CN108560262A - 一种湿摩擦牢度增强剂及其制备方法 - Google Patents
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Abstract
本发明公开了一种湿摩擦牢度增强剂及其制备方法,所述湿摩擦牢度增强剂由如下重量份数的原料组成:纳米二氧化钛颗粒3‑5份、棕榈蜡5‑10份、壳聚糖3‑5份、聚乙烯蜡乳液20‑30份、分散剂3‑5份、乙醇10‑20份、十二烷基甜菜碱5‑7份、柠檬酸2‑4份、烷基糖苷5‑7份、乳化剂3‑5份、碳酸氢钠3‑5份、消泡剂1‑3份、去离子水30‑40份。本发明的湿摩擦牢度增强剂固色效果好,可以提高织物的服用性能,湿摩擦牢度高,同时水洗不沾色,不变色,耐水洗牢度高。本发明的湿摩擦牢度增强剂制造工艺简单易操作,原料价格低廉易获得,且环保,对环境没有污染。
Description
技术领域
本发明属于纺织品技术领域,更具体是涉及一种湿摩擦牢度增强剂及其制备方法。
背景技术
目前提高湿摩擦牢度的方法有:对织物进行充分的前处理、选择合适的染色料及染色工艺、对织物进行适当的后整理。其中对织物进行适当的后整理主要是通过湿摩擦牢度增强剂去提高织物的湿摩擦牢度。因此,研发性能优异的湿摩擦牢度增强剂对于染整助剂行列甚至于整个纺织行业都具有重要的意义。
市场上用的最多的湿摩擦牢度增强剂是聚氨酯类的,主要存在以下缺陷:(1)成本高,用量大;(2)对织物色光及物理机械性能有影响;(3)有一些的合成原料毒性大,生产存在潜在风险,不符合环保要求。因此,寻找一种高效、环保的湿摩擦牢度增强剂是目前急需解决的问题。
发明内容
本发明的目的在于提供一种湿摩擦牢度增强剂及其制备方法,以解决上述背景技术中提出的问题。
为实现上述目的,本发明提供如下技术方案:
一种湿摩擦牢度增强剂,按照重要份数,包括以下组分:纳米二氧化钛颗粒3-5份、棕榈蜡5-10份、壳聚糖3-5份、聚乙烯蜡乳液20-30份、分散剂3-5份、乙醇10-20份、十二烷基甜菜碱5-7份、柠檬酸2-4份、烷基糖苷5-7份、乳化剂3-5份、碳酸氢钠3-5份、消泡剂1-3份、去离子水30-40份。
优选地,所述的纳米二氧化钛颗粒的粒径为5-50nm。
优选地,所述的聚乙烯蜡乳液固含量为30-40%。
优选地,所述的消泡剂为乳化硅油、磷酸三丁酯、高级醇中的一种或者一种以上。
优选地,所述的分散剂为木质素磺酸钠、纤维素磺酸钠、六偏磷酸钠中的一种或者一种以上。
优选地,所述的乙醇为无水乙醇,纯度为分析醇。
优选地,所述的乳化剂为月桂醇聚氧乙烯醚、十二烷基苯磺酸钠、石油磺酸钠、失水山梨醇月桂酸酯中的一种或者一种以上。
优选地,所述湿摩擦牢度增强剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入棕榈蜡5-10份,升高温度至80-100℃;
步骤2,待棕榈蜡完全融为液体,加入乳化剂3-5份、去离子水(100℃)30-40份,500-1000转/分钟,搅拌30-40分钟;
步骤3,加入聚乙烯蜡乳液20-30份,500-1000转/分钟,搅拌10-20分钟;
步骤4,先将纳米二氧化钛颗粒3-5份、分散剂3-5份、乙醇10-20份进行超声分散,分散功率为500-1000W,分散时间为20-30分钟;
步骤5,降低温度至40-60℃,将步骤4的混合液体加入步骤3的混合液中,500-1000转/分钟,搅拌10-20分钟;
步骤6,加入壳聚糖3-5份、十二烷基甜菜碱5-7份、柠檬酸2-4份、烷基糖苷5-7份、碳酸氢钠3-5份、消泡剂1-3份,500-1000转/分钟,搅拌30-40分钟;
步骤7,关停搅拌,得到配制好的液体湿摩擦牢度增强剂;
步骤8,静置冷却至反应釜中液体湿摩擦牢度增强剂低于20℃,放料封装,制得成品。
与现有技术相比,本发明的有益效果是:
1、本发明的湿摩擦牢度增强剂固色效果好,可以提高织物的服用性能,湿摩擦牢度高,同时水洗不沾色,不变色,耐水洗牢度高。
2、本发明的湿摩擦牢度增强剂制造工艺简单易操作,原料价格低廉易获得,且环保,对环境没有污染。
3、本发明的湿摩擦牢度增强剂成膜强度高,致密性与连续性好。
4、本发明的湿摩擦牢度增强剂对整理的织物无选择性,不发粘。
5、本发明的湿摩擦牢度增强剂所用各种原料之间相互配伍、协同作用,共同组成性能优异的产品。
6、简化工艺,操作安全简单,易于工业化生产。
7、本发明的使用可收到良好的经济效益。
具体实施实例
本发明公开了一种湿摩擦牢度增强剂,按照重要份数,包括以下组分:纳米二氧化钛颗粒3-5份、棕榈蜡5-10份、壳聚糖3-5份、聚乙烯蜡乳液20-30份、分散剂3-5份、乙醇10-20份、十二烷基甜菜碱5-7份、柠檬酸2-4份、烷基糖苷5-7份、乳化剂3-5份、碳酸氢钠3-5份、消泡剂1-3份、去离子水30-40份。
本发明还提供了一种湿摩擦牢度增强剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入棕榈蜡5-10份,升高温度至80-100℃;
步骤2,待棕榈蜡完全融为液体,加入乳化剂3-5份、去离子水(100℃)30-40份,500-1000转/分钟,搅拌30-40分钟;
步骤3,加入聚乙烯蜡乳液20-30份,500-1000转/分钟,搅拌10-20分钟;
步骤4,先将纳米二氧化钛颗粒3-5份、分散剂3-5份、乙醇10-20份进行超声分散,分散功率为500-1000W,分散时间为20-30分钟;
步骤5,降低温度至40-60℃,将步骤4的混合液体加入步骤3的混合液中,500-1000转/分钟,搅拌10-20分钟;
步骤6,加入壳聚糖3-5份、十二烷基甜菜碱5-7份、柠檬酸2-4份、烷基糖苷5-7份、碳酸氢钠3-5份、消泡剂1-3份,500-1000转/分钟,搅拌30-40分钟;
步骤7,关停搅拌,得到配制好的液体湿摩擦牢度增强剂;
步骤8,静置冷却至反应釜中液体湿摩擦牢度增强剂低于20℃,放料封装,制得成品。
实施例1
本发明公开了一种湿摩擦牢度增强剂,按照重要份数,包括以下组分:纳米二氧化钛颗粒3份、棕榈蜡5份、壳聚糖3份、聚乙烯蜡乳液20份、分散剂3份、乙醇10份、十二烷基甜菜碱5份、柠檬酸2份、烷基糖苷5份、乳化剂3份、碳酸氢钠3份、消泡剂1份、去离子水30份。
本发明还提供了一种湿摩擦牢度增强剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入棕榈蜡5份,升高温度至80℃;
步骤2,待棕榈蜡完全融为液体,加入乳化剂3份、去离子水(100℃)30份,1000转/分钟,搅拌30分钟;
步骤3,加入聚乙烯蜡乳液20份,500转/分钟,搅拌10分钟;
步骤4,先将纳米二氧化钛颗粒3份、分散剂3份、乙醇10份进行超声分散,分散功率为500W,分散时间为30分钟;
步骤5,降低温度至40℃,将步骤4的混合液体加入步骤3的混合液中,500转/分钟,搅拌10分钟;
步骤6,加入壳聚糖3份、十二烷基甜菜碱5份、柠檬酸2份、烷基糖苷5份、碳酸氢钠3份、消泡剂1份,500转/分钟,搅拌40分钟;
步骤7,关停搅拌,得到配制好的液体湿摩擦牢度增强剂;
步骤8,静置冷却至反应釜中液体湿摩擦牢度增强剂低于20℃,放料封装,制得成品。
实施例2
本发明公开了一种湿摩擦牢度增强剂,按照重要份数,包括以下组分:纳米二氧化钛颗粒4份、棕榈蜡8份、壳聚糖4份、聚乙烯蜡乳液25份、分散剂4份、乙醇15份、十二烷基甜菜碱6份、柠檬酸3份、烷基糖苷6份、乳化剂4份、碳酸氢钠4份、消泡剂2份、去离子水35份。
本发明还提供了一种湿摩擦牢度增强剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入棕榈蜡8份,升高温度至90℃;
步骤2,待棕榈蜡完全融为液体,加入乳化剂4份、去离子水(100℃)35份,900转/分钟,搅拌35分钟;
步骤3,加入聚乙烯蜡乳液25份,800转/分钟,搅拌15分钟;
步骤4,先将纳米二氧化钛颗粒4份、分散剂4份、乙醇15份进行超声分散,分散功率为800W,分散时间为25分钟;
步骤5,降低温度至50℃,将步骤4的混合液体加入步骤3的混合液中,900转/分钟,搅拌15分钟;
步骤6,加入壳聚糖4份、十二烷基甜菜碱6份、柠檬酸3份、烷基糖苷6份、碳酸氢钠4份、消泡剂2份,800转/分钟,搅拌35分钟;
步骤7,关停搅拌,得到配制好的液体湿摩擦牢度增强剂;
步骤8,静置冷却至反应釜中液体湿摩擦牢度增强剂低于20℃,放料封装,制得成品。
实施例3
本发明公开了一种湿摩擦牢度增强剂,按照重要份数,包括以下组分:纳米二氧化钛颗粒5份、棕榈蜡10份、壳聚糖5份、聚乙烯蜡乳液30份、分散剂5份、乙醇20份、十二烷基甜菜碱7份、柠檬酸4份、烷基糖苷7份、乳化剂5份、碳酸氢钠5份、消泡剂3份、去离子水40份。
本发明还提供了一种湿摩擦牢度增强剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入棕榈蜡10份,升高温度至100℃;
步骤2,待棕榈蜡完全融为液体,加入乳化剂5份、去离子水(100℃)40份,1000转/分钟,搅拌40分钟;
步骤3,加入聚乙烯蜡乳液30份,1000转/分钟,搅拌20分钟;
步骤4,先将纳米二氧化钛颗粒5份、分散剂5份、乙醇20份进行超声分散,分散功率为1000W,分散时间为20分钟;
步骤5,降低温度至60℃,将步骤4的混合液体加入步骤3的混合液中,1000转/分钟,搅拌10分钟;
步骤6,加入壳聚糖5份、十二烷基甜菜碱7份、柠檬酸4份、烷基糖苷7份、碳酸氢钠5份、消泡剂3份,1000转/分钟,搅拌30分钟;
步骤7,关停搅拌,得到配制好的液体湿摩擦牢度增强剂;
步骤8,静置冷却至反应釜中液体湿摩擦牢度增强剂低于20℃,放料封装,制得成品。
实施例4
本发明公开了一种湿摩擦牢度增强剂,按照重要份数,包括以下组分:纳米二氧化钛颗粒5份、棕榈蜡10份、壳聚糖3份、聚乙烯蜡乳液30份、分散剂5份、乙醇20份、十二烷基甜菜碱7份、柠檬酸3份、烷基糖苷6份、乳化剂4份、碳酸氢钠4份、消泡剂2份、去离子水30份。
本发明还提供了一种湿摩擦牢度增强剂的制备方法,具体步骤包括:
步骤1,在反应釜中加入棕榈蜡10份,升高温度至100℃;
步骤2,待棕榈蜡完全融为液体,加入乳化剂4份、去离子水(100℃)30份,1000转/分钟,搅拌30分钟;
步骤3,加入聚乙烯蜡乳液30份,1000转/分钟,搅拌10分钟;
步骤4,先将纳米二氧化钛颗粒5份、分散剂5份、乙醇20份进行超声分散,分散功率为800W,分散时间为20分钟;
步骤5,降低温度至40℃,将步骤4的混合液体加入步骤3的混合液中,800转/分钟,搅拌15分钟;
步骤6,加入壳聚糖3份、十二烷基甜菜碱7份、柠檬酸3份、烷基糖苷6份、碳酸氢钠4份、消泡剂2份,900转/分钟,搅拌30分钟;
步骤7,关停搅拌,得到配制好的液体湿摩擦牢度增强剂;
步骤8,静置冷却至反应釜中液体湿摩擦牢度增强剂低于20℃,放料封装,制得成品。
上述列举的各种实施例,在不矛盾的前提下,可以相互组合实施,本领域技术人员可结合上文对实施例的解释,作为对不同实施例中的技术特征进行组合的依据。
测试例
采用实施例1、2、3、4的湿摩擦牢度增强剂处理棉织物,将得到的棉织物进行性能测试,测试结果如下:
尽管已经示出和描述了本发明的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本发明的范围由所附权利要求及其等同物限定。
Claims (8)
1.一种湿摩擦牢度增强剂,其特征在于:所述湿摩擦牢度增强剂包括如下重量份数的原料:纳米二氧化钛颗粒3-5份、棕榈蜡5-10份、壳聚糖3-5份、聚乙烯蜡乳液20-30份、分散剂3-5份、乙醇10-20份、十二烷基甜菜碱5-7份、柠檬酸2-4份、烷基糖苷5-7份、乳化剂3-5份、碳酸氢钠3-5份、消泡剂1-3份、去离子水30-40份。
2.根据权利要求1所述的湿摩擦牢度增强剂,其特征在于:所述的纳米二氧化钛颗粒的粒径为5-50nm。
3.根据权利要求1所述的湿摩擦牢度增强剂,其特征在于:所述的聚乙烯蜡乳液固含量为30-40%。
4.根据权利要求1所述的湿摩擦牢度增强剂,其特征在于:所述的消泡剂为乳化硅油、磷酸三丁酯、高级醇中的一种或者一种以上。
5.根据权利要求1所述的湿摩擦牢度增强剂,其特征在于:所述的分散剂为木质素磺酸钠、纤维素磺酸钠、六偏磷酸钠中的一种或者一种以上。
6.根据权利要求1所述的湿摩擦牢度增强剂,其特征在于:所述的乙醇为无水乙醇,纯度为分析醇。
7.根据权利要求1所述的湿摩擦牢度增强剂,其特征在于:所述的乳化剂为月桂醇聚氧乙烯醚、十二烷基苯磺酸钠、石油磺酸钠、失水山梨醇月桂酸酯中的一种或者一种以上。
8.一种采用上述权利要求1-7中任一项所述湿摩擦牢度增强剂的制备方法,其特征在于:具体步骤包括:
步骤1,在反应釜中加入棕榈蜡5-10份,升高温度至80-100℃;
步骤2,待棕榈蜡完全融为液体,加入乳化剂3-5份、去离子水(100℃)30-40份,500-1000转/分钟,搅拌30-40分钟;
步骤3,加入聚乙烯蜡乳液20-30份,500-1000转/分钟,搅拌10-20分钟;
步骤4,先将纳米二氧化钛颗粒3-5份、分散剂3-5份、乙醇10-20份进行超声分散,分散功率为500-1000W,分散时间为20-30分钟;
步骤5,降低温度至40-60℃,将步骤4的混合液体加入步骤3的混合液中,500-1000转/分钟,搅拌10-20分钟;
步骤6,加入壳聚糖3-5份、十二烷基甜菜碱5-7份、柠檬酸2-4份、烷基糖苷5-7份、碳酸氢钠3-5份、消泡剂1-3份,500-1000转/分钟,搅拌30-40分钟;
步骤7,关停搅拌,得到配制好的液体湿摩擦牢度增强剂;
步骤8,静置冷却至反应釜中液体湿摩擦牢度增强剂低于20℃,放料封装,制得成品。
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