CN107151923B - A kind of cold-pad-batch process preparing grey black pure linen fabric - Google Patents
A kind of cold-pad-batch process preparing grey black pure linen fabric Download PDFInfo
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- CN107151923B CN107151923B CN201710380029.0A CN201710380029A CN107151923B CN 107151923 B CN107151923 B CN 107151923B CN 201710380029 A CN201710380029 A CN 201710380029A CN 107151923 B CN107151923 B CN 107151923B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
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Abstract
The present invention relates to textile dyeing field more particularly to a kind of cold-pad-batch processes for preparing grey black pure linen fabric.Using Chinese gall natural dye, bath raio 1:20, second dipping and rolling, is banked up at 20 °C, and clear water is washed, for use;The concentration of HAc is 1-4g/L, and the concentration of ferrous sulfate is 3-7g/L, bath raio 1:30, and constant temperature 30min at 40 DEG C washes, soaps, dries, grey black pure linen fabric is made.The present invention uses Chinese gall to extract natural dye for raw material; technique is banked up by cold rolling room temperature, extends the time of contact of pigment and fiber, improves pigment permeance property; mordant dyeing reaches grey black after again, can contaminate large-scale production plant flax black fabric and play directive function.
Description
Technical field
The present invention relates to textile dyeing field more particularly to a kind of cold-pad-batch processes for preparing grey black pure linen fabric.
Background technique
China has thousands of years natural pigments to the history of textile coloration fixation, is born from synthetic dyestuffs in the middle of the 19th century
Since, because its chromatography is complete, chromaticness is bright-coloured, washable sun-proof, it is cheap the advantages that, gradually replaced natural dye.However, with
The reinforcement of people's environmental consciousness and the attention to concept of health, partially synthetic dyestuff human health and ecological environment are produced
Raw seondary effect more and more attracts attention.A large amount of research it has also been shown that, have more than 100 kinds of common dyes to human body have aberration inducing,
The harm such as carcinogenic and cause allergy.Natural dye is examined closely again and is increasingly had been favored by people.Chinese herbal medicine Chinese gall times
The drying insect gall that Aphidiadae insect horned gall aphid or egg times aphid generate on its host Anacardiaceae plant, main active component is tannin,
Its molecular structural formula is as shown in Figure 1.There is unique medicinal and healthcare function to human body, there is-fixed astriction to wound.It is single
Complex compound would rather be formed in conjunction with metal ion, can also remove free radical, there is anti-oxidant and delaying cell aging function.
Phytochrome is refined by raw material of Chinese medicine Chinese gall, it is smaller to sodolin affinity due to a lack of active group,
The dark color of textile, grey black are relatively inaccessible to, and often could improve ramie cotton fabric to pigment by high-temperature process to pigment
Absorption generates grey with mordant dyeing after iron ion, can be only achieved grey black by multiple past counterstain, has not only consumed the energy but also has been interval
Formula production, causes labor intensity to increase.
Summary of the invention
The technical problem to be solved by the present invention is multiple in order to solve grey black pure linen fabric preparation process in the prior art
The problem of large-scale production miscellaneous, relatively difficult to achieve, the present invention provide a kind of cold-pad-batch process for preparing grey black pure linen fabric.
The technical solution adopted by the present invention to solve the technical problems is: a kind of cold rolling preparing grey black pure linen fabric
Heap technique, concrete operation step include:
(1) cold-pad-batch process
Using Chinese gall natural dye, bath raio 1:20, second dipping and rolling, is banked up at 20 °C, and clear water is washed, for use;
(2) mordant dyeing technique afterwards
The concentration of HAc is 1-4g/L, and the concentration of ferrous sulfate is 3-7g/L, bath raio 1:30, constant temperature 30min at 40 DEG C, water
It washes, soap, dry, grey black pure linen fabric is made.Processing step is as shown in Figure 2.
Preferably, the o.w.f of Chinese gall natural dye is 2%, 4%, 6%, 8%, 10% or 12% in step (1).
Preferably, stacking time is 4h, 6h, 8h, 10h, 12h or 14h in step (1).
Preferably, the concentration of HAc is 2g/L in step (2), the concentration of ferrous sulfate is 5g/L.
A kind of high-temperature dyeing process is provided, concrete operation step includes:
(1) dyeing
The o.w.f of Chinese gall natural dye is 2%, 4%, 6%, 8%, 10%, 12%, bath raio 1:20, in 60 DEG C of conditions
Lower dyeing 60min, clear water are washed, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;Clear water is washed, for use;
(3) technique is redyed
It after step (1) of repetitive operation and (2), washes, soap, dry, grey black pure linen fabric is made.Technique step
It is rapid as shown in Figure 3.
Wherein, the material used are as follows: pure 57 inch 20 × 16 128 × 60 of linen drill woven fabric of fabric;The drug used
Are as follows: Chinese gall natural dye (offer of Changzhou Mei Sheng biomaterial Co., Ltd), (HAc, ferrous sulfate are for HAc, ferrous sulfate
AR, Shanghai Ling Feng chemical reagent Co., Ltd provide), natural soaping agent (Jiangsu Hans Chemicals Co., Ltd.'s offer);Make
Equipment are as follows: the quick device for testing color of H-21CF type high temperature, PBU type strength are padded resin machine, and SF600 type Computer color testing is matched colors instrument,
Y571LA6 type crock fastness tester, SW-24A type color fastness to washing tester, YGB611 type solarization climate test instrument.
The invention has the advantages that the present invention uses Chinese gall to extract natural dye for raw material, pass through cold rolling room temperature heap
Technique is set, the time of contact of pigment and fiber is extended, improves pigment permeance property, then mordant dyeing reaches grey black after, it can be right
Large-scale production plant contaminates flax black fabric and plays directive function.Contaminate grey black cold-pad-batch process optimum condition are as follows: room temperature, five
Gall nut natural dye dosage is 10%, and the cold dome time is 12h.The color depth higher temperatures dyer of fabric obtained by cold rolling batch-dying process
Skill is slightly deep, and the uniformity is slightly inferior, but high-temperature dyeing process need to be redyed can just obtain biggish K/S value, and energy consumption greatly improves, work
Skill is more cumbersome, so cold rolling batch-dying process is more suitable for the scale dyeing of Chinese gall natural dye.Cold pad-batch method dyeing is knitted
Every color fastness of object reaches a high temperature every fastness value of fabric obtained by decoration method, and part index number is knitted higher than high-temperature dyeing
Object.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is the molecular structural formula schematic diagram of tannin.
Fig. 2 is cold rolling batch-dying process flow chart.
Fig. 3 is high-temperature dyeing process flow chart.
Fig. 4 be the sodolin of different dyeings K/S value compared with △ E value figure.
Specific embodiment
The present invention is described in more detail below by reference to embodiment, but protection scope of the present invention is not limited
In these embodiments.
Embodiment 1
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 2%, bath raio 1:20, and second dipping and rolling, banks up 10h, clear water at 20 °C
It washes, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Grey black pure linen fabric is prepared using high-temperature dyeing process:
(1) dyeing
The o.w.f of Chinese gall natural dye is 2%, bath raio 1:20, dyes 60min at 60 DEG C, clear water is washed, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;Clear water is washed, for use;
(3) technique is redyed
After step (1) of repetitive operation and (2), washing is soaped, and grey black pure linen fabric is made.
Embodiment 2
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 4%, bath raio 1:20, and second dipping and rolling, banks up 10h, clear water at 20 °C
It washes, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Grey black pure linen fabric is prepared using high-temperature dyeing process:
(1) dyeing
The o.w.f of Chinese gall natural dye is 4%, bath raio 1:20, dyes 60min at 60 DEG C, clear water is washed, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;Clear water is washed, for use;
(3) technique is redyed
After step (1) of repetitive operation and (2), washing is soaped, and grey black pure linen fabric is made.
Embodiment 3
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 6%, bath raio 1:20, and second dipping and rolling, banks up 10h, clear water at 20 °C
It washes, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Grey black pure linen fabric is prepared using high-temperature dyeing process:
(1) dyeing
The o.w.f of Chinese gall natural dye is 6%, bath raio 1:20, dyes 60min at 60 DEG C, clear water is washed, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;Clear water is washed, for use;
(3) technique is redyed
After step (1) of repetitive operation and (2), washing is soaped, and grey black pure linen fabric is made.
Embodiment 4
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 8%, bath raio 1:20, and second dipping and rolling, banks up 10h, clear water at 20 °C
It washes, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Grey black pure linen fabric is prepared using high-temperature dyeing process:
(1) dyeing
The o.w.f of Chinese gall natural dye is 8%, bath raio 1:20, dyes 60min at 60 DEG C, clear water is washed, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;Clear water is washed, for use;
(3) technique is redyed
After step (1) of repetitive operation and (2), washing is soaped, and grey black pure linen fabric is made.
Embodiment 5
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 10%, bath raio 1:20, and second dipping and rolling, banks up 10h, clearly at 20 °C
Washing, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Grey black pure linen fabric is prepared using high-temperature dyeing process:
(1) dyeing
The o.w.f of Chinese gall natural dye is 10%, bath raio 1:20, dyes 60min at 60 DEG C, clear water is washed, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;Clear water is washed, for use;
(3) technique is redyed
After step (1) of repetitive operation and (2), washing is soaped, and grey black pure linen fabric is made.
Embodiment 6
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 12%, bath raio 1:20, and second dipping and rolling, banks up 10h, clearly at 20 °C
Washing, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Grey black pure linen fabric is prepared using high-temperature dyeing process:
(1) dyeing
The o.w.f of Chinese gall natural dye is 12%, bath raio 1:20, dyes 60min at 60 DEG C, clear water is washed, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;Clear water is washed, for use;
(3) technique is redyed
After step (1) of repetitive operation and (2), washing is soaped, and grey black pure linen fabric is made.
Embodiment 7
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 10%, bath raio 1:20, and second dipping and rolling, banks up 4h, clear water at 20 °C
It washes, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Embodiment 8
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 10%, bath raio 1:20, and second dipping and rolling, banks up 6h, clear water at 20 °C
It washes, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Embodiment 9
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 10%, bath raio 1:20, and second dipping and rolling, banks up 8h, clear water at 20 °C
It washes, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Embodiment 10
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 10%, bath raio 1:20, and second dipping and rolling, banks up 12h, clearly at 20 °C
Washing, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Embodiment 11
Grey black pure linen fabric is prepared using the cold technique that flocks together:
(1) cold-pad-batch process
The o.w.f of Chinese gall natural dye is 10%, bath raio 1:20, and second dipping and rolling, banks up 14h, clearly at 20 °C
Washing, for use;
(2) mordant dyeing technique afterwards
HAc 2g/L, ferrous sulfate 5g/L, bath raio 1:30, constant temperature 30min at 40 DEG C;It washes, soap, dry, ash is made
Black pure linen fabric.
Performance test
Influence of the 1 Chinese gall natural dye cold dome concentration to dyeing effect
Mordant dyeing condition HAc 2g/L after fixation, ferrous sulfate 5g/L bank up 10h at 40 DEG C in the case of constant temperature 30min,
Chinese gall natural dye cold pad--batch concentration is tested by 2%, 4%, 6%, 8%, 10%, 12% (o.w.f), bath raio 1:20, strictly according to the facts
It applies shown in a 1-6.As shown in Table 1, with the increase of Chinese gall pigment concentration, dye level is gradually increased, when concentration reaches
After 10%, there is no be significantly increased for dye level.
Influence of the 1 Chinese gall natural dye cold dome concentration of table to K/S value and △ E
Influence of the 2 Chinese gall natural dye cold dome times to dyeing effect
It is 10% (o.w.f.) in fixed dye dosage, it is rear mordant dyeing condition HAc 2g/L, ferrous sulfate 5g/L, permanent at 40 DEG C
In the case of warm 30min, the plant gall pigment cold pad--batch time is 4h, 6h, 8h, 10h, 12h, 14h test, such as 5 He of embodiment
Shown in embodiment 7-11.As shown in Table 2, with the increase of cold pad--batch time, dye level is gradually increased, but stacking time reaches
After 12h, there is no be significantly increased for dye level.
Influence of the 2 Chinese gall natural dye cold dome time of table to K/S value and △ E
Compared with 3 high-temperature dyeing process dye color depth with cold rolling batch-dying process
Chinese gall natural dye dosage is 2%, 4%, 6%, 8%, 10%, 12% (o.w.f), bath raio 1:20, high temperature dye
The preparation of fabric obtained by color technique and cold rolling batch-dying process is as shown in embodiment 1-6.Compare high-temperature dyeing process and cold pad--batch
The K/S value and △ E value of K/S value obtained by dyeing and △ E value, as shown in figure 4, as shown in Figure 4, obtained by cold rolling batch-dying process
The color depth higher temperatures dyeing of fabric is slightly deep, and the uniformity is slightly inferior, but high-temperature dyeing process need to redye can just obtain it is biggish
K/S value, energy consumption greatly improve, and technique is more cumbersome, so cold rolling batch-dying process is more suitable for the rule of Chinese gall natural dye
Modelling dyeing.
The color fastness of 4 cold rail heap dyeing grey black finished products and high-temperature dyeing grey black finished product is tested
Color fastness testing standard are as follows: " textile color stability tests antifriction to colour fastness to rubbing referring to GB/T3920-2008
Wipe color fastness " measurement;Fastness to soaping is surveyed referring to GB/T3921-2008 " textile color stability test fastness to soaping "
It is fixed;Color fastness to light is measured referring to GB/T8426-1998 " textile color stability test color fastness to light ";Colour fastness to perspiration
It is measured referring to AATCC15-2009 " colour fastness to perspiration ".
As shown in Table 3, every color fastness of cold pad-batch method dyed fabric reaches a high temperature the items of fabric obtained by decoration method
Fastness value, and part index number is higher than high-temperature dyeing fabric.
The color fastness value of the dyeing sodolin of table 3
Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.
Claims (4)
1. a kind of cold-pad-batch process for preparing grey black pure linen fabric, which is characterized in that the concrete operation step of the technique
Include:
(1) Chinese gall natural dye is used, bath raio 1:20, second dipping and rolling, is banked up at 20 °C, and clear water is washed, for use;
(2) concentration of HAc is 1-4g/L, and the concentration of ferrous sulfate is 3-7g/L, bath raio 1:30, constant temperature 30min at 40 DEG C, water
It washes, soap, dry, grey black pure linen fabric is made.
2. preparing the cold-pad-batch process of grey black pure linen fabric as described in claim 1, which is characterized in that in step (1)
The o.w.f of Chinese gall natural dye is 2%, 4%, 6%, 8%, 10% or 12%.
3. preparing the cold-pad-batch process of grey black pure linen fabric as described in claim 1, which is characterized in that in step (1)
Stacking time is 4h, 6h, 8h, 10h, 12h or 14h.
4. preparing the cold-pad-batch process of grey black pure linen fabric as described in claim 1, which is characterized in that in step (2)
The concentration of HAc is 2g/L, and the concentration of ferrous sulfate is 5g/L.
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Citations (4)
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CN101545216A (en) * | 2009-04-30 | 2009-09-30 | 东华大学 | Dyeing method for common goldenrod herb natural dye |
KR101380374B1 (en) * | 2013-11-01 | 2014-04-10 | 주식회사 우성염직 | Method for natural-dyeing using cold pad batch |
CN103938398A (en) * | 2014-04-25 | 2014-07-23 | 何炽斌 | Mechanized pure natural fabric basking and dyeing technique |
CN105780532A (en) * | 2014-12-22 | 2016-07-20 | 董绍光 | Process for dyeing cloth with Chinese gall |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101545216A (en) * | 2009-04-30 | 2009-09-30 | 东华大学 | Dyeing method for common goldenrod herb natural dye |
KR101380374B1 (en) * | 2013-11-01 | 2014-04-10 | 주식회사 우성염직 | Method for natural-dyeing using cold pad batch |
CN103938398A (en) * | 2014-04-25 | 2014-07-23 | 何炽斌 | Mechanized pure natural fabric basking and dyeing technique |
CN105780532A (en) * | 2014-12-22 | 2016-07-20 | 董绍光 | Process for dyeing cloth with Chinese gall |
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