CN107828564A - A kind of soap for being capable of mosquito-expelling bactericidal and preparation method thereof - Google Patents
A kind of soap for being capable of mosquito-expelling bactericidal and preparation method thereof Download PDFInfo
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- CN107828564A CN107828564A CN201711052454.3A CN201711052454A CN107828564A CN 107828564 A CN107828564 A CN 107828564A CN 201711052454 A CN201711052454 A CN 201711052454A CN 107828564 A CN107828564 A CN 107828564A
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- soap
- mosquito
- extract solution
- liquid
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
Abstract
The invention discloses a kind of soap for being capable of mosquito-expelling bactericidal, is made up of by mass percentage following components：Anion surfactant 10 20%, grease 25 35%, sodium hydroxide solution 20 30%, natural product extraction liquid 2 6%, absolute ethyl alcohol 1 10%, glycerine 1 10%, diatomite 2 8%, sucrose 1 15%, enzyme preparation 1 2%, spices 0.2 0.5%, sodium hypochlorite 0.8 1.5%, remaining be deionized water；The invention also discloses the preparation method of the soap.The present invention is by regarding natural product extraction liquid (jasmine extract solution, lemon extract, sweet osmanthus extract solution, China pink extract solution, lily of the valley extract solution, violet extract solution, rose extract solution) and diatomite as bactericide and culicifuge for preparing pure natural soap, so that obtained soap has, mosquito-expelling bactericidal adsorption capacity is strong, clean effect is good, smell is pure and fresh, nourishes rough skin, it is nontoxic the characteristics of.
Description
Technical field
The invention belongs to daily living article technical field, and in particular to a kind of soap for being capable of mosquito-expelling bactericidal and its preparation
Method.
Background technology
Soap has had thousands of years history, is the general name of fatty acid metal salts, can be dissolved in water, there is washing decontamination.Its
Mainly saponification is occurred for grease and sodium hydroxide by basic preparation method, generates higher fatty acids sodium and glycerine, Ran Houzai
It is made by washing, adding the techniques such as spices, shaping and drying.Antimicrobial soap is in preparation process, adds antibacterial material,
Make it have certain antibacterial functions；Antimicrobial soap huge number at present, but the removal of bacteria effect on clothing and unobvious,
And Conventional soaps contain the material being harmful to human body skin：Such as bleaching powder, mercury, cleaning agent, corrosive agent.Therefore, exploitation contains
There is natural antibacterial ingredient and there is clean effect, and have great importance to the soap of human body fanout free region.
The production of soap product has a long history, and about with regard to useful grease and contains potassium carbonate at B.C. 2500
Plant ass produce potash soap, and the record of wool is washed with this soap；Since 19th century, due to the hair of Leblanc soda ash production method
Exhibition, makes the production of soap enter the industrialized stage；Now, as the improvement of people's living standards, people are for material
The requirement of life also more and more higher, soap products at present on the market are different, and people use rear dry skin, easy allergy, and
And mosquito repellent, bactericidal effect are bad.
The content of the invention
In view of this, it is a primary object of the present invention to provide a kind of soap for being capable of mosquito-expelling bactericidal, solves existing skill
Repelling effect is poor in art, sterilizes halfway problem；Present invention also offers the preparation method of the soap.
To reach above-mentioned purpose, the technical proposal of the invention is realized in this way：A kind of soap for being capable of mosquito-expelling bactericidal, by
Following components forms by mass percentage：It is made up of by mass percentage following components：Anion surfactant 10-20%,
Grease 25-35%, sodium hydroxide solution 20-30%, natural product extraction liquid 2-6%, absolute ethyl alcohol 1-10%, glycerine 1-
10%th, diatomite 2-8%, sucrose 1-15%, enzyme preparation 1-2%, spices 0.2-0.5%, sodium hypochlorite 0.8-1.5%, remaining
For deionized water.
Preferably, the natural product extraction liquid is jasmine extract solution, lemon extract, sweet osmanthus extract solution, China pink extraction
One or more in liquid, lily of the valley extract solution, violet extract solution, rose extract solution.
Preferably, the anion surfactant is C11-C18Alkylbenzenesulfonate, C12-C18Alkyl alkoxy sulfuric acid
Salt, α-sodium olefin sulfonate, C14-C18One or more in MES.
Preferably, the spices is the one or more in rose extract solution, pawpaw extract solution or lavender extract solution.
Preferably, the grease includes the one or more in butter, castor oil or coconut oil.
Preferably, the enzyme preparation is protease, amylase, cellulase, lipase, pectase, mannonase mistake
One or more in oxide enzyme.
What another technical scheme of the present invention was realized in：A kind of preparation method for the soap for being capable of mosquito-expelling bactericidal,
This method is achieved by the steps of：
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：Anion surfactant 10-
20%th, grease 25-35%, sodium hydroxide solution 20-30%, natural product extraction liquid 2-6%, absolute ethyl alcohol 1-10%, glycerine
1-10%, diatomite 2-8%, sucrose 1-15%, enzyme preparation 1-2%, spices 0.2-0.5%, sodium hypochlorite 0.8-1.5%, its
Remaining is deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 45-100 DEG C of progress saponification 2-10h, saponification
After the completion of reactions, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirs, is cooled to 35-80 DEG C,
Mixed solution among obtaining；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：Treat that the middle mixed solution that the step 3 obtains is cooled to 35-80 DEG C
When, natural product extraction liquid, diatomite, enzyme preparation, spices, the sodium hypochlorite described in step 1 are sequentially added wherein, stirring
Uniformly, and room temperature is cooled to, obtains mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
It is freeze-dried using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Preferably, the pH value of the middle mixed solution is 7-11.
Preferably, the temperature of the freeze-drying is -45--55 DEG C, and the time of freeze-drying is 20-50h.
Compared with prior art, the present invention is by by natural product extraction liquid (jasmine extract solution, lemon extract, sweet osmanthus
Extract solution, China pink extract solution, lily of the valley extract solution, violet extract solution, rose extract solution) and diatomite as bactericide and drive
Mosquito agent is used to prepare pure natural soap so that obtained soap has that mosquito-expelling bactericidal adsorption capacity is strong, clean effect is good, gas
Taste is pure and fresh, nourishes rough skin, it is nontoxic the characteristics of；And soap of the present invention is for the soap of prior art, also with user
Just, the advantages of antibacterial effect is substantially and production cost is low；Preparation method of the present invention, simple with method, production cost is low, and
The characteristics of large-scale production can be applied to and be widely popularized.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
A kind of soap for being capable of mosquito-expelling bactericidal provided in an embodiment of the present invention, is made up of by mass percentage following components：
Anion surfactant 10-20%, grease 25-35%, sodium hydroxide solution 20-30%, natural product extraction liquid 2-6%,
It is absolute ethyl alcohol 1-10%, glycerine 1-10%, diatomite 2-8%, sucrose 1-15%, enzyme preparation 1-2%, spices 0.2-0.5%, secondary
Sodium chlorate 0.8-1.5%, remaining be deionized water.
Wherein, natural product extraction liquid is jasmine extract solution, lemon extract, sweet osmanthus extract solution, China pink extract solution, the lily of the valley
One or more in extract solution, violet extract solution, rose extract solution；Rose, sweet osmanthus, violet, jasmine, lemon, rose,
Volatility oils has significant bactericidal action caused by the fragrant flowers such as China pink, the lily of the valley, crape myrtle；Crape myrtle, jasmine, lemon etc. are planted
Thing, can kills the probiotics such as diphtheria bacterium and dysentery bacillus, rose, China pink, the lily of the valley, violet, rose, sweet osmanthus etc. in 5 minutes
The fragrance that plant distributes has obvious inhibitory action to tubercle bacillus, pneumococcus, staphylococcic growth and breeding.
Wherein, anion surfactant C11~C18Alkylbenzenesulfonate, C12~C18Alkyl alkoxy sulfate, α-
Sodium olefin sulfonate, C14~C18One or more in MES；Spices is rose extract solution, pawpaw extract solution
Or the one or more in lavender extract solution；Grease includes the one or more in butter, castor oil or coconut oil；Enzyme preparation
For the one or more in protease, amylase, cellulase, lipase, pectase, mannonase peroxidase.
The embodiment of the present invention additionally provides a kind of preparation method for the soap for being capable of mosquito-expelling bactericidal, and this method by walking as follows
It is rapid to realize：
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate 10-
20%th, grease 25-35%, sodium hydroxide solution 20-30%, natural product extraction liquid 2-6%, absolute ethyl alcohol 1-10%, glycerine
1-10%, diatomite 2-8%, sucrose 1-15%, lipase 1-2%, rose extract solution 0.2-0.5%, sodium hypochlorite 0.8-
1.5%th, remaining is deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 45-100 DEG C of progress saponification 2-10h, saponification
After the completion of reactions, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirs, is cooled to 35-80 DEG C,
Obtain the middle mixed solution that pH value is 7-11；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：Treat that the middle mixed solution that the step 3 obtains is cooled to 35-80 DEG C
When, natural product extraction liquid, diatomite, enzyme preparation, spices, the sodium hypochlorite described in step 1 are sequentially added wherein, stirring
Uniformly, and room temperature is cooled to, obtains mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -45--55 DEG C, freeze-drying 20-50h is carried out using vacuum freeze drier, that is, obtains the fertilizer for being made and being capable of mosquito-expelling bactericidal
Soap.
Compared with prior art, the present invention is by by natural product extraction liquid (jasmine extract solution, lemon extract, sweet osmanthus
Extract solution, China pink extract solution, lily of the valley extract solution, violet extract solution, rose extract solution) and diatomite as bactericide and drive
Mosquito agent is used to prepare pure natural soap so that obtained soap has that mosquito-expelling bactericidal adsorption capacity is strong, clean effect is good, gas
Taste is pure and fresh, nourishes rough skin, it is nontoxic the characteristics of；And soap of the present invention is for the soap of prior art, also with user
Just, the advantages of antibacterial effect is substantially and production cost is low；Preparation method of the present invention, simple with method, production cost is low, and
The characteristics of large-scale production can be applied to and be widely popularized.
Embodiment 1
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
15%th, grease 20%, sodium hydroxide solution 25%, natural product extraction liquid 5%, absolute ethyl alcohol 5%, glycerine 5%, diatomite
4%th, sucrose 8%, lipase 1.5%, rose extract solution 0.3%, sodium hypochlorite 1%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 70 DEG C of progress saponification 6h, saponification is completed
Afterwards, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 55 DEG C, it is 7 to obtain pH value
~11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 55 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -50 DEG C, freeze-drying 40h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Embodiment 2
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
15%th, grease 20%, sodium hydroxide solution 25%, natural product extraction liquid 5%, absolute ethyl alcohol 5%, glycerine 5%, diatomite
4%th, sucrose 8%, lipase 1.5%, rose extract solution 0.3%, sodium hypochlorite 1%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 45 DEG C of progress saponification 2hh, saponification is complete
Cheng Hou, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 35 DEG C, obtaining pH value is
7~11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 35 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -45 DEG C, freeze-drying 20h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Embodiment 3
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
15%th, grease 20%, sodium hydroxide solution 25%, natural product extraction liquid 5%, absolute ethyl alcohol 5%, glycerine 5%, diatomite
4%th, sucrose 8%, lipase 1.5%, rose extract solution 0.3%, sodium hypochlorite 1%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 100 DEG C of progress saponification 10h, saponification is complete
Cheng Hou, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 80 DEG C, obtaining pH value is
7-11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 80 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -55 DEG C, freeze-drying 50h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Embodiment 4
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
10%th, grease 35%, sodium hydroxide solution 20%, natural product extraction liquid 2%, absolute ethyl alcohol 1%, glycerine 1%, diatomite
8%th, sucrose 15%, lipase 1%, rose extract solution 0.5%, sodium hypochlorite 1.5%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 70 DEG C of progress saponification 6h, saponification is completed
Afterwards, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 55 DEG C, it is 7 to obtain pH value
~11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 55 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -50 DEG C, freeze-drying 40h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Embodiment 5
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
10%th, grease 35%, sodium hydroxide solution 20%, natural product extraction liquid 2%, absolute ethyl alcohol 1%, glycerine 1%, diatomite
8%th, sucrose 15%, lipase 1%, rose extract solution 0.5%, sodium hypochlorite 1.5%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 45 DEG C of progress saponification 2hh, saponification is complete
Cheng Hou, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 35 DEG C, obtaining pH value is
7~11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 35 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -45 DEG C, freeze-drying 20h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Embodiment 6
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
10%th, grease 35%, sodium hydroxide solution 20%, natural product extraction liquid 2%, absolute ethyl alcohol 1%, glycerine 1%, diatomite
8%th, sucrose 15%, lipase 1%, rose extract solution 0.5%, sodium hypochlorite 1.5%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 100 DEG C of progress saponification 10h, saponification is complete
Cheng Hou, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 80 DEG C, obtaining pH value is
7-11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 80 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -55 DEG C, freeze-drying 50h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Embodiment 7
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
15%th, grease 20%, sodium hydroxide solution 25%, natural product extraction liquid 5%, absolute ethyl alcohol 5%, glycerine 5%, diatomite
4%th, sucrose 8%, lipase 1.5%, rose extract solution 0.3%, sodium hypochlorite 1%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 45 DEG C of progress saponification 10h, saponification is complete
Cheng Hou, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 35 DEG C, obtaining pH value is
7-11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 35 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -45 DEG C, freeze-drying 50h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Embodiment 8
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：C11~C18Alkylbenzenesulfonate
15%th, grease 20%, sodium hydroxide solution 25%, natural product extraction liquid 5%, absolute ethyl alcohol 5%, glycerine 5%, diatomite
4%th, sucrose 8%, lipase 1.5%, rose extract solution 0.3%, sodium hypochlorite 1%, remaining be deionized water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, anhydrous
Ethanol is added in described deionized water, is uniformly mixed, and obtains soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 100 DEG C of progress saponification 2h, saponification is complete
Cheng Hou, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, be cooled to 80 DEG C, obtaining pH value is
7-11 middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 80 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and
At -55 DEG C, freeze-drying 20h is carried out using vacuum freeze drier, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
Sterilizing ability is tested
In order to verify the sterilizing ability of soap of the present invention, sterilizing ability test is carried out；Experiment condition is：Using
The fertilizer and Conventional soaps that embodiment 1-3 is obtained, in wash conditions identical (dosage of soap, volume of water etc.)
In the case of, to the hand of 4 children of the first and second the third fourths (fourth for use the child of soap that comparative example obtains), (hand of 4 children is being washed
Multiple drug resistance is essentially identical before) washed, and with the residual condition of micro- sem observation hand bacterium, observe result such as following table
1：
The detection data of 1 soap of the present invention of table and existing soap sterilizing ability
| Bacterium residual rate | |
| First | 0.023% |
| Second | 0.016% |
| Third | 0.024% |
| Fourth | 0.105% |
As can be drawn from Table 1：The sterilization of the liquid containing natural product extraction and diatomaceous soap that are obtained using the present invention
Sterilizing ability ability of the ability better than the soap that (comparative example) of prior art obtains.
The foregoing is only a preferred embodiment of the present invention, is not intended to limit the scope of the present invention.
Claims (9)
1. a kind of soap for being capable of mosquito-expelling bactericidal, it is characterised in that be made up of by mass percentage following components：Anionic surface
Activating agent 10-20%, grease 25-35%, sodium hydroxide solution 20-30%, natural product extraction liquid 2-6%, absolute ethyl alcohol 1-
10%th, glycerine 1-10%, diatomite 2-8%, sucrose 1-15%, enzyme preparation 1-2%, spices 0.2-0.5%, sodium hypochlorite 0.8-
1.5%th, remaining is deionized water.
A kind of 2. soap for being capable of mosquito-expelling bactericidal according to claim 1, it is characterised in that the natural product extraction liquid
Carried for jasmine extract solution, lemon extract, sweet osmanthus extract solution, China pink extract solution, lily of the valley extract solution, violet extract solution, rose
Take the one or more in liquid.
A kind of 3. soap for being capable of mosquito-expelling bactericidal according to claim 2, it is characterised in that the anion surface active
Agent is C11-C18Alkylbenzenesulfonate, C12-C18Alkyl alkoxy sulfate, α-sodium olefin sulfonate, C14-C18Fatty acid methyl ester sulphur
One or more in hydrochlorate.
4. a kind of soap for being capable of mosquito-expelling bactericidal according to claim 3, it is characterised in that the spices extracts for rose
One or more in liquid, pawpaw extract solution or lavender extract solution.
A kind of 5. soap for being capable of mosquito-expelling bactericidal according to claim 4, it is characterised in that the grease include butter,
One or more in castor oil or coconut oil.
6. a kind of soap for being capable of mosquito-expelling bactericidal according to claim 5, it is characterised in that the enzyme preparation is albumen
One or more in enzyme, amylase, cellulase, lipase, pectase, mannonase peroxidase.
7. a kind of preparation method for the soap for being capable of mosquito-expelling bactericidal, it is characterised in that this method is achieved by the steps of：
Step 1, raw material is weighed：Following components is weighed respectively according to mass percent：Anion surfactant 10-20%, oil
Fat 25-35%, sodium hydroxide solution 20-30%, natural product extraction liquid 2-6%, absolute ethyl alcohol 1-10%, glycerine 1-10%,
Diatomite 2-8%, sucrose 1-15%, enzyme preparation 1-2%, spices 0.2-0.5%, sodium hypochlorite 0.8-1.5%, remaining for go from
Sub- water；
Step 2, soap lye is prepared：By the anion surfactant described in step 1, grease, sodium hydroxide solution, absolute ethyl alcohol
Add in described deionized water, be uniformly mixed, obtain soap lye；
Step 3, saponification：The soap lye that the step 2 obtains is heated to 45-100 DEG C of progress saponification 2-10h, saponification
After the completion of, the glycerine described in step 1 and the premixed liquid of sucrose are added thereto, stirred, is cooled to 35-80 DEG C, is obtained
Middle mixed solution；
Step 4, mosquito repellent antimicrobial soap liquid is prepared：, will when the middle mixed solution that the step 3 obtains is cooled to 35-80 DEG C
Natural product extraction liquid, diatomite, enzyme preparation, spices, sodium hypochlorite described in step 1 sequentially add wherein, stir,
And room temperature is cooled to, obtain mosquito repellent antimicrobial soap liquid；
Step 5, it is cooled and shaped：The mosquito repellent antimicrobial soap liquid that the step 4 obtains is poured into mould, is cooled and shaped, and use
Vacuum freeze drier is freeze-dried, that is, obtains the soap for being made and being capable of mosquito-expelling bactericidal.
8. a kind of soap for being capable of mosquito-expelling bactericidal according to claim 7, it is characterised in that in the step 3, in described
Between the pH value of mixed solution be 7-11.
9. a kind of soap for being capable of mosquito-expelling bactericidal according to claim 8, it is characterised in that described cold in the step 5
Lyophilized dry temperature is -45--55 DEG C, and the time of freeze-drying is 20-50h.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108359554A (en) * | 2018-04-12 | 2018-08-03 | 广州南芳化妆品有限公司 | A kind of soap and preparation method thereof with natural flower aroma |
| CN111205944A (en) * | 2020-03-28 | 2020-05-29 | 阚海辉 | Foamless non-brush paste and preparation method thereof |
| CN112574834A (en) * | 2020-12-23 | 2021-03-30 | 山东农业大学 | Sterilizing and inflammation-diminishing soap and preparation method thereof |
| CN112877153A (en) * | 2021-01-19 | 2021-06-01 | 北京圣永制药有限公司 | Perfumed soap with moisturizing and sterilizing functions and preparation method thereof |
-
2017
- 2017-10-30 CN CN201711052454.3A patent/CN107828564A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108359554A (en) * | 2018-04-12 | 2018-08-03 | 广州南芳化妆品有限公司 | A kind of soap and preparation method thereof with natural flower aroma |
| CN111205944A (en) * | 2020-03-28 | 2020-05-29 | 阚海辉 | Foamless non-brush paste and preparation method thereof |
| CN112574834A (en) * | 2020-12-23 | 2021-03-30 | 山东农业大学 | Sterilizing and inflammation-diminishing soap and preparation method thereof |
| CN112877153A (en) * | 2021-01-19 | 2021-06-01 | 北京圣永制药有限公司 | Perfumed soap with moisturizing and sterilizing functions and preparation method thereof |
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