CN102587154B - Method for dyeing silk fabrics by using purslane dye solution and bath mordant - Google Patents
Method for dyeing silk fabrics by using purslane dye solution and bath mordant Download PDFInfo
- Publication number
- CN102587154B CN102587154B CN201210035200.1A CN201210035200A CN102587154B CN 102587154 B CN102587154 B CN 102587154B CN 201210035200 A CN201210035200 A CN 201210035200A CN 102587154 B CN102587154 B CN 102587154B
- Authority
- CN
- China
- Prior art keywords
- purslane
- dyeing
- silk fabric
- dye
- mordant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention relates to a method for dyeing silk fabrics by using a purslane dye solution and bath mordant, in particular to the method for dyeing the silk fabrics by adopting an extracting solution of a natural medicinal plant, i.e. purslane. The method is characterized by comprising the following steps of: (1) preparing a purslane pigment stock solution and a purslane powder dye; (2) placing the cleaned silk fabrics in the dye solution for dyeing in a bath ratio of 1:200, wherein the dyeing concentration is 1-10% (o.w.f), the dyeing temperature is 60-90 DEG C, the pH value is 4-7, and the time is 30-90min, thereby finishing the dyeing; and obtaining the dyed silk fabrics after washing, centrifugal dewatering, and low temperature dying or airing; and (3) carrying out post-treatment on the dyed silk fabrics by using the mordant, wherein the dosage of the mordant accounts for 3%-15% of the weight of the dyed silk fabrics. The dyeing method has good dyeing effect.
Description
Technical field
The present invention relates to a kind of colouring method with bathing mordant dyeing silk fabric after purslane dye, the method that particularly adopts the extract of natural medicinal plant purslane to dye to silk fabric.
Background technology
Natural dye derives from plant, mineral, animal and microorganism mostly, wherein again take vegetable colour as main.And the plant itself that is much used for extracting dyestuff is exactly Chinese herbal medicine.Chinese Pharmacopoeia version in 1985 is recorded 554 kinds of vegetable drugs, and comprising 163 kinds of sibling species and mutation autonomic drugs, wherein some floristics medicine and dyeing floristics are in full accord.The relevant dyeing plant that pharmacopeia and book on Chinese herbal medicine are recorded has 15 kinds of safflower (red), cape jasmine (Huang), indigo plant (indigo plant), turmeric (Huang), bush (deep red), cortex acanthopanacis, Asian puccoon (purple), root tuber of aromatic turmeric (Huang), madder, Chinese honey locust, sargentodoxa cuneata, smilacis glabra, grape, Exocarpium Citri Rubrum, Cherokee roses (rose is red) etc.These vegetable colours have effect of anti-inflammation and sterilization mostly, originate also very extensive.Modern textile product can utilize medicinal plant dyestuff as natural antibacterial finishing agent, produce green health textiles.
Purslane is Portulacaceae annual herb plant, is medicine food dual purpose plant, plump succulence, and field and spacious wetland are born in happiness.Purslane body includes a large amount of flavone compounds, and its physiologically active is strong, has clearing heat and promoting diuresis, removing toxicity for detumescence, anti-inflammatory, quenches the thirst, diuresis, anti-bacteria and anti-virus anti-aging effects.In addition, purslane also can make veterinary drug and agricultural chemicals; Young stem and leaf can be done vegetables etc.Pigment in purslane is widely used as food coloring.
Purslane aboundresources, from south to north, there is growth in China more, almost all can adopt everywhere, if can be by rational extraction process, and the dyeing that can clean textiles easily,, in reaching the pharmacological functions such as antibacterial textile, attach and solve colouring problem, this is to improving the added value of textiles, and the Application Areas tool of widening weaving and Chinese herbal medicine product is of great significance.
Chinese patent 200710039385.2 (colouring method of dye yam extract to silk broadcloth), (200910103318.1 the extraction of mulberry leaf natural dyes and the colouring method of silk), (200610154538.3 preparation and the application thereof of Chinese chestnut element natural dye), the i.e. application in textile dyeing of extraction of some natural plant pigments has been reported in 200610155509.9 (preparation of spatholobus stem natural dye and application thereof) etc., and there is not yet both at home and abroad at present for the report of silk fabric dyeing about purslane pigment.
Summary of the invention
The object of the present invention is to provide a kind of colouring method with bathing mordant dyeing silk fabric after purslane dye, the method Color is good.
To achieve these goals, the technical solution adopted in the present invention is: a kind of colouring method with bathing mordant dyeing silk fabric after purslane dye, is characterized in that it comprises the steps:
1), the preparation of purslane pigment stoste, purslane dyestuff powder:
(1) purslane pigment stoste: get dry purslane (moisture content is not required), be chopped into the fragment of 0.01～10cm, the purslane after being shredded; Be 1: 30～200 by the purslane after chopping and the mass ratio of water, the purslane after chopping is soaked in water, at 20～90 ℃ of dipping 30～120min, remove by filter after residue, obtain purslane pigment stoste;
(2) purslane dyestuff powder: purslane pigment stoste normal temperature rotary evaporation is concentrated into initially (concentrated start before) purslane chromogen liquid long-pending 10～99%, the pre-freeze chamber that purslane pigment stoste after concentrated is put into freeze dryer is in-80～-86 ℃ of pre-freeze 1～2h (German Christ LSC type freeze dryer), when after purslane pigment stoste fully charge, and then (vacuum is 1～5bar to put into described freeze dryer vacuumize 15～18h, baking temperature is normal temperature temperature, is at other hothouse); Obtain purslane dyestuff powder;
2), adopt one of following 2 kinds of methods: 1. dyed 1～10% of silk fabric weight by the weight of purslane colouring substance in purslane pigment stoste, get purslane pigment stoste, as dye liquor; Be that in purslane pigment stoste, purslane colouring substance concentration is 1～10% (o.w.f);
2. or, dyed 1～10% of silk fabric weight by the weight of purslane dyestuff powder, get the purslane dyestuff powder dye liquor that is made into soluble in water, dye liquor concentration is 1～10% (o.w.f);
3), by clean silk fabric (by dye silk knit) take bath raio put at 1: 200 described dye liquor (purslane dye) dye (be the volume ratio of silk fabric quality and purslane dye as 1g: 200ml), dye liquor concentration is 1～10% (o.w.f), 60～90 ℃ of dyeing temperatures, pH value 3～7, time 30～90min, dyes complete; Through washing, centrifugal dehydration, low temperature (40～80 ℃) is dried or dries, and the silk fabric after being dyeed is stand-by;
4), the silk fabric after described dyeing is carried out to rear mordant dyeing processing, mordant concentration is 3～15% (o.w.f); bath raio is 1: 100～200 (the silk fabric quality after dyeing is 1g: 100～200ml with the volume ratio of mordant solution); at 40～80 ℃ of temperature, process after 30～60min; take out; through cleaning, centrifugal dehydration, 40～80 ℃ of oven dry of low temperature or dry, and obtains rear bath mordant dyeing silk fabric.
Described mordant is preferentially Al
3+or Fe
2+salt, be specially AlK (SO
4)
2or FeSO
4.
The brightness value L of described rear bath mordant dyeing silk fabric is 60-75, and red green value a* is-1-3, and champac value b* is 9-20, and soaping fastness is 3-4～5 grade, and crock fastness is 3-4～5 grade.
Rear bath mordant dyeing silk fabric can be used for generally wearing textiles and medical textile.
The invention has the beneficial effects as follows: the present invention carries out rear bath mordant dying to silk fabric, the silk fabric that color is uniform and stable, COLOR FASTNESS is high can dye.Dyestuff leaching process of the present invention is simple, convenient, pollution-free, and the natural antibiotics pharmacological function of silk fabric because of purslane dyes in institute, can be used for keeping healthy, antibacterial, anti-inflammatory, detumescence etc. wear textiles and medical textile.
The specific embodiment
For a better understanding of the present invention, further illustrate content of the present invention below in conjunction with embodiment, but content of the present invention is not limited only to the following examples.
Embodiment 1 (the rear bath mordant dying of purslane stoste to silk fabric):
1) get dry purslane 80g (moisture content is not required), after chopping (being chopped into the fragment of 0.01～10cm), be immersed in the water of 3kg, under 90 ℃ of constant temperature, flood after 90min, refilter and remove after residue, obtain purslane pigment stoste 2.41kg.The concentration of actual measurement purslane pigment stoste is 0.332wt%.
2) the purslane pigment stoste of gained is taken to 30g (concentration is 0.332wt%), be equivalent to 0.1g purslane colouring substance (weight of purslane colouring substance be dyed silk fabric weight 10%).Get clean 1g silk fabric, by bath raio dye at 1: 200 (volume ratio that is silk fabric quality and purslane dye is 1g: 200ml), the pH value of purslane dye is 3, silk fabric dyes after 50min in 70 ℃ of purslane dyes, take out, through washing, centrifugal dehydration, dry, the silk fabric after being dyeed, stand-by.
3) silk fabric after the dyeing after above-mentioned drying (dyeing silk fabric) is put into FeSO
4the aqueous solution in carry out rear mordant dyeing processing, FeSO
4concentration be 6% (o.w.f); bath raio 1: 200 (the silk fabric quality after dyeing is 1g: 200ml with the volume ratio of mordant solution); take out cleanly process 30min at 80 ℃ after, centrifugal dehydration, 60 ℃ of oven dry of low temperature, obtain the silk fabric of rear bath mordant dyeing.
Gained recorded to brightness value L as 72.68 to bathe mordant dyeing silk fabric after stoste on Shimadzu UV-2550 type ultra-violet and visible spectrophotometer (band integrating sphere and color software), red green value a* is-0.79, champac value b* is 11.85, measuring soaping fastness by GB/T 3921.1-1997 is 4 grades, and measuring fastness to wet rubbing by GB/T 3920-1997 is 4～5 grades.Illustrate that Color of the present invention is good.
Embodiment 2 (the rear bath mordant dying of purslane dyestuff powder to silk fabric):
1) the purslane pigment stoste in embodiment 1 is taken to 1.22kg normal temperature rotary evaporation and be concentrated into 100ml, pigment stoste after concentrated is put into freeze dryer (German Christ LSC type freeze dryer) the pre-freeze 2h that programmed cooling arrives-86 ℃, make it fully charge, use again freeze dryer freeze drying 16h, obtain purslane dyestuff powder (or claiming pulverous purslane dyestuff) (about 4.05g).
2) by prepared purslane dyestuff powder 3g (weight of purslane dyestuff powder be dyed silk fabric weight 6%), the water-soluble purslane dye that is made into; Get clean 50g silk fabric and put into the bath raio purslane dye of 1: 200 dyeing (volume ratio that is silk fabric quality and purslane dye is 1g: 200ml), dye liquor pH value is 3, at 70 ℃ of dyeing 60min, dye to finish and take out, through washing, centrifugal dehydration, dry, silk fabric after being dyeed, stand-by.
3) silk fabric after above-mentioned dyeing is put into FeSO
4the aqueous solution in carry out rear mordant dyeing processing, FeSO
4concentration be 9% (o.w.f), bath raio 1: 200 (i.e. silk fabric quality and FeSO after dyeing
4the volume ratio of the aqueous solution be 1g: 200ml), at 60 ℃, process after 30min, take out and clean, centrifugal dehydration, dry, obtain the silk fabric of rear bath mordant dyeing.
The silk fabric to bathe mordant dyeing after dyestuff powder of gained is recorded to brightness value L as 70.13 on Shimadzu UV-2550 type ultra-violet and visible spectrophotometer (band integrating sphere and color software), red green value a* is-0.86, champac value b* is 13.32, measuring soaping fastness by GB/T 3921.1-1997 is 4 grades, and measuring fastness to wet rubbing by GB/T 3920-1997 is 4 grades.Illustrate that Color of the present invention is good.
Embodiment 3
With a colouring method of bathing mordant dyeing silk fabric after purslane dye, it comprises the steps:
1), the preparation of purslane pigment stoste:
Get dry purslane (moisture content is not required), be chopped into the fragment of 0.01～10cm, the purslane after being shredded; Be 1: 30 by the purslane after chopping and the mass ratio of water, the purslane after chopping is soaked in water, at 20 ℃ of dipping 30min, remove by filter after residue, obtain purslane pigment stoste;
2), get clean silk fabric, dyed 1% of silk fabric weight by the weight of purslane colouring substance in purslane pigment stoste, get purslane pigment stoste;
3), by clean silk fabric (by dye silk knit) take bath raio put at 1: 200 described purslane dye dyeing (be the volume ratio of silk fabric quality and purslane dye as 1g: 200ml), dye liquor concentration is 1% (o.w.f), 60 ℃ of dyeing temperatures, pH value 3, time 30min, dyes complete; Through washing, centrifugal dehydration, low temperature (40 ℃) is dried, and the silk fabric after being dyeed is stand-by;
4), the silk fabric after described dyeing is carried out to rear mordant dyeing processing, mordant (AlK (SO
4)
2consumption be 3% (o.w.f); bath raio is 1: 100 (silk fabric quality and the volume ratio of mordant solution after dyeing is 1g: 100ml); at 40 ℃ of temperature, process after 30min; taking-up; through cleaning, centrifugal dehydration, 40 ℃ of oven dry of low temperature, obtain rear bath mordant dyeing silk fabric.
The silk fabric to bathe mordant dyeing after dyestuff powder of gained is recorded to brightness value L as 75 on Shimadzu UV-2550 type ultra-violet and visible spectrophotometer (band integrating sphere and color software), red green value a* is 3, champac value b* is 9, measuring soaping fastness by GB/T 3921.1-1997 is 3 grades, and measuring fastness to wet rubbing by GB/T 3920-1997 is 3 grades.Illustrate that Color of the present invention is good.
Embodiment 4
With a colouring method of bathing mordant dyeing silk fabric after purslane dye, it comprises the steps:
1), the preparation of purslane pigment stoste:
Get dry purslane (moisture content is not required), be chopped into the fragment of 0.01～10cm, the purslane after being shredded; Be 1: 200 by the purslane after chopping and the mass ratio of water, the purslane after chopping is soaked in water, at 90 ℃ of dipping 120min, remove by filter after residue, obtain purslane pigment stoste;
2), get clean silk fabric, dyed 10% of silk fabric weight by the weight of purslane colouring substance in purslane pigment stoste, get purslane pigment stoste;
3), by clean silk fabric (by dye silk knit) take bath raio put at 1: 200 described purslane dye dyeing (be the volume ratio of silk fabric quality and purslane dye as 1g: 200ml), dye liquor concentration is 10% (o.w.f), 90 ℃ of dyeing temperatures, pH value 7, time 90min, dyes complete; Through washing, centrifugal dehydration, low temperature (80 ℃) is dried, and the silk fabric after being dyeed is stand-by;
4), the silk fabric after described dyeing is carried out to rear mordant dyeing processing, mordant (AlK (SO
4)
2consumption be 15% (o.w.f); bath raio is 1: 200 (silk fabric quality and the volume ratio of mordant solution after dyeing is 1g: 200ml); at 80 ℃ of temperature, process after 60min; take out; through cleaning, centrifugal dehydration, 480 ℃ of oven dry of low temperature or dry, and obtains rear bath mordant dyeing silk fabric.
The silk fabric to bathe mordant dyeing after dyestuff powder of gained is recorded to brightness value L as 70 on Shimadzu UV-2550 type ultra-violet and visible spectrophotometer (band integrating sphere and color software), red green value a* is 2.5, champac value b* is 12, measuring soaping fastness by GB/T 3921.1-1997 is 3 grades, and measuring fastness to wet rubbing by GB/T 3920-1997 is 4 grades.Illustrate that Color of the present invention is good.
Embodiment 5
With a colouring method of bathing mordant dyeing silk fabric after purslane dye, it comprises the steps:
1), the preparation of purslane dyestuff powder:
(1) purslane pigment stoste: get dry purslane (moisture content is not required), be chopped into the fragment of 0.01～10cm, the purslane after being shredded; Be 1: 30 by the purslane after chopping and the mass ratio of water, the purslane after chopping is soaked in water, at 20 ℃ of dipping 30min, remove by filter after residue, obtain purslane pigment stoste;
(2) purslane dyestuff powder: purslane pigment stoste normal temperature rotary evaporation is concentrated into initially (concentrated start before) purslane chromogen liquid long-pending 10%, the pre-freeze chamber that purslane pigment stoste after concentrated is put into freeze dryer is in-80 ℃ of pre-freeze 1h (German Christ LSC type freeze dryer), when after purslane pigment stoste fully charge, and then (vacuum is 1～5bar to put into described freeze dryer vacuumize 15h, baking temperature is normal temperature temperature, is at other hothouse); Obtain purslane dyestuff powder;
2), dyed 1% of silk fabric weight by the weight of purslane dyestuff powder, get the purslane dyestuff powder dye liquor that is made into soluble in water, dye liquor concentration is 1% (o.w.f);
3), by clean silk fabric (by dye silk knit) take bath raio put at 1: 200 described purslane dye dyeing (be the volume ratio of silk fabric quality and purslane dye as 1g: 200ml), dye liquor concentration is 1% (o.w.f), 60 ℃ of dyeing temperatures, pH value 3, time 30min, dyes complete; Through washing, centrifugal dehydration, low temperature (40 ℃) is dried, and the silk fabric after being dyeed is stand-by;
4), the silk fabric after described dyeing is carried out to rear mordant dyeing processing, mordant FeSO
4concentration be 3% (o.w.f); bath raio is 1: 100 (silk fabric quality and the volume ratio of mordant solution after dyeing is 1g: 100ml); at 40 ℃ of temperature, process after 30min; taking-up; through cleaning, centrifugal dehydration, 40 ℃ of oven dry of low temperature, obtain rear bath mordant dyeing silk fabric.
The silk fabric to bathe mordant dyeing after dyestuff powder of gained is recorded to brightness value L as 75 on Shimadzu UV-2550 type ultra-violet and visible spectrophotometer (band integrating sphere and color software), red green value a* is 2.25, champac value b* is 10.65, measuring soaping fastness by GB/T3921.1-1997 is 4～5 grades, and measuring fastness to wet rubbing by GB/T 3920-1997 is 4～5 grades.Illustrate that Color of the present invention is good.
Embodiment 6
With a colouring method of bathing mordant dyeing silk fabric after purslane dye, it comprises the steps:
1), the preparation of purslane pigment stoste, purslane dyestuff powder:
(1) purslane pigment stoste: get dry purslane (moisture content is not required), be chopped into the fragment of 0.01～10cm, the purslane after being shredded; Be 1: 200 by the purslane after chopping and the mass ratio of water, the purslane after chopping is soaked in water, at 90 ℃ of dipping 120min, remove by filter after residue, obtain purslane pigment stoste;
(2) purslane dyestuff powder: purslane pigment stoste normal temperature rotary evaporation is concentrated into initially (concentrated start before) purslane chromogen liquid long-pending 99%, the pre-freeze chamber that purslane pigment stoste after concentrated is put into freeze dryer is in-86 ℃ of pre-freeze 2h (German Christ LSC type freeze dryer), when after purslane pigment stoste fully charge, and then (vacuum is 1～5bar to put into described freeze dryer vacuumize 18h, baking temperature is normal temperature temperature, is at other hothouse); Obtain purslane dyestuff powder;
2), dyed 10% of silk fabric weight by the weight of purslane dyestuff powder, get the purslane dyestuff powder dye liquor that is made into soluble in water, dye liquor concentration is 10% (o.w.f);
3), by clean silk fabric (by dye silk knit) take bath raio put at 1: 200 described purslane dye dyeing (be the volume ratio of silk fabric quality and purslane dye as 1g: 200ml), dye liquor concentration is 10% (o.w.f), 90 ℃ of dyeing temperatures, pH value 7, time 90min, dyes complete; Through washing, centrifugal dehydration, dry, the silk fabric after being dyeed, stand-by;
4), the silk fabric after described dyeing is carried out to rear mordant dyeing processing, mordant FeSO
4concentration be 15% (o.w.f); bath raio is 1: 200 (silk fabric quality and the volume ratio of mordant solution after dyeing is 1g: 200ml); at 80 ℃ of temperature, process after 60min; taking-up; through cleaning, centrifugal dehydration, dry, and obtains rear bath mordant dyeing silk fabric.
The silk fabric to bathe mordant dyeing after dyestuff powder of gained is recorded to brightness value L as 60 on Shimadzu UV-2550 type ultra-violet and visible spectrophotometer (band integrating sphere and color software), red green value a* is-1, champac value b* is 20, measuring soaping fastness by GB/T 3921.1-1997 is 3 grades, and measuring fastness to wet rubbing by GB/T 3920-1997 is 4 grades.Illustrate that Color of the present invention is good.
Claims (3)
1. with a colouring method of bathing mordant dyeing silk fabric after purslane dye, it is characterized in that it comprises the steps:
1), the preparation of purslane pigment stoste, purslane dyestuff powder:
(1) purslane pigment stoste: get dry purslane, be chopped into the fragment of 0.01～10cm, the purslane after being shredded; Be 1: 30～200 by the purslane after chopping and the mass ratio of water, the purslane after chopping is soaked in water, at 20～90 ℃ of dipping 30～120min, remove by filter after residue, obtain purslane pigment stoste;
(2) purslane dyestuff powder: by purslane pigment stoste normal temperature rotary evaporation be concentrated into initial purslane chromogen liquid long-pending 10～99%, the pre-freeze chamber that purslane pigment stoste after concentrated is put into freeze dryer is in-80～-86 ℃ of pre-freeze 1～2h, when after purslane pigment stoste fully charge, and then put into described freeze dryer vacuumize 15～18h; Obtain purslane dyestuff powder;
2), adopt one of following 2 kinds of methods: 1. dyed 1～10% of silk fabric weight by the weight of purslane colouring substance in purslane pigment stoste, get purslane pigment stoste, as dye liquor; Be that in purslane pigment stoste, purslane colouring substance concentration is 1～10%(o.w.f);
2. dyed 1～10% of silk fabric weight by the weight of purslane dyestuff powder, get the purslane dyestuff powder dye liquor that is made into soluble in water, dye liquor concentration is 1～10%(o.w.f);
3), clean silk fabric put into described purslane dye with bath raio 1:200 dye, dye liquor concentration is 1～10%(o.w.f), 60～90 ℃ of dyeing temperatures, pH value 3～7, time 30～90min, dyes complete; Through washing, centrifugal dehydration, low temperature drying or dry, the silk fabric after being dyeed, stand-by;
4), the silk fabric after described dyeing is carried out to rear mordant dyeing processing, mordant concentration is 3～15%(o.w.f); bath raio is 1:100～200; at 40～80 ℃ of temperature, process after 30～60min; take out; dry or dry through 40～80 ℃ of cleanings, centrifugal dehydration, low temperature, obtaining rear bath mordant dyeing silk fabric.
2. a kind of colouring method with bathing mordant dyeing silk fabric after purslane dye according to claim 1, is characterized in that, described mordant is FeSO
4the aqueous solution or AlK(SO
4)
2the aqueous solution.
3. a kind of colouring method with bathing mordant dyeing silk fabric after purslane dye according to claim 1, is characterized in that, the low temperature described in step 3) is 40～80 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210035200.1A CN102587154B (en) | 2012-02-16 | 2012-02-16 | Method for dyeing silk fabrics by using purslane dye solution and bath mordant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210035200.1A CN102587154B (en) | 2012-02-16 | 2012-02-16 | Method for dyeing silk fabrics by using purslane dye solution and bath mordant |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102587154A CN102587154A (en) | 2012-07-18 |
| CN102587154B true CN102587154B (en) | 2014-07-02 |
Family
ID=46476353
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210035200.1A Expired - Fee Related CN102587154B (en) | 2012-02-16 | 2012-02-16 | Method for dyeing silk fabrics by using purslane dye solution and bath mordant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102587154B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103938386B (en) * | 2014-04-25 | 2016-11-16 | 何炽斌 | Utilize the production method of pure natural dye juice dyed cloth |
| CN104559308B (en) * | 2015-02-02 | 2017-01-04 | 苏州爱立方服饰有限公司 | A kind of natural dye used for textiles and preparation method thereof |
| CN105421100A (en) * | 2015-12-09 | 2016-03-23 | 江苏苏丝丝绸股份有限公司 | Method for preparing spun silk and chitosan fiber blending antibacterial fabric |
| CN110306358B (en) * | 2019-08-08 | 2021-11-23 | 苏州虹锦生态纺织科技有限公司 | Processing method for dyeing real silk fabric by natural dye |
| CN115233470B (en) * | 2022-07-25 | 2023-10-24 | 达利(中国)有限公司 | Preparation method of anti-mite silk fabric based on bergamot pigment |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102220705A (en) * | 2011-04-20 | 2011-10-19 | 盐城纺织职业技术学院 | Method for dying silk fabric by using natural dye of Suaeda salsa |
-
2012
- 2012-02-16 CN CN201210035200.1A patent/CN102587154B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN102587154A (en) | 2012-07-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102561058B (en) | Method for improving dyeing property of cotton fabric natural dye by using silk peptide | |
| CN102587154B (en) | Method for dyeing silk fabrics by using purslane dye solution and bath mordant | |
| CN105256604A (en) | Method for dyeing textile by using traditional Chinese medicine | |
| CN102604423B (en) | Preparation method and application of plant medicinal dye | |
| CN102785276A (en) | Method for dyeing woods by using natural plant | |
| CN105348851A (en) | Preparation of anthocyanin dye and application of anthocyanin dye in cellulosic fiber fabric dyeing | |
| CN105297493A (en) | Method for dyeing real silk fabric by adopting natural dyestuff | |
| CN102604422B (en) | Preparation method of purslane natural dye and application of the purslane natural dye | |
| CN102561057B (en) | Method of improving dyeing property of natural dye for cotton fabrics by using sericin | |
| CN101348615B (en) | Preparation and use method of mimosa vegetable dye | |
| CN104179037A (en) | Tussah silk pajamas dyed by vegetable dye | |
| CN106381730A (en) | Bamboo pulp fiber fabric based on grape pigment dyeing and preparation method thereof | |
| CN102517651A (en) | Color fixing method of natural colorful mulberry silk | |
| CN102535189B (en) | Method for dyeing metachrome silk fabric by using parslane herb dye liquor | |
| CN104480745B (en) | The application of a kind of fabric dyeing process based on persimmon extract and relevant DYED FABRICS | |
| CN114182542A (en) | Method for dyeing green by vegetable dye one-bath process | |
| CN105778556A (en) | Violet dye extracting method and dyeing application | |
| CN108948781A (en) | The preparation method of spun gold emperor's chrysanthemum natural dye and the natural dye and colouring method prepared by this method | |
| Tutak et al. | Natural dyeing properties of wool fabrics by pomegranate (Punica granatum) peel | |
| CN104031403B (en) | A kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof | |
| CN106118128A (en) | Plant dye and the weaving material of this plant dye dyeing is prepared with Hebei Folium et Caulis Indigoferae Tinctoriae | |
| CN107686669B (en) | natural Chinese prickly ash dye and preparation method and application thereof | |
| CN103103812A (en) | Natural green cotton fabric | |
| CN105780530A (en) | Rose flower cloth dyeing technology | |
| CN107761405A (en) | A kind of antimicrobial form silk dyeing fabric and its dyeing |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140702 Termination date: 20150216 |
|
| EXPY | Termination of patent right or utility model |