CN108707030A - A kind of preparation method of Special fruit tree composite fertilizer - Google Patents

A kind of preparation method of Special fruit tree composite fertilizer Download PDF

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Publication number
CN108707030A
CN108707030A CN201810846948.7A CN201810846948A CN108707030A CN 108707030 A CN108707030 A CN 108707030A CN 201810846948 A CN201810846948 A CN 201810846948A CN 108707030 A CN108707030 A CN 108707030A
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parts
composite fertilizer
preparation
uniformly mixed
bauxite
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任其松
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Anhui Shucheng Jiu Fu Tian Economic Development Co Ltd
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Anhui Shucheng Jiu Fu Tian Economic Development Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/04Double-superphosphate; Triple-superphosphate; Other fertilisers based essentially on monocalcium phosphate
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Molecular Biology (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of preparation methods of Special fruit tree composite fertilizer, are related to composite fertilizer field;Include the following steps:(1) by crops stalk crushing, lactic acid bacteria, cellulase and water is added, ferments 2-3 days under oxygen-free environment, filtrate is collected in centrifugal filtration after fermentation;(2) above-mentioned filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride, copper sulphate, ammonium chloride, potassium sulfate, sodium nitrate are uniformly mixed, are put into the saturated vapour pressure of sodium hydroxide solution and fumigate;(3) bauxite is added into the mixture after fumigating and is modified edible fungi residue and dejection organic fertilizer, be put into homogenizer and stir, mixing in mixer is put into after stirring, pelletized using spray drying process after mixing, obtained composite fertilizer;Composite fertilizer's trophic structure of preparation is more rich, and compound fertilizer granules are small, and release rate is low, it is not easy to cause nutrient to waste, method is simple, and production efficiency is high, and production cost is low, and fruit yield can be improved by acting on fruit tree.

Description

A kind of preparation method of Special fruit tree composite fertilizer
Technical field:
The present invention relates to composite fertilizer fields, and in particular to a kind of preparation method of Special fruit tree composite fertilizer.
Background technology:
Compound fertilizer refers to the chemical fertilizer containing two or more nutrient, and composite fertilizer has nutrient content high, secondary The advantages that ingredient is few and physical behavior is good improves utilization rate of fertilizer, the stable high yield of crop is promoted to have ten for balance fertilizing Divide important role.
Fruit contains abundant nutriment, both contain multivitamin and inorganic salts, also contain sugar, starch, protein, Fat, organic acid, aromatic substance etc. are growth in humans's development and the necessary substance of nutrition.It is studied according to nutritionist, for each person every year 70~80kg fruits are needed, human normal needs could be met.Many fruits and seed can be used as medicine, and have therapeutic effect.Such as Walnut, lichee, longan etc. are good invigorants;Fruit tree is universal adaptable strong, can not only be planted in Plain, river two Before bank, road, rural area garden behind the house, it can also be grown on sandy wasteland, hills, tidal land and other places, suitable fruit tree is planted in choosing, not only increases warp Ji income, and can prevent erosion, increase green area coverage, regulate the climate, to afforest, beautify, environment purification. With the adjustment of the structure of rural undertaking and the relieving of market for farm products, especially on hills, mountainous region, sandy bare land etc., because of ground system Preferably develop production of fruit trees, can bring considerable benefit, China that there are abundant Fruit Tree Resources to peasant, production of fruit trees is in international city Field has very strong competitiveness, is the important sources that the export of farm produce is earned foreign exchange.
Current composite fertilizer producing process complex process, and grain granulation is big, nutrient loss is fast, and utilization rate is low.
Invention content:
Technical problem to be solved by the present invention lies in provide a kind of preparation method of Special fruit tree composite fertilizer, the preparation side Method is simple for process, and composite fertilizer's trophic structure of preparation is more rich, and compound fertilizer granules are small, and release rate is low, it is not easy to cause nutrient unrestrained Take.
The technical problems to be solved by the invention are realized using technical solution below:
A kind of preparation method of Special fruit tree composite fertilizer, includes the following steps:
(1) by crops stalk crushing, 1% lactic acid bacteria of addition agricultural crop straw weight, 2% cellulase and 2 times Water, ferment 2-3 days under oxygen-free environment, centrifugal filtration after fermentation, collect filtrate;
(2) by above-mentioned filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride, copper sulphate, ammonium chloride, sulfuric acid Potassium, sodium nitrate are uniformly mixed, and are put into 55-65 DEG C, are fumigated in the saturated vapour pressure of the sodium hydroxide solutions of 12-15% mass concentrations 40-50min;
(3) bauxite is added into the mixture after fumigating and is modified edible fungi residue and dejection organic fertilizer, be put into high-speed stirring It mixes and stirs 2-3h in machine under 600-700r/min rotating speeds, mixing in mixer is put into after stirring, using spray drying after mixing Method is pelletized, and composite fertilizer is made.
Each raw material is formed by following parts by weight:Bauxite is modified 100-160 parts of edible fungi residue, dejection organic fertilizer 80- 100 parts, 40-60 parts of urea, 35-55 parts of one-lime phosphate, 20-35 parts of ammonium phosphate, 10-15 parts of molybdenum trisulfate, 16-22 parts of potassium chloride, 13-18 parts of copper sulphate, 22-28 parts of ammonium chloride, 6-10 parts of potassium sulfate, 16-20 parts of sodium nitrate, 28-36 parts of agricultural crop straw.
The preparation method that the bauxite is modified edible fungi residue is:
(1) edible fungi residue is dried, is put into ball mill in 300-400r/min ball milling 20-30min, in pulverizer Powder and lactic acid bacteria, leukonid, water are ground into according to mass ratio 50:1:2:250 are uniformly mixed, in 30-35 DEG C of oxygen-free environment Sediment is collected in middle fermentation 3-4 days, centrifugal filtration after fermentation;
(2) by sediment and bauxite according to mass ratio 20:3 are uniformly mixed, and are dissolved in the quality of 1-1.5 times of mixture weight It in the sulfuric acid of a concentration of 12-15%, is put into reaction kettle at 120-150 DEG C and reacts 8-10h, centrifugal filtration after reaction is spent Ionized water filters cleaning to cleaning solution and is in neutrality;
(3) sediment after cleaning is dissolved in the sodium chloride solution that mass concentration is 6-8%, in 120W, 35 DEG C of ultrasounds 50-60min, centrifugal filtration after ultrasound, clean 4-5 time with deionized water, is put into vacuum drying oven dry, obtained bauxite modification Edible fungi residue.
The preparation method of the dejection organic fertilizer is:
(1) ox, sheep, swine excrement are collected to be uniformly mixed, the saturation of 1-1.5 times of stool weight of mixing is added into mixing excrement Limewash stirs evenly, and impregnates 8-12h, is dried after immersion;
(2) excrement dried is crushed, the lactic acid bacteria of addition stool weight 2%, 0.5% saccharomycete, 1.5% fixed nitrogen Bacterium, 12% zeolite powder and 2 times of water are uniformly mixed, ferment 3-4 days under 33-36 DEG C of oxygen free condition, filtered after fermentation, receive Collect filtrate and filter residue;
(3) by filter residue and iron chloride according to mass ratio 1:1 is uniformly mixed, and is put into homogenizer in 600-700r/min 2-3h is stirred under rotating speed, is put into nitrogen atmosphere stove at 150-200 DEG C sintering 2-3h after stirring, natural cooling after sintering, to mixed Closing addition hydrochloric acid in object makes solution pH value be 6-6.5, stands 3-4h, centrifugal filtration collects sediment, sediment is washed with water To neutrality;
(4) filtrate prepared by the sediment and step (2) prepared step (3) is uniformly mixed, and 4- is aged at 35-40 DEG C Dejection organic fertilizer is made in 5h.
The present invention provides a kind of preparation method of Special fruit tree composite fertilizer, advantage is:
(1) by fermenting crops straws, the fiber hydrolization in crops can be fallen, is converted agricultural crop straw to organic Fertilizer collects filtrate, removes filter residue, the inorganic fertilizers such as filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride is mixed equal It is even, it is put into the conjugation fumigated in sodium hydroxide solution saturated vapour pressure and can increase filtrate and inorganic fertilizer so that inorganic fertilizer is equal Organic nutriment of even combination filtrate is eventually adding bauxite and is modified edible fungi residue and dejection organic fertilizer, with mixer mixing, So that bauxite is modified edible fungi residue and package action is formed to other raw materials, to make composite fertilizer that there is slow release effect, with spraying Grain size prepared by seasoning granulation is small, is conducive to nutrient slow release, and plant recovery of nutrient is high;This method is simple, and production efficiency is high, Production cost is low, and fruit yield can be improved by acting on fruit tree.
(2) bauxite, which is modified edible fungi residue, can activate the activity of edible fungi residue nutritional ingredient, soften edible fungi The nutritional ingredient of slag makes nutritional ingredient slowly, effectively discharge, in its preparation process, first by edible fungi residue ball milling, hair Ferment removes the ingredient of nonnutritive value in bacteria residue, is mixed with bauxite, is put into reaction kettle reaction, makes bauxite excitation battalion Ingredients Active is supported, is finally putting into sodium chloride solution and impregnates, stablizes the structure that bauxite is modified edible fungi residue.
(3) dejection organic fertilizer is handled by specific process, has not only remained the original nutrient of excrement, but also can be with other inorganic fertilizers Material is combined closely, and the globality of composite fertilizer is increased, and extends the sustained release phase.
Specific implementation mode:
In order to make the technical means, the creative features, the aims and the efficiencies achieved by the present invention be easy to understand, tie below Specific embodiment is closed, the present invention is further explained.
Embodiment 1:
A kind of preparation method of Special fruit tree composite fertilizer, includes the following steps:
(1) by crops stalk crushing, 1% lactic acid bacteria of addition agricultural crop straw weight, 2% cellulase and 2 times Water, ferment 2 days under oxygen-free environment, centrifugal filtration after fermentation, collect filtrate;
(2) by above-mentioned filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride, copper sulphate, ammonium chloride, sulfuric acid Potassium, sodium nitrate are uniformly mixed, and are put into 55 DEG C, are fumigated 40min in the saturated vapour pressure of the sodium hydroxide solution of 12% mass concentration;
(3) bauxite is added into the mixture after fumigating and is modified edible fungi residue and dejection organic fertilizer, be put into high-speed stirring It mixes and stirs 2h in machine under 600r/min rotating speeds, mixing in mixer is put into after stirring, pelletized using spray drying process after mixing, Composite fertilizer is made.
Each raw material is formed by following parts by weight:Bauxite is modified 100 parts of edible fungi residue, 80 parts of dejection organic fertilizer, urine 40 parts of element, 35 parts of one-lime phosphate, 20 parts of ammonium phosphate, 10 parts of molybdenum trisulfate, 16 parts of potassium chloride, 13 parts of copper sulphate, 22 parts of ammonium chloride, sulphur 6 parts of sour potassium, 16 parts of sodium nitrate, 28 parts of agricultural crop straw.
Embodiment 2:
A kind of preparation method of Special fruit tree composite fertilizer, includes the following steps:
(1) by crops stalk crushing, 1% lactic acid bacteria of addition agricultural crop straw weight, 2% cellulase and 2 times Water, ferment 3 days under oxygen-free environment, centrifugal filtration after fermentation, collect filtrate;
(2) by above-mentioned filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride, copper sulphate, ammonium chloride, sulfuric acid Potassium, sodium nitrate are uniformly mixed, and are put into 65 DEG C, are fumigated 50min in the saturated vapour pressure of the sodium hydroxide solution of 15% mass concentration;
(3) bauxite is added into the mixture after fumigating and is modified edible fungi residue and dejection organic fertilizer, be put into high-speed stirring It mixes and stirs 3h in machine under 700r/min rotating speeds, mixing in mixer is put into after stirring, pelletized using spray drying process after mixing, Composite fertilizer is made.
Each raw material is formed by following parts by weight:Bauxite is modified 160 parts of edible fungi residue, 100 parts of dejection organic fertilizer, urine 60 parts of element, 55 parts of one-lime phosphate, 35 parts of ammonium phosphate, 15 parts of molybdenum trisulfate, 22 parts of potassium chloride, 18 parts of copper sulphate, 28 parts of ammonium chloride, sulphur 10 parts of sour potassium, 20 parts of sodium nitrate, 36 parts of agricultural crop straw.
The preparation method that the bauxite is modified edible fungi residue is:
(1) edible fungi residue is dried, is put into ball mill in 300r/min ball milling 20min, is ground into pulverizer Powder and lactic acid bacteria, leukonid, water are according to mass ratio 50:1:2:250 are uniformly mixed, and ferment 3 in 30 DEG C of oxygen-free environments It, sediment is collected in centrifugal filtration after fermentation;
(2) by sediment and bauxite according to mass ratio 20:3 are uniformly mixed, and are dissolved in the mass concentration of 1 times of mixture weight In 12% sulfuric acid, to be put into reaction kettle at 120 DEG C and reacting 8h, centrifugal filtration after reaction is filtered with deionized water and is cleaned It is in neutrality to cleaning solution;
(3) sediment after cleaning is dissolved in the sodium chloride solution that mass concentration is 6%, in 120W, 35 DEG C of ultrasounds 50min, centrifugal filtration after ultrasound, clean 4 times with deionized water, is put into vacuum drying oven dry, bauxite is made is modified and eat Bacterium bacteria residue.
Embodiment 3:
A kind of preparation method of Special fruit tree composite fertilizer, includes the following steps:
(1) by crops stalk crushing, 1% lactic acid bacteria of addition agricultural crop straw weight, 2% cellulase and 2 times Water, ferment 2 days under oxygen-free environment, centrifugal filtration after fermentation, collect filtrate;
(2) by above-mentioned filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride, copper sulphate, ammonium chloride, sulfuric acid Potassium, sodium nitrate are uniformly mixed, and are put into 60 DEG C, are fumigated 44min in the saturated vapour pressure of the sodium hydroxide solution of 13% mass concentration;
(3) bauxite is added into the mixture after fumigating and is modified edible fungi residue and dejection organic fertilizer, be put into high-speed stirring It mixes and stirs 2h in machine under 630r/min rotating speeds, mixing in mixer is put into after stirring, pelletized using spray drying process after mixing, Composite fertilizer is made.
Each raw material is formed by following parts by weight:Bauxite is modified 120 parts of edible fungi residue, 90 parts of dejection organic fertilizer, urine 50 parts of element, 45 parts of one-lime phosphate, 25 parts of ammonium phosphate, 12 parts of molybdenum trisulfate, 18 parts of potassium chloride, 15 parts of copper sulphate, 24 parts of ammonium chloride, sulphur 8 parts of sour potassium, 18 parts of sodium nitrate, 30 parts of agricultural crop straw.
The preparation method of the dejection organic fertilizer is:
(1) ox, sheep, swine excrement are collected to be uniformly mixed, the saturation lime of 1 times of stool weight of mixing is added into mixing excrement Water stirs evenly, and impregnates 8h, is dried after immersion;
(2) excrement dried is crushed, the lactic acid bacteria of addition stool weight 2%, 0.5% saccharomycete, 1.5% fixed nitrogen Bacterium, 12% zeolite powder and 2 times of water are uniformly mixed, ferment 3 days under 33 DEG C of oxygen free conditions, filtered after fermentation, collect filtrate And filter residue;
(3) by filter residue and iron chloride according to mass ratio 1:1 is uniformly mixed, and is put into homogenizer in 600r/min rotating speeds Lower stirring 2h is put into nitrogen atmosphere stove sintering 2h, natural cooling after sintering at 150 DEG C and salt is added into mixture after stirring Acid makes solution pH value be 6, stands 3h, and centrifugal filtration collects sediment, sediment is washed with water to neutrality;
(4) filtrate prepared by the sediment and step (2) prepared step (3) is uniformly mixed, and 4h is aged at 35 DEG C, makes Obtain dejection organic fertilizer.
Embodiment 4:
A kind of preparation method of Special fruit tree composite fertilizer, includes the following steps:
(1) by crops stalk crushing, 1% lactic acid bacteria of addition agricultural crop straw weight, 2% cellulase and 2 times Water, ferment 2 days under oxygen-free environment, centrifugal filtration after fermentation, collect filtrate;
(2) by above-mentioned filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride, copper sulphate, ammonium chloride, sulfuric acid Potassium, sodium nitrate are uniformly mixed, and are put into 60 DEG C, are fumigated 50min in the saturated vapour pressure of the sodium hydroxide solution of 14% mass concentration;
(3) bauxite is added into the mixture after fumigating and is modified edible fungi residue and dejection organic fertilizer, be put into high-speed stirring It mixes and stirs 3h in machine under 680r/min rotating speeds, mixing in mixer is put into after stirring, pelletized using spray drying process after mixing, Composite fertilizer is made.
Each raw material is formed by following parts by weight:Bauxite is modified 140 parts of edible fungi residue, 95 parts of dejection organic fertilizer, urine 55 parts of element, 50 parts of one-lime phosphate, 30 parts of ammonium phosphate, 14 parts of molybdenum trisulfate, 20 parts of potassium chloride, 17 parts of copper sulphate, 26 parts of ammonium chloride, sulphur 9 parts of sour potassium, 19 parts of sodium nitrate, 32 parts of agricultural crop straw.
The preparation method that the bauxite is modified edible fungi residue is:
(1) edible fungi residue is dried, is put into ball mill in 400r/min ball milling 30min, is ground into pulverizer Powder and lactic acid bacteria, leukonid, water are according to mass ratio 50:1:2:250 are uniformly mixed, and ferment 4 in 35 DEG C of oxygen-free environments It, sediment is collected in centrifugal filtration after fermentation;
(2) by sediment and bauxite according to mass ratio 20:3 are uniformly mixed, and the quality for being dissolved in 1.5 times of mixture weight is dense Degree is in 15% sulfuric acid, is put into reaction kettle at 150 DEG C and reacts 10h, centrifugal filtration after reaction, is filtered with deionized water clear Cleaning solution is washed till to be in neutrality;
(3) sediment after cleaning is dissolved in the sodium chloride solution that mass concentration is 8%, in 120W, 35 DEG C of ultrasounds 60min, centrifugal filtration after ultrasound, clean 5 times with deionized water, is put into vacuum drying oven dry, bauxite is made is modified and eat Bacterium bacteria residue.
The preparation method of the dejection organic fertilizer is:
(1) ox, sheep, swine excrement are collected to be uniformly mixed, the saturation stone of 1.5 times of stool weight of mixing is added into mixing excrement Buck stirs evenly, and impregnates 12h, is dried after immersion;
(2) excrement dried is crushed, the lactic acid bacteria of addition stool weight 2%, 0.5% saccharomycete, 1.5% fixed nitrogen Bacterium, 12% zeolite powder and 2 times of water are uniformly mixed, ferment 4 days under 36 DEG C of oxygen free conditions, filtered after fermentation, collect filtrate And filter residue;
(3) by filter residue and iron chloride according to mass ratio 1:1 is uniformly mixed, and is put into homogenizer in 700r/min rotating speeds Lower stirring 3h is put into nitrogen atmosphere stove sintering 3h, natural cooling after sintering at 200 DEG C and salt is added into mixture after stirring Acid makes solution pH value be 6.5, stands 4h, and centrifugal filtration collects sediment, sediment is washed with water to neutrality;
(4) filtrate prepared by the sediment and step (2) prepared step (3) is uniformly mixed, and 5h is aged at 40 DEG C, makes Obtain dejection organic fertilizer.
Comparative example:
A kind of Special fruit tree composite fertilizer, in parts by weight, including following components:
10 parts of plant ash, 10 parts of chitosan,
2 parts of humic acid, 5 parts of grouts,
10 parts of urea, 5 parts of potassium nitrate,
2 parts of calcium superphosphate, 1 part of water-retaining agent,
2 parts of nitrobacteria, 2 parts of achromobacter,
10 parts of deionized water, 2 parts of dispersant.
Preparation method includes the following steps:
(1) 10 parts of plant ash, 10 parts of chitosans, 5 portions of grouts and 5 parts of deionized waters are mixed evenly, are added 2 parts points Powder, 1 part of water-retaining agent, ultrasonic 40min obtain mixed slurry;
(2) 10 parts of urea, 2 parts of humic acids, 5 parts of potassium nitrate, 2 parts of calcium superphosphate and 5 parts of deionized waters are mixed, stirring is extremely Solid dissolves to obtain fertilizer solution;
(3) 2 parts of nitrobacterias, 2 parts of achromobacters are placed in the culture medium of culture solution, expand after numerous proliferation spend from Sub- water dilutes 180 times, obtains microbial inoculum;
(4) by the fertilizer solution that mixed slurry that step (1) obtains, step (2) obtain and the microorganism that step (3) obtains Bacterium solution is mixed evenly, and obtains Special fruit tree composite fertilizer.
Composite fertilizer prepared by the above various embodiments and comparative example is acted on to the different zones in an apple orchard, it is each to implement Example and comparative example administration area are one mu, and apply fertilizer 120 kg per acre, after applying fertilizer 2 months, detect the remaining of fertilizer in soil Apple production is detected after rate and ripe apples, it is as a result as follows:
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (4)

1. a kind of preparation method of Special fruit tree composite fertilizer, which is characterized in that include the following steps:
(1) by crops stalk crushing, 1% lactic acid bacteria of agricultural crop straw weight, 2% cellulase and 2 times of water is added, It ferments 2-3 days under oxygen-free environment, filtrate is collected in centrifugal filtration after fermentation;
(2) by above-mentioned filtrate and urea, one-lime phosphate, ammonium phosphate, molybdenum trisulfate, potassium chloride, copper sulphate, ammonium chloride, potassium sulfate, nitre Sour sodium is uniformly mixed, and is put into 55-65 DEG C, is fumigated 40- in the saturated vapour pressure of the sodium hydroxide solutions of 12-15% mass concentrations 50min;
(3) bauxite is added into the mixture after fumigating and is modified edible fungi residue and dejection organic fertilizer, be put into homogenizer In 2-3h is stirred under 600-700r/min rotating speeds, mixing in mixer is put into after stirring, after mixing using spray drying legal system Composite fertilizer is made in grain.
2. the preparation method of Special fruit tree composite fertilizer according to claim 1, which is characterized in that each raw material presses following weight Number forms:Bauxite is modified 100-160 parts of edible fungi residue, 80-100 parts of dejection organic fertilizer, 40-60 parts of urea, phosphoric acid one 35-55 parts of calcium, 20-35 parts of ammonium phosphate, 10-15 parts of molybdenum trisulfate, 16-22 parts of potassium chloride, 13-18 parts of copper sulphate, ammonium chloride 22-28 Part, 6-10 parts of potassium sulfate, 16-20 parts of sodium nitrate, 28-36 parts of agricultural crop straw.
3. the preparation method of Special fruit tree composite fertilizer according to claim 1, which is characterized in that the bauxite is modified food Preparation method with bacterium bacteria residue is:
(1) edible fungi residue is dried, is put into ball mill in 300-400r/min ball milling 20-30min, is crushed in pulverizer At powder and lactic acid bacteria, leukonid, water according to mass ratio 50:1:2:250 are uniformly mixed, and are sent out in 30-35 DEG C of oxygen-free environment Sediment is collected in ferment 3-4 days, centrifugal filtration after fermentation;
(2) by sediment and bauxite according to mass ratio 20:3 are uniformly mixed, and are dissolved in the mass concentration of 1-1.5 times of mixture weight In the sulfuric acid of 12-15%, to be put into reaction kettle at 120-150 DEG C and reacting 8-10h, deionization is used in centrifugal filtration after reaction Water filters cleaning to cleaning solution and is in neutrality;
(3) sediment after cleaning is dissolved in the sodium chloride solution that mass concentration is 6-8%, in 120W, 35 DEG C of ultrasound 50- 60min, centrifugal filtration after ultrasound, clean 4-5 time with deionized water, is put into vacuum drying oven dry, and bauxite modification is made and eats With bacterium bacteria residue.
4. the preparation method of Special fruit tree composite fertilizer according to claim 1, which is characterized in that the dejection organic fertilizer Preparation method is:
(1) ox, sheep, swine excrement are collected to be uniformly mixed, the saturation lime of 1-1.5 times of stool weight of mixing is added into mixing excrement Water stirs evenly, and impregnates 8-12h, is dried after immersion;
(2) excrement dried is crushed, be added the lactic acid bacteria of stool weight 2%, 0.5% saccharomycete, 1.5% nitrogen-fixing bacteria, 12% zeolite powder and 2 times of water are uniformly mixed, ferment 3-4 days under 33-36 DEG C of oxygen free condition, filtered after fermentation, collect filter Liquid and filter residue;
(3) by filter residue and iron chloride according to mass ratio 1:1 is uniformly mixed, and is put into homogenizer in 600-700r/min rotating speeds Lower stirring 2-3h is put into nitrogen atmosphere stove sintering 2-3h, natural cooling after sintering, to mixture at 150-200 DEG C after stirring Middle addition hydrochloric acid makes solution pH value be 6-6.5, stands 3-4h, and centrifugal filtration collects sediment, sediment is washed with water into Property;
(4) filtrate prepared by the sediment and step (2) prepared step (3) is uniformly mixed, and 4-5h is aged at 35-40 DEG C, Dejection organic fertilizer is made.
CN201810846948.7A 2018-07-27 2018-07-27 A kind of preparation method of Special fruit tree composite fertilizer Withdrawn CN108707030A (en)

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CN110577420A (en) * 2019-09-02 2019-12-17 李红佑 Special fertilizer for fruit trees and preparation method thereof

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