CN1367207A - Preparation method of plant dyestuff and method for dyeing wool fabric - Google Patents
Preparation method of plant dyestuff and method for dyeing wool fabric Download PDFInfo
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- CN1367207A CN1367207A CN 01138072 CN01138072A CN1367207A CN 1367207 A CN1367207 A CN 1367207A CN 01138072 CN01138072 CN 01138072 CN 01138072 A CN01138072 A CN 01138072A CN 1367207 A CN1367207 A CN 1367207A
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Abstract
A preparation method of plant dyestuff for dyeing wool fabric includes the following steps: (1). selecting plant raw material containing natural (colouring matter), pulverizing, adding water or solvent, boiling to extract natural dyestuff liquor; (2). evaporating or concentrating the extracted dyestuff liquor to dobtain liquid colouring matter substance; and (3) solidifying the above-mentioned liquid colouring matter substance and pulverizing so as to obtain the powdered natural dyestuff. Its wool fabric dyeing method is characterized by that the pH value of dye liquor is 4-9, bathing ratio is 1:20-150 and dyeing temp. is 60-100 deg.C.
Description
(1) technical field: the present invention relates to a kind of preparation method of vegetable dye and the method for dyeing wool fabric thereof.Belonging to dyestuff extracts and the fabrics printing and dyeing technical field.
(2) background technology: at present some raw materials, the intermediate of synthetic dyestuff commonly used belong to the carinogenicity material, not only severe contamination environment, the wearer or the producer are injured.For this reason, people turn to traditional natural dyestuff in recent years, have become the trend of one " back to nature ".Major cause is that natural dyestuff and ecotope consistency are good, biological degradation; And it is nontoxic even have a nourishing function; In addition, natural dyestuff has abundant natural energy resources and is the nature tone.But people understand lessly to the color and the structure of natural dyestuff, and because its traditional application art is not suitable for the requirement of modern industry, can't mass production.The source of the natural fabric dyestuff of being familiar with at present only is several edible natural pigments, because colour fastness is low, color is few, major part is unwell to industrialization.
(3) summary of the invention: the object of the present invention is to provide a kind of aboundresources, easily expansion plantation, good, the many methods that also can be useful for the natural plant dye and the dyeing wool fabric thereof of textile dyeing of chromatogram of colour fastness.Technology contents of the present invention is: a kind of natural plant dye comprises the following steps: successively
1. choose the plant material that contains natural pigment, add water or solvent boiling-off after the pulverizing and extract natural dyestuff liquid;
2. with the dye solution evaporation of extracting or concentrate, liquid chromatoplast;
3. with liquid chromatoplast through overcuring, pulverizing, powdered natural dyestuff.
The method of vegetable dye dyeing wool fabric is: the pH value 4-9 of its dye liquor, bath raio 1: 20-150, dyeing temperature are 60-100 ℃.
The present invention has following advantage:
1, plant material aboundresources, easily expansion plantation are nontoxic, harmless.
2, the dyeing colour fastness is good, does not fade, variable color, and dyeing is balanced, chromatogram is many.
3, color and luster is soft, simple and unsophisticated, natural, gives people's's a kind of " answer the Nature " impression.
4, do not exist synthetic dyestuff to the pollution of environment with to the injury of human body, also have nourishing function.
5, be applied to the cleaner production of woolen industry, but mass production.
(4) embodiment:
Embodiment 1:
1, choosing the plant material that contains natural pigment, can be shizandra berry or Flos Celosiae Cristatae, Root of Pubescent Holly, akebi, river wood mortar, duck head grass, Philippine Violet Herb, the bark of ash, Pueraria lobota, peppermint, orange, bamboo, giant knotweed.After the collection, clean, dry, have flower, branch and leaf with its flower, branch, leaf separately, be cut into small pieces, adding distil water boiling-off respectively, the ratio of plant material and distilled water is 1: 5, utilizes and coagulates the stream pipe, extraction natural dyestuff liquid.Temperature with the distilled water extraction dyestuff is 30 ℃.The time of extracting dyestuff is 1 hour.
2, the dye solution utilization of extracting is executed the evaporation of commentaries on classics evaporation instrument, made liquid natural dyestuff, utilize the powder machine to make the powder-type natural dyestuff again.
Embodiment 2:
1, choosing the plant material that contains natural pigment, can be shizandra berry or Flos Celosiae Cristatae, Root of Pubescent Holly, akebi, river wood mortar, duck head grass, Philippine Violet Herb, the bark of ash, Pueraria lobota, peppermint, orange, bamboo, giant knotweed.After the collection, clean, dry, have flower, branch, leaf with its flower, branch, leaf separately, be cut into small pieces, add the alcohol boiling-off respectively, the ratio of plant material and alcohol is 1: 10, utilizes and coagulates the stream pipe, extraction natural dyestuff liquid.Temperature with the distilled water extraction dyestuff is 100 ℃.The time of extracting dyestuff is 3 hours.
2, the dye solution heating of extracting is concentrated, make liquid natural dyestuff, utilize the powder machine to make the powder-type natural dyestuff again.
Embodiment 3:
In dyeing machinery, put into wool fabric, add the clear water rinsing, bleed off scavenging solution, add water by 1: 20 bath raio, heat, add the mordant dyeing of 0.5%owf metallic aluminium ion elder generation, the mordant dyeing temperature is 40 ℃, be 10 minutes heat-up time, soaking time 10 minutes adds dye liquor after the tapping, amount of dye is the 50ml/5g wool fabric, dye liquor pH value 4; bath raio 1: 20, the dyeing of heating, dyeing time totally 1 hour; be warmed up to 60 ℃; soaking time 30 minutes adds water then and cleans, and the finishing rolls arrangement is gone up in the dehydration back; tenter machine tentering, yardstick gained wool fabric.
Embodiment 4, put into wool fabric in dyeing machinery, add the clear water rinsing, bleed off scavenging solution, add dye liquor, amount of dye 10ml/5g wool fabric, dye liquor pH value 9; bath raio 1: 150; dyeing time totally 3 hours are warmed up to 100 ℃, soaking time 90 minutes; dyeing back tapping; add water by 1: 150 bath raio, add mordant dyeing behind the 10%owf metal copper ion then, and the mordant dyeing temperature is 100 ℃; be 1 hour heat-up time; soaking time 80 minutes, cleans, and the dehydration back is gone up finishing rolls and put in order; tenter machine tentering, yardstick gained wool fabric.
Embodiment 5, put into wool fabric in dyeing machinery, add the clear water rinsing, bleed off scavenging solution, add dye liquor, dye liquor pH value 7; bath raio 1: 40 adds 5%owf metallic iron ion again, heats same mordant dyeing; 80 ℃ of Heating temperatures, and be 40 minutes heat-up time, soaking time 60 minutes; add water after the tapping and clean; finishing rolls arrangement, tenter machine tentering, yardstick gained wool fabric are gone up in the dehydration back.
Claims (10)
1, a kind of preparation method of vegetable dye is characterized in that: comprise the following steps: successively
1. choose the plant material that contains natural pigment, add water or solvent boiling-off after the pulverizing and extract natural dyestuff liquid;
2. with the dye solution evaporation of extracting or concentrate, liquid chromatoplast;
3. liquid chromatoplast is pulverized powdered natural dyestuff through overcuring.
2, the preparation method of a kind of vegetable dye according to claim 1, the ratio that it is characterized in that plant material and water or solvent is 1: 5-10.
3, the preparation method of a kind of vegetable dye according to claim 1 utilizes when it is characterized in that boiling-off and coagulates the stream pipe, extracts natural dyestuff liquid.
4, the preparation method of a kind of vegetable dye according to claim 1 is characterized in that it is 30-100 ℃ that the temperature of dyestuff is extracted in boiling-off.
5,, it is characterized in that the described plant material that contains natural pigment is shizandra berry or Flos Celosiae Cristatae, Root of Pubescent Holly, akebi, river wood mortar, duck head grass, Philippine Violet Herb, the bark of ash, Pueraria lobota, peppermint, orange, bamboo, giant knotweed according to the preparation method of claim 1 or 2,3,4 described a kind of vegetable dyes.
6, a kind of method of vegetable dye dyeing wool fabric is characterized in that the pH value 4-9 of dye liquor, bath raio 1: 20-150.
7, the method for a kind of vegetable dye dyeing wool fabric according to claim 6 is characterized in that dyeing temperature is 60-100 ℃.
8, according to the method for claim 6 or 7 described a kind of vegetable dye dyeing wool fabrics, it is characterized in that being added with in the dyeing process mordant, mordant is aluminium or copper, ferrous metal ion, mordant can add before wool fabric drops into the plant dye liquor or after the dyeing rinsing, also can add in plant dye liquor dyeing course.
9, the method for a kind of vegetable dye dyeing wool fabric according to claim 8, the concentration that it is characterized in that mordant is 0.5-10%owf.
10,, it is characterized in that the mordant dyeing temperature is 40-100 ℃ according to the method for claim 6 or 7 described a kind of vegetable dye dyeing wool fabrics.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB011380721A CN1180033C (en) | 2001-12-30 | 2001-12-30 | Preparation method of plant dyestuff and method for dyeing wool fabric |
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| Application Number | Priority Date | Filing Date | Title |
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| CNB011380721A CN1180033C (en) | 2001-12-30 | 2001-12-30 | Preparation method of plant dyestuff and method for dyeing wool fabric |
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| CN1367207A true CN1367207A (en) | 2002-09-04 |
| CN1180033C CN1180033C (en) | 2004-12-15 |
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Cited By (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101983991A (en) * | 2010-07-26 | 2011-03-09 | 杭州集美印染有限公司 | Preparation method and dyeing method of sapelli wood natural dye |
| CN102010615A (en) * | 2010-11-29 | 2011-04-13 | 南通大学 | Bamboo leaf dye and extraction method and application thereof |
| CN102093749A (en) * | 2011-01-11 | 2011-06-15 | 烟台大学 | Preparation technology of schisandra chinensis natural pigment |
| CN102093746A (en) * | 2010-12-10 | 2011-06-15 | 盐城纺织职业技术学院 | Preparation method of basella rubra berry natural plant dye liquor and application of basella rubra berry natural plant dye liquor |
| CN102127309A (en) * | 2010-12-10 | 2011-07-20 | 盐城纺织职业技术学院 | Preparation method and application of natural plant dye solution of Phytolacca acinosa berries |
| RU2493306C1 (en) * | 2012-01-11 | 2013-09-20 | Федеральное Государственное Бюджетное Образовательное Учреждение Высшего Профессионального Образования "Дагестанский Государственный Технический Университет" (Дгту) | Method of mordant dyeing of woolen fabric with vegetable dye of musk thistle |
| CN103554964A (en) * | 2013-11-08 | 2014-02-05 | 哈尔滨市工艺美术有限责任公司 | Formula and production method for preparing tawny wheat straw dye |
| CN103725032A (en) * | 2013-12-13 | 2014-04-16 | 常州大学 | Preparation method and application of natural lotus receptacle pigment |
| CN104172827A (en) * | 2014-06-25 | 2014-12-03 | 惠州市欧野科技有限公司 | Plant-dyed infant pillow |
| CN104403357A (en) * | 2014-10-29 | 2015-03-11 | 宁波广源纺织品有限公司 | Orange peel vegetable dye extraction method |
| CN104988773A (en) * | 2015-07-31 | 2015-10-21 | 界首市双鑫纺织有限公司 | Dyeing method of environmentally-friendly bamboo fiber bath towel |
| CN105133135A (en) * | 2015-07-31 | 2015-12-09 | 界首市双鑫纺织有限公司 | Bamboo fiber and fibrilia fiber blending cloth |
| CN105401464A (en) * | 2015-12-22 | 2016-03-16 | 广州番禺职业技术学院 | Technology for printing and dyeing artificial leather by using kiwi fruit juice |
| CN105504867A (en) * | 2016-01-29 | 2016-04-20 | 辽东学院 | Plant-based natural dye for fabrics as well as preparation method and fabric dyeing method of dye |
| CN105733298A (en) * | 2016-01-29 | 2016-07-06 | 佛山市聚成生化技术研发有限公司 | Preparation method of cotton fabric yellow vegetable dye |
| CN106012607A (en) * | 2016-06-26 | 2016-10-12 | 江苏联宏纺织有限公司 | Decolored raccoon hair dyeing method |
| CN106283723A (en) * | 2016-08-11 | 2017-01-04 | 广东溢达纺织有限公司 | Modified Gardenia Yellow and the method that cation-modified cellulose base fiber fabric is dyeed thereof |
| CN107151924A (en) * | 2017-06-06 | 2017-09-12 | 中原工学院 | A kind of method of high humidity fastness plant dsred protein fiber |
| CN107446377A (en) * | 2017-08-09 | 2017-12-08 | 安徽省新旭堂茶业有限公司 | The preparation method of green natural tea dye liquor |
| CN107476084A (en) * | 2017-08-09 | 2017-12-15 | 安徽省新旭堂茶业有限公司 | Colouring method of the tea/menthyl dye liquor to fabric |
| CN107663796A (en) * | 2017-09-21 | 2018-02-06 | 安徽鞋匠世家新型鞋材科技有限公司 | A kind of coloring agent for preventing leather from fading and preparation method thereof |
| CN107955396A (en) * | 2017-12-19 | 2018-04-24 | 常熟市沪联印染有限公司 | A kind of preparation process of particulate plant dyestuff |
| CN108219515A (en) * | 2018-01-16 | 2018-06-29 | 浙江海明实业有限公司 | A kind of preparation method and colouring method of the yellow vegetable colour of giant knotweed dye |
| CN108276798A (en) * | 2018-01-16 | 2018-07-13 | 浙江海明实业有限公司 | A kind of giant knotweed incarnadines the preparation method and colouring method of vegetable colour |
| CN114316623A (en) * | 2020-10-10 | 2022-04-12 | 南京理工大学 | Method for extracting visible light response natural dye from orychophragmus violaceus leaves |
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- 2001-12-30 CN CNB011380721A patent/CN1180033C/en not_active Expired - Fee Related
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| CN101983991A (en) * | 2010-07-26 | 2011-03-09 | 杭州集美印染有限公司 | Preparation method and dyeing method of sapelli wood natural dye |
| CN102010615A (en) * | 2010-11-29 | 2011-04-13 | 南通大学 | Bamboo leaf dye and extraction method and application thereof |
| CN102010615B (en) * | 2010-11-29 | 2012-12-12 | 南通大学 | Bamboo leaf dye and extraction method and application thereof |
| CN102093746A (en) * | 2010-12-10 | 2011-06-15 | 盐城纺织职业技术学院 | Preparation method of basella rubra berry natural plant dye liquor and application of basella rubra berry natural plant dye liquor |
| CN102127309A (en) * | 2010-12-10 | 2011-07-20 | 盐城纺织职业技术学院 | Preparation method and application of natural plant dye solution of Phytolacca acinosa berries |
| CN102093749A (en) * | 2011-01-11 | 2011-06-15 | 烟台大学 | Preparation technology of schisandra chinensis natural pigment |
| RU2493306C1 (en) * | 2012-01-11 | 2013-09-20 | Федеральное Государственное Бюджетное Образовательное Учреждение Высшего Профессионального Образования "Дагестанский Государственный Технический Университет" (Дгту) | Method of mordant dyeing of woolen fabric with vegetable dye of musk thistle |
| CN103554964A (en) * | 2013-11-08 | 2014-02-05 | 哈尔滨市工艺美术有限责任公司 | Formula and production method for preparing tawny wheat straw dye |
| CN103725032A (en) * | 2013-12-13 | 2014-04-16 | 常州大学 | Preparation method and application of natural lotus receptacle pigment |
| CN103725032B (en) * | 2013-12-13 | 2016-05-04 | 常州大学 | The preparation method of natural lotus receptacle pigment and application thereof |
| CN104172827A (en) * | 2014-06-25 | 2014-12-03 | 惠州市欧野科技有限公司 | Plant-dyed infant pillow |
| CN104172827B (en) * | 2014-06-25 | 2016-02-24 | 惠州市欧野科技有限公司 | A kind of plant dyeing Pillow for infant |
| CN104403357A (en) * | 2014-10-29 | 2015-03-11 | 宁波广源纺织品有限公司 | Orange peel vegetable dye extraction method |
| CN104988773A (en) * | 2015-07-31 | 2015-10-21 | 界首市双鑫纺织有限公司 | Dyeing method of environmentally-friendly bamboo fiber bath towel |
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| CN105733298A (en) * | 2016-01-29 | 2016-07-06 | 佛山市聚成生化技术研发有限公司 | Preparation method of cotton fabric yellow vegetable dye |
| CN105504867A (en) * | 2016-01-29 | 2016-04-20 | 辽东学院 | Plant-based natural dye for fabrics as well as preparation method and fabric dyeing method of dye |
| CN106012607A (en) * | 2016-06-26 | 2016-10-12 | 江苏联宏纺织有限公司 | Decolored raccoon hair dyeing method |
| CN106283723A (en) * | 2016-08-11 | 2017-01-04 | 广东溢达纺织有限公司 | Modified Gardenia Yellow and the method that cation-modified cellulose base fiber fabric is dyeed thereof |
| CN106283723B (en) * | 2016-08-11 | 2019-05-14 | 广东溢达纺织有限公司 | Modified Gardenia Yellow and its method that cation-modified cellulose base fiber fabric is dyed |
| CN107151924A (en) * | 2017-06-06 | 2017-09-12 | 中原工学院 | A kind of method of high humidity fastness plant dsred protein fiber |
| CN107151924B (en) * | 2017-06-06 | 2019-07-19 | 中原工学院 | A kind of method of high humidity fastness plant dsred protein fiber |
| CN107476084A (en) * | 2017-08-09 | 2017-12-15 | 安徽省新旭堂茶业有限公司 | Colouring method of the tea/menthyl dye liquor to fabric |
| CN107446377A (en) * | 2017-08-09 | 2017-12-08 | 安徽省新旭堂茶业有限公司 | The preparation method of green natural tea dye liquor |
| CN107663796A (en) * | 2017-09-21 | 2018-02-06 | 安徽鞋匠世家新型鞋材科技有限公司 | A kind of coloring agent for preventing leather from fading and preparation method thereof |
| CN107955396A (en) * | 2017-12-19 | 2018-04-24 | 常熟市沪联印染有限公司 | A kind of preparation process of particulate plant dyestuff |
| CN108219515A (en) * | 2018-01-16 | 2018-06-29 | 浙江海明实业有限公司 | A kind of preparation method and colouring method of the yellow vegetable colour of giant knotweed dye |
| CN108276798A (en) * | 2018-01-16 | 2018-07-13 | 浙江海明实业有限公司 | A kind of giant knotweed incarnadines the preparation method and colouring method of vegetable colour |
| CN114316623A (en) * | 2020-10-10 | 2022-04-12 | 南京理工大学 | Method for extracting visible light response natural dye from orychophragmus violaceus leaves |
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| CN1180033C (en) | 2004-12-15 |
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Owner name: HAILAN GROUP CO.,LTD.; JIN CHENG ; DONGHUA UNIV. Free format text: FORMER NAME OR ADDRESS: HAILAN GROUP CO.,LTD.; JIN CHENG Owner name: HAILAN GROUP CO.,LTD.; JIN CHENG Free format text: FORMER NAME OR ADDRESS: SANMAO GROUP CO.,LTD.; JIN CHENG |
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