CN106811991A - A kind of colouring method of brocade of Zhang nationality line - Google Patents
A kind of colouring method of brocade of Zhang nationality line Download PDFInfo
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- CN106811991A CN106811991A CN201710051145.8A CN201710051145A CN106811991A CN 106811991 A CN106811991 A CN 106811991A CN 201710051145 A CN201710051145 A CN 201710051145A CN 106811991 A CN106811991 A CN 106811991A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/67341—Salts or hydroxides of elements different from the alkaline or alkaline-earth metals or with anions containing those elements
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
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- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
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Abstract
The invention discloses a kind of colouring method of brocade of Zhang nationality line, comprise the following steps：S1. coloring agent is prepared with dyeing plant, the dyeing plant includes yellow dyeing plant, red staining plant, purple dye plant, black-dyeing plant and green dyeing plant, and dyeing plant is size-reduced, add cellulase, immersion that coloring agent is obtained；S2. mix colours, be put into brocade of Zhang nationality line, add mordant to carry out first time dyeing；S3. to adding color fixing agent to be washed admittedly in overflow dyeing machine, then adding mordant carries out second dyeing, is dried after the completion of second dyeing, cleaned, and obtains final product the brocade of Zhang nationality line for having dyeed.Brocade of Zhang nationality line dye can be made more bright-coloured yellow, red, purple, black and green by the present invention, pure natural, to human body fanout free region.
Description
Technical field
Field, more particularly to a kind of colouring method of brocade of Zhang nationality line are made the present invention relates to brocade of Zhang nationality.
Background technology
Brocade of Zhang nationality, and Nanjing brocade, Sichuan brocade, Song Dynasty brocade and claims the big name brocade of China four, and the Song dynasty is originated from according to biography, is rare Chinese national culture
It is precious.The strong text of brocade of Zhang nationality is referred to as mbaw laiz fax, means the page of day line, is the exquisite technique woven using cotton thread or silk thread
Product, because lucuriant in design, pattern is unique, durable and famous, embody the Zhuang people to the worship in the world and to good life
Pursuit with yearn for.
The dyeing of brocade of Zhang nationality since ancient times is full the dyestuff using the processing of the natural materials such as the animal in nature, plant or mineral
Dye.In the modern society for advocating sustainable development, for chemical dyestuff, natural dye is undoubtedly more environmentally friendly, health,
Traditional dyeing process is more aobvious valuable and important.But, it is often difficult because traditional natural dye color is simpler, dimness
To attract the eyeball of consumer, therefore contaminate system using chemical dye more than brocade of Zhang nationality currently on the market at present to form, with people's ring
The continuous improvement of consciousness is protected, green consumption has turned into the trend of whole textile industry, it is healthy to people to reduce chemical dye
The injury for bringing, it is extremely to be necessary that how brocade of Zhang nationality line dye is made more gay colours by research using natural plants
's.
The content of the invention
The invention provides a kind of colouring method of brocade of Zhang nationality line, can by brocade of Zhang nationality line dye make more bright-coloured yellow,
Red, purple, black and green, it is pure natural, to human body fanout free region.
To achieve the above object, the technical scheme is that：
A kind of colouring method of brocade of Zhang nationality line, comprises the following steps：
S1. coloring agent is prepared with dyeing plant, the dyeing plant includes yellow dyeing plant, red staining plant, purple dye
Color plant, black-dyeing plant and green dye plant, and preparation process is：
Yellow colorant：Extracting yellow dyes plant, and the yellow dyeing plant is Yellow Fructus Gardeniae or big yellow ginger, is crushed, and adds weight 8
~ 20 times of water, is subsequently adding cellulase, pectase and sodium chloride, and yellow dyeing plant is 1 with the weight ratio of cellulase:
0.01 ~ 0.03, yellow dyeing plant is 1 with the weight ratio of pectase:0.005 ~ 0.02, yellow dyes the weight of plant and sodium chloride
Amount is than being 1:0.001 ~ 0.005,30 ~ 50h is soaked, boil, natural cooling, filter, obtain Yellow colorant；
Red staining agent：Red staining plant is taken, the red staining plant is the red fragrant thoroughwort of roundleaf, is crushed, and adds weight 8 ~ 20
Water again, is subsequently adding cellulase and sodium chloride, and red staining plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05,
Red staining plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,30 ~ 50h is soaked, boil, natural cooling, filter, obtain
Red staining agent；
Purple dye agent：Purple dye plant is taken, the purple dye plant is the red fragrant thoroughwort that comes into leaves, and is crushed, and adds weight 5 ~ 20
Water again, is subsequently adding cellulase and sodium chloride, and purple dye plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05,
Purple dye plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,30 ~ 50h is soaked, boil, natural cooling, filter, obtain
Purple dye agent；
Black dye：Black-dyeing plant is taken, the black-dyeing plant is maple leaf, is crushed, and adds the water of 3 ~ 8 times of weight,
Cellulase and sodium chloride are subsequently adding, black-dyeing plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05, black-dyeing
Plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,30 ~ 50h is soaked, filtering obtains black dye；
Green coloring agent：Green dyeing plant is taken, the green dyeing plant is mulberry leaf, is crushed, and first adds 2 ~ 3 times of weight
Water, adds cellulase and sodium chloride, and green dyeing plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05, green dyeing
Plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,5 ~ 10h is soaked, 8 ~ 20 times 50 ~ 70% of ethanol water is added,
10 ~ 30h of immersion, filtering is concentrated under reduced pressure and reclaims ethanol, and gained concentrate adds sodium hydroxide solution, and pH is to 7.2 ~ 7.8 for regulation,
Obtain green coloring agent；
S2. the coloring agent that S1 is obtained is mixed colours, the coloring agent mixed colours is put into overflow dyeing machine, be put into brocade of Zhang nationality line, plus
Entering mordant carries out first time dyeing；
S3. to adding color fixing agent to be washed admittedly in overflow dyeing machine, then adding mordant carries out second dyeing, second dyeing
After the completion of drying, clean, obtain final product the brocade of Zhang nationality line for having dyeed.
Further, in the step S1, yellow dyeing plant, red staining plant, purple dye plant, black-dyeing
Plant and green dyeing plant are crushed after addition water respectively, are also put into 5 ~ 15min of homogeneous in homogenizer, and homogenization pressure is 20 ~
30MPa。
Further, in the step S1, the Yellow colorant, red staining agent, purple dye agent, black dye are obtained
After toner and green dyeing plant, antioxidant is also separately added into, the weight of antioxidant is coloring agent weight 0.1 ~ 0.5%.
Further, the antioxidant is sodium ascorbate or sodium isoascorbate.
Further, in the step S2 and S3, the mordant is rare earth mordant.Further, the rare earth
Mordant is the one kind in rare earth chloride, rare earth oxide, Rare Earth Citric Acid Complexes.
Further, the color fixing agent is sodium chloride, and sodium chloride is 1 ~ 3 with the feed liquid weight ratio in overflow dyeing machine:100.
Further, in the step S2, the temperature of dyeing is 50 ~ 70 DEG C, and dyeing time is 20 ~ 40min.
Further, in the step S2, the temperature of dyeing is 50 ~ 60 DEG C, and dyeing time is 15 ~ 30min.
The colouring method of above-described brocade of Zhang nationality line, with advantages below：
（1）It is using natural plant extract pigment, environmentally friendly, degradable, to human body fanout free region, it is to avoid chemical dye is strong to human body
The pollution that health and environmental protection bring.
（2）Employ cellulase and pectase to destroy the cell membrane in plant, make the further dissolution of phytochrome, carry
The extraction and application rate of phytochrome high；In addition, the activity of cellulase and pectase is also improved further with sodium chloride,
Sodium chloride can also prevent the generation of plant oxidation effect in extraction process, to keep dyeing while pigment utilization rate is improved
Agent chromatic colour.
（3）The present invention has further selected rare earth as mordant, improves dye uptake and the color jail of vegetable dyeing agent
Degree.
（4）The present invention also further adds antioxidant in coloring agent, maintains coloring agent chromatic colour, prevents
There is the phenomenons such as discoloration, corruption during storage in coloring agent.
（5）Extensively, production process is simple and easy to control, is conducive to wide in brocade of Zhang nationality line colouring art for raw material sources of the invention
General popularization, the development of succession, the Zhuang culture to brocade of Zhang nationality handicraft has positive impetus.
Specific embodiment
Below in conjunction with specific embodiment, the invention will be further described, but protection scope of the present invention be not limited to it is following
Embodiment.
Embodiment 1
A kind of colouring method of brocade of Zhang nationality line, comprises the following steps：
S1. coloring agent is prepared with dyeing plant, the dyeing plant includes yellow dyeing plant, red staining plant, purple dye
Color plant, black-dyeing plant and green dye plant, and preparation process is：
Yellow colorant：Extracting yellow dyes plant, and yellow dyeing plant is big yellow ginger, is crushed, and adds the water of 10 times of weight, then
Cellulase, pectase and sodium chloride are added, yellow dyeing plant is 1 with the weight ratio of cellulase:0.02, yellow dyeing is planted
Thing is 1 with the weight ratio of pectase:0.01, yellow dyeing plant is 1 with the weight ratio of sodium chloride:0.005,50h is soaked, boil
Boiling, natural cooling, filtering obtains Yellow colorant；
Red staining agent：Red staining plant is taken, red staining plant is the red fragrant thoroughwort of roundleaf, is crushed, and adds the water of 10 times of weight,
Cellulase and sodium chloride are subsequently adding, red staining plant is 1 with the weight ratio of cellulase:0.02, red staining plant
It is 1 with the weight ratio of sodium chloride:0.005,50h is soaked, boil, natural cooling, filter, obtain red staining agent；
Purple dye agent：Purple dye plant is taken, purple dye plant is the red fragrant thoroughwort that comes into leaves, and is crushed, and adds the water of 10 times of weight,
Cellulase and sodium chloride are subsequently adding, purple dye plant is 1 with the weight ratio of cellulase:0.02, purple dye plant
It is 1 with the weight ratio of sodium chloride:0.005,50h is soaked, boil, natural cooling, filter, obtain purple dye agent；
Black dye：Black-dyeing plant is taken, black-dyeing plant is maple leaf, is crushed, and adds the water of 5 times of weight, Ran Houjia
Enter cellulase and sodium chloride, black-dyeing plant is 1 with the weight ratio of cellulase:0.02, black-dyeing plant and chlorination
The weight ratio of sodium is 1:0.005,50h is soaked, filtering obtains black dye；
Green coloring agent：Green dyeing plant is taken, green dyeing plant is mulberry leaf, is crushed, and first adds 2.5 times of water of weight, plus
Enter cellulase and sodium chloride, green dyeing plant is 1 with the weight ratio of cellulase:0.02, green dyeing plant and chlorination
The weight ratio of sodium is 1:0.005,7h is soaked, 10 times 50% of ethanol water is added, 30h is soaked, filtering is concentrated under reduced pressure back
Ethanol is received, gained concentrate adds sodium hydroxide solution, and pH is to 7.2 ~ 7.8 for regulation, obtains green coloring agent.
S2. the coloring agent that S1 is obtained is mixed colours, the coloring agent mixed colours is put into overflow dyeing machine, be put into brocade of Zhang nationality use
Line, adds rare earth chloride to carry out first time dyeing, and dyeing temperature is 65 DEG C, and dyeing time is 35min；
S3. to adding sodium chloride to be washed admittedly in overflow dyeing machine, sodium chloride is 1 with the feed liquid weight ratio in overflow dyeing machine:100, then
Adding rare earth chloride carries out second dyeing, and dyeing temperature is 60 DEG C, and dyeing time is 30min, after the completion of second is dyeed
Dry, clean, obtain final product the brocade of Zhang nationality line for having dyeed.
Embodiment 2
A kind of colouring method of brocade of Zhang nationality line, comprises the following steps：
S1. coloring agent is prepared with dyeing plant, the dyeing plant includes yellow dyeing plant, red staining plant, purple dye
Color plant, black-dyeing plant and green dye plant, and preparation process is：
Yellow colorant：Extracting yellow dyes plant, and yellow dyeing plant is big yellow ginger, is crushed, and adds the water of 8 times of weight, is put into
Homogeneous 10min in homogenizer, homogenization pressure is 25MPa, is subsequently adding cellulase, pectase and sodium chloride, and yellow dyeing is planted
Thing is 1 with the weight ratio of cellulase:0.01, yellow dyeing plant is 1 with the weight ratio of pectase:0.005, yellow dyeing is planted
Thing is 1 with the weight ratio of sodium chloride:0.001,50h is soaked, boil, natural cooling, filter, obtain Yellow colorant；
Red staining agent：Red staining plant is taken, red staining plant is the red fragrant thoroughwort of roundleaf, is crushed, and adds the water of 8 times of weight,
Be put into homogeneous 10min in homogenizer, homogenization pressure is 25MPa, be subsequently adding cellulase and sodium chloride, red staining plant with
The weight ratio of cellulase is 1:0.01, red staining plant is 1 with the weight ratio of sodium chloride:0.001,50h is soaked, boil,
Natural cooling, filtering, obtains red staining agent；
Purple dye agent：Purple dye plant is taken, purple dye plant is the red fragrant thoroughwort that comes into leaves, and is crushed, and adds the water of 5 times of weight,
Be put into homogeneous 10min in homogenizer, homogenization pressure is 25MPa, be subsequently adding cellulase and sodium chloride, purple dye plant with
The weight ratio of cellulase is 1:0.01, purple dye plant is 1 with the weight ratio of sodium chloride:0.001,50h is soaked, boil,
Natural cooling, filtering, obtains purple dye agent；
Black dye：Black-dyeing plant is taken, black-dyeing plant is maple leaf, is crushed, and adds the water of 3 times of weight, is put into
Homogeneous 10min in matter machine, homogenization pressure is 25MPa, is subsequently adding cellulase and sodium chloride, black-dyeing plant and cellulose
The weight ratio of enzyme is 1:0.01, black-dyeing plant is 1 with the weight ratio of sodium chloride:0.001,50h is soaked, filtering obtains black
Coloring agent；
Green coloring agent：Green dyeing plant is taken, green dyeing plant is mulberry leaf, is crushed, and first adds 2 times of water of weight, is added
Cellulase and sodium chloride, green dyeing plant are 1 with the weight ratio of cellulase:0.01, green dyeing plant and sodium chloride
Weight ratio be 1:0.001,10h is soaked, 8 times 70% of ethanol water is added, homogeneous 10min in homogenizer is put into,
Matter pressure is 25MPa, soaks 30h, and filtering is concentrated under reduced pressure and reclaims ethanol, and gained concentrate adds sodium hydroxide solution, adjusts pH
To 7.2 ~ 7.8, green coloring agent is obtained.
S2. the coloring agent that S1 is obtained is mixed colours, the coloring agent mixed colours is put into overflow dyeing machine, be put into brocade of Zhang nationality use
Line, adds rare earth oxide to carry out first time dyeing, and dyeing temperature is 55 DEG C, and dyeing time is 35min；
S3. to adding sodium chloride to be washed admittedly in overflow dyeing machine, sodium chloride is 1 with the feed liquid weight ratio in overflow dyeing machine:100, then
Adding rare earth oxide carries out second dyeing, and dyeing temperature is 55 DEG C, and dyeing time is 25min, after the completion of second is dyeed
Dry, clean, obtain final product the brocade of Zhang nationality line for having dyeed.
Embodiment 3
A kind of colouring method of brocade of Zhang nationality line, comprises the following steps：
S1. coloring agent is prepared with dyeing plant, the dyeing plant includes yellow dyeing plant, red staining plant, purple dye
Color plant, black-dyeing plant and green dye plant, and preparation process is：
Yellow colorant：Extracting yellow dyes plant, and yellow dyeing plant is big yellow ginger, is crushed, and adds the water of 10 times of weight, is put into
Homogeneous 5min in homogenizer, homogenization pressure is 30MPa, is subsequently adding cellulase, pectase and sodium chloride, yellow dyeing plant
It is 1 with the weight ratio of cellulase:0.02, yellow dyeing plant is 1 with the weight ratio of pectase:0.01, yellow dyeing plant
It is 1 with the weight ratio of sodium chloride:0.005,50h is soaked, boil, natural cooling, filter, obtain Yellow colorant；
Red staining agent：Red staining plant is taken, red staining plant is the red fragrant thoroughwort of roundleaf, is crushed, and adds the water of 10 times of weight,
Be put into homogeneous 5min in homogenizer, homogenization pressure is 30MPa, be subsequently adding cellulase and sodium chloride, red staining plant with
The weight ratio of cellulase is 1:0.02, red staining plant is 1 with the weight ratio of sodium chloride:0.005,50h is soaked, boil,
Natural cooling, filtering, obtains red staining agent；
Purple dye agent：Purple dye plant is taken, purple dye plant is the red fragrant thoroughwort that comes into leaves, and is crushed, and adds the water of 10 times of weight,
Be put into homogeneous 5min in homogenizer, homogenization pressure is 30MPa, be subsequently adding cellulase and sodium chloride, purple dye plant with
The weight ratio of cellulase is 1:0.02, purple dye plant is 1 with the weight ratio of sodium chloride:0.005,50h is soaked, boil,
Natural cooling, filtering, obtains purple dye agent；
Black dye：Black-dyeing plant is taken, black-dyeing plant is maple leaf, is crushed, and adds the water of 5 times of weight, is put into
Homogeneous 5min in matter machine, homogenization pressure is 30MPa, is subsequently adding cellulase and sodium chloride, black-dyeing plant and cellulose
The weight ratio of enzyme is 1:0.02, black-dyeing plant is 1 with the weight ratio of sodium chloride:0.005,50h is soaked, filtering obtains black
Coloring agent；
Green coloring agent：Green dyeing plant is taken, green dyeing plant is mulberry leaf, is crushed, and first adds 3 times of water of weight, is added
Cellulase and sodium chloride, green dyeing plant are 1 with the weight ratio of cellulase:0.02, green dyeing plant and sodium chloride
Weight ratio be 1:0.005,7h is soaked, 10 times 50% of ethanol water is added, it is put into homogeneous 5min, homogeneous in homogenizer
Pressure is 30MPa, soaks 30h, and filtering is concentrated under reduced pressure and reclaims ethanol, and thickening temperature is 55 DEG C, and gained concentrate adds hydroxide
Sodium solution, pH is to 7.2 ~ 7.8 for regulation, obtains green coloring agent；
Above-mentioned coloring agent is also separately added into oxidation preventive isoascorbic acid sodium, and the weight of sodium isoascorbate is coloring agent weight
0.1%。
S2. the coloring agent that S1 is obtained is mixed colours, the coloring agent mixed colours is put into overflow dyeing machine, be put into brocade of Zhang nationality use
Line, adds rare earth chloride to carry out first time dyeing, and dyeing temperature is 65 DEG C, and dyeing time is 35min；
S3. to adding sodium chloride to be washed admittedly in overflow dyeing machine, sodium chloride is 1.5 with the feed liquid weight ratio in overflow dyeing machine:100, so
After add rare earth chloride and carry out second dyeing, dyeing temperature is 60 DEG C, and dyeing time is 30min, and second dyeing is completed
Dry afterwards, clean, obtain final product the brocade of Zhang nationality line for having dyeed.
Embodiment 4
A kind of colouring method of brocade of Zhang nationality line, comprises the following steps：
S1. coloring agent is prepared with dyeing plant, the dyeing plant includes yellow dyeing plant, red staining plant, purple dye
Color plant, black-dyeing plant and green dye plant, and preparation process is：
Yellow colorant：Extracting yellow dyes plant, and yellow dyeing plant is Yellow Fructus Gardeniae, is crushed, and adds the water of 20 times of weight, is put into
Homogeneous 15min in homogenizer, homogenization pressure is 20MPa, is subsequently adding cellulase, pectase and sodium chloride, and yellow dyeing is planted
Thing is 1 with the weight ratio of cellulase:0.03, yellow dyeing plant is 1 with the weight ratio of pectase:0.02, yellow dyeing is planted
Thing is 1 with the weight ratio of sodium chloride:0.003,30h is soaked, boil, natural cooling, filter, obtain Yellow colorant；
Red staining agent：Red staining plant is taken, red staining plant is the red fragrant thoroughwort of roundleaf, is crushed, and adds the water of 20 times of weight,
Be put into homogeneous 15min in homogenizer, homogenization pressure is 20MPa, be subsequently adding cellulase and sodium chloride, red staining plant with
The weight ratio of cellulase is 1:0.05, red staining plant is 1 with the weight ratio of sodium chloride:0.003,30h is soaked, boil,
Natural cooling, filtering, obtains red staining agent；
Purple dye agent：Purple dye plant is taken, purple dye plant is the red fragrant thoroughwort that comes into leaves, and is crushed, and adds the water of 20 times of weight,
Be put into homogeneous 15min in homogenizer, homogenization pressure is 20MPa, be subsequently adding cellulase and sodium chloride, purple dye plant with
The weight ratio of cellulase is 1:0.05, purple dye plant is 1 with the weight ratio of sodium chloride:0.003,30h is soaked, boil,
Natural cooling, filtering, obtains purple dye agent；
Black dye：Black-dyeing plant is taken, black-dyeing plant is maple leaf, is crushed, and adds the water of 8 times of weight, is put into
Homogeneous 15min in matter machine, homogenization pressure is 20MPa, is subsequently adding cellulase and sodium chloride, black-dyeing plant and cellulose
The weight ratio of enzyme is 1:0.05, black-dyeing plant is 1 with the weight ratio of sodium chloride:0.003,30h is soaked, filtering obtains black
Coloring agent；
Green coloring agent：Green dyeing plant is taken, green dyeing plant is mulberry leaf, is crushed, and first adds 3 times of water of weight, is added
Cellulase and sodium chloride, green dyeing plant are 1 with the weight ratio of cellulase:0.05, green dyeing plant and sodium chloride
Weight ratio be 1:0.003,5h is soaked, 20 times 60% of ethanol water is added, homogeneous 15min in homogenizer is put into,
Matter pressure is 20MPa, soaks 10h, and filtering is concentrated under reduced pressure and reclaims ethanol, and thickening temperature is 60 DEG C, and gained concentrate adds hydrogen-oxygen
Change sodium solution, pH is to 7.2 ~ 7.8 for regulation, obtains green coloring agent；
Above-mentioned coloring agent is also separately added into oxidation preventive isoascorbic acid sodium, and the weight of sodium isoascorbate is coloring agent weight
0.5%
S2. the coloring agent that S1 is obtained is mixed colours, the coloring agent mixed colours is put into overflow dyeing machine, be put into brocade of Zhang nationality line, plus
Entering rare earth chloride carries out first time dyeing, and dyeing temperature is 65 DEG C, and dyeing time is 35min；
S3. to adding sodium chloride to be washed admittedly in overflow dyeing machine, sodium chloride is 1.5 with the feed liquid weight ratio in overflow dyeing machine:100, so
After add Rare Earth Citric Acid Complexes and carry out second dyeing, dyeing temperature is 60 DEG C, and dyeing time is 30min, second
Dried after the completion of dyeing, cleaned, obtain final product the brocade of Zhang nationality line for having dyeed.
The obtained brocade of Zhang nationality line for having dyeed of above-described embodiment 1 ~ 4, after testing, the dyefastness data of outward appearance and detection are shown in
Following table：
Claims (9)
1. a kind of colouring method of brocade of Zhang nationality line, it is characterised in that comprise the following steps：
S1. coloring agent is prepared with dyeing plant, the dyeing plant includes yellow dyeing plant, red staining plant, purple dye
Color plant, black-dyeing plant and green dye plant, and preparation process is：
Yellow colorant：Extracting yellow dyes plant, and the yellow dyeing plant is Yellow Fructus Gardeniae or big yellow ginger, is crushed, and adds weight 8
~ 20 times of water, is subsequently adding cellulase, pectase and sodium chloride, and yellow dyeing plant is 1 with the weight ratio of cellulase:
0.01 ~ 0.03, yellow dyeing plant is 1 with the weight ratio of pectase:0.005 ~ 0.02, yellow dyes the weight of plant and sodium chloride
Amount is than being 1:0.001 ~ 0.005,30 ~ 50h is soaked, boil, natural cooling, filter, obtain Yellow colorant；
Red staining agent：Red staining plant is taken, the red staining plant is the red fragrant thoroughwort of roundleaf, is crushed, and adds weight 8 ~ 20
Water again, is subsequently adding cellulase and sodium chloride, and red staining plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05,
Red staining plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,30 ~ 50h is soaked, boil, natural cooling, filter, obtain
Red staining agent；
Purple dye agent：Purple dye plant is taken, the purple dye plant is the red fragrant thoroughwort that comes into leaves, and is crushed, and adds weight 5 ~ 20
Water again, is subsequently adding cellulase and sodium chloride, and purple dye plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05,
Purple dye plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,30 ~ 50h is soaked, boil, natural cooling, filter, obtain
Purple dye agent；
Black dye：Black-dyeing plant is taken, the black-dyeing plant is maple leaf, is crushed, and adds the water of 3 ~ 8 times of weight,
Cellulase and sodium chloride are subsequently adding, black-dyeing plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05, black-dyeing
Plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,30 ~ 50h is soaked, filtering obtains black dye；
Green coloring agent：Green dyeing plant is taken, the green dyeing plant is mulberry leaf, is crushed, and first adds 2 ~ 3 times of weight
Water, adds cellulase and sodium chloride, and green dyeing plant is 1 with the weight ratio of cellulase:0.01 ~ 0.05, green dyeing
Plant is 1 with the weight ratio of sodium chloride:0.001 ~ 0.005,5 ~ 10h is soaked, 8 ~ 20 times 50 ~ 70% of ethanol water is added,
10 ~ 30h of immersion, filtering is concentrated under reduced pressure and reclaims ethanol, and gained concentrate adds sodium hydroxide solution, and pH is to 7.2 ~ 7.8 for regulation,
Obtain green coloring agent；
S2. the coloring agent that S1 is obtained is mixed colours, the coloring agent mixed colours is put into overflow dyeing machine, be put into brocade of Zhang nationality line, plus
Entering mordant carries out first time dyeing；
S3. to adding color fixing agent to be washed admittedly in overflow dyeing machine, then adding mordant carries out second dyeing, second dyeing
After the completion of drying, clean, obtain final product the brocade of Zhang nationality line for having dyeed.
2. the colouring method of brocade of Zhang nationality line according to claim 1, it is characterised in that：
In the step S1, yellow dyeing plant, red staining plant, purple dye plant, black-dyeing plant and green dye
Color plant is crushed after addition water respectively, is also put into 5 ~ 15min of homogeneous in homogenizer, and homogenization pressure is 20 ~ 30MPa.
3. the colouring method of brocade of Zhang nationality line according to claim 1, it is characterised in that：
In the step S1, the Yellow colorant, red staining agent, purple dye agent, black dye and green dye are obtained
After color plant, antioxidant is also separately added into, the weight of antioxidant is coloring agent weight 0.1 ~ 0.5%.
4. the colouring method of brocade of Zhang nationality line according to claim 1, it is characterised in that：
In the step S2 and S3, the mordant is rare earth mordant.
5. the colouring method of brocade of Zhang nationality line according to claim 1, it is characterised in that：
The color fixing agent is sodium chloride, and sodium chloride is 1 ~ 3 with the feed liquid weight ratio in overflow dyeing machine:100.
6. the colouring method of brocade of Zhang nationality line according to claim 1, it is characterised in that：
In the step S2, the temperature of dyeing is 50 ~ 70 DEG C, and dyeing time is 20 ~ 40min.
7. the colouring method of brocade of Zhang nationality line according to claim 1, it is characterised in that：
In the step S2, the temperature of dyeing is 50 ~ 60 DEG C, and dyeing time is 15 ~ 30min.
8. the colouring method of brocade of Zhang nationality line according to claim 4, it is characterised in that：
The rare earth mordant is the one kind in rare earth chloride, rare earth oxide, Rare Earth Citric Acid Complexes.
9. the colouring method of brocade of Zhang nationality line according to claim 3, it is characterised in that：
The antioxidant is sodium ascorbate or sodium isoascorbate.
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| CN109610198A (en) * | 2018-12-22 | 2019-04-12 | 张德龙 | It is a kind of using maple leaf as the linen colouring method of coloring agent |
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