CN101348615B - Preparation and use method of mimosa vegetable dye - Google Patents
Preparation and use method of mimosa vegetable dye Download PDFInfo
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- CN101348615B CN101348615B CN2008100424766A CN200810042476A CN101348615B CN 101348615 B CN101348615 B CN 101348615B CN 2008100424766 A CN2008100424766 A CN 2008100424766A CN 200810042476 A CN200810042476 A CN 200810042476A CN 101348615 B CN101348615 B CN 101348615B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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Abstract
The invention discloses a method for preparing and applying sensitive plant dye in the dye technical field. The method comprises the following preparation steps that: sensitive plants are collected, cleaned, aired, ground, added to an ethanol solution, digested and extracted at room temperature and filtered so as to obtain a dye solution; an extracted stock solution of the dye solution is decompressed, concentrated and made into a paste-shaped concentrated solution; and the dye concentrated solution is cured, concentrated and made into natural powder-shaped dye powder. Under the alum mordant dyeing condition, an obtained fabric is yellow; under the copper salt mordant dyeing condition, obtained real silk fabrics are deep yellow, while cotton or woolen fabrics are green; and under the metallic ferrous salt mordant dyeing condition, the obtained fabrics are olive. The method utilizes the natural nontoxic sensitive plants to dye real silk, cotton or woolen fabrics, provides a technical basis for reducing the use of synthetic dye and developing natural dye, can be applied to the clean production of the textile industry, and can be used for mass production.
Description
Technical field
What the present invention relates to is a kind of preparation and application method of technical field of dye, specifically, is a kind of preparation and application method of Touch-me-notAction Plant vegetable dye.
Background technology
Touch-me-notAction Plant is the herb of pulse family (Leguminosae) Mimosa plant Touch-me-notAction Plant (Mimosa pudica).Touch-me-notAction Plant originates in the torrid areas, South America, and the happiness warm and moist is not tight to the soil requirement, happiness light, but ability half is cloudy, admires so can do indoor potted flower.The Touch-me-notAction Plant leaflet is tiny, and pinniform is arranged, and touches leaflet with hand, after leaflet is accepted to stimulate, promptly can close up, big as shaking force, can make to stimulate to reach full leaf, then common petiole also can be sagging, even also can be delivered to adjacent blades and make its petiole sagging, so the coy and powder face that hangs low of Miss seemingly is the name Touch-me-notAction Plant.
Touch-me-notAction Plant also is a kind of medicine, has the effect of clearing away heat and promoting diuresis, preventing phlegm from forming and stopping coughing, ataralgesia, cooling blood for hemostasis, the clinical diseases such as acute hepatitis, neurasthenia, insomnia, hemoptysis of pulmonary tuberculosis, blood urine, zoster that are used for more.External existing report separates compositions such as obtaining free flavones, flavonoid glycoside, phenolic acids from Touch-me-notAction Plant.
Through to existing technical literature retrieval find Chinese patent open (bulletin) number: CN1823879, patent name " Touch-me-notAction Plant has the new purposes of the medicine for the treatment of spinal nerve diseases ".This invention relates to the medicine that material contained in Touch-me-notAction Plant extract, the Touch-me-notAction Plant is used to prepare prevention and treatment spinal nerve diseases, its preparation method: choose Sensitiveplat Root dry weight 3-30g, make soup about 250g with the 500g decocting.Because the extraction process condition is to carry out in the aqueous solution, so extraction efficiency is low, in addition, this invents only suitable medicine production, can not satisfy the production of dye preparations.In addition, about the application method of Touch-me-notAction Plant vegetable dye, not seeing both at home and abroad at present has report.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of preparation and application method of Touch-me-notAction Plant vegetable dye is provided.The present invention utilizes the Touch-me-notAction Plant of Nantural non-toxic to do dyestuff, has reduced the pollution of chemical synthetic dye, and its aboundresources, be easy to artificial growth, colour fastness is better.
The present invention is achieved by the following technical solutions:
The preparation method of Touch-me-notAction Plant vegetable dye involved in the present invention may further comprise the steps:
The first step. collect the Touch-me-notAction Plant plant and clean, dry, pulverize the back and add ethanolic soln, wherein the weight ratio of Touch-me-notAction Plant plant material and ethanolic soln is 1:10-1:20, this solidliquid mixture placed under 10 ℃ of-35 ℃ of conditions of room temp mix, natural dye liquor is extracted in lixiviate under the room temperature, filter then dye solution;
Described ethanolic soln, its volumetric concentration are 25%-95%.
Described pulverizing is meant: with medicinal herb grinder the Touch-me-notAction Plant plant is ground into 10-100 purpose textile powder.
Described lixiviate is extracted, and its time is 12-24 hour.
Second step. the dye solution stoste extracted under the condition of vacuumizing, and is placed 40 ℃ of-50 ℃ of following water-baths with extracting solution, extracting solution is concentrated, make the paste concentrated solution;
The described condition that vacuumizes is meant to vacuumize under-0.1 normal atmosphere that reduces pressure.
The 3rd step. dye concentrated solution through solidifying, concentrating, is made natural powder powder dyestuff pulvis, i.e. the Touch-me-notAction Plant vegetable dye.
The method of application Touch-me-notAction Plant vegetable dye involved in the present invention is meant with above-mentioned Touch-me-notAction Plant vegetable dye fabric is carried out substantive dyeing or the pre-painted method of matchmaker.
Described application Touch-me-notAction Plant vegetable dye carries out substantive dyeing to fabric method, be specially: with 30%-50% (with the ratio of fabric quality, W/W) Touch-me-notAction Plant vegetable dye dyes on being added to and carrying out on the fabric; bath raio is (part by weight of fabric and dye liquor) 1:10; slowly heating, and temperature heated 30-60 minute down at 80 ℃, and the room temperature cooling is 1 hour then; take out the fabric that dyed, washing is dried.
Described application Touch-me-notAction Plant vegetable dye carries out the painted method of pre-matchmaker to fabric, is specially:
1. fabrics such as real silk, cotton, wool are immersed in the water, allow its abundant moistening back take out, water is extracted, stand-by.
2. after the above-mentioned processing, fabric is carried out pre-mordant dyeing with mordant handle, wherein, mordant is that (with the ratio of fabric quality, W/W), bath raio (part by weight of fabric and dye liquor) is 1:10 to 10%-30%, boiled 30-120 minute, and at room temperature cooled off 1 hour then.
Described mordant is meant a kind of in alum, copper sulfate or the ferrous sulfate.
3. with 30%-50% (with the ratio of fabric quality, W/W) Touch-me-notAction Plant vegetable dye powder dyes on being added to and carrying out on the fabric; bath raio is 1:10 (part by weight of fabric and dye liquor); slowly heating; temperature heated 30-60 minute down at 80 ℃; the room temperature cooling is 1 hour then, takes out the fabric that dyed, and washing is dried.
Under the condition of different mordant dyeing agent, under alum mordant dyeing condition, the gained fabric is yellow; Under mantoquita mordant dyeing condition, gained fabric real silk is for being deep yellow, and cotton, wool is green; Under metal ferrous salt mordant dyeing condition, the gained fabric is olive colour.
The present invention extracts dyestuff from Touch-me-notAction Plant, real silk, cotton, wool fabric dyeed, and plant material Touch-me-notAction Plant aboundresources, nontoxic, easy artificial growth; Dyefastness is good simultaneously, the dye uptake height, and even dyeing, color and luster is soft, nature, using the environmental protection mordant to handle can increase chromatogram; The dyeing of Touch-me-notAction Plant vegetable dye is simple, steady quality, and cost is lower, and does not have pollution and " three cause " effect to environment, is easy to degraded.
Embodiment
Below embodiments of the invention are elaborated: following examples are to be the enforcement of carrying out under the prerequisite with the technical solution of the present invention, provided embodiment and operating process, but protection scope of the present invention are not limited to following embodiment.
Embodiment 1
Collect and cross 10 mesh sieves after the Touch-me-notAction Plant plant is cleaned, dries, pulverizes, take by weighing the ethanolic soln of 1kg vegetable material adding 25%, wherein the weight ratio of Touch-me-notAction Plant plant material and solvent is 1:10, solidliquid mixture placed under 10 ℃ of conditions of room temp mix, lixiviate was extracted natural dye liquor 12 hours under the room temperature, filter then dye solution, with the 40 ℃ of following concentrating under reduced pressure of dye solution stoste that extract, make the paste concentrated solution, with dye concentrated solution through solidifying, concentrating, make natural powder powder dyestuff pulvis, i.e. the Touch-me-notAction Plant vegetable dye.
Embodiment 2
Collect and cross 50 mesh sieves after the Touch-me-notAction Plant plant is cleaned, dries, pulverizes, take by weighing the ethanolic soln of 1kg vegetable material adding 50%, wherein the weight ratio of Touch-me-notAction Plant plant material and solvent is 1:15, solidliquid mixture placed under 20 ℃ of conditions of room temp mix, lixiviate was extracted natural dye liquor 18 hours under the room temperature, filter then dye solution, with the 45 ℃ of following concentrating under reduced pressure of dye solution stoste that extract, make the paste concentrated solution, with dye concentrated solution through solidifying, concentrating, make natural powder powder dyestuff pulvis, i.e. the Touch-me-notAction Plant vegetable dye.
Embodiment 3
Collect and cross 100 mesh sieves after the Touch-me-notAction Plant plant is cleaned, dries, pulverizes, take by weighing the ethanolic soln of 1kg vegetable material adding 95%, wherein the weight ratio of Touch-me-notAction Plant plant material and solvent is 1:20, solidliquid mixture placed under 35 ℃ of conditions of room temp mix, lixiviate was extracted natural dye liquor 24 hours under the room temperature, filter then dye solution, with the 50 ℃ of following concentrating under reduced pressure of dye solution stoste that extract, make the paste concentrated solution, with dye concentrated solution through solidifying, concentrating, make natural powder powder dyestuff pulvis, i.e. the Touch-me-notAction Plant vegetable dye.
Embodiment 4
Get real silk, cotton, wool and add the clear water rinsing, bleed off scavenging solution, extract.With 40% (with the ratio of fabric quality, Touch-me-notAction Plant vegetable dye W/W) dyes on being added to and carrying out on the fabric, and bath raio is 1:10, and temperature is 80 ℃ of heating 30 minutes down, and the room temperature cooling is 1 hour then, dye complete, washing, fabric be a yellow.
Present embodiment uses the Touch-me-notAction Plant vegetable dye directly real silk, cotton, wool to be dyeed, and the gained fabric is yellow, and Color is general, and uniformity coefficient is poor slightly.But do not exist to the pollution of environment with to the harm of human body, aboundresources, be easy to artificial growth.
Embodiment 5
Get real silk, cotton, wool and add the clear water rinsing, bleed off scavenging solution, extract.Add water by the 1:10 bath raio, (with the ratio of fabric quality, alum W/W), boiled 30 minutes, room temperature is taken out fabric after cooling off at least one hour then, cleans to put into 10% after the heating.Then with 30% (with the ratio of fabric quality, Touch-me-notAction Plant vegetable dye W/W) dyes on being added to and carrying out on the fabric, and bath raio is 1:10, and temperature is 80 ℃ of heating 30 minutes down, and the room temperature cooling is one hour then, dye complete, washing, fabric be a yellow.
Present embodiment uses the Touch-me-notAction Plant vegetable dye under the condition of alum as mordant, and real silk, cotton, wool are carried out mordant dyeing.The gained fabric is yellow, even dyeing, and color and luster is soft, and colour fastness is better, and does not exist to the pollution of environment with to the harm of human body, aboundresources, is easy to artificial growth.
Embodiment 6
Get real silk, cotton, wool and add the clear water rinsing, bleed off scavenging solution, extract.Add water by the 1:10 bath raio, (with the ratio of fabric quality, copper sulfate W/W), boiled 60 minutes, room temperature is taken out wool after cooling off at least one hour then, cleans to put into 20% after the heating.Then (with the ratio of fabric quality, Touch-me-notAction Plant vegetable dye W/W) dyes on being added to and carrying out on the fabric, and bath raio is 1:10, and temperature is 80 ℃ of heating 45 minutes down with 40%, room temperature cooling is one hour then, dye complete, washing, get the fabric real silk for being deep yellow, cotton, wool is green.
Present embodiment uses the Touch-me-notAction Plant vegetable dye under the condition of mantoquita as mordant, and real silk, cotton, wool are carried out mordant dyeing.In the gained fabric, real silk is for for deep yellow, and cotton, wool be a green, even dyeing, and color and luster is soft, and colour fastness is better, and does not exist to the pollution of environment with to the harm of human body, aboundresources, is easy to artificial growth.
Embodiment 7
Get real silk, cotton, wool and add the clear water rinsing, bleed off scavenging solution, extract.Add water by the 1:10 bath raio, (with the ratio of fabric quality, ferrous sulfate W/W), boiled 120 minutes, room temperature is taken out wool after cooling off at least one hour then, cleans to put into 30% after the heating.Then with 50% (with the ratio of fabric quality, Touch-me-notAction Plant vegetable dye W/W) dyes on being added to and carrying out on the fabric, and bath raio is 1:10, and temperature is 80 ℃ of heating 60 minutes down, and the room temperature cooling is one hour then, dye complete, washing, fabric is olive colour.
Present embodiment uses the Touch-me-notAction Plant vegetable dye under the condition of metal ferrous salt as mordant, and real silk, cotton, wool are carried out mordant dyeing.The gained fabric is olive colour, even dyeing, and color and luster is soft, and colour fastness is better, and does not exist to the pollution of environment with to the harm of human body, aboundresources, is easy to artificial growth.
Claims (9)
1. the preparation method of a Touch-me-notAction Plant vegetable dye is characterized in that, may further comprise the steps:
The first step. collect the Touch-me-notAction Plant plant and clean, dry, pulverize the back and add ethanolic soln, wherein the weight ratio of Touch-me-notAction Plant plant material and ethanolic soln is 1: 10-1: 20, this solidliquid mixture placed under 10 ℃ of-35 ℃ of conditions of room temp mix, natural dye liquor is extracted in lixiviate under the room temperature, filter then dye solution;
Second step. the dye solution stoste extracted under the condition of vacuumizing, and is placed 40 ℃ of-50 ℃ of following water-baths with extracting solution, extracting solution is concentrated, make the paste concentrated solution;
The 3rd step. dye concentrated solution through solidifying, concentrating, is made natural powder powder dyestuff pulvis, i.e. the Touch-me-notAction Plant vegetable dye.
2. the preparation method of Touch-me-notAction Plant vegetable dye according to claim 1 is characterized in that, described ethanolic soln, and its volumetric concentration is 25%-95%.
3. the preparation method of Touch-me-notAction Plant vegetable dye according to claim 1 is characterized in that, described pulverizing is meant: with medicinal herb grinder the Touch-me-notAction Plant plant is ground into 10-100 purpose textile powder.
4. the preparation method of Touch-me-notAction Plant vegetable dye according to claim 1 is characterized in that, described lixiviate is extracted, and its time is 12-24 hour.
5. the preparation method of Touch-me-notAction Plant vegetable dye according to claim 1 is characterized in that, the described condition that vacuumizes is meant to vacuumize under-0.1 normal atmosphere that reduces pressure.
6. an application rights requires the method for the Touch-me-notAction Plant vegetable dye of 1 preparation to the fabric substantive dyeing, it is characterized in that, the Touch-me-notAction Plant vegetable dye of the 30%-50% of fabric quality is added to dyes on carrying out on the fabric; bath raio is 1: 10; slowly heating, in 80 ℃ of heating 30-60 minute down, room temperature cooling then; take out the fabric that dyed, washing is dried.
7. application Touch-me-notAction Plant vegetable dye according to claim 6 is characterized in that to the method for fabric substantive dyeing the gained fabric is yellow.
8. an application rights requires the 1 Touch-me-notAction Plant vegetable dye for preparing to the painted method of the pre-matchmaker of fabric, it is characterized in that, comprises the steps:
1. fabric is immersed in the water, allow its abundant moistening back take out, water is extracted, stand-by;
2. after the above-mentioned processing, fabric is carried out pre-mordant dyeing with mordant handle, wherein, mordant is the 10%-30% of fabric quality, and bath raio is 1: 10, boils 30-120 minute, at room temperature cools off 1 hour then;
3. the Touch-me-notAction Plant vegetable dye powder of the 30%-50% of fabric quality is added to and dyes on carrying out on the fabric, bath raio is 1: 10, slowly heating, and temperature is 80 ℃ of heating 30-60 minute down, and the room temperature cooling is 1 hour then, takes out the fabric that dyed, and washing is dried;
Described mordant is meant a kind of in alum, copper sulfate or the ferrous sulfate.
9. application Touch-me-notAction Plant vegetable dye according to claim 8 is characterized in that to the method for the pre-mordant dying of fabric under alum mordant dyeing condition, the gained fabric is yellow; Under mantoquita mordant dyeing condition, gained fabric real silk is a deep yellow, and cotton, wool is green; Under metal ferrous salt mordant dyeing condition, the gained fabric is olive colour.
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| CN2008100424766A CN101348615B (en) | 2008-09-04 | 2008-09-04 | Preparation and use method of mimosa vegetable dye |
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| CN2008100424766A CN101348615B (en) | 2008-09-04 | 2008-09-04 | Preparation and use method of mimosa vegetable dye |
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| CN101348615A CN101348615A (en) | 2009-01-21 |
| CN101348615B true CN101348615B (en) | 2011-06-29 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102153883B (en) * | 2011-03-02 | 2013-12-25 | 上海交通大学 | Preparation and application of wool dye prepared by walnut plant |
| CN102767098B (en) * | 2011-12-30 | 2014-12-31 | 上海水星家用纺织品股份有限公司 | Preparation method of isatis root tie-dyed fabrics |
| CN105421113B (en) * | 2015-12-22 | 2017-11-14 | 广州番禺职业技术学院 | A kind of technique for Animal Skin of being printed and dyed using mangosteen skin juice |
| CN106245355A (en) * | 2016-07-27 | 2016-12-21 | 杨江源 | A kind of technique utilizing vegetable colour that textile is carried out dyeing process |
| CN106835759A (en) * | 2017-01-21 | 2017-06-13 | 达利(中国)有限公司 | The preparation method and applications of natural dye Freehandhand-drawing real silk fabric |
| CN110243852A (en) * | 2019-06-06 | 2019-09-17 | 上海交通大学 | Plant leaf blade wax content measurement method |
| CN111155337A (en) * | 2020-01-19 | 2020-05-15 | 中国科学院昆明植物研究所 | Green dyeing-assisted buddleja officinalis cloth dyeing method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1765894A (en) * | 2004-10-29 | 2006-05-03 | 广州莱泰制药有限公司 | Novel flavane derivative and its preparation method and uses |
| CN1823879A (en) * | 2005-12-22 | 2006-08-30 | 陈成华 | New use of mimosae pudicae herba medicine for treating spine nerve disease |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1765894A (en) * | 2004-10-29 | 2006-05-03 | 广州莱泰制药有限公司 | Novel flavane derivative and its preparation method and uses |
| CN1823879A (en) * | 2005-12-22 | 2006-08-30 | 陈成华 | New use of mimosae pudicae herba medicine for treating spine nerve disease |
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