CN108640802A - A kind of matrimony vine special fertilizer of resisting drought saving water and preparation method thereof - Google Patents
A kind of matrimony vine special fertilizer of resisting drought saving water and preparation method thereof Download PDFInfo
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- CN108640802A CN108640802A CN201810910509.8A CN201810910509A CN108640802A CN 108640802 A CN108640802 A CN 108640802A CN 201810910509 A CN201810910509 A CN 201810910509A CN 108640802 A CN108640802 A CN 108640802A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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Abstract
The invention discloses matrimony vine special fertilizers of a kind of resisting drought saving water and preparation method thereof, the matrimony vine special fertilizer is using nanometer soil material as carrier, organic matter, zeolite powder and other matrimony vines growth needed nutrient matter substep is added to carry out hybrid process and be made, its need fertilizer curve that can be grown according to matrimony vine discharges suitable nutriment, improve the drought resisting heat-resisting ability of matrimony vine, the usage amount of water resource is reduced, while improving the quality and yield of matrimony vine.
Description
Technical field
The present invention relates to matrimony vine planting technology fields, more particularly, to a kind of matrimony vine special fertilizer of resisting drought saving water and its preparation
Method.
Background technology
Matrimony vine happiness water is again afraid of water, therefore water management occupies an important position in its production management.Pour water 10 the matrimony vine anniversary
It is secondary or so, year irrigation quantity be 7350-8250 cubic metres/hectare.In recent years, with the continuous aggravation of water resource pressure,
Traditional irrigation principle on the basis of method, there has been proposed many new concepts and method, as limited irrigation, it is non-fully
Irrigation and deficit irrigation etc., the proposition of these concepts and method are implemented, water-saving excellent to irrigating steering by traditional abundance of water high yield type
Production type is irrigated, or according to physiological function of plants, it is believed that is carried out water deficit processing to the crop a certain stage, is controlled plant root cap
Than promoting the growth of the formation and fruit of later stage plant seed, improving efficiency of water application and play positive effect.But these
Method only considers to carry out readjust-loss to water in time and optimization distributes, and there is no consider root system of plant to improving water utilization
The effect of efficiency.On this basis, the relationship and root system that people open according to the rising dehydration of crop with Stoma of Leaves are to carrying
The physiological function of high-moisture utilization ratio, it is proposed that the farmland water-saving of controlled alternate irrigation regulates and controls thinking, but due to needing
Continuous adjustment irrigation position, increases the technical difficulty of irrigation, significantly increases labour cost, be not easy to promote.Cause
This, carries out the water-saving culture Study of way of matrimony vine, gives full play to its drought resisting potential, is reduced while improving efficiency of water application
Production cost, maintaining existing wolfberry industry development and further expansion to develop wolfberry industry many water-deficient areas has weight
Want realistic meaning.
Effect of the calcium in plant is mainly physiology of balance activity, and cell wall and born of the same parents are participated in the form of Calcium Pectate
The synthesis of interbed and the movable adjusting of related enzyme.Calcium ion can connect phosphatide, phosphate and protein carboxyl on cell membrane
Improve biological water regime in plant as important membrane protective substance, reduces membrane permeability, improve the water conservation of blade
Ability, maintains the integrality of membrane structure, and increases the ABA contents in plant, the generation of ethylene is reduced, to reduce
Transpiration.Thus, under drought stress conditions, plant leaf blade transpiration rate can be reduced by applying calcium, improve efficiency of water application, be increased
Its strong drought-resistant ability.
Inorganic selenium is generally acknowledged drought resisting element, and inorganic selenium, which mainly passes through, to be reduced free radical injury and improve chlorophyll function etc.
Mode drought resisting high temperature resistance, but for plant, the content of selenium show as the high suppression of low rush (promote plant growth when concentration is low, it is dense
When spending high, inhibit plant growth), and selenium element is extremely low using concentration, and range is also extremely narrow.If not using sustained release and controllable
The technology and material of release first can be in the fertilizer containing selenium is manured into soil by we according to the dosage of advantageous plant growth
In weakly acidic pH to acid soil, forms water-soluble very low oxide or hydrous oxide with iron and be fixed, it is also possible to water
It is lost in and desired effect is not achieved；If sowing amount is excessive, and can cause to poison to plant immediately.So containing the micro of selenium
Element fertilizer mainly uses foliage-spray.But in arid, since manpower condition is limited, it is difficult to timely and effectively supplement, together
Shi Qicong, which is absorbed into play a role, is also required to the regular hour, and therefore, people are more desirable to can have one kind that can keep calcium, selenium etc.
The chemism of drought resisting material, and its effect can be effectively played in special time period, while the nutrient need of matrimony vine can be met again
It asks, and by sustained release and controlled release, the matrimony vine special fertilizer for making it grow and need fertile curve to match with matrimony vine.
Invention content
The present invention provides matrimony vine special fertilizers of a kind of resisting drought saving water and preparation method thereof, are planted with solving existing matrimony vine
In, the problem of grower is difficult the drought resisting potential for accurately controlling the additive amount of selenium, calcium constituent to excite matrimony vine.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention is summarized as follows：
A kind of matrimony vine special fertilizer of resisting drought saving water, includes the component of following parts by weight：Natural nano soil material 30-90
Part, 5-20 parts of zeolite powder, 1-5 parts of calcium nitrate, 0.04-0.07 parts of inorganic selenium salt, 1.2-2.5 parts of vitamin C, organic matter 15-36
Part, 12-30 parts of water, 9-15 parts of urea, 10-15 parts of Diammonium phosphate (DAP), 8-12 parts of potassium sulfate, 1-3 parts of zinc sulfate.
The matrimony vine special fertilizer that grower provides this programme is applied according to conventional fertilizer application method in the soil, in fertilizer
Calcium, plasma selenium can improve the ability that matrimony vine adapts to the poor environments such as high temperature and drought.Wherein, calcium ion can reduce plant leaf blade
Transpiration rate, improve efficiency of water application, enhance the drought-resistant ability of matrimony vine；Inorganic selenium mainly by reduce free radical injury and
Improve the drought resisting high-temperature resistance that the modes such as chlorophyll function improve matrimony vine.In the specific use process, nanometer soil material will
Calcium, plasma selenium are adsorbed on a nanometer interlayer, pass through the factors such as the water content of soil interlayer, temperature, microbial activities and ph values
Comprehensive function discharges calcium, plasma selenium to have the function that resisting drought saving water by different level in different time；Plasma selenium exists simultaneously
The high suppression phenomenon of low rush, and the usable concentration of plasma selenium can further improve by the absorption of nanometer soil material in this programme,
And root system of plant can be protected not injured by high concentration plasma selenium, moreover it is possible to by with different levels release system, plasma selenium and calcium from
The synergistic effect of son, it is maximized to enhance resisting drought saving water ability；And the need fertilizer curve by matching matrimony vine, rational proportioning are supported
Point, play the effect increased production for matrimony vine upgrading.It is not necessarily to constantly to containing calcium, selenium in conclusion the advantages of this programme is grower
Supplement is adjusted in the Fertilizer application amount of ion, you can the drought resisting heat-resisting ability for promoting matrimony vine reduces plantation difficulty, together
When also optimize personnel proportioning, reduce maintenance of plant cost；Meanwhile after applying the fertilizer that this programme provides, nutriment
Release can be carried out with the need fertilizer curve of matrimony vine, improve the quality and yield of matrimony vine.
Further, the matrimony vine special fertilizer of above-mentioned resisting drought saving water includes the component of following parts by weight：Natural nano soil property
30-45 parts of material, 5-10 parts of zeolite powder, 1-5 parts of calcium nitrate, 0.04-0.07 parts of inorganic selenium salt, 1.2-2.5 parts of vitamin C,
15-25 parts of organic matter, 12-20 parts of water, 12-15 parts of urea, 10-15 parts of Diammonium phosphate (DAP), 8-12 parts of potassium sulfate, zinc sulfate 1-3
Part.
Further, the natural nano soil material is in calcium-base bentonite, sodium bentonite, sepiolite and talcum
At least one；Above-mentioned natural nano soil material can increase the solvability of water, improve cell biological permeability, can be to calcium, selenium
Equal nutrients ion is adsorbed.
Further, the inorganic selenium salt is at least one of sodium selenite, potassium selenite；Above two inorganic selenium
Salt is cheap, can save production cost, while potassium ion is also used as the nutritional ingredient of matrimony vine growth, achieves many things at one stroke.
Further, the organic matter is at least one of bacteria residue, plant residue, vinasse and flyash；It is above-mentioned to have
Machine matter is conveniently easy to get, and helps to eliminate Al, Mn, Fe in residual toxicity and heavy metal pollution and the acid medium in soil
Toxicity, improve the growing environment of matrimony vine, promote the quality and yield of matrimony vine.
The preparation method of the matrimony vine special fertilizer of above-mentioned resisting drought saving water, includes the following steps：
S1, natural nano soil material and zeolite powder are uniformly mixed, add water that slurry is made；
S2, after slurry is heated to 45~50 DEG C, calcium nitrate is added, is stirred 45~60min, obtains mixed slurry；
S3, after mixed slurry is heated to 60~75 DEG C, inorganic selenium salt, vitamin C and water is added, it is stirred 30~
45min obtains mixed solution；
Inorganic acid is added in S4, the mixed solution obtained to step S3, it is 6.1~6.5 to adjust solution ph, and urine is added
The mixed liquor of element, Diammonium phosphate (DAP), potassium sulfate, zinc sulfate is mixed 2~3h, obtains mixture；
S5, the obtained mixtures of step S4 are filtered, heated-air drying, crushing, be eventually adding organic matter, be mixed
10-15min is to get to the matrimony vine special fertilizer of resisting drought saving water.
Further, its solid and liquid weight ratio of the slurry in the step S1 is 1:(2-4.5).
Further, it is dense to be configured to quality with water in advance for the mixture of the inorganic selenium salt in the step S3 and vitamin
Degree is the solution of 0.1-0.5%.
Further, the organic acid be carbonic acid, nitrous acid, metaboric acid, sulfuric acid, nitric acid, phosphoric acid, in molybdic acid extremely
Few one kind.
In conclusion by adopting the above-described technical solution, the beneficial effects of the invention are as follows：
1. calcium, plasma selenium can excite the drought resisting high temperature resistant potential of matrimony vine, to promote the drought resisting heat-resisting ability of matrimony vine,
Reduce the consumption of water resource；
2. calcium, plasma selenium are adsorbed on a nanometer interlayer by nanometer soil material, become by factors such as the water content of soil interlayer
Change, discharges calcium, plasma selenium by different level to have the function that resisting drought saving water in different time, both improve the utilization of water resource
Rate also makes the release of calcium, plasma selenium that can be adapted with the growth curve of matrimony vine；
3. the content of plasma selenium for matrimony vine growth there are the high suppression phenomenon of low rush, need to use it in general use
Amount is strictly controlled, and in order to improve the drought-resistant ability of matrimony vine, just needs manually to carry out adjusting supplement in real time, this is for worker
Operational capacity and opportunity control require all high, the growth of matrimony vine will be caused serious injury once control is inaccurate, and
It is added with nanometer soil material in this programme, plasma selenium can be adsorbed, and discharged by different level, make itself and matrimony vine
Growth curve be adapted, can further improve use the concentration of plasma selenium, make it that can promote the growth of matrimony vine, raising Chinese holly
The drought resisting heat-resisting ability of Qi, and matrimony vine root system can be protected not injured by high concentration plasma selenium, moreover it is possible to avoid artificial tune in real time
Save the trouble of supplement so that plantation is more convenient；
4. being used in compounding zeolite powder as slow-release material and organic matter, inorganic nutrients, it is bent to form compound sustained release
Line makes the release of nutriment be adapted with the need fertilizer curve of plant；
5. using nanometer soil material as carrier, addition calcium, plasma selenium and various nutriments, under its coordinated both
Heavy metal ion, pesticide residue in soil etc. can be reduced to injure caused by matrimony vine, and the growth curve of matrimony vine can be coordinated
And fertile curve is needed to provide suitable nutrient for matrimony vine, make matrimony vine that not only there is high drought resisting heat-resisting ability, reduces water resource
Consumption, moreover it is possible to which the growing state for improving matrimony vine has the function that upgrading is increased production.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that described herein, specific examples are only used to explain the present invention, is not used to
The present invention is limited, i.e., described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Therefore, the model of claimed invention is not intended to limit to the detailed description of the embodiment of the present invention below
It encloses, but is merely representative of the selected embodiment of the present invention.Based on the embodiment of the present invention, those skilled in the art are not doing
The every other embodiment obtained under the premise of going out creative work, shall fall within the protection scope of the present invention.
It should be noted that the relational terms of term " first " and " second " or the like be used merely to an entity or
Operation is distinguished with another entity or operation, and without necessarily requiring or implying between these entities or operation, there are any
This actual relationship or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to non-row
His property includes, so that the process, method, article or equipment including a series of elements includes not only those elements, and
And further include other elements that are not explicitly listed, or further include solid by this process, method, article or equipment
Some elements.In the absence of more restrictions, the element limited by sentence "including a ...", it is not excluded that wrapping
Include in the process, method, article or equipment of the element that there is also other identical elements.
The present invention provides a kind of matrimony vine special fertilizer of resisting drought saving water, includes the component of following parts by weight：
Further, the matrimony vine special fertilizer of above-mentioned resisting drought saving water, includes the component of following parts by weight：
Further, the natural nano soil material is in calcium-base bentonite, sodium bentonite, sepiolite and talcum
It is at least one.
Further, the inorganic selenium salt is at least one of sodium selenite, potassium selenite.
Further, the organic matter is at least one of bacteria residue, plant residue, vinasse and flyash.
The present invention also provides the preparation methods of the matrimony vine special fertilizer of above-mentioned resisting drought saving water comprising following steps：
S1, natural nano soil material and zeolite powder are uniformly mixed, add water that slurry is made；
S2, after slurry is heated to 45~50 DEG C, calcium nitrate is added, is stirred 45~60min, obtains mixed slurry；
S3, after mixed slurry is heated to 60~75 DEG C, inorganic selenium salt, vitamin C and water is added, it is stirred 30~
45min obtains mixed solution；
Inorganic acid is added in S4, the mixed solution obtained to step S3, it is 6.1~6.5 to adjust solution ph, and urine is added
The mixed liquor of element, Diammonium phosphate (DAP), potassium sulfate, zinc sulfate is mixed 2~3h, obtains mixture；
S5, the obtained mixtures of step S4 are filtered, heated-air drying, crushing, be eventually adding organic matter, be mixed
10-15min is to get to the matrimony vine special fertilizer of resisting drought saving water, wherein when using heated-air drying, by the mixture after heated-air drying
In water parts by weight control at 12-30 parts.
Further, its solid and liquid weight ratio of the slurry in the step S1 is 1:2-4.5.
Further, the mixture of the inorganic selenium salt in the step S3 and vitamin is configured to mass concentration with water in advance
For the solution of 0.1-0.5%.
Further, the organic acid be carbonic acid, nitrous acid, metaboric acid, sulfuric acid, nitric acid, phosphoric acid, in molybdic acid at least
It is a kind of.
Embodiment 1
The weight of component used is as follows in the present embodiment：
Said components are prepared to the matrimony vine special fertilizer of resisting drought saving water according to preparation method provided by the invention.
Embodiment 2
The weight of component used is as follows in the present embodiment：
Said components are prepared to the matrimony vine special fertilizer of resisting drought saving water according to preparation method provided by the invention.
Embodiment 3
The weight of component used is as follows in the present embodiment：
Said components are prepared to the matrimony vine special fertilizer of resisting drought saving water according to preparation method provided by the invention.
Embodiment 4
The weight of component used is as follows in the present embodiment：
Said components are prepared to the matrimony vine special fertilizer of resisting drought saving water according to preparation method provided by the invention.
Comparative example
Three kinds of urea, Diammonium phosphate (DAP), potassium sulfate fertilizer are selected to carry out composite application, the wherein active ingredient of urea to matrimony vine
Content is 46%, and the active constituent content of diammonium is 46%, and the active constituent content of potassium sulfate is 50%.
Test method
Testing site is located at seven groups, the roads Ning'an Zhen Wa Li Jiaqiang tri- ages wolfberry orchards, 229 ㎜ of the base annual rainfall, evaporation capacity
2129.7 ㎜ are 9.3 times of annual rainfall, and drought is short of rain, evaporation is strong, illumination is sufficient, and day and night temperature is big, weather item
Part is particularly well suited for matrimony vine growth and development, and the accumulation of fruit nutrient and system are dry.
Tested in 2017, test selection matrimony vine kind be peaceful Qi 1,5 age of the age of tree, 220 plants of planting density/
Mu, seeding row spacing 1m × 3m, items management is fine consistent, only applies the matrimony vine special fertilizer and comparative example of embodiment 1-4 respectively
The irrigation amount of fertilizer and embodiment 1-4 are the 80% of control row.In fertilising, each fertilizer of each testing site is handled respectively
60 plants；Wherein 5 progress of fertilising point, fertilising for the first time is before April 30, and before June 5, third time is applied fertilizer for second of fertilising
Before June 30, the 4th fertilising is before July 30, and the 5th fertilising is before August 30 days.And to each dose and examination
Irrigation amount is recorded during testing；Meanwhile the fertility respectively at 25-July 10 June, September 20-October 11 to matrimony vine
Index is recorded, wherein when recording, embodiment 1-4 and comparative example are numbered according to 1-5 respectively.
Following table is fertilising and irrigation amount data record：
Each age fertilizing, watering quantity table of 1 point of table
Following table is matrimony vine Growth Character summary sheet：
2 Growth Character summary sheet of table
Following table is that matrimony vine production fruit character contrast table is weighed with 100 fruits together wherein when being weighed for fruit again,
And weigh 3 times and be averaged, and fruit weight unit is g/ in table 3：
Table 3 produces fruit character contrast table
After applying matrimony vine special fertilizer of the present invention as can be seen from Table 1, compared with comparative example, 20% irrigation amount has been saved,
It comes once being promoted, a large amount of water resource can be saved by just cultivating this part from matrimony vine every year, can be largely
Alleviate the situation of current water resource anxiety, while also improving the heat safe ability of matrimony vine drought resisting so that the environment of matrimony vine adapts to
Ability is stronger.
From table 2 it can be seen that relative to comparative example, seven cun of branches, the autumn fruit branch item of the matrimony vine of embodiment 1-4 increase,
And fruit away from, internode away from being declined, old eye, seven cun, autumn branch fresh leaf, cured leaf weight increase, the fertilizer of this explanation application present invention
After material, the nutrient growth of matrimony vine makes moderate progress, and reproductive growth improves obviously, is embodied in into the enhancing of flower bearing capacity, fallen flowers
Fruit drop rate reduces, functional period of leaf extends, photosynthesis enhancing.
From table 3 it can be seen that relative to comparative example, the old eye of the matrimony vine of embodiment 1-4, seven cun, the fresh fruit of autumn branch and dry
Fruit obviously increases, i.e., effect of increasing production is apparent, meanwhile, Ratio of dry to fresh matter of leaves declines, and illustrates that the organic matter accumulation in fruit is reinforced, i.e. Chinese holly
The mass rate of production of Qi is improved significantly.
It is the embodiment of the present invention as described above.The present invention is not limited to the above-described embodiments, anyone should learn that
The structure change made under the inspiration of the present invention, the technical schemes that are same or similar to the present invention each fall within this
Within the protection domain of invention.
Claims (9)
1. a kind of matrimony vine special fertilizer of resisting drought saving water, which is characterized in that include the component of following parts by weight：Natural nano soil property material
30-90 parts of material, 5-20 parts of zeolite powder, 1-5 parts of calcium nitrate, 0.04-0.07 parts of inorganic selenium salt, 1.2-2.5 parts of vitamin C are organic
15-36 parts of matter, 12-30 parts of water, 9-15 parts of urea, 10-15 parts of Diammonium phosphate (DAP), 8-12 parts of potassium sulfate, 1-3 parts of zinc sulfate.
2. a kind of matrimony vine special fertilizer of resisting drought saving water as described in claim 1, which is characterized in that include the group of following parts by weight
Point：30-45 parts of natural nano soil material, 5-10 parts of zeolite powder, 1-5 parts of calcium nitrate, 0.04-0.07 parts of inorganic selenium salt, dimension life
It is C1.2-2.5 parts plain, 15-25 parts of organic matter, 12-20 parts of water, 12-15 parts of urea, 10-15 parts of Diammonium phosphate (DAP), potassium sulfate 8-12
Part, 1-3 parts of zinc sulfate.
3. a kind of matrimony vine special fertilizer of resisting drought saving water as described in claim 1, which is characterized in that the natural nano soil property material
Material is at least one of calcium-base bentonite, sodium bentonite, sepiolite and talcum.
4. a kind of matrimony vine special fertilizer of resisting drought saving water as described in claim 1, which is characterized in that the inorganic selenium salt is sub- selenium
At least one of sour sodium, potassium selenite.
5. a kind of matrimony vine special fertilizer of resisting drought saving water as described in claim 1, which is characterized in that the organic matter be bacteria residue,
At least one of plant residue, vinasse and flyash.
6. a kind of preparation method of the matrimony vine special fertilizer of resisting drought saving water as described in claim 1, which is characterized in that including following
Step：
S1, natural nano soil material and zeolite powder are uniformly mixed, add water that slurry is made；
S2, after slurry is heated to 45~50 DEG C, calcium nitrate is added, is stirred 45~60min, obtains mixed slurry；
S3, after mixed slurry is heated to 60~75 DEG C, inorganic selenium salt, vitamin C and water is added, is stirred 30~45min,
Obtain mixed solution；
Inorganic acid is added in S4, the mixed solution obtained to step S3, it is 6.1~6.5 to adjust solution ph, and urea, phosphorus is added
The mixed liquor of sour diammonium, potassium sulfate, zinc sulfate is mixed 2~3h, obtains mixture；
S5, the obtained mixtures of step S4 are filtered, heated-air drying, crushing, be eventually adding organic matter, 10- be mixed
15min is to get to the matrimony vine special fertilizer of resisting drought saving water.
7. a kind of preparation method of the matrimony vine special fertilizer of resisting drought saving water as claimed in claim 6, which is characterized in that the step
Its solid and liquid weight ratio of slurry in S1 is 1:(2-4.5).
8. a kind of preparation method of the matrimony vine special fertilizer of resisting drought saving water as claimed in claim 6, which is characterized in that the step
Inorganic selenium salt and vitamin mixtures in S3 shift to an earlier date is configured to the solution that mass concentration is 0.1-0.5% with water.
9. a kind of preparation method of the matrimony vine special fertilizer of resisting drought saving water as claimed in claim 6, which is characterized in that described organic
Acid is at least one of carbonic acid, nitrous acid, metaboric acid, sulfuric acid, nitric acid, phosphoric acid, molybdic acid.
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| CN110240519A (en) * | 2019-06-26 | 2019-09-17 | 四川四季正光农林科技有限公司 | One kind Canker-Resistance fertilizer of nano controlled-release containing zirconium and preparation method thereof |
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