CN108699240B - 制备基于呋喃的聚酰胺的无溶剂熔融缩聚方法 - Google Patents

制备基于呋喃的聚酰胺的无溶剂熔融缩聚方法 Download PDF

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CN108699240B
CN108699240B CN201680081896.8A CN201680081896A CN108699240B CN 108699240 B CN108699240 B CN 108699240B CN 201680081896 A CN201680081896 A CN 201680081896A CN 108699240 B CN108699240 B CN 108699240B
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diamines
polyamide
furan
reaction mixture
acid
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CN108699240A (zh
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S.帕彻
S.N.巴尔
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Ruixun Co ltd
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Ruixun Co ltd
EI Du Pont de Nemours and Co
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/40Polyamides containing oxygen in the form of ether groups
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/06Halogens; Compounds thereof
    • B01J27/08Halides
    • B01J27/10Chlorides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14Phosphorus; Compounds thereof
    • B01J27/16Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr
    • B01J27/18Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr with metals other than Al or Zr
    • B01J27/1802Salts or mixtures of anhydrides with compounds of other metals than V, Nb, Ta, Cr, Mo, W, Mn, Tc, Re, e.g. phosphates, thiophosphates
    • B01J27/1806Salts or mixtures of anhydrides with compounds of other metals than V, Nb, Ta, Cr, Mo, W, Mn, Tc, Re, e.g. phosphates, thiophosphates with alkaline or alkaline earth metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/20Carbon compounds
    • B01J27/232Carbonates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0201Oxygen-containing compounds
    • B01J31/0211Oxygen-containing compounds with a metal-oxygen link
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C49/00Blow-moulding, i.e. blowing a preform or parison to a desired shape within a mould; Apparatus therefor
    • B29C49/0005Blow-moulding, i.e. blowing a preform or parison to a desired shape within a mould; Apparatus therefor characterised by the material
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16Dicarboxylic acids and dihydroxy compounds
    • C08G63/18Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181Acids containing aromatic rings
    • C08G63/183Terephthalic acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/66Polyesters containing oxygen in the form of ether groups
    • C08G63/668Polyesters containing oxygen in the form of ether groups derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/672Dicarboxylic acids and dihydroxy compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • C08G63/82Preparation processes characterised by the catalyst used
    • C08G63/85Germanium, tin, lead, arsenic, antimony, bismuth, titanium, zirconium, hafnium, vanadium, niobium, tantalum, or compounds thereof
    • C08G63/86Germanium, antimony, or compounds thereof
    • C08G63/866Antimony or compounds thereof
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/26Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
    • C08G69/28Preparatory processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/26Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
    • C08G69/28Preparatory processes
    • C08G69/30Solid state polycondensation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2067/00Use of polyesters or derivatives thereof, as moulding material
    • B29K2067/003PET, i.e. poylethylene terephthalate
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2995/00Properties of moulding materials, reinforcements, fillers, preformed parts or moulds
    • B29K2995/0037Other properties
    • B29K2995/0065Permeability to gases
    • B29K2995/0067Permeability to gases non-permeable
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29LINDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
    • B29L2031/00Other particular articles
    • B29L2031/712Containers; Packaging elements or accessories, Packages
    • B29L2031/7158Bottles
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2230/00Compositions for preparing biodegradable polymers

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Polyamides (AREA)
CN201680081896.8A 2015-12-15 2016-12-15 制备基于呋喃的聚酰胺的无溶剂熔融缩聚方法 Active CN108699240B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562267344P 2015-12-15 2015-12-15
US62/267344 2015-12-15
PCT/US2016/066761 WO2017106405A1 (en) 2015-12-15 2016-12-15 A solvent-free melt polycondensation process of making furan-based polyamides

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CN108699240A CN108699240A (zh) 2018-10-23
CN108699240B true CN108699240B (zh) 2024-06-25

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US (4) US20180371167A1 (enExample)
EP (1) EP3390495A1 (enExample)
JP (2) JP6905983B2 (enExample)
KR (1) KR20180093026A (enExample)
CN (1) CN108699240B (enExample)
AU (3) AU2016370673A1 (enExample)
CA (1) CA3006986C (enExample)
MX (1) MX2018007279A (enExample)
WO (1) WO2017106405A1 (enExample)

Families Citing this family (11)

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Publication number Priority date Publication date Assignee Title
CN110256668B (zh) * 2019-06-04 2021-12-10 中国科学技术大学 高分子量呋喃基芳香聚酰胺及其制备方法和应用
CN111234207A (zh) * 2020-03-04 2020-06-05 东华大学 一种透明生物基聚酰胺及其制备方法
CN111961199B (zh) * 2020-09-02 2022-01-28 中国科学院宁波材料技术与工程研究所 生物基耐高温聚酰胺复合材料、其制备方法及应用
CN111995746B (zh) * 2020-09-02 2022-01-28 中国科学院宁波材料技术与工程研究所 生物基耐高温聚酰胺复合材料、其低温预缩聚制法及应用
CN112111058B (zh) * 2020-10-16 2022-07-05 天津工业大学 一种呋喃二甲酸二胺高聚物的制备方法
CN113429569B (zh) * 2021-07-23 2022-08-16 四川大学 一种高分子量呋喃聚酰胺的制备方法
CN113896886B (zh) * 2021-09-24 2023-07-25 珠海万通特种工程塑料有限公司 一种呋喃二酸基聚酰胺及其制备方法和一种呋喃二酸基聚酰胺组合物
CN116082634B (zh) * 2022-12-30 2025-05-23 安徽利科新材料科技有限公司 磺酸基改性呋喃基聚酰胺及其制备方法及装置
CN116815344B (zh) * 2023-08-29 2023-11-21 泰和新材集团股份有限公司 一种生物基聚酰胺纤维及其制备方法
EP4582466A1 (en) 2024-01-05 2025-07-09 Arkema France Process for the manufacture of semi-aromatic polyamides
CN118745245B (zh) * 2024-07-19 2025-10-31 南京工业大学 一种呋喃基聚酰胺及其制备方法

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CN101456949A (zh) * 2007-12-14 2009-06-17 金发科技股份有限公司 一种半芳香族聚酰胺及其制备方法
WO2015060718A1 (en) * 2013-10-21 2015-04-30 Furanix Technologies B.V. Process for preparing a furan-based polyamide, a furan-based oligomer and compositions and articles comprising the furan-based polyamide

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JP5812791B2 (ja) * 2011-03-28 2015-11-17 キヤノン株式会社 プリンター、複写機
JP6185981B2 (ja) * 2012-03-30 2017-08-23 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company フラン系ポリアミド
KR101465466B1 (ko) * 2013-02-12 2014-11-27 한국과학기술연구원 고상중합 방법을 이용한 바이오매스 유래 퓨란계 코폴리아미드의 제조방법
JP6168985B2 (ja) * 2013-12-24 2017-07-26 花王株式会社 接着剤
DK3137547T3 (da) * 2014-05-01 2023-09-18 Covation Inc Transesterificerede furanbaserede polyestere og genstand fremstillet deraf
PL3307515T3 (pl) * 2015-06-11 2021-06-28 Dupont Industrial Biosciences Usa, Llc Zwiększona wydajność bariery dzięki mieszankom poli(furandikarboksylanu etylenu) i poli(tereftalanu etylenu)
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CN101456949A (zh) * 2007-12-14 2009-06-17 金发科技股份有限公司 一种半芳香族聚酰胺及其制备方法
WO2015060718A1 (en) * 2013-10-21 2015-04-30 Furanix Technologies B.V. Process for preparing a furan-based polyamide, a furan-based oligomer and compositions and articles comprising the furan-based polyamide

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JP2018537573A (ja) 2018-12-20
WO2017106405A1 (en) 2017-06-22
US20210108032A1 (en) 2021-04-15
EP3390495A1 (en) 2018-10-24
US20230212354A1 (en) 2023-07-06
AU2023202677A1 (en) 2023-05-18
KR20180093026A (ko) 2018-08-20
CA3006986A1 (en) 2017-06-22
CN108699240A (zh) 2018-10-23
US20180371167A1 (en) 2018-12-27
JP7296427B2 (ja) 2023-06-22
JP2021152183A (ja) 2021-09-30
AU2016370673A1 (en) 2018-06-14
CA3006986C (en) 2024-01-02
AU2021203972A1 (en) 2021-07-08
JP6905983B2 (ja) 2021-07-21
US20200283577A1 (en) 2020-09-10
MX2018007279A (es) 2018-09-06

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