CN112574834A - Sterilizing and inflammation-diminishing soap and preparation method thereof - Google Patents

Sterilizing and inflammation-diminishing soap and preparation method thereof Download PDF

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Publication number
CN112574834A
CN112574834A CN202011546435.8A CN202011546435A CN112574834A CN 112574834 A CN112574834 A CN 112574834A CN 202011546435 A CN202011546435 A CN 202011546435A CN 112574834 A CN112574834 A CN 112574834A
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China
Prior art keywords
parts
soap
sterilizing
inflammation diminishing
surfactant
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Pending
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CN202011546435.8A
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Chinese (zh)
Inventor
李培强
王亚馨
李淑红
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Dongping Jiuxin Biochemical Co ltd
Shandong Agricultural University
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Dongping Jiuxin Biochemical Co ltd
Shandong Agricultural University
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Priority to CN202011546435.8A priority Critical patent/CN112574834A/en
Publication of CN112574834A publication Critical patent/CN112574834A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/045Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/72Ethers of polyoxyalkylene glycols

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a sterilizing and inflammation diminishing soap and a preparation method thereof, wherein the soap is prepared from the following raw materials in percentage by mass: 35-45 parts of zanthoxylum oil, 10-15 parts of sodium hydroxide, 5-10 parts of surfactant, 10-15 parts of xanthium extract, 5-15 parts of absolute ethyl alcohol, 1-10 parts of glycerol, 2-8 parts of diatomite, 1-10 parts of sucrose, 1-2 parts of enzyme preparation and the balance of deionized water. The soap prepared by the invention has the characteristics of strong sterilization and adsorption capacity, good decontamination effect, fresh smell, skin nourishing, no toxicity and no harm, does not generate gas and liquid harmful to the environment in production and preparation, and is very suitable for research, development and popularization.

Description

Sterilizing and inflammation-diminishing soap and preparation method thereof
Technical Field
The invention relates to the field of daily chemicals, in particular to a sterilizing and inflammation diminishing soap and a preparation method thereof.
Background
The basic function of soap is to clean and wash, and to remove dirt, skin secretions, chemicals, etc. when applied to the skin. The basic preparation method is usually to make the grease and sodium hydroxide produce saponification reaction to produce higher fatty acid sodium and glycerin, then to make the product through washing, forming and drying. The prior soap has the functions of cleaning and decontaminating, and generally has the function of sterilization, and the antibacterial soap is prepared by adding antibacterial substances into the soap during the preparation process so that the soap has a certain antibacterial function. Currently, there are many kinds of antibacterial soaps, but the bacteria removing effect on clothes is not obvious, and the conventional soap contains substances harmful to human skin such as bleaching powder, mercury, detergent, corrosive, etc. Therefore, it is of great significance to develop a soap which contains natural antibacterial components, has a decontamination effect, and is harmless to the human body.
Disclosure of Invention
In view of the above, the present invention aims to overcome the defects in the prior art: provides a sterilizing and inflammation diminishing soap, which solves the problems.
The invention adopts the following technical scheme: the material is prepared from the following raw materials in percentage by mass: 35-45 parts of zanthoxylum oil, 10-15 parts of sodium hydroxide, 5-10 parts of surfactant, 10-15 parts of xanthium extract, 5-15 parts of absolute ethyl alcohol, 1-10 parts of glycerol, 2-8 parts of diatomite, 1-10 parts of sucrose, 1-2 parts of enzyme preparation and the balance of deionized water.
Preferably, the surfactant is alkyl glycoside polyoxyethylene ether. The alkyl glycoside polyoxyethylene ether has the characteristics of common nonionic and anionic surfactants, has high surface activity, good ecological safety and intermiscibility, excellent wetting and foaming performances, rich and fine foam, hard water resistance and detergency improvement, good intermiscibility and dissolubility with skin, mild property, no toxicity, no stimulation, easy biodegradation, good conditioning, emulsifying and moisturizing performances and broad-spectrum antibacterial performance, and has the functions of resisting bacteria and diminishing inflammation.
Preferably, the diatomite is at least two of primary diatomite, secondary diatomite and tertiary diatomite. The diatomite has a large number of micropores arranged in order, so that the diatomite has a large specific surface area, and thousands of nanometer micropores are contained in the diatomite body, so that the diatomite has strong adsorption force and adsorption capacity, can play a role in removing bacteria, impurities and peculiar smell, and has stable chemical properties.
Preferably, the enzyme preparation is one or more of protease, lipase, amylase. The enzyme can promote the decomposition of macromolecular compounds as a biocatalyst, and the enzymatic reaction has the remarkable characteristics of high efficiency, safety, mild conditions and the like, and is convenient to apply. The protease can efficiently decompose protein stains such as milk stains and the like at low temperature, the lipase can specifically break greasy stains to achieve the purpose of removing, and the amylase can decompose and remove starch stains. The enzyme preparation can be added to achieve the purpose of enhancing the decontamination effect of the soap.
The invention also provides a preparation method of the sterilizing and inflammation diminishing soap, which comprises the following steps: according to the formula, the surfactant, the zanthoxylum oil, the sodium hydroxide and the absolute ethyl alcohol are added into the deionized water, and the mixture is uniformly stirred at the temperature of 45-90 ℃ to carry out saponification reaction for 2-8 hours. After the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 35-75 ℃ to obtain a mixed soap solution. And cooling the obtained mixed soap liquid to 35-75 ℃, sequentially adding the xanthium extract, the diatomite and the enzyme preparation into the mixed soap liquid, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid. And pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10-20 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated and dry place for one day, trimming and packaging to obtain the sterilizing and inflammation diminishing soap.
Compared with the prior art, the invention has the beneficial effects that:
the invention takes purely natural green plant pepper as a raw material, the pepper has obvious inhibition effect on 10 gram-positive bacteria such as bacillus anthracis, hemolytic streptococcus, diphtheria bacillus, diplococcus pneumoniae, staphylococcus aureus, lemon and white staphylococcus, bacillus subtilis and the like, and intestinal pathogenic bacteria such as escherichia coli, Shigella sonnei, proteus, typhoid and paratyphoid bacillus, pseudomonas aeruginosa, vibrio cholerae and the like, and the volatile oil in the pepper can improve the phagocytic activity of macrophages in human bodies, thereby enhancing the immunity of organisms. The soap produced by matching with the natural plant extract and the diatomite has the beneficial effects of strong sterilization and adsorption capacity, no residue, good decontamination effect, fresh smell and no damage to hands.
The herba Xanthii extract has effects of warming spleen and stomach, relieving pain, sterilizing and diminishing inflammation, and can also relieve skin pruritus caused by eczema. The extract contains terpineol which has obvious killing effect on escherichia coli, candida albicans, pseudomonas aeruginosa, staphylococcus aureus and the like; eucalyptus oil having good antibacterial and bactericidal properties; the safe and nontoxic bacteriostatic substance limonene has an obvious inhibiting effect on common rot-causing bacteria; toosendanin which can kill acarid, nematode, part of bacteria, fungi and virus and has therapeutic effect on certain inflammation of human body; and caryophyllene with wide bioactivity and anti-inflammatory and analgesic effects.
Compared with the soap in the prior art, the soap has the characteristics of obvious sterilization and anti-inflammation effects, simple preparation method, low production cost, and suitability for large-scale production and wide popularization.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail with reference to specific embodiments. It should be understood that the detailed description and specific examples, while indicating the invention, are intended for purposes of illustration only and are not intended to limit the scope of the invention.
Example 1:
the soap with the functions of sterilization and inflammation diminishing provided by the embodiment of the invention is prepared from the following raw materials in percentage by mass: weighing 35 parts of pepper oil, 15 parts of sodium hydroxide, 5 parts of alkyl glycoside polyoxyethylene ether serving as a surfactant, 14 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of sucrose, 1 part of protease, 1 part of lipase and the balance of deionized water.
Adding oleum Zanthoxyli Bungeani, sodium hydroxide, anhydrous alcohol, and alkyl glycoside into deionized water, stirring at 45 deg.C, and performing saponification reaction for 8 hr. After the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 35 ℃ to obtain a mixed soap solution. And cooling the obtained mixed soap liquid to 35 ℃, sequentially adding the xanthium extract, the diatomite and the protease into the mixed soap liquid, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid. And pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated and dry place for one day, trimming and packaging to obtain the sterilizing and inflammation diminishing soap.
Example 2:
the soap with the functions of sterilization and inflammation diminishing provided by the embodiment of the invention is prepared from the following raw materials in percentage by mass: weighing 35 parts of pepper oil, 15 parts of sodium hydroxide, 5 parts of alkyl glycoside polyoxyethylene ether serving as a surfactant, 14 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of sucrose, 1 part of protease, 1 part of lipase and the balance of deionized water.
Adding oleum Zanthoxyli Bungeani, sodium hydroxide, anhydrous alcohol, and alkyl glycoside into deionized water, stirring at 90 deg.C, and performing saponification for 4 hr. After the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 75 ℃ to obtain a mixed soap solution. And cooling the obtained mixed soap liquid to 75 ℃, sequentially adding the xanthium extract, the diatomite and the protease into the mixed soap liquid, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid. And pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated and dry place for one day, trimming and packaging to obtain the sterilizing and inflammation diminishing soap.
Example 3:
the soap with the functions of sterilization and inflammation diminishing provided by the embodiment of the invention is prepared from the following raw materials in percentage by mass: weighing 40 parts of pepper oil, 15 parts of sodium hydroxide, 5 parts of alkyl glycoside polyoxyethylene ether serving as a surfactant, 14 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of sucrose, 1 part of protease, 1 part of amylase and the balance of deionized water.
Adding oleum Zanthoxyli Bungeani, sodium hydroxide, anhydrous alcohol, and alkyl glycoside into deionized water, stirring at 45 deg.C, and performing saponification reaction for 8 hr. After the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 35 ℃ to obtain a mixed soap solution. And cooling the obtained mixed soap liquid to 35 ℃, sequentially adding the xanthium extract, the diatomite and the protease into the mixed soap liquid, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid. And pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated and dry place for one day, trimming and packaging to obtain the sterilizing and inflammation diminishing soap.
Example 4:
the soap with the functions of sterilization and inflammation diminishing provided by the embodiment of the invention is prepared from the following raw materials in percentage by mass: weighing 40 parts of pepper oil, 15 parts of sodium hydroxide, 5 parts of alkyl glycoside polyoxyethylene ether serving as a surfactant, 14 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of sucrose, 1 part of protease, 1 part of amylase and the balance of deionized water.
Adding oleum Zanthoxyli Bungeani, sodium hydroxide, anhydrous alcohol, and alkyl glycoside into deionized water, stirring at 90 deg.C, and performing saponification for 4 hr. After the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 75 ℃ to obtain a mixed soap solution. And cooling the obtained mixed soap liquid to 75 ℃, sequentially adding the xanthium extract, the diatomite and the protease into the mixed soap liquid, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid. And pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated and dry place for one day, trimming and packaging to obtain the sterilizing and inflammation diminishing soap.
Example 5:
the soap with the functions of sterilization and inflammation diminishing is prepared from the following raw materials in percentage by mass: weighing raw materials of 35 parts of zanthoxylum oil, 10 parts of sodium hydroxide, 5 parts of surfactant alkyl glycoside polyoxyethylene ether, 15 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of cane sugar, 1 part of protease, 1 part of amylase and the balance of deionized water.
Adding oleum Zanthoxyli Bungeani, sodium hydroxide, anhydrous alcohol, and alkyl glycoside into deionized water, stirring at 45 deg.C, and performing saponification reaction for 8 hr. After the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 35 ℃ to obtain a mixed soap solution. And cooling the obtained mixed soap liquid to 35 ℃, sequentially adding the xanthium extract, the diatomite and the protease into the mixed soap liquid, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid. And pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated and dry place for one day, trimming and packaging to obtain the sterilizing and inflammation diminishing soap.
Example 6:
the soap with the functions of sterilization and inflammation diminishing is prepared from the following raw materials in percentage by mass: weighing raw materials of 35 parts of zanthoxylum oil, 10 parts of sodium hydroxide, 5 parts of surfactant alkyl glycoside polyoxyethylene ether, 15 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of cane sugar, 1 part of protease, 1 part of amylase and the balance of deionized water.
Adding oleum Zanthoxyli Bungeani, sodium hydroxide, anhydrous alcohol, and alkyl glycoside into deionized water, stirring at 90 deg.C, and performing saponification for 4 hr. After the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 75 ℃ to obtain a mixed soap solution. And cooling the obtained mixed soap liquid to 75 ℃, sequentially adding the xanthium extract, the diatomite and the protease into the mixed soap liquid, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid. And pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated and dry place for one day, trimming and packaging to obtain the sterilizing and inflammation diminishing soap.
While the invention has been described above with reference to an embodiment, various modifications may be made and equivalents may be substituted without departing from the scope of the invention. In particular, as long as there is no conflict, the various features of the disclosed embodiments of the present invention can be used in any combination with each other, and the combinations are not exhaustively described in this specification only for the sake of brevity and resource conservation. Therefore, it is intended that the invention not be limited to the particular embodiments disclosed, but that the invention will include all embodiments falling within the scope of the appended claims.

Claims (9)

1. The soap with the functions of sterilization and inflammation diminishing is characterized by being prepared from the following raw materials in percentage by mass: 35-45 parts of zanthoxylum oil, 10-15 parts of sodium hydroxide, 5-10 parts of surfactant, 10-15 parts of xanthium extract, 5-15 parts of absolute ethyl alcohol, 1-10 parts of glycerol, 2-8 parts of diatomite, 1-10 parts of sucrose, 1-2 parts of enzyme preparation and the balance of deionized water.
2. The soap of claim 1, wherein said surfactant is an alkyl glycoside polyoxyethylene ether.
3. The soap of claim 1, wherein the diatomaceous earth is at least two of primary diatomaceous earth, secondary diatomaceous earth, and tertiary diatomaceous earth.
4. The soap of any one of claims 1, 2, or 3, wherein said enzyme is one or more of protease, lipase, and amylase.
5. The soap with sterilizing and inflammation diminishing functions as claimed in claim 1, wherein the soap with sterilizing and inflammation diminishing functions is prepared from the following raw materials in percentage by mass: 35 parts of zanthoxylum oil, 15 parts of sodium hydroxide, 5 parts of surfactant alkyl glycoside polyoxyethylene ether, 14 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of cane sugar, 1 part of protease, 1 part of lipase and the balance of deionized water.
6. The soap with sterilizing and inflammation diminishing functions as claimed in claim 1, wherein the soap with sterilizing and inflammation diminishing functions is prepared from the following raw materials in percentage by mass: weighing 35 parts of pepper oil, 15 parts of sodium hydroxide, 5 parts of alkyl glycoside polyoxyethylene ether serving as a surfactant, 14 parts of xanthium extract, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of diatomite, 3 parts of sucrose, 1 part of protease, 1 part of lipase and the balance of deionized water.
7. The soap with sterilizing and inflammation diminishing functions as claimed in claim 1, wherein the soap with sterilizing and inflammation diminishing functions comprises 40 parts of zanthoxylum oil, 15 parts of sodium hydroxide, 5 parts of alkyl glycoside polyoxyethylene ether serving as a surfactant, 14 parts of xanthium sibiricum extracting solution, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of kieselguhr, 3 parts of sucrose, 1 part of protease, 1 part of amylase and the balance of deionized water.
8. The soap with sterilizing and inflammation diminishing functions as claimed in claim 1, wherein the soap with sterilizing and inflammation diminishing functions comprises 35 parts of zanthoxylum oil, 10 parts of sodium hydroxide, 5 parts of alkyl glycoside polyoxyethylene ether serving as a surfactant, 15 parts of xanthium sibiricum extracting solution, 5 parts of absolute ethyl alcohol, 6 parts of glycerol, 8 parts of kieselguhr, 3 parts of sucrose, 1 part of protease, 1 part of amylase and the balance of deionized water.
9. The preparation method of the soap with the functions of sterilization and inflammation diminishing is characterized by comprising the following steps:
(1) weighing the following raw materials in percentage by mass: 35-45 parts of zanthoxylum oil, 10-15 parts of sodium hydroxide, 5-10 parts of surfactant, 10-15 parts of xanthium extract, 5-15 parts of absolute ethyl alcohol, 1-10 parts of glycerol, 2-8 parts of diatomite, 1-10 parts of sucrose, 1-2 parts of enzyme preparation and the balance of deionized water.
(2) Adding a surfactant, zanthoxylum oil, sodium hydroxide and absolute ethyl alcohol into the deionized water, and uniformly stirring at the temperature of 45-90 ℃ to perform saponification reaction for 2-8 hours;
(3) after the saponification reaction is finished, adding glycerol and sucrose, stirring uniformly, and cooling to 35-75 ℃ to obtain a mixed soap solution;
(4) cooling the obtained mixed soap liquid to 35-75 ℃, sequentially adding the xanthium extract, the diatomite and the enzyme preparation, uniformly stirring, and cooling to room temperature to obtain the sterilizing and inflammation diminishing soap liquid;
(5) and pouring the obtained sterilizing and inflammation diminishing soap liquid into a mold, cooling and molding for 10-20 hours, demolding after the soap liquid is solidified, placing in a cool and ventilated drying place for one day, trimming and packaging to obtain a finished product.
CN202011546435.8A 2020-12-23 2020-12-23 Sterilizing and inflammation-diminishing soap and preparation method thereof Pending CN112574834A (en)

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CN114350456A (en) * 2021-05-25 2022-04-15 广州尚芊日用品有限公司 Mite-removing antibacterial soap and preparation method thereof

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CN114350456A (en) * 2021-05-25 2022-04-15 广州尚芊日用品有限公司 Mite-removing antibacterial soap and preparation method thereof

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Application publication date: 20210330