CN108622915B - 在模板1,6-双(甲基哌啶鎓)己烷二溴化物的存在下合成izm-2沸石的方法 - Google Patents

在模板1,6-双(甲基哌啶鎓)己烷二溴化物的存在下合成izm-2沸石的方法 Download PDF

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CN108622915B
CN108622915B CN201810245524.5A CN201810245524A CN108622915B CN 108622915 B CN108622915 B CN 108622915B CN 201810245524 A CN201810245524 A CN 201810245524A CN 108622915 B CN108622915 B CN 108622915B
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fau
sio
zeolite
izm
mixture
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CN108622915A (zh
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R.马蒂内斯弗兰科
N.巴茨
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IFP Energies Nouvelles IFPEN
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B01J20/18—Synthetic zeolitic molecular sieves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/305—Addition of material, later completely removed, e.g. as result of heat treatment, leaching or washing, e.g. for forming pores
    • B01J20/3057—Use of a templating or imprinting material ; filling pores of a substrate or matrix followed by the removal of the substrate or matrix
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
CN201810245524.5A 2017-03-24 2018-03-23 在模板1,6-双(甲基哌啶鎓)己烷二溴化物的存在下合成izm-2沸石的方法 Active CN108622915B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1752473 2017-03-24
FR1752473A FR3064262B1 (fr) 2017-03-24 2017-03-24 Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane

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CN108622915A CN108622915A (zh) 2018-10-09
CN108622915B true CN108622915B (zh) 2023-03-10

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Country Link
US (1) US10875778B2 (https=)
EP (1) EP3378830B1 (https=)
JP (1) JP7005399B2 (https=)
CN (1) CN108622915B (https=)
FR (1) FR3064262B1 (https=)
ZA (1) ZA201801813B (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3081347B1 (fr) 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
FR3095199B1 (fr) 2019-04-19 2021-10-29 Ifp Energies Now Procédé de synthèse rapide d'une zeolithe de type structural AFX avec une source de faujasite
FR3095967A1 (fr) * 2019-05-16 2020-11-20 IFP Energies Nouvelles Procédé de préparation d'une zéolithe de type structural MER
FR3101342B1 (fr) 2019-09-26 2021-10-15 Ifp Energies Now Procede de preparation d’une zeolithe izm-2 en presence d’un melange de structurants organiques azotes sous forme hydroxyde et bromure et d’un chlorure de metal alcalin
FR3101341B1 (fr) * 2019-09-26 2021-10-15 Ifp Energies Now Procede de preparation d’une zeolithe izm-2 en presence d’un structurant organique azote sous forme hydroxyde et d’un chlorure de metal alcalin, en milieu fluore ou non
CN110961148A (zh) * 2019-12-14 2020-04-07 中触媒新材料股份有限公司 一种aei/lev结构共生复合分子筛及其制备方法和scr应用
FR3109103A1 (fr) * 2020-04-08 2021-10-15 IFP Energies Nouvelles Méthode de synthèse de la zéolithe mordénite (MOR) de haut rapport Si/Al
FR3156130B1 (fr) * 2023-12-04 2025-11-14 Ifp Energies Now Synthese d’une zeolithe izm-2 en presence d’ethanol

Citations (3)

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CN102119123A (zh) * 2008-08-08 2011-07-06 Ifp新能源公司 包含izm-2沸石和至少一种金属的催化剂及其在烃转化中的用途
CN104803396A (zh) * 2014-01-28 2015-07-29 中国石油化工股份有限公司 一种制备mww结构分子筛的方法
CN105271300A (zh) * 2014-07-02 2016-01-27 中国石油化工股份有限公司 一种分子筛催化剂、制备方法以及应用

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US3222583A (en) * 1962-03-23 1965-12-07 Gen Electric Control systems
US5716593A (en) * 1996-07-31 1998-02-10 Chevron U.S.A. Inc. Preparation of Y-type faujasite using an organic template
JP5475289B2 (ja) * 2005-12-28 2014-04-16 シェブロン ユー．エス．エー． インコーポレイテッド 分子ふるいｓｓｚ−７４組成物及びその合成
FR2918050B1 (fr) * 2007-06-29 2011-05-06 Inst Francais Du Petrole Solide cristallise izm-2 et son procede de preparation
FR2924110B1 (fr) * 2007-11-26 2010-02-26 Inst Francais Du Petrole Solide cristallise izm-3 et son procede de preparation
FR2934796B1 (fr) * 2008-08-08 2010-09-03 Inst Francais Du Petrole Catalyseur a base de zeolithe izm-2 et procede d'hydroconversion/hydrocraquage de charges hydrocarbonees
FR2934795B1 (fr) * 2008-08-08 2010-11-26 Inst Francais Du Petrole Catalyseur comprenant au moins une zeolithe izm-2 et son utilisation pour la transformation de charges hydrocarbonees
US9156706B2 (en) * 2012-07-03 2015-10-13 Chevron U.S.A. Inc. Method for preparing high-silica LEV-type zeolites
US9938157B2 (en) * 2014-07-23 2018-04-10 Chevron U.S.A. Inc. Interzeolite transformation and metal encapsulation in the absence of an SDA
US9802831B2 (en) * 2014-07-23 2017-10-31 Chevron U.S.A. Inc. Synthesis of high silica zeolite via interzeolite transformation without OSDAs
WO2016080547A1 (ja) * 2014-11-21 2016-05-26 三菱化学株式会社 Ａｅｉ型ゼオライト、その製造方法及びその用途

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CN102119123A (zh) * 2008-08-08 2011-07-06 Ifp新能源公司 包含izm-2沸石和至少一种金属的催化剂及其在烃转化中的用途
CN104803396A (zh) * 2014-01-28 2015-07-29 中国石油化工股份有限公司 一种制备mww结构分子筛的方法
CN105271300A (zh) * 2014-07-02 2016-01-27 中国石油化工股份有限公司 一种分子筛催化剂、制备方法以及应用

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IZM-2: A promising new zeolite for the selective hydroisomerization of long-chain n-alkanes;Mota. FM et al.;《Journal of Catalysis》;20130228;第301卷;第20-29页 *
Topology reconstruction from FAU to MWW structure;Yanchun Shi et al.;《Microporous and Mesoporous Materials》;20140906;第200卷;第269-278页 *

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Publication number Publication date
US20180273393A1 (en) 2018-09-27
JP7005399B2 (ja) 2022-01-21
EP3378830A1 (fr) 2018-09-26
US10875778B2 (en) 2020-12-29
ZA201801813B (en) 2019-01-30
FR3064262A1 (fr) 2018-09-28
EP3378830B1 (fr) 2019-10-16
CN108622915A (zh) 2018-10-09
FR3064262B1 (fr) 2019-03-22
JP2018162206A (ja) 2018-10-18

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