CN101545216A - Dyeing method for common goldenrod herb natural dye - Google Patents
Dyeing method for common goldenrod herb natural dye Download PDFInfo
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- CN101545216A CN101545216A CN200910050388A CN200910050388A CN101545216A CN 101545216 A CN101545216 A CN 101545216A CN 200910050388 A CN200910050388 A CN 200910050388A CN 200910050388 A CN200910050388 A CN 200910050388A CN 101545216 A CN101545216 A CN 101545216A
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Abstract
The invention relates to a dyeing method for a common goldenrod herb natural dye. The dyeing method comprises the following steps: preparing a 2 to 20 g/I common goldenrod herb dye, and setting a dyeing temperature of 40 to 100 DEG C, a bath ratio of 1:50 to 200 and dyeing time of 10 to 90 minutes; taking a 2 to 20 g/I mordant solution, and setting a mordanting temperature of 40 to 100 DEG C and mordanting time of 10 to 90 minutes; and adding a mordant before or after natural fiber yarn or natural fiber textile is added into common goldenrod herb dye liquor or simultaneously when the natural fiber yarn or the natural fiber textile is added into the common goldenrod herb dye liquor for one-bath dyeing. The method uses the prior textile dyeing device for direct dyeing without adding devices or increasing cost. The textile dyed by the method is soft, primitive and simple and natural color, and has good dye fastness, no fading, no discoloring, good reproducibility, and chromatic aberration around a half level. The method is suitable for the industrialized production, and has no toxicity, no harm and no pollution.
Description
Technical field
The invention belongs to the dyeing field of textiles, particularly relate to the colouring method of common goldenrod herb natural dye.
Background technology
Solidago Canadensis, another name sweet vernal grass, snakehead king, grass all over the mountain or hundred grass originate in the North America, and be otherwise known as " coarse goldenrod " is the composite family herbaceos perennial.According to record, nineteen thirty-five Solidago Canadensis introduce China as ornamental plant, at first as the flower garden flower culture in Shanghai and Nanjing one band, the back ease is given birth to open-air.Begin diffusion the eighties in 20th century and spreading to China Jiangsu and Zhejiang Provinces one band, can appear in the time of in autumn in some florist's shops in area, Jiangsu and Zhejiang Provinces as being similar to the same the joining of babysbreath and spend and sell.Developed into a kind of Alien Weeds of extensive distribution at present in China East China.The Solidago Canadensis plant is sturdy, and Gao Keda is more than 2.50 meters, and the normal in the fall tall and big single sociales group that forms shows very strong competitive advantage, is assert it is a kind of typical Alien invasive species.Habitats such as these species are more common in around abandoned land, roadside, ridge, the dwelling house, orchard and farmland have had a strong impact on the normal growths of endemic plant and crops.
How preventing from the alien species invasion and effectively control it to spread, is the difficult problem that the whole society faces.Artificial removing still is the current major measure of blocking the Solidago Canadensis expansion and spreading, but the effect of failing to obtain.But as a kind of plant, goldenrod is if can obtain timely development and application, and then the plant of this overgrowing also is a kind of precious resources that can regenerate rapidly.Therefore, utilize Solidago Canadensis, it is turned waste into wealth, will become the breach that solves Solidago Canadensis harm.
Goldenrod is a kind of natural fabric plant, medicinal effects such as nontoxic, harmless and tool anti-inflammatory and anticancer, and the fabric that the dyestuff that extracts from goldenrod dyes does not have toxic and side effect to human body skin.The main pigment composition that goldenrod is extracted dye liquor is the flavonoids dyestuff, is main with quercetin (C.I.Natural Yellow 10) and Kaempferol (C.I.Natural Yellow 13,10), can be used for natural fabric yarn and coloration of textile materials.
CN101054475 discloses a kind of preparation method and tint applications from golden rod natural dyestuff.Its colouring method is " fuel factor direct dyeing ", " fabric is entered dye liquor, 1 part in fabric, 20～50 parts of dye liquors; boil then stir, and keep 10～60min, cool the temperature to 15～25 ℃ then; with the woollen rinsing of fabric, dry, obtain yellow Color ".Because this colouring method is simple, only there are intermolecular force or simple physical effect between dye molecule and the plant, therefore adopt DYED FABRICS washability that this patent obtains with very poor, be not suitable for suitability for industrialized production.
Summary of the invention
Technical problem to be solved by this invention provides the colouring method of common goldenrod herb natural dye, and this method utilization has the direct dyeing of textile dyeing equipment now, does not increase equipment, does not increase cost; Textile dyeing fastness through the present invention dyeing is good, does not fade, nondiscolouring, favorable reproducibility, and aberration is about half grade; Can obtain soft, simple and unsophisticated, the natural yellow of color and luster; Be suitable for suitability for industrialized production, nontoxic, harmless, pollution-free.
The colouring method of common goldenrod herb natural dye of the present invention comprises:
The goldenrod extract (is gathered the petal of fresh Solidago Canadensis, pulverizing the back drops in the water, boiling the back filters, with the filtrate concentrate drying of collecting, obtain the dyestuff pulvis, during dyeing pulvis is configured to certain density dye liquor) as dyestuff, adopt the mordant dyeing mode to natural fabric yarn or fabric carry out pre-matchmaker, with matchmaker or back mordant dyeing look;
Detailed process is: compound concentration is the goldenrod dyestuff of 2～20g/l, dyeing temperature is 40～100 ℃; bath raio is 1:50～200; dyeing time is 10～90 minutes; getting concentration is the mordant solution of 2～20g/l; the mordant dyeing temperature is 40～100 ℃, and the mordant dyeing time is 10～90 minutes, and mordant adds or adds with bathing with the goldenrod dye liquor before natural fabric yarn or natural fabric drop into the goldenrod dye liquor, after dropping into the goldenrod dye liquor.
Described natural fabric yarn is cotton, wool yarn line, real silk yarn or linen thread and yarn.
Described natural fabric is COTTON FABRIC, woollens, real silk fabric or sodolin.
Mordant is any one or a few in titanium salt, molysite or the rare-earth salts.
Titanium salt in the described mordant is one or more in titanium sulfate, titanium tetrachloride, the titanyl sulfate.
Described molysite is one or more in frerrous chloride, ferric sulfate, ferrous sulfate ammonia, iron chloride, the ferric sulfate.
Described rare-earth salts is one or more in mixed chlorinated rare earth, lanthanum chloride, cerium chloride, neodymium chloride, vanadic sulfate, lanthanum nitrate, cerous nitrate, neodymium nitrate, the Cericammoniumsulfate.
When factory uses, earlier the dyeing and weaving thing for the treatment of after the refining is immersed rinsing in the warm water, the residue when removing refining dyes then.The dyeing back is cleaned, dehydration, again through mechanical finishing, finishes overall process.
The mordant that dyeing is used all has affinity to coloring material and fiber, anchor at micro-surface thereby can form coordinate bond with mordant the metal ion effect on the fiber of being adsorbed on during natural dye dying, increases dyefastness.Simultaneously, use different mordants can also produce different form and aspect.
Beneficial effect
(1) the existing textile dyeing equipment direct dyeing of the inventive method utilization does not increase equipment, does not increase cost, is applied to the cleaner production of textile industry, can produce in a large number;
(2) the textile dyeing fastness through the present invention dyeing is good, does not fade, nondiscolouring, favorable reproducibility, and aberration is about half grade; Can obtain soft, simple and unsophisticated, the natural yellow of color and luster;
(3) the inventive method does not exist synthetic dyestuffs to the pollution of environment with to the injury of human body; And the plant material aboundresources can also solve present goldenrod to the ecological balance damage problem, changes harmful to treasure.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only to be used to the present invention is described and be not used in and limit the scope of the invention.Should be understood that in addition those skilled in the art can make various changes or modifications the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
Embodiment 1
The titanium sulfate of getting concentration and be 2g/l is as mordant, and bath raio is 1:50, and the mordant dyeing temperature is 40 ℃, and COTTON FABRIC is carried out mordant dyeing, the mordant dyeing time is 60 minutes, takes out fabric, puts in the goldenrod dye liquor of 2g/l and dyes; bath raio is 1:50, and dyeing temperature is 95 ℃, adds water after the tapping and cleans and dry.
Embodiment 2
The frerrous chloride of getting concentration and be 2g/l is as mordant, and bath raio is 1:50, and the mordant dyeing temperature is 40 ℃, and real silk fabric is carried out mordant dyeing, the mordant dyeing time is 60 minutes, takes out fabric, puts in the goldenrod dye liquor of 2g/l and dyes; bath raio is 1:50, and dyeing temperature is 95 ℃, adds water after the tapping and cleans and dry.
Embodiment 3
The goldenrod dye liquor of getting concentration and be 2g/l dyes to COTTON FABRIC; bath raio is 1:50; dyeing temperature is 95 ℃; after the dyeing COTTON FABRIC is taken out, put into and carry out mordant dyeing in the titanium sulfate mordanting bath, mordant concentration is 2g/l; bath raio is 1:50; the mordant dyeing temperature is 40 ℃, and the mordant dyeing time is 90 minutes, adds water then and cleans and dry.
Embodiment 4
The goldenrod dye liquor of getting concentration and be 2g/l dyes to cotton; bath raio is 1:50; dyeing temperature is 95 ℃; after the dyeing cotton is taken out, put into and carry out mordant dyeing in the titanium sulfate mordanting bath, mordant concentration is 2g/l; bath raio is 1:50; the mordant dyeing temperature is 40 ℃, and the mordant dyeing time is 90 minutes, adds water then and cleans and dry.
Claims (8)
1. the colouring method of common goldenrod herb natural dye comprises:
Compound concentration is the goldenrod dyestuff of 2～20g/l, dyeing temperature is 40～100 ℃; bath raio is 1:50～200; dyeing time is 10～90 minutes; getting concentration is the mordant solution of 2～20g/l; the mordant dyeing temperature is 40～100 ℃, and the mordant dyeing time is 10～90 minutes, and mordant drops into the forward and backward or bath interpolation together simultaneously of goldenrod dye liquor at natural fabric yarn or natural fabric.
2. the colouring method of common goldenrod herb natural dye according to claim 1, it is characterized in that: described natural fabric yarn is cotton, wool yarn line, real silk yarn or linen thread and yarn.
3. the colouring method of common goldenrod herb natural dye according to claim 1, it is characterized in that: described natural fabric is COTTON FABRIC, woollens, real silk fabric or sodolin.
4. the colouring method of common goldenrod herb natural dye according to claim 1, it is characterized in that: mordant is any one or a few in titanium salt, molysite or the rare-earth salts.
5. the colouring method of common goldenrod herb natural dye according to claim 4, it is characterized in that: described titanium salt is one or more in titanium sulfate, titanium tetrachloride, the titanyl sulfate.
6. the colouring method of common goldenrod herb natural dye according to claim 4, it is characterized in that: described molysite is one or more in frerrous chloride, ferric sulfate, ferrous sulfate ammonia, iron chloride, the ferric sulfate.
7. the colouring method of common goldenrod herb natural dye according to claim 1, it is characterized in that: described rare-earth salts is one or more in mixed chlorinated rare earth, lanthanum chloride, cerium chloride, neodymium chloride, vanadic sulfate, lanthanum nitrate, cerous nitrate, neodymium nitrate, the Cericammoniumsulfate.
8. the colouring method of common goldenrod herb natural dye according to claim 1 is characterized in that: clean after the dyeing, dewater, mechanical finishing.
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| CN200910050388A CN101545216A (en) | 2009-04-30 | 2009-04-30 | Dyeing method for common goldenrod herb natural dye |
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| CN200910050388A CN101545216A (en) | 2009-04-30 | 2009-04-30 | Dyeing method for common goldenrod herb natural dye |
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101927032A (en) * | 2010-08-04 | 2010-12-29 | 陈启忠 | Dyeing preparation method of surgical sutures produced by tail tendons of nutria |
| CN102220705A (en) * | 2011-04-20 | 2011-10-19 | 盐城纺织职业技术学院 | Method for dying silk fabric by using natural dye of Suaeda salsa |
| CN102433772A (en) * | 2011-09-07 | 2012-05-02 | 浙江理工大学 | Natural dye dyeing method based on non-damaging modification of real silk fabrics |
| CN103174041A (en) * | 2013-04-12 | 2013-06-26 | 祝洪哲 | Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye |
| CN103757942A (en) * | 2014-01-03 | 2014-04-30 | 蒋立宪 | Method for harmless dyeing of school uniform fabric |
| CN104109404A (en) * | 2014-07-08 | 2014-10-22 | 浙江理工大学 | Extracting and dyeing methods of natural cordyceps militaris dye |
| CN104674569A (en) * | 2015-01-23 | 2015-06-03 | 大连工业大学 | Natural dye dyeing method of cellulosic fiber fabric |
| CN106280541A (en) * | 2016-08-10 | 2017-01-04 | 常州云卿生物科技有限公司 | Herba Solidaginis dye liquor and preparation method thereof and purposes |
| CN106436271A (en) * | 2016-09-21 | 2017-02-22 | 东莞市联洲知识产权运营管理有限公司 | Dyed fabric based on aerogel surface modification and preparation method of dyed fabric |
| CN106758332A (en) * | 2016-11-25 | 2017-05-31 | 中原工学院 | The preparation method of goldenrod dyeing cellulosic fabric |
| CN106811991A (en) * | 2017-01-23 | 2017-06-09 | 广西大学 | A kind of colouring method of brocade of Zhang nationality line |
| CN107151923A (en) * | 2017-05-25 | 2017-09-12 | 常州美胜生物材料有限公司 | A kind of cold-pad-batch process for preparing grey black pure linen fabric |
| CN107354771A (en) * | 2017-07-26 | 2017-11-17 | 武汉纺织大学 | A kind of colouring method of the regulation textile dyeing form and aspect based on sophora flower dyestuff |
| CN109371715A (en) * | 2018-11-29 | 2019-02-22 | 刘日昇 | A method of it extracting cordate houttuynia pigment and cotton-spinning fabric is dyed |
| CN109826029A (en) * | 2019-01-20 | 2019-05-31 | 林燕 | A method of it extracting cordate houttuynia pigment and cotton-spinning fabric is dyed |
| CN109866294A (en) * | 2019-03-28 | 2019-06-11 | 南京林业大学 | A kind of preparation method of bamboo weaving house decorative material |
| CN113863026A (en) * | 2021-09-16 | 2021-12-31 | 珠海建轩服装有限公司 | Chinese holly pigment extracting solution and application thereof in fabric dyeing |
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2009
- 2009-04-30 CN CN200910050388A patent/CN101545216A/en active Pending
Cited By (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101927032A (en) * | 2010-08-04 | 2010-12-29 | 陈启忠 | Dyeing preparation method of surgical sutures produced by tail tendons of nutria |
| CN102220705A (en) * | 2011-04-20 | 2011-10-19 | 盐城纺织职业技术学院 | Method for dying silk fabric by using natural dye of Suaeda salsa |
| CN102433772A (en) * | 2011-09-07 | 2012-05-02 | 浙江理工大学 | Natural dye dyeing method based on non-damaging modification of real silk fabrics |
| CN102433772B (en) * | 2011-09-07 | 2014-04-09 | 浙江理工大学 | Natural dye dyeing method based on non-damaging modification of real silk fabrics |
| CN103174041A (en) * | 2013-04-12 | 2013-06-26 | 祝洪哲 | Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye |
| CN103174041B (en) * | 2013-04-12 | 2015-01-21 | 祝洪哲 | Method for low-temperature ultrasonic dyeing and soaping of short fiber by using Chinese herbal medicine plant dye |
| CN103757942A (en) * | 2014-01-03 | 2014-04-30 | 蒋立宪 | Method for harmless dyeing of school uniform fabric |
| CN104109404A (en) * | 2014-07-08 | 2014-10-22 | 浙江理工大学 | Extracting and dyeing methods of natural cordyceps militaris dye |
| CN104109404B (en) * | 2014-07-08 | 2016-09-14 | 浙江理工大学 | The extracting method of a kind of Cordyceps militaris (L.) Link. natural dye and colouring method thereof |
| CN104674569A (en) * | 2015-01-23 | 2015-06-03 | 大连工业大学 | Natural dye dyeing method of cellulosic fiber fabric |
| CN104674569B (en) * | 2015-01-23 | 2016-10-05 | 大连工业大学 | A kind of natural dye dying method of cellulose base fiber fabric |
| CN106280541A (en) * | 2016-08-10 | 2017-01-04 | 常州云卿生物科技有限公司 | Herba Solidaginis dye liquor and preparation method thereof and purposes |
| CN106436271A (en) * | 2016-09-21 | 2017-02-22 | 东莞市联洲知识产权运营管理有限公司 | Dyed fabric based on aerogel surface modification and preparation method of dyed fabric |
| CN106436271B (en) * | 2016-09-21 | 2019-06-21 | 汕头市鼎泰丰实业有限公司 | A kind of dyed fabric and preparation method thereof modified based on aeroge surface |
| CN106758332A (en) * | 2016-11-25 | 2017-05-31 | 中原工学院 | The preparation method of goldenrod dyeing cellulosic fabric |
| CN106811991A (en) * | 2017-01-23 | 2017-06-09 | 广西大学 | A kind of colouring method of brocade of Zhang nationality line |
| CN107151923A (en) * | 2017-05-25 | 2017-09-12 | 常州美胜生物材料有限公司 | A kind of cold-pad-batch process for preparing grey black pure linen fabric |
| CN107151923B (en) * | 2017-05-25 | 2019-07-09 | 常州美胜生物材料有限公司 | A kind of cold-pad-batch process preparing grey black pure linen fabric |
| CN107354771A (en) * | 2017-07-26 | 2017-11-17 | 武汉纺织大学 | A kind of colouring method of the regulation textile dyeing form and aspect based on sophora flower dyestuff |
| CN109371715A (en) * | 2018-11-29 | 2019-02-22 | 刘日昇 | A method of it extracting cordate houttuynia pigment and cotton-spinning fabric is dyed |
| CN109826029A (en) * | 2019-01-20 | 2019-05-31 | 林燕 | A method of it extracting cordate houttuynia pigment and cotton-spinning fabric is dyed |
| CN109866294A (en) * | 2019-03-28 | 2019-06-11 | 南京林业大学 | A kind of preparation method of bamboo weaving house decorative material |
| CN109866294B (en) * | 2019-03-28 | 2021-06-04 | 南京林业大学 | Preparation method of bamboo-woven interior decoration material |
| CN113863026A (en) * | 2021-09-16 | 2021-12-31 | 珠海建轩服装有限公司 | Chinese holly pigment extracting solution and application thereof in fabric dyeing |
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