CN101240225A - Highly effective sterilization laundry soap - Google Patents

Highly effective sterilization laundry soap Download PDF

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Publication number
CN101240225A
CN101240225A CNA2008101017748A CN200810101774A CN101240225A CN 101240225 A CN101240225 A CN 101240225A CN A2008101017748 A CNA2008101017748 A CN A2008101017748A CN 200810101774 A CN200810101774 A CN 200810101774A CN 101240225 A CN101240225 A CN 101240225A
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Prior art keywords
soap
highly effective
effective sterilization
laundry soap
sterilant
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CNA2008101017748A
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CN101240225B (en
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宁月胜
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Ning Yuesheng
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BEIJING LUDAOYUAN BEE PRODUCTS Co Ltd
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Abstract

The invention discloses a sterilization laundry soap belonging to sanitation field. The object of the invention is to provide a high efficiency, safe laundry soap adapting modern biotechnical production. The ingredient of the product comprises genuine soap, bacteriocides, lotion-assisting, enzymes, dye transferring inhibitor, whitening agent and spice. The process is simple and the cost is low. The laundry soap is high sterilization, safe, cheap and advanced technology. The bactericide incorporating the invention which is made by modern biotechnology from savageness fermentation material has anticorrosive function and is safe and efficient.

Description

A kind of highly effective sterilization laundry soap
Technical field: the invention belongs to field of hygiene products, relate to special washing soap.
Background technology:
The washing soap class is indispensable daily necessities in people's daily life.The major function of washing soap is to remove dirt at present.The washing soap of selling on the market mainly contains the function of removing the clothing dirt.At present, the washing soap of selling on the market is sodium soap normally, and the adding washing assistant processes.This class washing soap has only the effect of washing usually, can not the bacterium on the clothing effectively be killed.At present, locate in family, hotel, railway, airport, school etc., washing machine has obtained using widely.If the easy breed bacteria of washing machine not to its disinfection, then causes people's infection easily, and people's health is brought threat.
Also occur some on the market and had the washing soap of disinfecting and sterilizing functions.Mainly be to have added some sterilizing agents, make washing powder have certain germicidal efficacy.These sterilizing agents, some is not really safe to people, if rinsing is unclean, people's skin is had certain stimulation.Some sterilizing agent costs an arm and a leg, and is unfavorable for reducing production costs and increasing competitiveness of product.At present, it is strong to be starved of a kind of soil removability on the market, and sterilizing power is strong, safety, cheap washing soap.
At present, the disinfection soap great majority of selling on the market are to have added chemical bactericide.In the market, having the washing soap of sterilizing function, mainly is to have the characteristic of killing common intestinal bacteria, Salmonellas and streptococcus aureus.
Summary of the invention:
The purpose of this invention is to provide a kind of highly effective and safe, adopt the sterilization laundry soap product of modern biotechnology product processing.
Consisting of of product of the present invention: soap base, sterilant, washing assistant, enzyme, dye transfer inhibitor, whitening agent, spices.
The part by weight of each component in product is sterilant 0.5~5% among the present invention, washing assistant 3~10%, and enzyme 0.5~1%, dye transfer inhibitor 0.01~3%, whitening agent 1~4%, essence 0.0001~0.001%, all the other are soap base.
Soap base is commercially available industrial chemicals.
Washing assistant among the present invention is: phosphoric acid salt, poly-phosphate, carbonate, silicate etc.
The enzyme of selecting for use among the present invention mainly is to act on soap to be difficult to the dissolved spot, and these enzymes comprise proteolytic enzyme, amylase, lipase etc.
Dye-transfer mainly is to prevent clothing color verity and strength reduction.Mainly contain the polyvinyl piperidines, a kind of or mixture in the polyvinylimidazol copolymer etc.
SYNTHETIC OPTICAL WHITNER is a kind of or mixture in Sodium peroxoborate or the SPC-D etc.
Whitening agent is a white dyes.Used essence can add according to the odor type of product, makes product have different odor types, satisfies different human consumers' needs.
Manufacturing process and product of the present invention is as follows: according to the proportional interpolation soap base of group of products, and enzyme, washing assistant, dye-transfer adds after white dyes, essence, sterilant are dissolved in water; The mixing above-mentioned raw materials grinds homogenizing, and material temperature rises to 85-90 ℃.Material sprays into cooling room, and the pressure of cooling room is 3.3kPa, and soap solidifies on wall, after scraping with scraper, becomes soap flakes, soap flakes press strip, stripping and slicing, dries, and can obtain highly effective sterilization laundry soap.
Major technique feature of the present invention be added have inexpensive, highly effective and safe, the sterilant through modern biotechnology processing of All Pure Nature.The used sterilant of the present invention is the inventor's an invention achievement.Sterilant is subtilis LD-8 (Bacillus subtilis LD-8) fermentation broth extract, and culture presevation is in China Microbial Culture Preservation Commission common micro-organisms center, and CGMCC 2294 is numbered in culture presevation).
Fungus characteristic is as follows:
1. somatic cells is life or the living Gram-positive of near-end in direct rod shape, the gemma.
2. colony characteristics is that white is circular, protuberance, and smooth surface, opaque, moistening, provoke adhesion.
3. can utilize various saccharides, as glucose, semi-lactosi, wood sugar, cellobiose, raffinose etc.; Produce amylase, proteolytic enzyme, can gelatin hydrolysate, V.P, the methyl red positive.
4. 37 ℃ of the suitableeest culture temperature, optimal pH 7.0.
This bacterium classification status is as follows: bacterium territory (Bacteria); Firmicutes (Firmicutes); Genus bacillus guiding principle (Bacillales); Genus bacillus order (Bacillaceae); Bacillaceae (Bacillus); Bacillus (Bacillus); Bacillus subtilis bacterial classification (Bacillus subtilis).
The preparation method of fermentation broth extract is as follows among the present invention:
The seed culture medium of bacterial strain is a broth culture, extractum carnis 3g wherein, peptone 10g, NaCl 5g, water 1000ml, pH value 7.0~7.2, high pressure steam sterilization.
The seed liquor culture condition: culture temperature is 37 ℃, and shaking speed is 140 rev/mins, and fermentation time is 10~14 hours.
Inoculum size is 6%~10% o'clock, helps the formation of antibacterial substance.
The fermention medium of optimizing consists of: sucrose 0.3%, and peptone 1%, NaCl 0.5%, MgSO 4.7H 2O 0.7%, KH 2PO 40.7%, pH8.0.
The fermentation culture conditions of optimizing is: culture temperature is 37 ℃, and shaking speed is 140 rev/mins, and fermentation time is about 24 hours.
Extracting the antibacterial substance method from fermented liquid is organic solvent precipitation method.The available organic solvent is acetone, methyl alcohol, ethanol.
At first with fermented liquid, add supercentrifuge, temperature 0-4 ℃, rotating speed is 10000 rev/mins, centrifugal ten minutes, remove precipitation, and keep supernatant liquor.
With the supernatant that obtains, add isopyknic methyl alcohol, the temperature of system is reduced to-5 ℃ rapidly, preserved 2 hours for-5 ℃.Collect organic phase, adopt vacuum distillation method to remove organic solvent.Distillation temperature 30-60 ℃, distilled 20 minutes, organic solvent is removed.The collecting precipitation material.This promptly is the crude extract of our bacteriocidal substance that obtains.
The crude extract of bacteriocidal substance, after water dissolution, concentration is 1% (mass volume ratio).Lysate can kill common pathogenic bacterium effectively.For example not only can kill intestinal bacteria effectively, Salmonellas, the pathogenic micro-organism that golden yellow common coccus etc. are common, and can kill the common coccus of methicillin-resistant staphylococcus.
This disinfecting liquid has high security, in the emergency toxicology experiment, we gavage 5 groups of 200 mouse with this disinfecting liquid, and the mouse of experimental group none occur dead, and subtilis is present in occurring in nature widely, and many important industrial bacterial strains are exactly subtilis.Substantially can conclude that this disinfecting liquid is safe for the user, can relievedly use.After adding it to washing soap, find that it still has good fungicidal activity.Bacterial classification subtilis LD-8 of the present invention (Bacillus subtilis LD-8), its biological property is: somatic cells is life or the living Gram-positive of near-end in direct rod shape, the gemma; Colony characteristics is that white is circular, protuberance, and smooth surface, opaque, moistening, provoke adhesion; Can utilize various saccharides, as glucose, semi-lactosi, wood sugar, cellobiose, raffinose etc.; Produce amylase, proteolytic enzyme, can gelatin hydrolysate, V.P, the methyl red positive; 37 ℃ of the suitableeest culture temperature, optimal pH 7.0.
This bacterium classification belongs to bacterium territory (Bacteria); Firmicutes (Firmicutes); Genus bacillus guiding principle (Bacillales); Genus bacillus order (Bacillaceae); Bacillaceae (Bacillus); Bacillus (Bacillus); Bacillus subtilis bacterial classification (Bacillus subtilis).
Beneficial effect:
The present invention realized that not only washing soap removes the function of dirt, and washability is outstanding, and strong detergency is easy to use, has especially possessed good sterilization and disinfectant function, particularly can kill the characteristic of methicillin-resistant staphylococcus aureus.The emergency toxicology experiment has also verified the sterilant that adds in this washing powder people and animals to be had very high security.Scientist has found methicillin-resistant staphylococcus aureus in 1961, find that at present it spreads all over the world, and becomes important infectious bacteria, has brought great threat for people's health.The production of the sterilant that adds in the washing soap utilizes fermentation raw material with low cost, adopts modern biotechnology, and technology is simple, and is with low cost.Make the present invention, it is outstanding to become a kind of washability, and sterilizing power is strong, safety, cheapness, washing soap with high content of technology.
That adds among the present invention has the rot-resistant function by the pure natural fermentation raw material through the sterilant that modern biotechnology processes, and has characteristics safely and efficiently.Need not to add again sanitas in the washing soap.
Specific embodiment: the invention will be further described below in conjunction with specific embodiment, but be not limited to embodiment.
Embodiment 1 preparation 100kg product
Sumizyme MP (Savinase 8.0, Novo company), amylase (Termamyl, Novo company), alkaline low-temperature lipase (Lipolase, Novo) each 0.3kg, tertiary sodium phosphate (Na 3PO 4) 2kg, tripoly phosphate sodium STPP (Na 5P 3O 10) 2kg, polyvinyl piperidines 0.5kg, white dyes 0.5kg.The essence of adding 0.0005% adds dissolving back adding in 1 premium on currency with the 0.5kg sterilant, and all the other are soap base (fatty acid content is 60~63%).
Raw material is fully stirred, make it abundant mixing, send into shredder behind the mixing and grind, make it homogenizing, each several part composition unanimity.Material temperature is risen to 90 ℃.Material with 90 ℃ sprays into cooling room, and the pressure of cooling room is 3.3kPa, and the boiling point of water is 26 ℃ under this pressure.Soap solidifies on wall, after scraping with scraper, becomes soap flakes, and soap flakes are joined in the press strip hopper, and press strip forms soap bar.After the soap bar stripping and slicing, dry, can obtain highly effective sterilization laundry soap.
Embodiment 2 manufacture method are with example 1
Sumizyme MP (Savinase 8.0, Novo company), amylase (Termamyl, Novo company), alkaline low-temperature lipase (Lipolase, Novo) each 0.3kg, tertiary sodium phosphate (Na 3PO 4) 2kg, tripoly phosphate sodium STPP (Na 5P 3O 10) 1kg, polyvinyl piperidines 0.5kg, white dyes 0.5kg.The essence of adding 0.0005% adds dissolving back adding in 3 premium on currency with the 2kg sterilant, and all the other are soap base (fatty acid content is 60~63%).
Raw material is fully stirred, make it abundant mixing, send into shredder behind the mixing and grind, make it homogenizing, each several part composition unanimity.Material temperature is risen to 85 ℃.Material is sprayed into cooling room, and the pressure of cooling room is 3.3kPa, and the boiling point of water is 26 ℃ under this pressure.Soap solidifies on wall, after scraping with scraper, becomes soap flakes, and soap flakes are joined in the press strip hopper, and press strip forms soap bar.After the soap bar stripping and slicing, dry, can obtain highly effective sterilization laundry soap.
Get 5% concentration product of the present invention, adopt conventional microorganism detection sterilization effect, test-results shows that product sterilization effect of the present invention reaches more than 90%, and sterilization effect is obvious.Microorganism is selected intestinal bacteria, Salmonellas, golden yellow common coccus.

Claims (7)

1. a highly effective sterilization laundry soap is made up of soap base, washing assistant, enzyme, dye transfer inhibitor and whitening agent, it is characterized in that wherein containing sterilant, and described sterilant is the fermentation broth extract of subtilis CGMCC 2294.
2. according to the described highly effective sterilization laundry soap of claim 1, the part by weight that it is characterized in that each component in the described sterilant is as follows: sterilant 0.5~5%, washing assistant 3~10%, enzyme 0.5~1%, dye transfer inhibitor 0.01~3%, whitening agent 1~4%, essence 0.0001~0.001%, all the other are soap base.
3. according to the described highly effective sterilization laundry soap of claim 1, it is characterized in that described washing assistant is phosphoric acid salt, poly-phosphate, carbonate or silicate.
4. according to the described highly effective sterilization laundry soap of claim 1, it is characterized in that described enzyme is proteolytic enzyme, amylase or lipase.
5. according to the described highly effective sterilization laundry soap of claim 1, it is characterized in that described dye-transfer is a kind of or its mixture in polyvinyl piperidines, the polyvinylimidazol copolymer.
6. according to the described highly effective sterilization laundry soap of claim 1, it is characterized in that described SYNTHETIC OPTICAL WHITNER is a kind of or mixture in Sodium peroxoborate or the SPC-D etc.
7. a highly effective sterilization laundry soap preparation method according to claim 1 comprises the steps: according to the proportional interpolation soap base of group of products, enzyme, and washing assistant, dye-transfer, white dyes and essence, the sterilant back that is dissolved in water adds; The mixing above-mentioned raw materials grinds homogenizing, and material temperature rises to 85-90 ℃.Material sprays into cooling room, and the pressure of cooling room is 3.3kPa, and soap solidifies on wall, after scraping with scraper, becomes soap flakes, soap flakes press strip, stripping and slicing, dries.
CN2008101017748A 2008-03-12 2008-03-12 Highly effective sterilization laundry soap Active CN101240225B (en)

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Application Number Priority Date Filing Date Title
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CN101240225B CN101240225B (en) 2010-08-18

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102816646A (en) * 2012-09-14 2012-12-12 苏州谷力生物科技有限公司 Bacteriostatic bleaching laundry detergent for hospitals and preparation method thereof
CN102899200A (en) * 2012-10-11 2013-01-30 南风化工集团股份有限公司 Color particles for washing soap and preparation method thereof
CN103387891A (en) * 2012-07-14 2013-11-13 宁夏天地经纬电力设备工程有限公司 Laundry soap
CN106753915A (en) * 2016-11-29 2017-05-31 东莞市萌创保健科技有限公司 A kind of preparation method of the ferment gel perfumed soap of the strong skin of fragrant body
CN108285836A (en) * 2017-01-07 2018-07-17 潮州市龙植馨生物科技实业有限公司 A kind of plant polypeptide low molecule glue protein perfumed soap manufacturing method

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103387891A (en) * 2012-07-14 2013-11-13 宁夏天地经纬电力设备工程有限公司 Laundry soap
CN102816646A (en) * 2012-09-14 2012-12-12 苏州谷力生物科技有限公司 Bacteriostatic bleaching laundry detergent for hospitals and preparation method thereof
CN102899200A (en) * 2012-10-11 2013-01-30 南风化工集团股份有限公司 Color particles for washing soap and preparation method thereof
CN106753915A (en) * 2016-11-29 2017-05-31 东莞市萌创保健科技有限公司 A kind of preparation method of the ferment gel perfumed soap of the strong skin of fragrant body
CN108285836A (en) * 2017-01-07 2018-07-17 潮州市龙植馨生物科技实业有限公司 A kind of plant polypeptide low molecule glue protein perfumed soap manufacturing method

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Assignee: Beijing Lvhua Shengyi Daily Chemicals Co., Ltd.

Assignor: Beijing Ludaoyuan Bee Products Co., Ltd.

Contract record no.: 2011990000250

Denomination of invention: Sterilizing laundry soap

Granted publication date: 20100818

License type: Exclusive License

Open date: 20080813

Record date: 20110413

ASS Succession or assignment of patent right

Free format text: FORMER OWNER: BEIJING LUDAOYUAN BEE PRODUCTS CO., LTD.

Effective date: 20120504

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 101121 TONGZHOU, BEIJING TO: 100029 XICHENG, BEIJING

TR01 Transfer of patent right

Effective date of registration: 20120504

Address after: 100029, Beijing, Xicheng District Middle East Building No. 26, 3 door, room 402

Patentee after: Ning Yuesheng

Address before: 101121, 1 Cui Lu, Liyuan, Tongzhou District, Beijing, Zhenjiang

Patentee before: Beijing Ludaoyuan Bee Products Co., Ltd.