make dyeing firm; After secondary fixation, reaction and unreacted dyestuff on bamboo fibre are carried out coated closing by plant color-fixing agent, increase the smoothness on bamboo fibre bath towel surface simultaneously, reduce coefficient of friction, in addition, the magnesium of the trace that plant color-fixing agent contains, aluminum metal ion are good natural mordants, can improve the adhesion between bamboo fibre and dyestuff, contribute to the raising of dyefastness, improve crock fastness.
The invention has the beneficial effects as follows: the present invention adopts fixation, dyeing and a secondary fixation to combine and to dye to bamboo fibre bath towel, and technique is simple, color fast, and fixation liquid can be reused, cost-saving; Ultrasonic wave dyeing method not only dyes fast, evenly, can also softening bamboo fibre bath towel; Using plant extracts as color-fixing agent and coloring agent, not containing heavy metal ion, natural plants, painted environmental protection, can remove weeds, be beneficial to production, cost is low, again can be clearing heat and detoxicating, and antibacterial bacteriostatic, has good protective effect to skin.
The present invention adopts fixation, dyeing and a secondary fixation to combine and to dye to bamboo fibre bath towel, and technique is simple, color fast, and fixation liquid can be reused, cost-saving; Ultrasonic wave dyeing method not only dyes fast, evenly, can also softening bamboo fibre bath towel; Using plant extracts as color-fixing agent and coloring agent, not containing heavy metal ion, natural plants, dyeing environmental protection, can remove weeds, be beneficial to production, cost is low, again can be clearing heat and detoxicating, and antibacterial bacteriostatic, has good protective effect to skin.
Detailed description of the invention
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the amendment not having creative contribution as required after reading this description, as long as but be all subject to the protection of Patent Law in right of the present invention.
Embodiment 1
A colouring method for Environmental-protection bamboo fiber bath towel, processing step is as follows:
(aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian clean by 1, making beating, and 120 orders sieve, and obtain juice;
(2) juice is carried out vacuum freeze drying, obtain plant color-fixing agent;
(3) acalypha copperleaf, lady's-grass and wartwort are cleaned, smash, temperature 38 DEG C, carry out supercritical carbon dioxide extracting, obtain vegetable dyeing agent under the condition of pressure 36MPa, being adjusted to concentration is 5%;
(4) by the blanching in the hot water of bamboo fibre bath towel, temperature 90 DEG C, blanching 20 minutes, takes out, rinses by normal-temperature water;
(5) fixation: water bamboo fibre bath towel being put into 45 DEG C, add plant color-fixing agent 1g/L, bath raio 1:30, stir immersion 40 minutes, take out, rinse by normal-temperature water;
(6) dye: the bamboo fibre bath towel through soaking is put into vegetable dyeing agent by bath raio 1:20, and carry out ultrasonic wave immersion under the condition of frequency 30kHz, temperature is 50 DEG C, is incubated 5 minutes, with 1 DEG C/min of intensification, to 70 DEG C, is incubated 20 minutes;
(7) secondary fixation: the plant color-fixing agent bamboo fibre bath towel after dyeing being put into step 5), stirs immersion 20 minutes, takes out, rinses by normal-temperature water;
(8) dewater, dry.
Embodiment 2
A colouring method for Environmental-protection bamboo fiber bath towel, processing step is as follows:
(1) aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian are cleaned, making beating, 160 orders sieve, and obtain juice;
(2) juice is carried out vacuum freeze drying, obtain plant color-fixing agent;
(3) acalypha copperleaf, lady's-grass and wartwort are cleaned, smash, temperature 38 DEG C, carry out supercritical carbon dioxide extracting, obtain vegetable dyeing agent under the condition of pressure 36MPa, being adjusted to concentration is 5%;
(4) by the blanching in the hot water of bamboo fibre bath towel, temperature 95 DEG C, blanching 25 minutes, takes out, rinses by normal-temperature water;
(5) fixation: water bamboo fibre bath towel being put into 50 DEG C, add plant color-fixing agent 1.5g/L, bath raio 1:32, stir immersion 45 minutes, take out, rinse by normal-temperature water;
(6) dye: the bamboo fibre bath towel through soaking is put into vegetable dyeing agent by bath raio 1:23, and carry out ultrasonic wave immersion under the condition of frequency 30kHz, temperature is 53 DEG C, is incubated 7 minutes, with 1.5 DEG C/min of intensifications, to 75 DEG C, is incubated 25 minutes;
(7) secondary fixation: the plant color-fixing agent bamboo fibre bath towel after dyeing being put into step 5), stirs immersion 25 minutes, takes out, rinses by normal-temperature water;
(8) dewater, dry.
Embodiment 3
A colouring method for Environmental-protection bamboo fiber bath towel, processing step is as follows:
(1) aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian are cleaned, making beating, 200 orders sieve, and obtain juice;
(2) juice is carried out vacuum freeze drying, obtain plant color-fixing agent;
(3) acalypha copperleaf, lady's-grass and wartwort are cleaned, smash, temperature 38 DEG C, carry out supercritical carbon dioxide extracting, obtain vegetable dyeing agent under the condition of pressure 36MPa, being adjusted to concentration is 5%;
(4) by the blanching in the hot water of bamboo fibre bath towel, temperature 100 DEG C, blanching 30 minutes, takes out, rinses by normal-temperature water;
(5) fixation: water bamboo fibre bath towel being put into 55 DEG C, add plant color-fixing agent 2g/L, bath raio 1:35, stir immersion 50 minutes, take out, rinse by normal-temperature water;
(6) dye: the bamboo fibre bath towel through soaking is put into vegetable dyeing agent by bath raio 1:25, and carry out ultrasonic wave immersion under the condition of frequency 30kHz, temperature is 55 DEG C, is incubated 10 minutes, with 2 DEG C/min of intensifications, to 80 DEG C, is incubated 30 minutes;
(7) secondary fixation: the plant color-fixing agent bamboo fibre bath towel after dyeing being put into step 5), stirs immersion 30 minutes, takes out, rinses by normal-temperature water;
(8) dewater, dry.
Comparative example 1
Be that processing step is as follows by the method design comparative example that tealeaves dyes to bamboo fiber in the Chinese patent of CN201210384097.1 according to publication number:
(1) coloring liquid boiling extraction, tealeaves and water are loaded in stainless-steel pan with weight ratio 1:40, be warming up to 100 DEG C, after boiling 30 ~ 50 minutes, elimination tea grounds obtains coloring liquid;
(2) design, employing pressure tongue rod, ice-cream stick rod, washing-free chopstick are made pattern design tool and the bamboo fiber of precolor are carried out painted cloth design;
(3) soak, the bamboo fiber through design is put into temperature be 28 ~ 45 DEG C water soak 20 ~ 40 minutes; Analysis for soybean powder is added in described water; The weight ratio of described analysis for soybean powder and water is 1:20 ~ 1:40;
(4) once painted, the bamboo fiber through soaking being put into by bath raio 1:20 ~ 1:40 the coloring liquid that step a) prepared, being warming up to 56 ~ 64 DEG C, being incubated 30 ~ 45 minutes;
(5) matchmaker is painted, will put into matchmaker's coloring liquid matchmaker painted 20 ~ 30 minutes through once painted bamboo fiber; The aqueous solution that described matchmaker's coloring liquid is made up of lime and ethylenediamine tetra-acetic acid; Described lime and water form with 1:20 ~ 1:30 weight ratio; Described lime is 3 ~ 5% of described bamboo fiber weight; Described ethylenediamine tetra-acetic acid is 1 ~ 2% of described bamboo fiber weight;
(6) secondary coloring, takes out the bamboo fiber painted through matchmaker and wrings out from matchmaker's coloring liquid, then puts into the coloring liquid that step a) prepared, and is warming up to 75 ~ 80 DEG C, is incubated 30 ~ 45 minutes;
(7) namely soft treatment, by the taking-up from coloring liquid of the bamboo fiber through secondary coloring softener soft treatment, then obtain painted bamboo fiber through washing post-drying.
Comparative example 2
Processing step is as follows:
(1) aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian are cleaned, making beating, 200 orders sieve, and obtain juice;
(2) juice is carried out vacuum freeze drying, obtain plant color-fixing agent;
(3) acalypha copperleaf, lady's-grass and wartwort are cleaned, smash, temperature 38 DEG C, carry out supercritical carbon dioxide extracting, obtain vegetable dyeing agent under the condition of pressure 36MPa, being adjusted to concentration is 5%;
(4) by the blanching in the hot water of bamboo fibre bath towel, temperature 100 DEG C, blanching 30 minutes, takes out, rinses by normal-temperature water;
(5) dye: the bamboo fibre bath towel through soaking is put into vegetable dyeing agent by bath raio 1:25, and carry out ultrasonic wave immersion under the condition of frequency 30kHz, temperature is 55 DEG C, is incubated 10 minutes, with 2 DEG C/min of intensifications, to 80 DEG C, is incubated 30 minutes;
(6) fixation: the bamboo fibre bath towel after dyeing is put into plant color-fixing agent, plant color-fixing agent 1.5g/L, bath raio 1:32, stirs immersion 30 minutes, takes out, rinses by normal-temperature water;
(7) dewater, naturally dry.
The test sample of the embodiment of the present invention and comparative example is bamboo fiber, bamboo fiber after the embodiment of the present invention is painted and comparative example dyeing after bamboo fiber press AATCC16-19933 method of testing mensuration light fastness, ISO-105-C06 method of testing measures washing fastness, GB/T3920-1997 standard test crock fastness.Table 1 for after the bamboo fiber after embodiment of the present invention dyeing and comparative example dyeing the test result of bamboo fiber.
After bamboo fiber after the dyeing of table 1 embodiment of the present invention and comparative example dyeing the test result of bamboo fiber
| Test case | Light fastness/level | Washing fastness/level | Dry fastness/level | Fastness to wet rubbing/level |
| Embodiment 1 | 7 | 4~5 | 3 | 2~3 |
| Embodiment 2 | 7 | 4 | 3~4 | 3 |
| Embodiment 3 | 7~8 | 4 | 3~4 | 3 |
| Comparative example 1 | 6 | 2~3 | 2~3 | 1~2 |
| Comparative example 2 | 6 | 3 | 3 | 2 |
(1) as can be seen from table 1 test result, bamboo fiber light fastness progression after embodiment of the present invention dyeing higher than after being dyeed by comparative example the light fastness progression of bamboo fiber, illustrate the bamboo fiber after embodiment of the present invention dyeing have than after being dyeed by comparative example bamboo fiber there is better light fastness.
(2) as can be seen from table 1 test result, bamboo fiber washing fastness progression after embodiment of the present invention dyeing higher than after being dyeed by comparative example the washing fastness progression of bamboo fiber, illustrate the bamboo fiber after embodiment of the present invention dyeing have than after being dyeed by comparative example bamboo fiber there is better washing fastness.
(3) as can be seen from table 1 test result, bamboo fiber friction (dry friction and wet friction) fastness progression after embodiment of the present invention dyeing, higher than friction (dry friction and wet friction) the fastness progression of the bamboo fiber after being dyeed by comparative example, illustrates that the bamboo fiber after embodiment of the present invention dyeing has and has better friction (dry friction and wet friction) fastness than the bamboo fiber after being dyeed by comparative example.
Claims (5)
1. a colouring method for Environmental-protection bamboo fiber bath towel, is characterized in that, processing step is as follows:
(1) aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian are cleaned, making beating, 120 ~ 200 orders sieve, and obtain juice;
(2) juice is carried out vacuum freeze drying, obtain plant color-fixing agent;
(3) acalypha copperleaf, lady's-grass and wartwort are cleaned, smash, supercritical carbon dioxide extracting, obtain vegetable dyeing agent, being adjusted to concentration is 5%;
(4) by the blanching in the hot water of bamboo fibre bath towel, temperature 90 ~ 100 DEG C, blanching 20 ~ 30 minutes, takes out, rinses by normal-temperature water;
(5) fixation: water bamboo fibre bath towel being put into 45 ~ 55 DEG C, add plant color-fixing agent 1 ~ 2g/L, bath raio 1:30 ~ 35, stir immersion 40 ~ 50 minutes, take out, rinse by normal-temperature water;
(6) dye: the bamboo fibre bath towel through soaking is put into vegetable dyeing agent by bath raio 1:20 ~ 25, ultrasonic wave soaks, and temperature is 50 ~ 55 DEG C, is incubated 5 ~ 10 minutes, with 1 ~ 2 DEG C/min of intensification, to 70 ~ 80 DEG C, is incubated 20 ~ 30 minutes;
(7) secondary fixation: the plant color-fixing agent bamboo fibre bath towel after dyeing being put into step 5), stirs immersion 20 ~ 30 minutes, takes out, rinses by normal-temperature water;
(8) dewater, dry.
2. the colouring method of a kind of Environmental-protection bamboo fiber bath towel as claimed in claim 1, is characterized in that, described supercritical carbon dioxide extracting condition is temperature 38 DEG C, pressure 36MPa.
3. the colouring method of a kind of Environmental-protection bamboo fabric as claimed in claim 1, is characterized in that, in step 6), the frequency of institute's Ultrasonic Dyeing is 30kHz.
4. the colouring method of a kind of Environmental-protection bamboo fabric as claimed in claim 1, is characterized in that, described aloe, the thousand pines in generation field, Gem flower-shaped three-dimensional jig-saw puzzle, corn stone and special Yu Lian are by weight 3:0.8:1.2:2:0.6 mixing.
5. the colouring method of a kind of Environmental-protection bamboo fabric as claimed in claim 1, is characterized in that, described acalypha copperleaf, lady's-grass and wartwort are by weight 12:4:8.5 mixing.
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| CN105177979A (en) * | 2015-10-29 | 2015-12-23 | 成都纺织高等专科学校 | Ozone-ultrasonic wave synergetic textile scouring, bleaching and dyeing method and device |
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| CN105839432A (en) * | 2016-04-06 | 2016-08-10 | 常州市好利莱光电科技有限公司 | Preparation method of natural dye fixing agent |
| CN106835775A (en) * | 2016-12-23 | 2017-06-13 | 句容市申兔工艺针织厂 | A kind of preparation method of plant color fixing agent |
| CN107541965A (en) * | 2017-10-27 | 2018-01-05 | 苏州市叶绣工艺厂 | The colouring method of embroidery yarn |
| CN108824027A (en) * | 2018-07-05 | 2018-11-16 | 佛山市衣香蒂丝服装设计有限公司 | A kind of textile fabric coloring agent |
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| CN107541965A (en) * | 2017-10-27 | 2018-01-05 | 苏州市叶绣工艺厂 | The colouring method of embroidery yarn |
| CN108824027A (en) * | 2018-07-05 | 2018-11-16 | 佛山市衣香蒂丝服装设计有限公司 | A kind of textile fabric coloring agent |
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