CN101747658B - Preparation process of Flaveria bidentis (L.) Kuntze series dyes and usage thereof - Google Patents
Preparation process of Flaveria bidentis (L.) Kuntze series dyes and usage thereof Download PDFInfo
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- CN101747658B CN101747658B CN 200910250534 CN200910250534A CN101747658B CN 101747658 B CN101747658 B CN 101747658B CN 200910250534 CN200910250534 CN 200910250534 CN 200910250534 A CN200910250534 A CN 200910250534A CN 101747658 B CN101747658 B CN 101747658B
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Abstract
The invention relates to a Flaveria bidentis (L.) Kuntze as raw material for preparing Flaveria bidentis (L.) Kuntze, Flaveria bidentis (L.) Kuntze and indigo plant, and Flaveria bidentis (L.) Kuntze and madder as dyes, a dye process and a dyeing usage on cotton, silk, linen, wool and various fibers (including chemical fiber, cotton fiber, protein fiber and plant fiber).
Description
Technical field
The present invention relates to adopt with Huang Dingju [Flaveria bidentis (L.) Kuntze] is raw material, for the preparation of plant pigments dye technology and purposes.Specifically relate to yellow top chrysanthemum dyestuff preparation technology and purposes.
Background technology
Along with the reinforcement of people's environmental consciousness and to the pay attention to day by day of human health, the partial synthesis dyestuff more and more receives publicity to the side effect that human health and ecotope produce.Studies show that in recent years has more than 100 kind of common dyes might produce carcinogenic substance.Developed countries such as Germany had promulgated the rules of forbidding these dyestuffs in 1994.Moreover, along with earth consumption of petroleum resources, the raw material problem of synthetic dyestuff comes out, so the scientific research personnel begins to be devoted to exploitation " natural environmental-protective dyestuff " and " environment-protecting clean dyeing and finishing technology ".
Have a long history in China with natural dyestuff and pigment dyeing, the period of Ming and Qing, the preparation of China's natural dyestuff and staining technique have all reached very high level, and dyestuff also exports except personal in a large number.
Adventive invasion just constantly aggravate in China, and Huang Dingju is exactly one of them, it in calendar year 2001 first in China Tianjin, the Hebei discovery.Extremely strong adaptive faculty, the competitive capacity of yellow top chrysanthemum, seriously tie up the living space of other plant, and strive water with other plant, strive fertilizer, strive sunlight, have a strong impact on the growth of other plant, particularly the greenery patches ecosystem there is great destructiveness, makes many omnicide.In a single day Huang Dingju invades the farmland, will threaten husbandry production and ecological environment security, therefore is called again " ecological killer ".How to prevent and treat and utilize and compel as pressing as a fire singeing one's eyebrows, become the common problem of paying close attention in the whole world.
The invention provides Huang Dingju as preparation technology and the purposes of dyestuff.
Summary of the invention
The object of the present invention is to provide Huang Dingju is raw material, for the preparation of plant pigments dye technology and purposes.
Another object of the present invention is to provide Huang Dingju to be used for the purposes of cotton, silk, hair, fiber crops, vegetable fibre, cotton fibre, thiozell, man-made fiber dyeing fabric as dyestuff.
Characteristic of the present invention
Pushing up chrysanthemum with the exotic invasive weed Huang is raw material, and preparation is gone into Huang Dingju and is used as dyeing of dyestuff and uses thereof; The residue burning is used for the thermal source of dyeing course; Ashes are used for dyeing auxiliaries.Really accomplish environmental protection.
The objective of the invention is to realize by the following technical solutions:
What the present invention carried is raw material for the yellow top of exotic invasive weed chrysanthemum, the preparation dye technology.
Description of drawings
Fig. 1 is yellow top chrysanthemum Flaveria bidentis (L.) Kuntze series dyes preparation technology schema
Embodiment
Embodiment 1, Huang Dingju [Flaveria bidentis (L.) Kuntze] dyestuff preparation technology (seeing accompanying drawing in addition)
1) dyestuff preparation technology
Be raw material with Huang Dingju (do or fresh) herb, after cleaning, pulverizing, two kinds of methods of used water cold soaking (or heat is carried) are extracted, and the ratio of water and raw material should be (10: 1～30: 1).Concrete extraction process: first kind of extracting method be under the room temperature with the raw material flooding of pulverizing, the time is 12～24 hours, filtration, filter residue is lixiviate at room temperature again, and the time is 6～12 hours, the elimination residue, merge filtrate twice, it is standby as dyestuff that filtrate concentrates the back; Second method is with raw material water heating and refluxing extraction half an hour to 1 hour, filters then, and filter residue is water reflux half an hour again.Residue filters, and twice filtrate merges, and is standby as dyestuff.After residue dries, can be used as thermal source, the ashes after the burning are used for colour additive, increase the colour fastness of pigment on fabric.
2) dyeing
Pollutant after colour additive is handled [cotton, silk, fiber crops, hair, comprise each fibrid such as chemistry, cotton, albumen, plant] is immersed in [dye liquor and pollutant ratio 20～50: 1 (v/w)] in the dye vat that contains dye solution, dye liquor temperature is 20～95 ℃, and dyeing time is 1～5 hour.
Add mordant during this time and carry out fixation and color development (time is 0.5～1 hour), the order that mordant adds be colored specifically that textile properties and color and luster determine to add earlier, the centre adds in dyeing course or after add.Mordant commonly used has (mordant: dye solution=1～3 gram: 1 liter) or with ashes replace (consumption is as the criterion with pH7～11) such as aluminium salt, calcium salt, sylvite, mantoquita, molysite.
3) aftertreatment
The pollutant that taking-up is colored [behind cotton, silk, fiber crops, hair, each fibrid (comprising chemistry, cotton, albumen, plant), further soap, wash, drying.
4) other auxiliary material preparations
Be starting material with indigo plant (Polygonum tinctorium) and madder (Rubia cordifolia) respectively, preparation technology is with 1), 2) and 3).
Claims (3)
1. the dyeing method of a dyestuff, described dyestuff contains the single extract of yellow top chrysanthemum does yellow dyes, or Huang Dingju does different green colouring materials with indigo plant with different ratios mixing in 10: 1～1: 10, or Huang Dingju and madder mix with 10: 1～1: 10 different ratios and do different orange, redness and purple dye, it is characterized by: do or fresh plant is raw material with Huang Dingju, after cleaning, pulverizing, water cold soaking or heat are put forward two kinds of methods and are extracted, and the ratio of water and raw material should be 10: 1～and 5: 1; Concrete extraction process: first kind of extracting method be under the room temperature with the raw material flooding of pulverizing, the time is 12～24 hours, filtration, filter residue is lixiviate at room temperature again, and the time is 6～12 hours, the elimination residue, merge filtrate twice, it is standby as dyestuff that filtrate concentrates the back; Second method is with raw material water heating and refluxing extraction half an hour to 1 hour, filters then, and filter residue is water reflux half an hour again, and residue filters, and twice filtrate merges the back and concentrates, and is standby as dyestuff; After residue dried, as thermal source, the ashes after the burning were used for colour additive, and consumption is as the criterion with pH11, increases the colour fastness of pigment on fabric; Dyestuff is selected single or mixed plant dyestuff according to required color, with different proportionings, different concns, adds mordant, with 10～60 minutes, cotton, fiber crops, silk and chemical ﹠ blended fabric is dyeed.
2. dyeing method according to claim 1, it is characterized by: the pollutant after colour additive is handled, be immersed in the dye vat that contains dye solution, dye solution and pollutant ratio 20～50: 1 (v/w), the dye solution temperature is 20～95 ℃, dyeing time is 1 hour, add mordant during this time and carry out fixation and color development, time is 0.5～1 hour, the order that mordant adds determines to add earlier in dyeing course by specifically being colored textile properties and color and luster, the centre add or after add, mordant commonly used has aluminium salt, calcium salt, sylvite, mantoquita, molysite, mordant: dye solution=1～3 gram: 1 liter.
3. dyeing method according to claim 1 is characterized by: after taking out the pollutant that is colored, further soap, wash, drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200910250534 CN101747658B (en) | 2009-12-15 | 2009-12-15 | Preparation process of Flaveria bidentis (L.) Kuntze series dyes and usage thereof |
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| CN 200910250534 CN101747658B (en) | 2009-12-15 | 2009-12-15 | Preparation process of Flaveria bidentis (L.) Kuntze series dyes and usage thereof |
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| CN101747658A CN101747658A (en) | 2010-06-23 |
| CN101747658B true CN101747658B (en) | 2013-08-21 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105401464B (en) * | 2015-12-22 | 2018-04-13 | 广州番禺职业技术学院 | A kind of technique using unusual fruit juice printing and dyeing artificial leather |
| CN106118128A (en) * | 2016-06-28 | 2016-11-16 | 河北科技大学 | Plant dye and the weaving material of this plant dye dyeing is prepared with Hebei Folium et Caulis Indigoferae Tinctoriae |
| CN106245366A (en) * | 2016-08-25 | 2016-12-21 | 常熟市华谊织造有限公司 | The colouring method of silk fabric |
| CN106758349A (en) * | 2016-12-01 | 2017-05-31 | 西南大学 | Colouring method of the sulfuretin to bafta |
| CN108252119B (en) * | 2018-01-11 | 2020-03-27 | 珠海建轩服装有限公司 | Polygonum multiflorum dye solution, preparation method and application thereof, and fabric dyeing method |
| CN108797151A (en) * | 2018-04-19 | 2018-11-13 | 北京林业大学 | A method of using timber hydro-thermal process waste liquid to fabric or/and dyeing textile fibers |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5221289A (en) * | 1991-06-26 | 1993-06-22 | Hiroki Miyamatsu | Dyed textile products and a method of producing them |
| CN1810888A (en) * | 2006-02-21 | 2006-08-02 | 海澜集团公司 | Yellow chrysanthemum dye extracting process and its usage in dyeing mercerized wool and mercerized wool fabric |
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2009
- 2009-12-15 CN CN 200910250534 patent/CN101747658B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5221289A (en) * | 1991-06-26 | 1993-06-22 | Hiroki Miyamatsu | Dyed textile products and a method of producing them |
| CN1810888A (en) * | 2006-02-21 | 2006-08-02 | 海澜集团公司 | Yellow chrysanthemum dye extracting process and its usage in dyeing mercerized wool and mercerized wool fabric |
Non-Patent Citations (1)
| Title |
|---|
| 任艳萍等.外来植物黄顶菊（Flaveria bidentis）的研究进展.《热带亚热带植物学报》.2008,第16卷(第4期),第394页. * |
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| CN101747658A (en) | 2010-06-23 |
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