CN108623417A - A kind of preparation method of oil tea composite fertilizer full of nutrition - Google Patents

A kind of preparation method of oil tea composite fertilizer full of nutrition Download PDF

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Publication number
CN108623417A
CN108623417A CN201810665885.5A CN201810665885A CN108623417A CN 108623417 A CN108623417 A CN 108623417A CN 201810665885 A CN201810665885 A CN 201810665885A CN 108623417 A CN108623417 A CN 108623417A
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Prior art keywords
nutrition
oil tea
composite fertilizer
prefabricated material
preparation
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CN201810665885.5A
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Chinese (zh)
Inventor
吴海德
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Anhui Daxin Ecological Agriculture And Forestry Technology Development Co Ltd
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Anhui Daxin Ecological Agriculture And Forestry Technology Development Co Ltd
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Priority to CN201810665885.5A priority Critical patent/CN108623417A/en
Publication of CN108623417A publication Critical patent/CN108623417A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/90Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Soil Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of preparation methods of oil tea composite fertilizer full of nutrition, include the following steps:By polylactic acid, polyethylene glycol, stannous octoate stirring; whipping temp is 182 194 DEG C; phenolic resin is added to stir evenly; it is added dropwise in mineral oil; the drop formed and drying are collected, is put into the tube furnace of nitrogen protection and calcines, it is cooling; urea, starch, polyacrylic acid mixed grinding is added, granulation obtains prefabricated material a;Peanut shell powder, riverway sludge, corn germ cake, kelp residue, saccharomycete, bacillus licheniformis, Paenibacillus polymyxa are mixed evenly to obtain prefabricated material b;Prefabricated material a, ammonium nitrate, calcium superphosphate, plant ash, diatomite, ammonium molybdate, EDTA chelated zincs, three nitric acid, six urea conjunction iron, weathered coal mixed grinding is uniform, cross 60 mesh sieve, prefabricated material b is added to stir evenly, granulation obtains oil tea composite fertilizer full of nutrition.

Description

A kind of preparation method of oil tea composite fertilizer full of nutrition
Technical field
The present invention relates to oil tea planting technology field more particularly to a kind of preparation sides of oil tea composite fertilizer full of nutrition Method.
Background technology
Tea oil is the major product of oil tea, has unique fragrance, is rich in polyphenols, has anti-oxidant, shelf-stable Feature, and the aflatoxins for causing human carcinogen is not generated.Tea oil contains there are many vitamin and trace element beneficial to human body, Unsaturated fatty acid reaches 90% or more, and easily digested, long-term consumption can reduce cholesterol, inhibit and prevent hat The Common Cardiovascular Diseases such as worry, hypertension, enhance human immunity, and have very high nutritive value and health-care effect, are A kind of high-grade, the natural of high nutritive value, safety, health care high-quality characteristic woody edible oil, " east is described as by international market Olive oil ".But the technical issues of it is single that there are nutrition during current tea tree planting, and soil hardening cures, it would be highly desirable to solve.
Invention content
Technical problems based on background technology, the present invention propose a kind of system of oil tea composite fertilizer full of nutrition Preparation Method, gained fertilizer can more fully meet the needs of each growth period development of oil tea is to nutrient, can promote oil tea young growth Growth and development is yielded positive results ahead of time, moreover it is possible to be improved soil, be improved the yield and quality.
A kind of preparation method of oil tea composite fertilizer full of nutrition proposed by the present invention, includes the following steps:
S1, polylactic acid, polyethylene glycol, stannous octoate are stirred, whipping temp is 182-194 DEG C, and phenolic resin is added and stirs It mixes uniformly, is added dropwise in mineral oil, collects the drop of formation and drying, be put into the tube furnace of nitrogen protection and calcine, it is cooling, add Enter urea, starch, polyacrylic acid mixed grinding, granulation obtains prefabricated material a;
S2, by peanut shell powder, riverway sludge, corn germ cake, kelp residue, saccharomycete, bacillus licheniformis, mostly viscous class bud Spore bacillus is mixed evenly to obtain prefabricated material b;
S3, by prefabricated material a, ammonium nitrate, calcium superphosphate, plant ash, diatomite, ammonium molybdate, EDTA chelated zincs, three nitric acid six Urea conjunction iron, weathered coal mixed grinding are uniform, cross 60 mesh sieve, prefabricated material b is added and stirs evenly, granulation obtains oil full of nutrition Tea composite fertilizer.
Preferably, in S1, calcination temperature is 1000-1100 DEG C, calcination time 10-20min.
Preferably, in S1, polylactic acid, polyethylene glycol, stannous octoate weight ratio be 25-32:0.5-2:0.01- 0.02。
Preferably, in S1, urea, starch, polyacrylic acid weight ratio be 10-30:1-4:1-2.
Preferably, in S1, by weight by 25-32 parts of polylactic acid, 0.5-2 parts of polyethylene glycol, 0.01-0.02 parts of octanoic acids Stannous stirs 5-12min, and whipping temp is 182-194 DEG C, and 42-55 parts of phenolic resin are added and stir evenly, are added dropwise to 500-600 In part mineral oil, the drop of formation and drying are collected, is put into the tube furnace of nitrogen protection and calcines 10-20min, calcination temperature is It is 1000-1100 DEG C, cooling, 10-30 parts of urea, 1-4 parts of starch, 1-2 parts of polyacrylic acid mixed grindings are added, granulation obtains prefabricated Expect a.
Preferably, in S2, peanut shell powder, riverway sludge, corn germ cake, kelp residue weight ratio be 30-43:1-4: 24-35:1-5.
Preferably, in S2, compound bacteria includes saccharomycete, bacillus licheniformis, Paenibacillus polymyxa.
Preferably, in S2, saccharomycete, bacillus licheniformis, Paenibacillus polymyxa weight ratio be 0.02-0.08: 0.01-0.04:0.01-0.02.
Preferably, in S3, by weight by 60-76 parts of prefabricated material a, 24-35 parts of ammonium nitrate, 22-30 parts of calcium superphosphate, 5-12 parts of plant ash, 1-2 parts of diatomite, 0.4-1 parts of ammonium molybdates, 0.2-0.5 parts of EDTA chelated zincs, three nitric acid six of 0.2-0.5 parts Urea conjunction iron, 0.2-0.5 parts of weathered coal mixed grindings are uniform, cross 60 mesh sieve, and 2-8 parts of prefabricated material b are added and stir evenly, pelletize To oil tea composite fertilizer full of nutrition.
The present invention can more fully meet the needs of each growth period development of oil tea is to nutrient, and oil tea young growth can be promoted to give birth to Long development, yields positive results ahead of time, and flower and fruit protecting improves the yield and quality, while improving the drought resistance of tea oil tree, effectively prevention oil Tea forest land subterranean pest-insect and effectively prevent all kinds of germs and grow, maximumlly reduces the damage brought by nutritional deficiency disease and pest disaster It loses.
In S1 of the present invention, polylactic acid is reacted under the catalysis of stannous octoate with polyethylene glycol, at polylactic acid surface grafting end Hydroxyl is fabulous with phenolic compatible, and mutual combination degree is high, hydrophilic in phenolic surface grafted polylactic acid segment Property it is fabulous, high-temperature calcination is passed through under nitrogen protection, charing microballoon sphericity is high, and adsorption activity is high, with urea, starch, poly- Acrylic acid mixed grinding, not only the slow release effect of urea is fabulous after granulation, but also can degrade in the soil;In S2, using peanut Shell powder is compounded with riverway sludge, corn germ cake, kelp residue, not only full of nutrition, but also bonding is good with adsorption effect;In S3, Prefabricated material b and prefabricated material a, ammonium nitrate, calcium superphosphate, plant ash coordinate, and can not only slow down nutriment and be lost in speed, enhancing soil Earth fertility, is effectively improved soil texture, keeps hardened soil loose, and good water is created for plant root growth development Point, ventilation, temperature condition, promote oil tea aerial growth development, further with saccharomycete, bacillus licheniformis, mostly viscous Series bacillus acts synergistically, apparent to oil tea cell viability stimulation, moreover it is possible to improve soil, keep oil tea volume increase bright It is aobvious.
The present invention is to produce Special fertilizer for oil tea to the Absorption Characteristics of N, P, K according to oil tea, and coincide suction of the oil tea to N, P, K It receives, fertilizer efficiency period is long, and plant recovery of nutrient is high, safe and environment-friendly, is the ideal fertilizer of oil tea good quality and high output, the present invention is remarkably improved Nitrogen utilization efficiency, amplification is 9.6% or more, and fertilizer efficiency period is grown 150 days or more, under the conditions of same nutrient, can be increased using the present invention Oiling tea fruit yield 11.4% or so, can be obviously improved camellia oleifera fruit quality, and oil content promotes 0.75% or more.
Specific implementation mode
In the following, technical scheme of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of preparation method of oil tea composite fertilizer full of nutrition, includes the following steps:
S1,25kg polylactic acid, 2kg polyethylene glycol, 0.01kg stannous octoates being stirred to 12min, whipping temp is 182 DEG C, 55kg phenolic resin is added to stir evenly, is added dropwise in 500kg mineral oil, collects the drop of formation and drying, is put into nitrogen guarantor 20min is calcined in the tube furnace of shield, calcination temperature is 1000 DEG C, cooling, and 30kg urea, 1kg starch, 2kg polyacrylic acid is added Mixed grinding, granulation obtain prefabricated material a;
S2, by 30kg peanut shell powders, 4kg riverway sludges, 24kg corn germ cakes, 5kg kelp residues, 0.02kg saccharomycete, 0.04kg bacillus licheniformis, 0.01kg Paenibacillus polymyxas are mixed evenly to obtain prefabricated material b;
S3, by prefabricated material a, 24kg ammonium nitrate of 76kg, 30kg calcium superphosphate, 5kg plant ash, 2kg diatomite, 0.4kg molybdenums Sour ammonium, 0.5kgEDTA chelated zincs, tri- nitric acid of 0.2kg, six urea conjunction iron, 0.5kg weathered coal mixed grindings are uniform, cross 60 mesh sieve, The prefabricated material b of 2kg are added to stir evenly, granulation obtains oil tea composite fertilizer full of nutrition.
Embodiment 2
A kind of preparation method of oil tea composite fertilizer full of nutrition, includes the following steps:
S1,32kg polylactic acid, 0.5kg polyethylene glycol, 0.02kg stannous octoates being stirred to 5min, whipping temp is 194 DEG C, 42kg phenolic resin is added to stir evenly, is added dropwise in 600kg mineral oil, collects the drop of formation and drying, is put into nitrogen guarantor 10min is calcined in the tube furnace of shield, calcination temperature is 1100 DEG C, cooling, and 10kg urea, 4kg starch, 1kg polyacrylic acid is added Mixed grinding, granulation obtain prefabricated material a;
S2, by 43kg peanut shell powders, 1kg riverway sludges, 35kg corn germ cakes, 1kg kelp residues, 0.08kg saccharomycete, 0.01kg bacillus licheniformis, 0.02kg Paenibacillus polymyxas are mixed evenly to obtain prefabricated material b;
S3, by prefabricated material a, 35kg ammonium nitrate of 60kg, 22kg calcium superphosphate, 12kg plant ash, 1kg diatomite, 1kg molybdic acids Ammonium, 0.2kgEDTA chelated zincs, tri- nitric acid of 0.5kg, six urea conjunction iron, 0.2kg weathered coal mixed grindings are uniform, cross 60 mesh sieve, add Enter the prefabricated material b of 8kg to stir evenly, granulation obtains oil tea composite fertilizer full of nutrition.
Embodiment 3
A kind of preparation method of oil tea composite fertilizer full of nutrition, includes the following steps:
S1,28kg polylactic acid, 1.5kg polyethylene glycol, 0.012kg stannous octoates are stirred into 10min, whipping temp 186 DEG C, 52kg phenolic resin is added and stirs evenly, is added dropwise in 530kg mineral oil, collects the drop of formation and drying, be put into nitrogen 18min is calcined in the tube furnace of protection, calcination temperature is 1020 DEG C, cooling, and 25kg urea, 2kg starch, 1.8kg poly- third is added Olefin(e) acid mixed grinding, granulation obtain prefabricated material a;
S2, by 35kg peanut shell powders, 3kg riverway sludges, 28kg corn germ cakes, 4kg kelp residues, 0.04kg saccharomycete, 0.03kg bacillus licheniformis, 0.012kg Paenibacillus polymyxas are mixed evenly to obtain prefabricated material b;
S3, by prefabricated material a, 28kg ammonium nitrate of 70kg, 28kg calcium superphosphate, 6kg plant ash, 1.7kg diatomite, 0.6kg Ammonium molybdate, 0.4kgEDTA chelated zincs, tri- nitric acid of 0.3kg, six urea conjunction iron, 0.4kg weathered coal mixed grindings are uniform, cross 60 mesh Sieve is added the prefabricated material b of 4kg and stirs evenly, and granulation obtains oil tea composite fertilizer full of nutrition.
Embodiment 4
A kind of preparation method of oil tea composite fertilizer full of nutrition, includes the following steps:
S1,30kg polylactic acid, 1kg polyethylene glycol, 0.018kg stannous octoates being stirred to 8min, whipping temp is 190 DEG C, 48kg phenolic resin is added to stir evenly, is added dropwise in 570kg mineral oil, collects the drop of formation and drying, is put into nitrogen guarantor 12min is calcined in the tube furnace of shield, calcination temperature is 1080 DEG C, cooling, and 15kg urea, 3kg starch, 1.2kg polypropylene is added Sour mixed grinding, granulation obtain prefabricated material a;
S2, by 40kg peanut shell powders, 2kg riverway sludges, 32kg corn germ cakes, 2kg kelp residues, 0.06kg saccharomycete, 0.02kg bacillus licheniformis, 0.018kg Paenibacillus polymyxas are mixed evenly to obtain prefabricated material b;
S3, by prefabricated material a, 32kg ammonium nitrate of 64kg, 24kg calcium superphosphate, 10kg plant ash, 1.3kg diatomite, 0.8kg Ammonium molybdate, 0.3kgEDTA chelated zincs, tri- nitric acid of 0.4kg, six urea conjunction iron, 0.3kg weathered coal mixed grindings are uniform, cross 60 mesh Sieve is added the prefabricated material b of 6kg and stirs evenly, and granulation obtains oil tea composite fertilizer full of nutrition.
Embodiment 5
A kind of preparation method of oil tea composite fertilizer full of nutrition, includes the following steps:
S1,29kg polylactic acid, 1.2kg polyethylene glycol, 0.015kg stannous octoates are stirred into 9min, whipping temp 188 DEG C, 50kg phenolic resin is added and stirs evenly, is added dropwise in 550kg mineral oil, collects the drop of formation and drying, be put into nitrogen 15min is calcined in the tube furnace of protection, calcination temperature is 1050 DEG C, cooling, and it is poly- that 20kg urea, 2.5kg starch, 1.5kg is added Acrylic acid mixed grinding, granulation obtain prefabricated material a;
S2, by 38kg peanut shell powders, 2.5kg riverway sludges, 30kg corn germ cakes, 3kg kelp residues, 0.05kg yeast Bacterium, 0.025kg bacillus licheniformis, 0.015kg Paenibacillus polymyxas are mixed evenly to obtain prefabricated material b;
S3, by prefabricated material a, 30kg ammonium nitrate of 67kg, 26kg calcium superphosphate, 8kg plant ash, 1.5kg diatomite, 0.7kg Ammonium molybdate, 0.35kgEDTA chelated zincs, tri- nitric acid of 0.35kg, six urea conjunction iron, 0.35kg weathered coal mixed grindings are uniform, cross 60 Mesh sieves, and the prefabricated material b of 5kg are added and stir evenly, granulation obtains oil tea composite fertilizer full of nutrition.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (7)

1. a kind of preparation method of oil tea composite fertilizer full of nutrition, which is characterized in that include the following steps:
S1, polylactic acid, polyethylene glycol, stannous octoate are stirred, whipping temp is 182-194 DEG C, and it is equal that phenolic resin stirring is added It is even, it is added dropwise in mineral oil, collects the drop of formation and drying, be put into the tube furnace of nitrogen protection and calcine, it is cooling, urine is added Element, starch, polyacrylic acid mixed grinding, granulation obtain prefabricated material a;
S2, by peanut shell powder, riverway sludge, corn germ cake, kelp residue, saccharomycete, bacillus licheniformis, mostly viscous class gemma bar Bacterium is mixed evenly to obtain prefabricated material b;
S3, by prefabricated material a, ammonium nitrate, calcium superphosphate, plant ash, diatomite, ammonium molybdate, EDTA chelated zincs, three nitric acid, six urea It is uniform to close iron, weathered coal mixed grinding, crosses 60 mesh sieve, prefabricated material b is added and stirs evenly, granulation obtains oil tea full of nutrition and uses Composite fertilizer.
2. the preparation method of oil tea composite fertilizer full of nutrition according to claim 1, which is characterized in that in S1, Calcination temperature is 1000-1100 DEG C, calcination time 10-20min.
3. the preparation method of oil tea composite fertilizer full of nutrition according to claim 1 or 2, which is characterized in that in S1 In, polylactic acid, polyethylene glycol, stannous octoate weight ratio be 25-32:0.5-2:0.01-0.02.
4. according to the preparation method of claim 1-3 any one of them oil tea composite fertilizer full of nutrition, which is characterized in that In S1, urea, starch, polyacrylic acid weight ratio be 10-30:1-4:1-2.
5. according to the preparation method of claim 1-4 any one of them oil tea composite fertilizer full of nutrition, which is characterized in that In S2, peanut shell powder, riverway sludge, corn germ cake, kelp residue weight ratio be 30-43:1-4:24-35:1-5.
6. according to the preparation method of claim 1-5 any one of them oil tea composite fertilizer full of nutrition, which is characterized in that In S2, compound bacteria includes saccharomycete, bacillus licheniformis, Paenibacillus polymyxa.
7. the preparation method of oil tea composite fertilizer full of nutrition according to claim 6, which is characterized in that in S2, Saccharomycete, bacillus licheniformis, Paenibacillus polymyxa weight ratio be 0.02-0.08:0.01-0.04:0.01-0.02.
CN201810665885.5A 2018-06-26 2018-06-26 A kind of preparation method of oil tea composite fertilizer full of nutrition Pending CN108623417A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2090752A5 (en) * 1970-04-27 1972-01-14 Armour Hess Chemicals
CN107840751A (en) * 2017-09-26 2018-03-27 安庆市望马楼生态农业发展有限公司 A kind of compound fertilizer for improving tea-oil tree yield

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2090752A5 (en) * 1970-04-27 1972-01-14 Armour Hess Chemicals
CN107840751A (en) * 2017-09-26 2018-03-27 安庆市望马楼生态农业发展有限公司 A kind of compound fertilizer for improving tea-oil tree yield

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Application publication date: 20181009