CN113736578A - Plant antibacterial laundry detergent and preparation method thereof - Google Patents
Plant antibacterial laundry detergent and preparation method thereof Download PDFInfo
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- CN113736578A CN113736578A CN202111112692.5A CN202111112692A CN113736578A CN 113736578 A CN113736578 A CN 113736578A CN 202111112692 A CN202111112692 A CN 202111112692A CN 113736578 A CN113736578 A CN 113736578A
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- Prior art keywords
- dispersion machine
- solution
- laundry detergent
- essence
- fatty alcohol
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/381—Microorganisms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
Abstract
The invention discloses a plant antibacterial laundry detergent and a preparation method thereof, and relates to the field of laundry detergents. The paint is prepared from the following components in percentage by mass: 10-30% of gleditsia sinensis extractive solution; 10-20% of ferment stock solution; 10-15% of fatty alcohol-polyoxyethylene ether sodium sulfate (AES); 1-5% of cocamidopropyl betaine; 1-5% of potassium cocoate; 0.5 to 2 percent of sodium citrate; 0.2-2% of Meyer sedge extract; 0.05 to 0.1 percent of essence; the balance of deionized water. The laundry detergent provided by the invention is a natural renewable resource, has a simple synthesis process, and is high in decontamination, antibacterial, clothes-protecting, smooth and easy to degrade.
Description
Technical Field
The invention discloses a plant antibacterial laundry detergent and a preparation method thereof, and belongs to the field of washing.
Background
Along with the development of social science and technology economy, the living and consumption level of people is improved, the demand of the detergent is larger and larger, and the development speed of the detergent is very high. In 2015, the sales of washing products in China are 7.5 hundred million. 2019 and has a sale rate of 860 hundred million for washing products in China. The rapid increase in detergent consumption has exacerbated the environmental pollution caused by this. In recent years, the government of China continuously advocates the development concepts of green, environmental protection, energy conservation, emission reduction and the like, and the concept of green, environmental protection, energy conservation and emission reduction is deeply popular. The development of efficient environment-friendly liquid detergent, and the reduction of the dosage of the detergent or the dosage of the surfactant serving as the main component of the detergent is an effective way for reducing environmental pollution. The laundry detergent is used as a main member in a large family of detergents, plant raw materials are used for replacing biochemical raw materials to produce the laundry detergent, and the emission of harmful substances in the detergents can be effectively reduced, so that the pollution to the environment is reduced.
Disclosure of Invention
The invention aims to produce the laundry detergent by using plant raw materials instead of biochemical raw materials, and the laundry detergent replaces biochemical surfactants and disinfectants by using the effects of sterilization, inflammation diminishing, insect killing and surfactants of the plant raw materials, thereby reducing the pollution of chemical raw materials to human bodies and the environment.
1. The formula of the invention is as follows:
10-30% of gleditsia sinensis extractive solution; 10-20% of ferment stock solution; 10-15% of fatty alcohol-polyoxyethylene ether sodium sulfate; 1-5% of cocamidopropyl betaine; 1-5% of potassium cocoate; 0.5 to 2 percent of sodium citrate; 0.2-2% of Meyer sedge extract; 0.05 to 0.1 percent of essence; the balance of deionized water;
wherein: the saponin extraction liquid is a plant-derived surfactant and has the effects of resisting bacteria, diminishing inflammation and killing insects.
The ferment stock solution is fruit ferment, contains various active enzymes, and has the effects of removing dirt and nourishing various plants.
The sodium fatty alcohol-polyoxyethylene ether sulfate is selected from sodium fatty alcohol-polyoxyethylene ether sulfate with a fatty alcohol carbon chain of C10-C18, an ethylene oxide addition number of 2-4 and an ethylene oxide addition number of 7-15, and is an anionic surfactant.
The cocamidopropyl betaine is a zwitterionic surfactant.
The potassium cocoate is a fiber flexibilizer.
The sodium citrate is a kneading agent and also a food additive.
The Meyer sedge extract is a plant sterilizing, anti-inflammatory and insect killing agent.
2. The preparation method is realized by the following steps:
the method comprises the following steps: preparing the following components in percentage by mass:
step two: adding 20% of the water in the formula into a No. 1 dispersion machine, slowly adding the Meyer sedge extracting solution and the essence under the condition that the rotation speed of the dispersion machine per minute is 800-;
step three; adding 80% of the total amount of water in the formula into a No. 2 dispersion machine, and heating to 30-38 ℃. The rotating speed of the dispersion machine is 800-;
step four, slowly adding the fatty alcohol-polyoxyethylene ether sodium sulfate, the cocamidopropyl betaine, the gleditsia sinensis lam extract, the ferment stock solution and the potassium cocoate oleate under the condition of stirring without adjusting the rotating speed and the temperature of a No. 2 dispersing machine, and stirring until the fatty alcohol-polyoxyethylene ether sodium sulfate, the cocamidopropyl betaine, the gleditsia sinensis lam extract, the ferment stock solution and the potassium cocoate oleate are completely dissolved;
step five, slowly adding the wula sedge extracting solution and the essence solution in the No. 1 dispersion machine into the No. 2 dispersion machine under stirring, and continuously stirring until the wula sedge extracting solution and the essence solution are completely fused;
step six: aging for 12-24 hours;
step seven: sampling detection and finished product packaging;
the invention has the following advantages:
the antibacterial laundry detergent provided by the invention adopts plant extracted surfactants, antibacterial agents and plant enzymes as main raw materials, is nontoxic and degradable, and has the following advantages compared with the traditional surfactants and antibacterial agents: the raw materials are natural renewable resources, are harmless to human bodies, the synthesis process is environment-friendly and safe, the biodegradation is easy, the performance is excellent, the decontamination performance and the antibacterial performance of the laundry detergent can be obviously improved by adding a small amount of the raw materials, and the effects of energy conservation and emission reduction are achieved.
Detailed Description
The present invention will be described in detail with reference to specific embodiments.
Example 1
The method comprises the following steps: preparing the following components in percentage by mass:
10% of gleditsia sinensis extractive solution;
10% of enzyme stock solution;
12% of fatty alcohol-polyoxyethylene ether sodium sulfate;
cocamidopropyl betaine 4%;
2% of sodium cocoate;
1% of sodium citrate;
1% of Meyer sedge extracting solution;
0.05% of essence;
the balance of deionized water;
step two: adding 20% of the deionized water in the formula at normal temperature into a No. 1 dispersion machine, slowly adding the Meyer sedge extracting solution and the essence under the condition that the rotation speed of the dispersion machine per minute is 800-;
step three; adding 80% of deionized water in the formula into a No. 2 dispersion machine, heating to 30-38 ℃, wherein the rotating speed of the dispersion machine is 800-;
and step four, the rotating speed and the temperature of the No. 2 disperser do not need to be adjusted. Slowly adding sodium fatty alcohol-polyoxyethylene ether sulfate, cocamidopropyl betaine, gleditsia sinensis lam extract, ferment stock solution and potassium cocoate under stirring until the materials are completely dissolved;
step five, the Meyer sedge extracting solution and the essence solution in the No. 1 dispersion machine are mixed. Slowly adding into No. 2 disperser under stirring, and continuously stirring until completely fusing;
step six: aging for 12-24 hours;
step seven: sampling detection and finished product packaging;
example 2
The method comprises the following steps: preparing the following components in percentage by mass:
15% of gleditsia sinensis extractive solution;
10% of enzyme stock solution;
10% of fatty alcohol-polyoxyethylene ether sodium sulfate;
cocamidopropyl betaine 3%;
2% of sodium cocoate;
1% of sodium citrate;
0.8 percent of Meyer sedge extract;
0.05% of essence;
the balance of deionized water;
step two: adding 20% of the deionized water in the formula at normal temperature into a No. 1 dispersion machine, slowly adding the Meyer sedge extracting solution and the essence under the condition that the rotation speed of the dispersion machine per minute is 800-;
step three; adding 80% of deionized water in the formula into a No. 2 dispersion machine, heating to 30-38 ℃, wherein the rotating speed of the dispersion machine is 800-;
and step four, the rotating speed and the temperature of the No. 2 disperser do not need to be adjusted. Slowly adding sodium fatty alcohol-polyoxyethylene ether sulfate, cocamidopropyl betaine, gleditsia sinensis lam extract, ferment stock solution and potassium cocoate under stirring until the materials are completely dissolved;
step five, slowly adding the wula sedge extracting solution and the essence solution in the No. 1 dispersion machine into the No. 2 dispersion machine under stirring, and continuously stirring until the wula sedge extracting solution and the essence solution are completely fused;
step six: aging for 12-24 hours;
step seven: sampling detection and finished product packaging;
example 3
The method comprises the following steps: preparing the following components in percentage by mass:
20% of gleditsia sinensis extractive solution;
ferment stock solution 15%
8 percent of fatty alcohol-polyoxyethylene ether sodium sulfate;
cocamidopropyl betaine 3%;
2% of sodium cocoate;
1% of sodium citrate;
0.9 percent of Meyer sedge extract;
0.06% of essence;
the balance of deionized water
Step two: adding 20% of the deionized water in the formula at normal temperature into a No. 1 dispersion machine, slowly adding the Meyer sedge extracting solution and the essence under the condition that the rotation speed of the dispersion machine per minute is 800-;
step three; adding 80% of deionized water in the formula into a No. 2 dispersion machine, and heating to 30-38 ℃. The rotating speed of the dispersion machine is 800-;
step four, slowly adding the fatty alcohol-polyoxyethylene ether sodium sulfate, the cocoanut oil amide propyl betaine, the gleditsia sinensis lam extract, the ferment stock solution and the potassium cocoate oleate under the condition of stirring without adjusting the rotating speed and the temperature of a No. 2 dispersing machine, and stirring until the fatty alcohol-polyoxyethylene ether sodium sulfate, the cocoanut oil amide propyl betaine, the gleditsia sinensis lam extract, the ferment stock solution and the potassium cocoate oleate are completely dissolved;
step five, slowly adding the wula sedge extracting solution and the essence solution in the No. 1 dispersion machine into the No. 2 dispersion machine under stirring, and continuously stirring until the wula sedge extracting solution and the essence solution are completely fused;
step six: aging for 12 hours or even 24 hours;
step seven: sampling detection and finished product packaging;
the detection conditions and results of the laundry detergent are as follows:
1) detection conditions are as follows: implementing the QB/T1224-2012 Standard
2) And (3) a detergency detection result:
example 1 JB 01: 1.07 to 1.20
Example 2 JB 02: 1.10 to 1.25
Example 3 JB 03: 1.13 to 1.30
The invention is not limited to the examples, and any equivalent changes to the technical solution of the invention by a person skilled in the art after reading the description of the invention are covered by the claims of the invention.
Claims (2)
1. A plant antibacterial laundry detergent and a preparation method thereof are characterized in that the laundry detergent comprises the following raw materials by weight:
10-30% of gleditsia sinensis extractive solution; fermenting fruit 10-20%; 10-15% of fatty alcohol-polyoxyethylene ether sodium sulfate; 1-5% of cocamidopropyl betaine; 1-5% of potassium cocoate; 0.5 to 2 percent of sodium citrate; 0.2-2% of Meyer sedge extract; 0.05 to 0.1 percent of essence; the balance of deionized water.
2. The plant antibacterial laundry detergent and the preparation method thereof according to the claim one, characterized in that:
the method comprises the following steps: the components are prepared according to the following mass percent.
Step two: adding 20% of deionized water in the formula into a No. 1 dispersion machine, slowly adding the Meyer sedge extracting solution and the essence under the condition that the rotation speed of the dispersion machine per minute is 800-.
Step three; adding 80% of water in the total amount of deionized water in the formula into a No. 2 dispersion machine, heating to 30-38 ℃, slowly adding sodium citrate until the sodium citrate is completely dissolved, wherein the rotating speed of the dispersion machine is 800-1000 revolutions per minute.
And step four, cooling is not needed, and speed change is not needed. Then slowly adding the sodium fatty alcohol-polyoxyethylene ether sulfate, the cocamidopropyl betaine, the saponin extract, the ferment stock solution and the potassium cocoate oleate in sequence under the condition of stirring until the sodium fatty alcohol-polyoxyethylene ether sulfate, the cocamidopropyl betaine, the saponin extract, the ferment stock solution and the potassium cocoate oleate are completely dissolved by stirring.
And step five, slowly adding the wula sedge extract and the essence solution in the No. 1 dispersion machine into the No. 2 dispersion machine while stirring, and continuously stirring until the wula sedge extract and the essence solution are completely dissolved.
Step six: the aging treatment is carried out for 12 hours to 24 hours.
Step seven: sampling and detecting, and packaging finished products.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111112692.5A CN113736578A (en) | 2021-09-16 | 2021-09-16 | Plant antibacterial laundry detergent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111112692.5A CN113736578A (en) | 2021-09-16 | 2021-09-16 | Plant antibacterial laundry detergent and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN113736578A true CN113736578A (en) | 2021-12-03 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111112692.5A Pending CN113736578A (en) | 2021-09-16 | 2021-09-16 | Plant antibacterial laundry detergent and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114307711A (en) * | 2021-12-14 | 2022-04-12 | 浙江永金生物科技有限公司 | Enzyme down feather cleaning agent with fluffy deodorization effect and processing equipment |
-
2021
- 2021-09-16 CN CN202111112692.5A patent/CN113736578A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114307711A (en) * | 2021-12-14 | 2022-04-12 | 浙江永金生物科技有限公司 | Enzyme down feather cleaning agent with fluffy deodorization effect and processing equipment |
| CN114307711B (en) * | 2021-12-14 | 2023-11-10 | 浙江永金生物科技有限公司 | Enzyme eiderdown cleaner with fluffy deodorization is effectual and processing equipment |
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