CN102634421A - Clothes washing agent and preparation method thereof - Google Patents
Clothes washing agent and preparation method thereof Download PDFInfo
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- CN102634421A CN102634421A CN2012100942738A CN201210094273A CN102634421A CN 102634421 A CN102634421 A CN 102634421A CN 2012100942738 A CN2012100942738 A CN 2012100942738A CN 201210094273 A CN201210094273 A CN 201210094273A CN 102634421 A CN102634421 A CN 102634421A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 238000005406 washing Methods 0.000 title abstract description 22
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000010438 heat treatment Methods 0.000 claims abstract description 22
- -1 chloromethane isothiazole chinoline ketone Chemical class 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims abstract description 12
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 claims abstract description 10
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 10
- 229910021538 borax Inorganic materials 0.000 claims abstract description 10
- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical compound CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 claims abstract description 10
- HEGSGKPQLMEBJL-RKQHYHRCSA-N octyl beta-D-glucopyranoside Chemical compound CCCCCCCCO[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HEGSGKPQLMEBJL-RKQHYHRCSA-N 0.000 claims abstract description 10
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 10
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 10
- 239000000463 material Substances 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 230000001954 sterilising effect Effects 0.000 claims abstract description 8
- 238000005303 weighing Methods 0.000 claims abstract description 8
- 239000003599 detergent Substances 0.000 claims description 28
- 238000003756 stirring Methods 0.000 claims description 28
- 238000001816 cooling Methods 0.000 claims description 21
- 239000008367 deionised water Substances 0.000 claims description 16
- 229910021641 deionized water Inorganic materials 0.000 claims description 16
- 239000000843 powder Substances 0.000 claims description 13
- FKMHSNTVILORFA-UHFFFAOYSA-N 2-[2-(2-dodecoxyethoxy)ethoxy]ethanol Chemical compound CCCCCCCCCCCCOCCOCCOCCO FKMHSNTVILORFA-UHFFFAOYSA-N 0.000 claims description 9
- 239000001110 calcium chloride Substances 0.000 claims description 9
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 9
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims description 9
- 229940057905 laureth-3 Drugs 0.000 claims description 9
- GJWJYZYRBDJBHK-UHFFFAOYSA-N quinoline;sodium Chemical compound [Na].N1=CC=CC2=CC=CC=C21 GJWJYZYRBDJBHK-UHFFFAOYSA-N 0.000 claims description 9
- RRLOOYQHUHGIRJ-UHFFFAOYSA-M sodium;ethyl sulfate Chemical compound [Na+].CCOS([O-])(=O)=O RRLOOYQHUHGIRJ-UHFFFAOYSA-M 0.000 claims description 9
- DWHIUNMOTRUVPG-UHFFFAOYSA-N 2-[2-[2-[2-[2-[2-(2-dodecoxyethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethanol Chemical compound CCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCO DWHIUNMOTRUVPG-UHFFFAOYSA-N 0.000 claims description 7
- 229920002884 Laureth 4 Polymers 0.000 claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 7
- 229940031674 laureth-7 Drugs 0.000 claims description 7
- 229940062711 laureth-9 Drugs 0.000 claims description 7
- ONJQDTZCDSESIW-UHFFFAOYSA-N polidocanol Chemical compound CCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO ONJQDTZCDSESIW-UHFFFAOYSA-N 0.000 claims description 7
- 238000004659 sterilization and disinfection Methods 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 7
- 244000178870 Lavandula angustifolia Species 0.000 claims description 2
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims description 2
- 241000220317 Rosa Species 0.000 claims description 2
- 239000000796 flavoring agent Substances 0.000 claims description 2
- 235000019634 flavors Nutrition 0.000 claims description 2
- 239000001102 lavandula vera Substances 0.000 claims description 2
- 235000018219 lavender Nutrition 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 2
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 abstract 4
- 239000003795 chemical substances by application Substances 0.000 abstract 3
- 239000004382 Amylase Substances 0.000 abstract 1
- 102000013142 Amylases Human genes 0.000 abstract 1
- 108010065511 Amylases Proteins 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 108091005804 Peptidases Proteins 0.000 abstract 1
- 239000004365 Protease Substances 0.000 abstract 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 abstract 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 1
- 150000001335 aliphatic alkanes Chemical group 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 235000019418 amylase Nutrition 0.000 abstract 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- ZPNJWPCCRZGDRL-UHFFFAOYSA-N sodium 2-ethyl-4,5-dihydroimidazol-3-ide Chemical compound C(C)C=1N(CCN1)[Na] ZPNJWPCCRZGDRL-UHFFFAOYSA-N 0.000 abstract 1
- 239000007788 liquid Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 230000008417 skin turnover Effects 0.000 description 4
- 206010040844 Skin exfoliation Diseases 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- 206010040880 Skin irritation Diseases 0.000 description 2
- 230000036556 skin irritation Effects 0.000 description 2
- 231100000475 skin irritation Toxicity 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 206010028980 Neoplasm Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
Landscapes
- Detergent Compositions (AREA)
Abstract
The invention discloses a clothes washing agent and a preparation method thereof. The preparation method comprises the following preparation steps of: weighing raw materials, mixing water with lauryl alcohol polyether-7, lauryl alcohol polyether-9, Prifer 6813, lauryl alcohol polyether-3 and lauryl alcohol sulfate sodium to obtain a basic material; pouring water into a cold-hot cylinder and dissolve anhydrous calcium chloride in water; adding the basic material, and heating for sterilizing; adding C14-17 secondary alkane sulphonate sodium when the temperature is reduced to 58-62 DEG C, and mixing and dissolving; adding octyl glucoside when the temperature is reduced to 48-52 DEG C, mixing and dissolving, and adjusting pH (potential of hydrogen); adding two dicarboxylic ethyl coco phosphoric ethyl imidazolinyl sodium, methanol and borax when the temperature is reduced to 43-47 DEG C, and uniformly mixing; and adding alkali protease, amylase, chloromethane isothiazole chinoline ketone, methylisothiazolinone and essence when the temperature is reduced to 36-40 DEG C, uniformly mixing, thus obtaining the washing agent. The clothing washing agent provided by the invention has slight skin stimulus, and has good cleaning effect.
Description
Technical field
The invention belongs to the household cleaning product, relate to a kind of laundry detergent and preparation method thereof specifically.
Background technology
With average annual 27.2% speed increment, nearest 3 years growth has surpassed 100% in the washing liquid market of China.Simultaneously, the average annual growth rate in washing powder market is merely 2.2%.It was expected that domestic washing liquid will reach 30% after 2015.And in the U.S., the market share of washing liquid has surpassed washing powder at present, and accounting reaches more than 80%, has much the gesture that substitutes washing powder.
No matter be washing liquid or washing powder; Topmost requirement is that the adversary does not produce stimulation; Promptly when washing clothes, do not hinder hand; Tradition washing liquid detersive power is not strong, rinsing is difficult, water consumption is big, chemical residual is more, has all added chemical assistant in most of on the market washing liquid simultaneously, for example white dyes, sequestrant, organic solvent etc.Especially white dyes is the chemical ingredients that causes and bring out cancer, the stimulation that also has the adversary that has.
Summary of the invention
The objective of the invention is to overcome the deficiency of prior art, provide a kind of biological degradation rate high, the Man & Nature environment is had no effect.Poisonous chemical ingredientss such as without phosphorus, no aluminium, no white dyes, adversary's bland laundry detergent simultaneously.
Second purpose of the present invention provides a kind of preparation method of laundry detergent.
Technical scheme of the present invention is summarized as follows:
A kind of preparation method of laundry detergent comprises the steps:
(1) takes by weighing raw material by weight percentage: Calcium Chloride Powder Anhydrous 0.01-0.02%, laureth sodium sulfovinate 4-8%, laureth-93-5%, laureth-73-5%; Laureth-3 1-3%, Prifer 6813 0.5-1.2%, octyl glucoside 1-3%, borax 1-2%; C14-17 SAS 2-4%, two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium 1-2%, methyl alcohol 0.5-1%; Sumizyme MP 0.3-0.5%, methylchloroisothiazandnone 0.01-0.03%, methylisothiazolinone 0.01-0.03%; Glycase 0.2-0.5%, essence 0.1-0.2%, all the other are deionized water;
(2) under the normal temperature condition, said laureth-7, laureth-9, Prifer 6813, laureth-3 and laureth sodium sulfovinate are added in first Cooling or heating jar, add small amount of deionized water, make its mixing, obtain basestocks;
(3) under the normal temperature condition, will remain deionized water and pour in second Cooling or heating jar, drop into said Calcium Chloride Powder Anhydrous, stirring and dissolving;
(4) under the normal temperature condition said basestocks is rendered in second Cooling or heating jar, fully stirred and treat that material all is warming up to 85 ℃-90 ℃ sterilizations 10-15 minute after the dissolving;
(5) be cooled to 58-62 ℃, add said C14-17 SAS, stirring and dissolving;
(6) be cooled to 48-52 ℃, add said octyl glucoside, the insulated and stirred dissolving adds Hydrocerol A and regulates pH=6-8;
(7) be cooled to 43-47 ℃, add said two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium, methyl alcohol and borax, stir;
(8) be cooled to 36-40 ℃, add said Sumizyme MP, glycase, methylchloroisothiazandnone, methylisothiazolinone and essence, after stirring, promptly get a kind of laundry detergent.
Said essence is rose scent essence or lavender flavor type essence.
The laundry detergent of method for preparing.
A kind of cleaning clothes washing composition of the present invention not only is rich in the activeconstituents of taking from natural matter; Clean effective; Test the moisture of skin turnover rate before proof laundry detergent of the present invention uses the back to the very approaching use of moisture of skin turnover rate; Explain that laundry detergent of the present invention is little to skin irritation, a kind of cleaning clothes washing composition of the present invention can save energy, reduce accumulation and the harm of Harmful chemicals in environment, is beneficial to the protection environment.
Embodiment
Embodiment below in conjunction with concrete is further described the present invention.
The proportioning raw materials of embodiment 1-embodiment 5 is seen table 1
Table 1
ProductName Prifer 6813 is that Croda Singapore Pte Ltd production is sold composition title: Alkyl ester.
Embodiment 6
A kind of preparation method of laundry detergent comprises the steps:
(1) take by weighing raw material shown in the embodiment 1 by weight percentage:
(2) under the normal temperature condition, said laureth-7, laureth-9, Prifer 6813, laureth-3 and laureth sodium sulfovinate are added in first Cooling or heating jar, add small amount of deionized water, make its mixing, obtain basestocks;
(3) under the normal temperature condition, will remain deionized water and pour in second Cooling or heating jar, drop into said Calcium Chloride Powder Anhydrous, stirring and dissolving;
(4) under the normal temperature condition said basestocks is rendered in second Cooling or heating jar, fully stirred and treat that material all is warming up to 87 ℃ of sterilizations 13 minutes after the dissolving;
(5) be cooled to 6 () ℃, add said C14-17 SAS, stirring and dissolving;
(6) be cooled to 50 ℃, add said octyl glucoside, the insulated and stirred dissolving adds Hydrocerol A and regulates pH=7;
(7) be cooled to 45 ℃, add said two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium, methyl alcohol and borax, stir;
(8) be cooled to 38 ℃, add said Sumizyme MP, glycase, methylchloroisothiazandnone, methylisothiazolinone and essence, after stirring, promptly get a kind of laundry detergent.
Embodiment 7
A kind of preparation method of laundry detergent comprises the steps:
(1) take by weighing raw material shown in the embodiment 2 by weight percentage:
(2) under the normal temperature condition, said laureth-7, laureth-9, Prifer 6813, laureth-3 and laureth sodium sulfovinate are added in first Cooling or heating jar, add small amount of deionized water, make its mixing, obtain basestocks;
(3) under the normal temperature condition, will remain deionized water and pour in second Cooling or heating jar, drop into said Calcium Chloride Powder Anhydrous, stirring and dissolving;
(4) under the normal temperature condition said basestocks is rendered in second Cooling or heating jar, fully stirred and treat that material all is warming up to 85 ℃ of sterilizations 15 minutes after the dissolving;
(5) be cooled to 58 ℃, add said C14-17 SAS, stirring and dissolving;
(6) be cooled to 48 ℃, add said octyl glucoside, the insulated and stirred dissolving adds Hydrocerol A and regulates pH=8;
(7) be cooled to 43 ℃, add said two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium, methyl alcohol and borax, stir;
(8) be cooled to 36 ℃, add said Sumizyme MP, glycase, methylchloroisothiazandnone, methylisothiazolinone and essence, after stirring, promptly get a kind of laundry detergent.
Embodiment 8
A kind of preparation method of laundry detergent comprises the steps:
(1) take by weighing raw material shown in the embodiment 3 by weight percentage:
(2) under the normal temperature condition, said laureth-7, laureth-9, Prifer 6813, laureth-3 and laureth sodium sulfovinate are added in first Cooling or heating jar, add small amount of deionized water, make its mixing, obtain basestocks;
(3) under the normal temperature condition, will remain deionized water and pour in second Cooling or heating jar, drop into said Calcium Chloride Powder Anhydrous, stirring and dissolving;
(4) under the normal temperature condition said basestocks is rendered in second Cooling or heating jar, fully stirred and treat that material all is warming up to 86 ℃ of sterilizations 13 minutes after the dissolving;
(5) be cooled to 59 ℃, add said C14-17 SAS, stirring and dissolving;
(6) be cooled to 49 ℃, add said octyl glucoside, the insulated and stirred dissolving adds Hydrocerol A and regulates pH=7;
(7) be cooled to 44 ℃, add said two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium, methyl alcohol and borax, stir;
(8) be cooled to 37 ℃, add said Sumizyme MP, glycase, methylchloroisothiazandnone, methylisothiazolinone and essence, after stirring, promptly get a kind of laundry detergent.
Embodiment 9
A kind of preparation method of laundry detergent comprises the steps:
(1) take by weighing raw material shown in the embodiment 4 by weight percentage:
(2) under the normal temperature condition, said laureth-7, laureth-9, Prifer 6813, laureth-3 and laureth sodium sulfovinate are added in first Cooling or heating jar, add small amount of deionized water, make its mixing, obtain basestocks;
(3) under the normal temperature condition, will remain deionized water and pour in second Cooling or heating jar, drop into said Calcium Chloride Powder Anhydrous, stirring and dissolving;
(4) under the normal temperature condition said basestocks is rendered in second Cooling or heating jar, fully stirred and treat that material all is warming up to 88 ℃ of sterilizations 11 minutes after the dissolving;
(5) be cooled to 61 ℃, add said C14-17 SAS, stirring and dissolving;
(6) be cooled to 51 ℃, add said octyl glucoside, the insulated and stirred dissolving adds Hydrocerol A and regulates pH=8;
(7) be cooled to 46 ℃, add said two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium, methyl alcohol and borax, stir;
(8) be cooled to 39 ℃, add said Sumizyme MP, glycase, methylchloroisothiazandnone, methylisothiazolinone and essence, after stirring, promptly get a kind of laundry detergent.
Embodiment 10
A kind of preparation method of laundry detergent comprises the steps:
(1) take by weighing raw material shown in the embodiment 5 by weight percentage:
(2) under the normal temperature condition, said laureth-7, laureth-9, Prifer 6813, laureth-3 and laureth sodium sulfovinate are added in first Cooling or heating jar, add small amount of deionized water, make its mixing, obtain basestocks;
(3) under the normal temperature condition, will remain deionized water and pour in second Cooling or heating jar, drop into said Calcium Chloride Powder Anhydrous, stirring and dissolving;
(4) under the normal temperature condition said basestocks is rendered in second Cooling or heating jar, fully stirred and treat that material all is warming up to 90 ℃ of sterilizations 10 minutes after the dissolving;
(5) be cooled to 62 ℃, add said C14-17 SAS, stirring and dissolving;
(6) be cooled to 52 ℃, add said octyl glucoside, the insulated and stirred dissolving adds Hydrocerol A and regulates pH=6;
(7) be cooled to 47 ℃, add said two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium, methyl alcohol and borax, stir;
(8) be cooled to 40 ℃, add said Sumizyme MP, glycase, methylchloroisothiazandnone, methylisothiazolinone and essence, after stirring, promptly get a kind of laundry detergent.
Embodiment 11
Moisture of skin loss test experiments.Moisture of skin loss TEWL is unusual important parameters to the function of assessing skin moisture resist, has obtained approval widely in the world.The moisture of skin resist is intact more, and the content of moisture will be high more, and the numerical value of moisture of skin loss TEWL is just low more, and the unit of TEWL is: g/hm
2Skinanalysis apparatus is Tewameter TM300.
Choose 20-50 women 90 people between year; Be divided into 6 groups at random; Every group 15 people; Under identical relative humidity (50%), temperature (25 ℃) condition, use common commercially available washing liquid of certain brand and laundry detergent of the present invention (being followed successively by embodiment 6-10 preparation) to clean hand respectively, get to reach before same area is cleaned and clean the back skin test.Use laundry detergent of the present invention (being followed successively by embodiment 6-10 preparation) to clean front and back water loss difference and on average be followed successively by 11.3g/hm
2, 12.1g/hm
2, 12.0g/hm
2, 11.8g/hm
2And 12.4g/hm
2, use the common commercially available washing liquid of certain brand to clean front and back water loss difference average out to 27.1g/hm
2, experimental result shows that the moisture of skin turnover rate before laundry detergent of the present invention uses the back to the very approaching use of moisture of skin turnover rate explains that laundry detergent of the present invention is little to skin irritation.
Embodiment 12
Get 18 underwears (upper and lower clothing one cover) of wearing 5 days, be divided into 6 groups at random, every group 3 cover, the 1st group is with commercially available common washing composition, machine washing, water consumption 10L, clean-out system consumption 20mL; The 2-6 group is followed successively by the laundry detergent of embodiment 6-10 preparation, water consumption 10L, clean-out system consumption 10mL; Each warm water soaking 20 minutes before washing, the 1st group when using 20 minutes, underwear is cleaned, the 2-6 group time spent was followed successively by 14,15,15,14 and 15 minutes, and underwear is cleaned.
Claims (3)
1. the preparation method of a laundry detergent is characterized in that comprising the steps:
(1) takes by weighing raw material by weight percentage: Calcium Chloride Powder Anhydrous 0.01-0.02%, laureth sodium sulfovinate 4-8%, laureth-93-5%, laureth-73-5%; Laureth-3 1-3%, Prifer 68130.5-1.2%, octyl glucoside 1-3%, borax 1-2%; C14-17 SAS 2-4%, two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium 1-2%, methyl alcohol 0.5-1%; Sumizyme MP 0.3-0.5%, methylchloroisothiazandnone 0.01-0.03%, methylisothiazolinone 0.01-0.03%; Glycase 0.2-0.5%, essence 0.1-0.2%, all the other are deionized water;
(2) under the normal temperature condition, said laureth-7, laureth-9, Prifer 6813, laureth-3 and laureth sodium sulfovinate are added in first Cooling or heating jar, add small amount of deionized water, make its mixing, obtain basestocks;
(3) under the normal temperature condition, will remain deionized water and pour in second Cooling or heating jar, drop into said Calcium Chloride Powder Anhydrous, stirring and dissolving;
(4) under the normal temperature condition said basestocks is rendered in second Cooling or heating jar, fully stirred and treat that material all is warming up to 85 ℃-90 ℃ sterilizations 10-15 minute after the dissolving;
(5) be cooled to 58-62 ℃, add said C14-17 SAS, stirring and dissolving;
(6) be cooled to 48-52 ℃, add said octyl glucoside, the insulated and stirred dissolving adds Hydrocerol A and regulates pH=6-8;
(7) be cooled to 43-47 ℃, add said two propyloic cocoyl phosphoric acid ethyl imidazol(e) quinoline sodium, methyl alcohol and borax, stir;
(8) be cooled to 36-40 ℃, add said Sumizyme MP, glycase, methylchloroisothiazandnone, methylisothiazolinone and essence, after stirring, promptly get a kind of laundry detergent.
2. the preparation method of a kind of laundry detergent according to claim 1 is characterized in that said essence is rose scent essence or lavender flavor type essence.
3. the laundry detergent of claim 1 or 2 method preparation.
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| CN201210094273.8A CN102634421B (en) | 2012-03-31 | 2012-03-31 | laundry detergent and preparation method thereof |
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| CN102634421A true CN102634421A (en) | 2012-08-15 |
| CN102634421B CN102634421B (en) | 2016-02-17 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103740492A (en) * | 2013-12-27 | 2014-04-23 | 天津天狮生物发展有限公司 | Concentrated washing solution and preparation method thereof |
| CN107418765A (en) * | 2017-07-27 | 2017-12-01 | 合肥远科服装设计有限公司 | A kind of degerming liquid detergent not hurt hands of color protection |
| CN107603758A (en) * | 2017-10-13 | 2018-01-19 | 洛娃科技实业集团有限公司 | A kind of liquid detergent and preparation method |
| CN108441299A (en) * | 2018-04-13 | 2018-08-24 | 华阳新兴科技（天津）集团有限公司 | A kind of water displaced type film rust proof oil and preparation method thereof |
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- 2012-03-31 CN CN201210094273.8A patent/CN102634421B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1322802A (en) * | 2001-06-04 | 2001-11-21 | 贾发颂 | Phosphate-free liquid detergent and its compounding process |
| CN102154068A (en) * | 2011-03-03 | 2011-08-17 | 天津天狮生物发展有限公司 | Multifunctional detergent and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103740492A (en) * | 2013-12-27 | 2014-04-23 | 天津天狮生物发展有限公司 | Concentrated washing solution and preparation method thereof |
| CN107418765A (en) * | 2017-07-27 | 2017-12-01 | 合肥远科服装设计有限公司 | A kind of degerming liquid detergent not hurt hands of color protection |
| CN107603758A (en) * | 2017-10-13 | 2018-01-19 | 洛娃科技实业集团有限公司 | A kind of liquid detergent and preparation method |
| CN108441299A (en) * | 2018-04-13 | 2018-08-24 | 华阳新兴科技（天津）集团有限公司 | A kind of water displaced type film rust proof oil and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102634421B (en) | 2016-02-17 |
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