CN106906071A - A kind of except mite liquid detergent and preparation method thereof - Google Patents
A kind of except mite liquid detergent and preparation method thereof Download PDFInfo
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- CN106906071A CN106906071A CN201710156380.1A CN201710156380A CN106906071A CN 106906071 A CN106906071 A CN 106906071A CN 201710156380 A CN201710156380 A CN 201710156380A CN 106906071 A CN106906071 A CN 106906071A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/162—Organic compounds containing Si
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2041—Dihydric alcohols
- C11D3/2044—Dihydric alcohols linear
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/78—Neutral esters of acids of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/92—Sulfobetaines ; Sulfitobetaines
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of except mite liquid detergent and preparation method thereof, its composition is made up of saponification component, clean enhancing component and except mite traditional Chinese medicinal components：Saponification component is the saponification resultant of soybean oil, lard and NaOH；Cleaning enhancing component is the mixture of nonionic surfactant, amphoteric surfactant and except mite agent；Except mite traditional Chinese medicinal components are the mixtures of tea tree ethereal oil and safflower extract.The except mite soap has excellent sebum detergency, foam performance, and except mite rate can reach more than 97%, remote super market products in the prior art.
Description
Technical field
The present invention relates to a kind of liquid detergent, and in particular to a kind of except mite liquid detergent, more particularly relate to a kind of suitable for clothing
The except mite liquid detergent of thing, bed clothes.
Background technology
Allergic is common a kind of illness in clinical medicine, and with the complexity of environment, allergic anaphylactogen is got over
Come more, common dust, pollen can all cause allergic, and wherein acarid is the attention for causing medical worker in recent years,
And acarid can also cause numerous skin problems.Acarid, can be the parasite for being lodged in human body also known as follicle mites, mainly have
Demodex folliculorum and sebaceous glands vermiform mite, the infection of vermiform mite is very common to have serious harm to health, and they both may be used
Cause insect bite dermatitis directly to bite skin, it is also possible to which skin is caused by its secretion such as excrement, saliva etc. for producing
Inflammation, if acarid living directly invades human body, can cause bigger internal organs internal diseases.
Acarid also has substantial amounts of presence in addition to being lived away from home in human body in wool textile, carpet, sofa, down toy,
The acarid of very high quantity level is may detect that on clothing and bed clothes.Have been reported that there are up to ten million dirt using the sheet of 8 years
Mite, quantity is imagined out of people.Therefore how efficiently to remove the emphasis that these dust mites are existing research.Liquid detergent is now daily
A kind of most cleaning supplies are used in life, is often used in clothing, the cleaning of bedding, therefore, obtain a kind of to clothing, quilt
The liquid detergent that cotton-padded mattress etc. has good except mite effect is suitable means.And the report of except mite liquid detergent is also related in the prior art,
But remained after effect on driving birds is not good, or use to the irritant component of human body, or except mite effect on driving birds is not good, it is difficult to obtain recognizing for market
Can.The conventional except mite agent of prior art has antibacterial and mouldproof to drive mite agent MGU-350 (CN104694277A), antimildew and antibacterial liquid nm
After SKG (CN104450290A) and CN105886147A is disclosed except acaricidal composition, but inventor actually attempts to, all
Supported with different degrees of deficiency.By long-term research, obtain a kind of thering is good except mite effect to wash to clothing, bed clothes etc.
Clothing liquid, meanwhile, the cleaning performance of other dirts is also very excellent.
The content of the invention
In order to solve the above problems, the invention provides a kind of liquid detergent with high-efficient washing and except mite function.This hair
Outside ensureing to have excellent carbon black detergency, sebum detergency, foam performance is excellent, and except mite rate can reach for bright liquid detergent
More than 99%, excellent combination property be far superior to prior art it has been reported that except mite agent.
The concrete technical scheme for reaching above-mentioned technique effect is：
(1) a kind of except mite liquid detergent, its main active component is：Nonionic surfactant, amphoteric surfactant, remove
Mite agent, laundry care agent, preservative, thickener, small molecular alcohol and essence.
(2) the except mite liquid detergent according to (1), the nonionic surfactant is coconut oil fat acyl diethanol amine
One or more mixture in phosphate, coconut oil fat acyl diethanol amine, castor oil polyoxyethylene ether.
(3) the except mite liquid detergent according to (1), the amphoteric surfactant is dodecyl ethyoxyl sulfobetaines
One or more mixing in alkali, dodecyl dimethyl hydroxypropyl sulfobetaines, dodecanamide propyl amine-oxides
Thing.
(4) the except mite liquid detergent according to (1), the except mite agent is propylene glycol mono-oleate, propane diols list linoleic acid
One or more mixture in ester, propane diols list linolenate.
(5) the except mite liquid detergent according to (1), the laundry care agent is organosilicon laundry care agent.
(6) the except mite liquid detergent according to (1), the small molecular alcohol is the one kind or two in methyl alcohol, ethanol, propane diols
Plant the mixture of the above.
(7) according to the except mite liquid detergent described in (1), main active component is：Nonionic surfactant 2-5 weight portions,
Amphoteric surfactant 10-12 weight portions, except mite agent 0.1-0.3 weight portions, laundry care agent 2-5 weight portions, preservative 0.2-
0.3 weight portion, thickener 1-3 weight portions, small molecular alcohol 0.5-1 weight portions and essence 0.1-0.5 weight portions.
(8) ratio of the except mite liquid detergent according to (1), nonionic surfactant and amphoteric surfactant is 3：
10-12。
(9) according to the except mite liquid detergent described in (1) or (7) or (8), main active component is：Nonionic surfactant 3
Weight portion, the weight portion of amphoteric surfactant 11, the weight portion of except mite agent 0.1, the weight portion of laundry care agent 3, the weight of preservative 0.2
Part, the weight portion of thickener 1, the weight portion of small molecular alcohol 0.8 and the weight portion of essence 0.1.
(10) preparation method of except mite liquid detergent, comprises the following steps：It is standby each component to be weighed according to weight portion；By it is non-from
Sub- surfactant, amphoteric surfactant, except mite agent, laundry care agent sequentially add reactor, are slowly stirred；Add small point
Sub- alcohol and appropriate deionized water, after each component is uniform, are eventually adding preservative, thickener and essence, stir, and stand
More than 1 hour, packed.
The selection of surfactant
Present invention employs two kinds of surfactants, respectively nonionic surfactant and amphoteric surfactant, on
State two kinds of surfactants and be used in mixed way and be much better than using individually a kind of, and better than using cationic surfactant and anion
Surfactant.Wherein nonionic surfactant selection has backbone, specially coconut oil fat acyl diethanol amine phosphorus
One or more mixture in acid esters, coconut oil fat acyl diethanol amine, castor oil polyoxyethylene ether.Amphoteric surface
Activating agent equally uses encourage honesty structure, specially dodecyl ethyoxyl sulfobetaines, dodecyl dimethyl hydroxypropyl sulphur
One or more mixture in base glycine betaine, dodecanamide propyl amine-oxides.
Improve to long-chain moiety to the affinity of grease using the surfactant with backbone, meanwhile, to mite
The oily matter on worm surface also has preferable affinity, in liquid detergent when using, can quickly be cut grease and acarid
Cut, the ratio of removal is higher.Ionic requirement using the surfactant of independent ion to use in washing machine water is higher, height from
Under conditions of sub- content, Loss of Surfactants is more.
The selection of except mite agent
The mite-proof agent that the present invention is used is selected by characteristic, and the except mite agent is preferably propylene glycol mono-oleate, third
One or more mixture in glycol list linoleate, propane diols list linolenate.The except mite agent is much better than background
Species in technology, has good dispersiveness and stability better than above-mentioned three kinds in liquid detergent.Propylene glycol mono-oleate, third
Glycol list linoleate, propane diols list linolenate all aliphatic chains containing long-chain, this arrangement enhances dispersiveness and stability,
Without the material of aliphatic chain long, the reduction of except mite performance is a lot, and such as Propylene glycol monoacetate, propane diols mono-propionate all cannot
Reach preferable except mite effect.Meanwhile, the except mite agent is nontoxic to human body, nonirritant.
The selection of small molecular alcohol
Contain substantial amounts of deionized water in liquid detergent, in order to adjust the surface tension etc. of system, inventor has found to add few
The small molecular alcohol of amount, improves the dispersion stabilization of each component, on the basis of stable dispersion, the soil release performance of liquid detergent, except mite
Property all increases, and detailed mechanism is not still apparent.Specific small molecular alcohol is preferably the one kind in methyl alcohol, ethanol, propane diols
Or two or more mixtures
The selection of amounts of components
Performance of the selection of above-mentioned each component also to final liquid detergent has a major impact, most important for non-ionic surface is lived
Property agent and amphoteric surfactant ratio selection, most preferably 3：10-12.Within this range, dirt-removing power is strong, if nonionic
Surfactant is higher, dirt-removing power reduction；If amphoteric surfactant is higher, the requirement to clothes water is high, and applicable surface is received
To influence.Most preferred amount ratio is：The weight portion of nonionic surfactant 3, the weight portion of amphoteric surfactant 11, except mite agent
0.1 weight portion, the weight portion of laundry care agent 3, the weight portion of preservative 0.2, the weight portion of thickener 1, the weight portion of small molecular alcohol 0.8 and
The weight portion of essence 0.1.Deionized water to be added actually is prepared in said components, optimum amount is 3-8 times of said components total amount.
Beneficial technique effect
The present invention uses a certain proportion of nonionic surfactant and amphoteric surfactant, particular types by comprehensive
Mite-proof agent, the addition of small molecular alcohol and the adjustment of each component consumption obtained with excellent carbon black detergency, sebum detergency
Outside, foam performance is excellent, and except mite rate can reach more than 99%, the product of remote super prior art report.
With reference to specific embodiment, the invention will be further described.
Specific embodiment
Can be so that the present invention will be further elaborated, however, the scope of the present invention not office by the following examples
It is limited to following embodiments.Those skilled in the art are it can be appreciated that in the premise without departing substantially from the spirit and scope of the present invention
Under, various change and modification can be carried out to the present invention.The present invention to used in experiment to material and test method enter
Row is general and/or specifically describes.Although to realize that many materials that the object of the invention used and operating method are abilities
Known to domain, but the present invention still makees description as detailed as possible herein.
Embodiment 1：
A kind of except mite liquid detergent, is made up of the raw material of following weight portion：Nonionic surfactant coconut oil fat acyl two
The weight portion of ethanolamine-phosphate 3, the weight portion of amphoteric surfactant dodecyl dimethyl hydroxypropyl sulfobetaines 11, except mite
The weight portion of agent propane diols list linoleate 0.1, the weight portion of organosilicon laundry care agent 3, the weight portion of preservative 0.2, the weight of thickener 1
Amount part, the weight portion of propane diols 0.8 and the weight portion of essence 0.1, plus deionized water are to 100 weight portions.
Embodiment 2：
A kind of except mite liquid detergent, is made up of the raw material of following weight portion：Nonionic surfactant coconut oil fat acyl two
The weight portion of monoethanolamine 3, the weight portion of amphoteric surfactant dodecanamide propyl amine-oxides 12, except mite agent propane diols list linolenate
0.1 weight portion, the weight portion of organosilicon laundry care agent 3, the weight portion of preservative 0.2, the weight portion of thickener 1, the weight of propane diols 0.8
Part and the weight portion of essence 0.1, plus deionized water is to 100 weight portions.
Comparative example 1:
By the weight portion of nonionic surfactant coconut oil fat acyl diethanol amine phosphate 3 and both sexes table in embodiment 1
The weight portion of face activating agent dodecyl dimethyl hydroxypropyl sulfobetaines 11 is revised as nonionic surfactant coconut grease
The weight portion of fat acyl diethanol amine phosphate 14, other are with embodiment 1.
Comparative example 2:
By the weight portion of nonionic surfactant coconut oil fat acyl diethanol amine phosphate 3 and both sexes table in embodiment 1
The weight portion of face activating agent dodecyl dimethyl hydroxypropyl sulfobetaines 11 is revised as amphoteric surfactant dodecyl two
The weight portion of methylhydroxypropyl sulfobetaines 14, other are with embodiment 1.
Comparative example 3：
Except mite agent propane diols list linolenate in embodiment 1 is revised as antibacterial and mouldproof and drives mite agent MGU-350, consumption 0.1
Weight portion, other are with embodiment 1.
Comparative example 4：
Except mite agent propane diols list linolenate in embodiment 1 is revised as antimildew and antibacterial liquid nm SKG, the weight of consumption 0.2
Part, other are with embodiment 1.
Comparative example 5：
Except mite agent propane diols list linolenate in embodiment 1 is revised as N, N diethyl phenyl acetamide compounds, consumption
0.1 weight portion, other are with embodiment 1.
Comparative example 6：
Propane diols in embodiment 2 is not used, and other are with embodiment 2.
Comparative example 7：
Except mite agent is not used in embodiment 1, other are with embodiment 1.
Comparative example 8：
Except mite agent propane diols list linoleate replaces with except mite agent Propylene glycol monoacetate in embodiment 1, and other are with implementation
Example 1.
Comparative example 9：
A kind of except mite liquid detergent, is made up of the raw material of following weight portion：Nonionic surfactant coconut oil fat acyl two
The weight portion of ethanolamine-phosphate 1, the weight portion of amphoteric surfactant dodecyl dimethyl hydroxypropyl sulfobetaines 13, except mite
The weight portion of agent propane diols list linoleate 0.1, the weight portion of organosilicon laundry care agent 3, the weight portion of preservative 0.2, the weight of thickener 1
Amount part, the weight portion of propane diols 0.8 and the weight portion of essence 0.1, plus deionized water are to 100 weight portions.
Comparative example 10：
A kind of except mite liquid detergent, is made up of the raw material of following weight portion：Nonionic surfactant coconut oil fat acyl two
The weight portion of ethanolamine-phosphate 7, the weight portion of amphoteric surfactant dodecyl dimethyl hydroxypropyl sulfobetaines 7, except mite
The weight portion of agent propane diols list linoleate 0.1, the weight portion of organosilicon laundry care agent 3, the weight portion of preservative 0.2, the weight of thickener 1
Amount part, the weight portion of propane diols 0.8 and the weight portion of essence 0.1, plus deionized water are to 100 weight portions.
Method of testing：
The detergency test of liquid detergent sample is with reference to GB/T13174-2008《Dress material detergent detergency and circulation washing
The measure of performance》Carry out.
Standard liquid detergent following table composition is defined：
The foaming power test of liquid detergent sample is with reference to GB/13173-2008《Surfactant detergent experimental technique》Enter
OK.
The except mite of liquid detergent sample is tested according to GB13917.2-92《Agriculture chemical registration hygienic insecticide indoor harmacological effect is determined
The indoor harmacological effect assay method of method aerosol》Carry out.Specially：Acarid is inserted into transparent organic glass cylinder bottom, sky is tested
Adjust device except mite liquid detergent to distinguish wound packages on electronic spraying controller frame trestle, electronic spraying controller rack post be laid flat,
At regulation electronic controller time control button to the time of spray usage amount medicament, pressing operations button uses plug immediately after spraying
Circular hole is clogged into (culture dish surface contact dose is 0.1g), immediately timing, and start recording, culture dish is taken after 30 minutes
Go out, be placed in 26 DEG C of incubators, miticidal effect was observed when 24 hours, as a result take three average values.
The except mite clean result of liquid detergent sample, acarid culture is carried out in the pieces of cloth of 10*10cm, and culture is added after 24 hours
Laundry liquor (liquid detergent：Water=1:30) in washing machine, dry in the shade 24 hours and observe sterilizing rate.Same liquid detergent sample test
3 times, as a result take three average values (test water contains 0.2% sodium chloride).
Test result
-- expression is tested.
From test result as can be seen that the selection of nonionic surfactant and amphoteric surfactant, particular kind of
The adjustment of the selection of mite-proof agent, the addition of small molecular alcohol and each component consumption is all to carbon black detergency, the skin of final liquid detergent
Fat detergency, foam performance and except mite rate have a major impact, and are also that prior art is not yet reported.
Claims (10)
1. a kind of except mite liquid detergent, it is characterised in that its main active component is：Nonionic surfactant, amphoteric surface live
Property agent, except mite agent, laundry care agent, preservative, thickener, small molecular alcohol and essence.
2. except mite liquid detergent according to claim 1, it is characterised in that：The nonionic surfactant is coconut grease
In fat acyl diethanol amine phosphate, coconut oil fat acyl diethanol amine, castor oil polyoxyethylene ether one or more
Mixture.
3. except mite liquid detergent according to claim 1, it is characterised in that：The amphoteric surfactant is dodecyl second
One kind or two in epoxide sulfobetaines, dodecyl dimethyl hydroxypropyl sulfobetaines, dodecanamide propyl amine-oxides
Plant the mixture of the above.
4. except mite liquid detergent according to claim 1, it is characterised in that：The except mite agent is propylene glycol mono-oleate, third
One or more mixture in glycol list linoleate, propane diols list linolenate.
5. except mite liquid detergent according to claim 1, it is characterised in that：The laundry care agent is organosilicon laundry care
Agent.
6. except mite liquid detergent according to claim 1, it is characterised in that：The small molecular alcohol is methyl alcohol, ethanol, propane diols
In one or more mixture.
7. except mite liquid detergent according to claim 1, it is characterised in that：Main active component is：Non-ionic surface active
Agent 2-5 weight portions, amphoteric surfactant 10-12 weight portions, except mite agent 0.1-0.3 weight portions, laundry care agent 2-5 weight
Part, preservative 0.2-0.3 weight portions, thickener 1-3 weight portions, small molecular alcohol 0.5-1 weight portions and essence 0.1-0.5 weight
Part.
8. except mite liquid detergent according to claim 1, it is characterised in that：Nonionic surfactant and amophoteric surface active
The ratio of agent is 3：10-12.
9. the except mite liquid detergent according to claim 1 or 7 or 8, it is characterised in that：Main active component is：Nonionic table
It is the weight portion of face activating agent 3, the weight portion of amphoteric surfactant 11, the weight portion of except mite agent 0.1, the weight portion of laundry care agent 3, anti-
The weight portion of rotten agent 0.2, the weight portion of thickener 1, the weight portion of small molecular alcohol 0.8 and the weight portion of essence 0.1.
10. the preparation method of the except mite liquid detergent any one of claim 1-9, it is characterised in that：Comprise the following steps：
（1）It is standby each component to be weighed according to weight portion；
（2）Nonionic surfactant, amphoteric surfactant, except mite agent, laundry care agent are sequentially added into reactor, slowly
Stirring；
（3）In step（2）After add small molecular alcohol, after each component is uniform, be eventually adding preservative, thickener and essence, put
Put more than 1 hour, packed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710156380.1A CN106906071A (en) | 2017-03-15 | 2017-03-15 | A kind of except mite liquid detergent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710156380.1A CN106906071A (en) | 2017-03-15 | 2017-03-15 | A kind of except mite liquid detergent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106906071A true CN106906071A (en) | 2017-06-30 |
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| CN201710156380.1A Pending CN106906071A (en) | 2017-03-15 | 2017-03-15 | A kind of except mite liquid detergent and preparation method thereof |
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|---|---|---|---|---|
| CN108441340A (en) * | 2018-02-27 | 2018-08-24 | 洛娃日化(江苏)股份有限公司 | A kind of Green environment-friendlyhome home cleaning agent and preparation method thereof |
| CN110591844A (en) * | 2019-09-29 | 2019-12-20 | 广州香枝化妆品有限公司 | Plant acarid-removing and acarid-inhibiting laundry detergent and preparation method thereof |
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Application publication date: 20170630 |