CN108359554A - A kind of soap and preparation method thereof with natural flower aroma - Google Patents
A kind of soap and preparation method thereof with natural flower aroma Download PDFInfo
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- CN108359554A CN108359554A CN201810325079.3A CN201810325079A CN108359554A CN 108359554 A CN108359554 A CN 108359554A CN 201810325079 A CN201810325079 A CN 201810325079A CN 108359554 A CN108359554 A CN 108359554A
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- Prior art keywords
- parts
- soap
- natural flower
- flower aroma
- preparation
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of soap with natural flower aroma, the soap in parts by weight each group be grouped as it is as follows:25 35 parts of grease, 20 30 parts of sodium hydroxide solution, 5 10 parts of anion surfactant, 26 parts of plants essential oil, 4 10 parts of absolute ethyl alcohol, 4 10 parts of glycerine, 28 parts of diatomite, 12 parts of enzyme preparation, 10 20 parts of deionized water;Soap of the natural flower aroma and preparation method thereof, formula is reasonable, prepares simply, and the soap with the nature fragrance of a flower can be produced by weighing raw material, preparing soap lye, saponification, preparation liquid soap and cooling and shaping with natural flower aroma.
Description
Technical field
The invention belongs to daily necessities technical fields, and in particular to a kind of soap and its preparation with natural flower aroma
Method.
Background technology
Soap is the general name of fatty acid metal salts, can be dissolved in water, there is washing decontamination.Its basic preparation method is mainly
Saponification is occurred into for grease and sodium hydroxide, generates higher fatty acids sodium and glycerine, then using washing, addition fragrance,
Molding and the techniques such as dry and be made.Soap with natural flower aroma is to add plants essential oil in preparation process.Add plant
The soap of essential oil boosts metabolism, channels and collaterals of invigorating blood circulation, accelerates allay nervousness, make us the multi-effects such as euthymia.Cause
This, develops the soap with natural flower aroma and has great importance.
The production of soap product has a long history, and about with regard to useful grease and contains potassium carbonate at B.C. 2500
Plant ass produce potash soap, the record of this soap washing wool is used in combination;Since 19th century, due to the hair of Leblanc soda ash production method
Exhibition, makes the production of soap enter the industrialized stage;And now as the improvement of people's living standards, people for substance
The requirement of life is also higher and higher, and soap products at present on the market are different, does not have the natural fragrance of a flower mostly.
Invention content
The main purpose of the present invention is to provide a kind of soap with natural flower aroma, solve in the prior art that soap is not
Has the shortcomings that natural flower aroma;The present invention also provides the preparation methods of the soap with natural flower aroma.
To achieve the above object, the present invention provides the following technical solutions:A kind of soap with natural flower aroma, the soap
Each group is grouped as follows in parts by weight:25-35 parts of grease, 20-30 parts of sodium hydroxide solution, anion surfactant 5-10
Part, 2-6 parts of plants essential oil, 4-10 parts of absolute ethyl alcohol, 4-10 parts of glycerine, 2-8 parts of diatomite, 1-2 parts of enzyme preparation, deionized water
10-20 parts.
Preferably, the plants essential oil is that Rosa Damascana and peppermint oil press proportion 2:1 is made, by Rosa Damascana and peppermint oil
Plants essential oil is obtained after stirring evenly.
Preferably, the grease includes one or more in peanut oil, soya-bean oil, linseed oil, castor oil, olive oil.
Preferably, the anion surfactant is C11-C18 alkylbenzene sulfonates, C12-C18 alkyl alkoxy sulphur
It is one or more in hydrochlorate, α-sodium olefin sulfonate, C14-C18 fatty acid methyl ester sulfonate.
Preferably, the enzyme preparation is protease, amylase, cellulase, lipase, one kind in pectase or more
Kind.
A kind of preparation method of soap with natural flower aroma provided by the invention, includes the following steps:
S1, raw material is weighed:Weigh following components respectively in parts by weight:25-35 parts of grease, sodium hydroxide solution 20-
30 parts, 5-10 parts of anion surfactant, 2-6 parts of plants essential oil, 4-10 parts of absolute ethyl alcohol, 4-10 parts of glycerine, diatomite 2-8
Part, 1-2 parts of enzyme preparation, 10-20 parts of deionized water;
S2, soap lye is prepared:Grease, absolute ethyl alcohol, anion surfactant, sodium hydroxide solution described in S1 is added
Enter in the deionized water, be uniformly mixed, obtains soap lye;
S3, saponification is carried out:The S2 soap lyes obtained are heated to 80-100 DEG C of progress saponification 6-12h, saponification is anti-
After the completion of answering, by described in S1 glycerine and diatomaceous premixed liquid be added thereto, stir evenly, be cooled to 30-50 DEG C, obtain
Intermediate mixed solution;
S4, the liquid soap with natural flower aroma is prepared:It, will when the intermediate mixed solution that S3 is obtained is cooled to 30-50 DEG C
Plants essential oil and enzyme preparation described in S1 sequentially add wherein, stir evenly, and be cooled to room temperature, and obtaining has natural flower aroma
Liquid soap;
S5, cooling and shaping:The S4 liquid soaps with natural flower aroma obtained are poured into mold, are cooled and shaped, and use
Vacuum freecing-dry machine is freeze-dried, that is, obtains the soap with natural flower aroma.
Preferably, in S3, the pH value of the intermediate mixed solution is 10-12.
Preferably, in S5, the temperature of the freeze-drying is -50--60 DEG C, and the time of freeze-drying is 10-15h.
The technique effect and advantage of the present invention:The present invention by by plants essential oil and diatomite be used as natural flower aroma come
Source, has the characteristics that nontoxic, and the fragrance of a flower is naturally strong;Preparation method of the present invention has method simple, and production cost is low,
And the characteristics of large-scale production can be suitable for and be widely popularized.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.Based on the embodiments of the present invention, those of ordinary skill in the art are not before making creative work
The every other embodiment obtained is put, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of soap with natural flower aroma, the soap in parts by weight each group be grouped as it is as follows:26 parts of grease, hydrogen-oxygen
Change 22 parts of sodium solution, 7 parts of anion surfactant, 3 parts of plants essential oil, 5 parts of absolute ethyl alcohol, 5 parts of glycerine, 3 parts of diatomite, enzyme
1 part of preparation, 12 parts of deionized water.
Specifically, the plants essential oil, which is Rosa Damascana and peppermint oil, presses proportion 2:1 is made, by Rosa Damascana and peppermint oil
Plants essential oil is obtained after stirring evenly.
Specifically, the grease includes peanut oil and olive oil.
Specifically, the anion surfactant is C11-C18 alkylbenzene sulfonates and C12-C18 alkyl alkoxy sulphur
Hydrochlorate.
Specifically, the enzyme preparation is protease, amylase and cellulase.
A kind of preparation method of soap with natural flower aroma provided by the invention, includes the following steps:
S1, raw material is weighed:Weigh following components respectively in parts by weight:26 parts of grease, 22 parts of sodium hydroxide solution, the moon
7 parts of ionic surface active agent, 3 parts of plants essential oil, 5 parts of absolute ethyl alcohol, 5 parts of glycerine, 3 parts of diatomite, 1 part of enzyme preparation, deionization
12 parts of water;
S2, soap lye is prepared:Grease, absolute ethyl alcohol, anion surfactant, sodium hydroxide solution described in S1 is added
Enter in the deionized water, be uniformly mixed, obtains soap lye;
S3, saponification is carried out:The S2 soap lyes obtained are heated to 82 DEG C of progress saponification 7h, saponification is completed
Afterwards, by described in S1 glycerine and diatomaceous premixed liquid be added thereto, stir evenly, be cooled to 35 DEG C, obtain intermediate mixing
Solution;
S4, the liquid soap with natural flower aroma is prepared:It, will be in S1 when the intermediate mixed solution that S3 is obtained is cooled to 35 DEG C
The plants essential oil and enzyme preparation sequentially adds wherein, stirs evenly, and be cooled to room temperature, and obtains the fertilizer with natural flower aroma
Soap lye;
S5, cooling and shaping:The S4 liquid soaps with natural flower aroma obtained are poured into mold, are cooled and shaped, and use
Vacuum freecing-dry machine is freeze-dried, that is, obtains the soap with natural flower aroma.
Specifically, in S3, the pH value of the intermediate mixed solution is 10.5.
Specifically, in S5, the temperature of the freeze-drying is -53 DEG C, and the time of freeze-drying is 12h.
Embodiment 2
A kind of soap with natural flower aroma, the soap in parts by weight each group be grouped as it is as follows:27 parts of grease, hydrogen-oxygen
Change 28 parts of sodium solution, 8 parts of anion surfactant, 5 parts of plants essential oil, 6 parts of absolute ethyl alcohol, 6 parts of glycerine, 5 parts of diatomite, enzyme
2 parts of preparation, 14 parts of deionized water.
Specifically, the plants essential oil, which is Rosa Damascana and peppermint oil, presses proportion 2:1 is made, by Rosa Damascana and peppermint oil
Plants essential oil is obtained after stirring evenly.
Specifically, the grease includes castor oil and olive oil.
Specifically, the anion surfactant is α-sodium olefin sulfonate and C14-C18 fatty acid methyl ester sulfonate.
Specifically, the enzyme preparation is cellulase, lipase and pectase.
A kind of preparation method of soap with natural flower aroma provided by the invention, includes the following steps:
S1, raw material is weighed:Weigh following components respectively in parts by weight:27 parts of grease, 28 parts of sodium hydroxide solution, the moon
8 parts of ionic surface active agent, 5 parts of plants essential oil, 6 parts of absolute ethyl alcohol, 6 parts of glycerine, 5 parts of diatomite, 2 parts of enzyme preparation, deionization
14 parts of water;
S2, soap lye is prepared:Grease, absolute ethyl alcohol, anion surfactant, sodium hydroxide solution described in S1 is added
Enter in the deionized water, be uniformly mixed, obtains soap lye;
S3, saponification is carried out:The S2 soap lyes obtained are heated to 88 DEG C of progress saponification 8h, saponification is completed
Afterwards, by described in S1 glycerine and diatomaceous premixed liquid be added thereto, stir evenly, be cooled to 40 DEG C, obtain intermediate mixing
Solution;
S4, the liquid soap with natural flower aroma is prepared:It, will be in S1 when the intermediate mixed solution that S3 is obtained is cooled to 40 DEG C
The plants essential oil and enzyme preparation sequentially adds wherein, stirs evenly, and be cooled to room temperature, and obtains the fertilizer with natural flower aroma
Soap lye;
S5, cooling and shaping:The S4 liquid soaps with natural flower aroma obtained are poured into mold, are cooled and shaped, and use
Vacuum freecing-dry machine is freeze-dried, that is, obtains the soap with natural flower aroma.
Specifically, in S3, the pH value of the intermediate mixed solution is 11.
Specifically, in S5, the temperature of the freeze-drying is -56 DEG C, and the time of freeze-drying is 13h.
Embodiment 3
A kind of soap with natural flower aroma, the soap in parts by weight each group be grouped as it is as follows:29 parts of grease, hydrogen-oxygen
Change 22 parts of sodium solution, 6 parts of anion surfactant, 6 parts of plants essential oil, 8 parts of absolute ethyl alcohol, 7 parts of glycerine, 7 parts of diatomite, enzyme
2 parts of preparation, 16 parts of deionized water.
Specifically, the plants essential oil, which is Rosa Damascana and peppermint oil, presses proportion 2:1 is made, by Rosa Damascana and peppermint oil
Plants essential oil is obtained after stirring evenly.
Specifically, the grease is linseed oil.
Specifically, the anion surfactant is C14-C18 fatty acid methyl ester sulfonate.
Specifically, the enzyme preparation includes protease, amylase, cellulase, lipase, pectase.
A kind of preparation method of soap with natural flower aroma provided by the invention, includes the following steps:
S1, raw material is weighed:Weigh following components respectively in parts by weight:29 parts of grease, 22 parts of sodium hydroxide solution, the moon
6 parts of ionic surface active agent, 6 parts of plants essential oil, 8 parts of absolute ethyl alcohol, 7 parts of glycerine, 7 parts of diatomite, 2 parts of enzyme preparation, deionization
16 parts of water;
S2, soap lye is prepared:Grease, absolute ethyl alcohol, anion surfactant, sodium hydroxide solution described in S1 is added
Enter in the deionized water, be uniformly mixed, obtains soap lye;
S3, saponification is carried out:The S2 soap lyes obtained are heated to 93 DEG C of progress saponification 10h, saponification is completed
Afterwards, by described in S1 glycerine and diatomaceous premixed liquid be added thereto, stir evenly, be cooled to 45 DEG C, obtain intermediate mixing
Solution;
S4, the liquid soap with natural flower aroma is prepared:It, will be in S1 when the intermediate mixed solution that S3 is obtained is cooled to 45 DEG C
The plants essential oil and enzyme preparation sequentially adds wherein, stirs evenly, and be cooled to room temperature, and obtains the fertilizer with natural flower aroma
Soap lye;
S5, cooling and shaping:The S4 liquid soaps with natural flower aroma obtained are poured into mold, are cooled and shaped, and use
Vacuum freecing-dry machine is freeze-dried, that is, obtains the soap with natural flower aroma.
Specifically, in S3, the pH value of the intermediate mixed solution is 11.5.
Specifically, in S5, the temperature of the freeze-drying is -56 DEG C, and the time of freeze-drying is 14h.
In summary:A kind of soap and preparation method thereof with natural flower aroma provided by the invention, by weigh raw material,
The fertilizer with the nature fragrance of a flower can be produced by preparing soap lye, saponification, preparation liquid soap and cooling and shaping with natural flower aroma
Soap has the characteristics that nontoxic by the way that plants essential oil and diatomite to be used as to the source of natural flower aroma, and the fragrance of a flower is naturally dense
It is strong;Preparation method of the present invention has method simple, and production cost is low, and can be suitable for large-scale production and be widely popularized
The characteristics of.
Finally it should be noted that:The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
With technical scheme described in the above embodiments is modified or equivalent replacement of some of the technical features,
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in the present invention's
Within protection domain.
Claims (8)
1. a kind of soap with natural flower aroma, it is characterised in that:The soap in parts by weight each group be grouped as it is as follows:Grease
25-35 parts, 20-30 parts of sodium hydroxide solution, 5-10 parts of anion surfactant, 2-6 parts of plants essential oil, absolute ethyl alcohol 4-10
Part, 4-10 parts of glycerine, 2-8 parts of diatomite, 1-2 parts of enzyme preparation, 10-20 parts of deionized water.
2. a kind of soap with natural flower aroma according to claim 1, it is characterised in that:The plants essential oil is rose
Essential oil and peppermint oil press proportion 2:1 is made, and plants essential oil is obtained after Rosa Damascana and peppermint oil are stirred evenly.
3. a kind of soap with natural flower aroma according to claim 1, it is characterised in that:The grease includes peanut
It is one or more in oil, soya-bean oil, linseed oil, castor oil, olive oil.
4. a kind of soap with natural flower aroma according to claim 1, it is characterised in that:The anion surface active
Agent is C11-C18 alkylbenzene sulfonates, C12-C18 alkyl alkoxy sulfates, α-sodium olefin sulfonate, C14-C18 fatty acid methyls
It is one or more in sulfonated ester.
5. a kind of soap with natural flower aroma according to claim 1, it is characterised in that:The enzyme preparation is albumen
It is one or more in enzyme, amylase, cellulase, lipase, pectase.
6. a kind of preparation method of the soap described in claim 1 with natural flower aroma, it is characterised in that:Including walking as follows
Suddenly:
S1, raw material is weighed:Weigh following components respectively in parts by weight:25-35 parts of grease, 20-30 parts of sodium hydroxide solution,
5-10 parts of anion surfactant, 2-6 parts of plants essential oil, 4-10 parts of absolute ethyl alcohol, 4-10 parts of glycerine, 2-8 parts of diatomite, enzyme
1-2 parts of preparation, 10-20 parts of deionized water;
S2, soap lye is prepared:Institute is added in grease, absolute ethyl alcohol, anion surfactant, sodium hydroxide solution described in S1
It in the deionized water stated, is uniformly mixed, obtains soap lye;
S3, saponification is carried out:The soap lye obtained in S2 is heated to 80-100 DEG C of progress saponification 6-12h, saponification
After the completion, by described in S1 glycerine and diatomaceous premixed liquid be added thereto, stir evenly, be cooled to 30-50 DEG C, in acquisition
Between mixed solution;
S4, the liquid soap with natural flower aroma is prepared:It, will be in S1 when the intermediate mixed solution that S3 is obtained is cooled to 30-50 DEG C
The plants essential oil and enzyme preparation sequentially adds wherein, stirs evenly, and be cooled to room temperature, and obtains the fertilizer with natural flower aroma
Soap lye;
S5, cooling and shaping:The liquid soap with natural flower aroma that the S4 is obtained is poured into mold, is cooled and shaped, and use
Vacuum freecing-dry machine is freeze-dried, that is, obtains the soap with natural flower aroma.
7. a kind of preparation method of soap with natural flower aroma according to claim 6, it is characterised in that:In S3, institute
The pH value for stating intermediate mixed solution is 10-12.
8. a kind of preparation method of soap with natural flower aroma according to claim 6, it is characterised in that:In S5, institute
The temperature for stating freeze-drying is -50--60 DEG C, and the time of freeze-drying is 10-15h.
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CN201810325079.3A CN108359554A (en) | 2018-04-12 | 2018-04-12 | A kind of soap and preparation method thereof with natural flower aroma |
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CN201810325079.3A CN108359554A (en) | 2018-04-12 | 2018-04-12 | A kind of soap and preparation method thereof with natural flower aroma |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111205944A (en) * | 2020-03-28 | 2020-05-29 | 阚海辉 | Foamless non-brush paste and preparation method thereof |
CN112574834A (en) * | 2020-12-23 | 2021-03-30 | 山东农业大学 | Sterilizing and inflammation-diminishing soap and preparation method thereof |
CN112877153A (en) * | 2021-01-19 | 2021-06-01 | 北京圣永制药有限公司 | Perfumed soap with moisturizing and sterilizing functions and preparation method thereof |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107828564A (en) * | 2017-10-30 | 2018-03-23 | 胡国剑 | A kind of soap for being capable of mosquito-expelling bactericidal and preparation method thereof |
-
2018
- 2018-04-12 CN CN201810325079.3A patent/CN108359554A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107828564A (en) * | 2017-10-30 | 2018-03-23 | 胡国剑 | A kind of soap for being capable of mosquito-expelling bactericidal and preparation method thereof |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111205944A (en) * | 2020-03-28 | 2020-05-29 | 阚海辉 | Foamless non-brush paste and preparation method thereof |
CN112574834A (en) * | 2020-12-23 | 2021-03-30 | 山东农业大学 | Sterilizing and inflammation-diminishing soap and preparation method thereof |
CN112877153A (en) * | 2021-01-19 | 2021-06-01 | 北京圣永制药有限公司 | Perfumed soap with moisturizing and sterilizing functions and preparation method thereof |
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